3 3M Environm ental Laboratory E05-0210 Interim R eport#13 Interim Report #13: Analysis of Tennessee River Water Samples Study Title A P (PFBS), Pn a l y s i s o f e r f l u o r o b u t a n e s u l f o n a t e erfluo ro hexanesulfonate (PFHS), a n d Pe r f l u o r o o c t a n e s u l f o n a t e (PFOS) in Wa t e r , So i l , Se d i m e n t , Fi s h , C , V , Sl a m s e g e t a t i o n m a l l Ma m m a l Liv e r a n d Sm a l l M Sa m m a l e r u m Us i n g LC/MS/MS 3M D M Pf o r t h e e c a t u r o n it o r in g r o g r a m Data Requirement EPA TSCA Good Laboratory Practice Standards 40 CFR 792 Author Michelle D.

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-^ 226-/607 From Barnard J *% 0 tQOOfcOOl 08:19 AM To rwily_bemfeOhemwl.oom cc rmratHy Q 6H > r*c nat aaipaCtthafoliogroup com. ]matzvHrningtontrutcorn Subject Oct 20 Hi Bern, Foggy beginning of the day here, but pretty good weather predicted, mom and I going to Lancashire later today for dinner, Joe's folks coming down, I am sure we can find some project to chip away at. certain I need to shorten the hot water line to the sink and midbath, could be easy or a bitch depending on luck.

3M Environmental Laboratory R126-0005 M ethod A nalysis of Potassium Perfluorooctanesulfonate or O ther Fluorochemicals in Serum Extracts U sing H PLC-Electrospray/M ass Spectrometry Method Number: ETS-8-5.1 Author: Lisa Clemen, Robert Wynne Approved By: 'L l Laboratory Manager Adoption Date: 03/01/99 Revision Date: <V / 2 C / Date Group Leader Technical Reviewer Date dh i / m Date 1.0 S c o p e a n d A p p l ic a t io n __________________________________________________________________ 1.1 Scope: This method describes the analysis of serum extracts for fluorochemical surfactants using HPLC-electrospray/mass spectrometry. 1.2 Applicable Compounds: Fluorochemical surfactants or other fluorinated compounds, or other ionizable compounds. 1.3 Matrices: Rabbit, rat, bovine, monkey, and human serum, or other fluids as designated in the validation report.

CLIENT PRIVATE AF26-OI6I fk -- PROTOCOL TITLE: Range finding Cytotoxicity Assay of T-6292, T-6293, T-6294, T-6295 in R at Hepatocytes SRI Study No.

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BACK TO MAIN 3M Environmental Laboratory Biodegradation Studies Executive Summary of Biodegradation Studies 3M has completed a series of studies of the biodegradability of various fluorochemical materials based on EPA Guidelines OPPTS 835.3200, OPPTS 835.3210 and/or OPPTS 835.5045.

AR226-0(61 DT15 3M MEDICAL DEPARTMENT, CORPORATE TOXICOLOGY - ST-43: Standard Procedure fo r Liver Subcelular Fractionation - Study Objective: Perfluorochemical compounds such as perfluorooctane sulfonate (PFOS) have been linked with reduction in serum cholesterol levels and liver has been identified as the primary target site.

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Northwest Bioanalytical Study No.

A(U2rO51% PFOA and Associated Salts Ecotoxicity Elements Title Activated Sludge R espiration Inhibition T es t - F C -1 0 1 5 -X Acute Toxicity o f F C -1 01 5 to the Fathead Minnow, Pim ephales prom elas Growth and Reproduction Toxicity Test with F C -1 01 5 and the Freshw ater Alga, Selenastrum capricornutum Acute Toxicity o f F C -1 0 1 5 to the Daphnd, D aphnia m agna Laboratory or Author 3M Env.

3M ENVIRONMENTAL LABORATORY REPORT NO.