Document zoQdY4nJpLKazpxbp92jkr4Qa

PLAINTIFF'S EXHIBIT { i. ] ] :j - 0 [] i COMPLETE REMOVAL 1970 VINTAGE CONGOLEUM VINYL ASBESTOS TILE RESIDENTIAL BATHROOM * June 27, 2002 BYI Project #1941A-7237 Boelter & Yates environmental engineers and scientists Boelter & Yates environmental engineers and scientists COMPLETE REMOVAL 1970 VINTAGE CONGOLEUM VINYL ASBESTOS TILE RESIDENTIAL BATHROOM ] -n t Boelter & Yates, Inc. 1300 Higgins Road Suite 301 Park Ridge, Illinois 60068-5772 847/ 692-470C Fas 847/ 692-3121 i June 27, 2002 BYI Project #1941A-7237 I I TABLE OF CONTENTS PAGE 3 EXECUTIVE SUMMARY ................................................................................................................. 1 Boelter & Yates, Inc Objectives............................................................................................................................. 1 NOTES ~ METHODOLOGY............................................................................................................................... 2 j PCM Sampling Procedure ................................................................................................. 2 J "Personal" Samples ............................................................................................................ 2 Homogeneous Sampling Area .......................................................................................... 2 *"] "Average Room Air" Samples............................................................................................. 2 -3 "Background Air' Samples for TEMAnalysis.................................................................... 2 PCM Light Microscopy Analysis....................................................................................... 3 '} Fiber Type Determination by Electron Microscopy.......................................................... 3 . j AHERA Electron Microscopy Analysis.............................................................................. 3 PLM Light Microscopy Analysis ........................................................................................ 4 Statistical Comparisons ..................................................................................................... 4 j Laboratory Accreditation...................................................................................................... 4 Video Recording.................................................................................................................. 4 j DISCUSSION OF FINDINGS.......................................................................................................... 5 Residential Setting ............................................................................................................. 5 Background Sampling Results.......................................................................................... 5 ) Existing Congoleum VAT .................................................................................................... 7 J Tile Removal Test.................................................................................................................. 8 Sampling Results During Test ........................................................................................ 10 5 CONCLUSIONS.............................................................................................................................. 11 APPENDICES j A Compilation Spreadsheets and Graphs - TESTING RESULTS B - Compilation Spreadsheets and Graphs - PRE-TEST BACKGROUND RESULTS and DURING TEST OUTDOOR AREA BACKGROUND RESULTS C - NIOSH 7400 PCM and NIOSH 7402 TEM Laboratory Reports A D - AHERA TEM Laboratory Reports E - PLM Bulk Sample Report COMPLETE REMOVAL 1970 VINTAGE CONGOLEUM VINYL ASBESTOS TILE RESIDENTIAL BATHROOM EXECUTIVE SUMMARY Objectives The purpose of the test was to determine the concentration of fibers in the air while completely removing 1970 vintage Congoleum vinyl asbestos tile (VAT) from a residential bathroom. Boelter & Yates, Inc NOTES Background The testwas performed in a residential bathroom where original 1970's vintage Congoleum VATs were existing. The original bathroom tiles have been in use since the time of installation. One week earlier of the date of this test, about one half (%) of the original tiles had been removed and replaced with a new old stock (N.O.S.) 1970's vintage Congoleum vinyl asbestos tile. The residence, located at 225 Fremont Avenue in Seaside Heights, New Jersey, was that of Mr. Don Golemme.1 The test was conducted in an actual residence and therefore is representative of actual conditions. The test was conducted to represent the activities of a worker who would be completely removing flooring materials utilizing pre-1970's techniques. Sampling was performed to reflect the entire term of the activities required to completely remove the floor tile. The test was performed on May 29,2002 by Mr. Scott Wynder, a professional flooring installer of Dunes Floor Covering in Chesterton, Indiana, and Mr. Fred Boelter, serving as a helper. This report presents the results of the test described herein. f Sample Results All samples measured concentrations of total fibers in air which were well below the current U.S. Department of Labor Occupational Safety and Health Administration (USDOL-OSHA) 8-hrTime Weighted Average (TWA) Permissible Exposure Limit (PEL) of 0.1 fiber per cubic centimeter (f/cc). Subsequent definitive analysis determined there were no asbestos fibers present in any area or personal sample. Sample results are presented in the accompanying tables. 1 Mr. Golemme is employed by the Congoleum Corporation of Mercerville, New Jersey. 3 0 Complete Removal -1970 Vintage Congoleum VAT - Residential Bathroom June 27,2002 Page 2 1 METHODOLOGY 1 PCM Sampling Procedure Boelter & Yates, Inc. 2-5 NOTES Samples were collected and analyzed by Phase Contrast Microscopy (PCM) following NIOSH 1. -? Method 7400. Air was drawn through a 25mm, conductive cowl cassette with an 0.8 micron mixed cellulose ester (MCE) filter for collecting airborne particulate. The cassette was connected to a dedicated Gilian servo-drive pump. The pump was used to maintain a flow rate of two (2) titers per minute (Ipm) for both personal and area room air samples. .1T A Brooks rotameter was used to calibrate the pumps prior to and post sample collection. The rotameter was calibrated against a primary standard. ..J The samples were sealed, labeled and shipped to the laboratory for analysis. Samples were signed, placed in an overnight shipping container, sealed, tracked by Airborne, and arrived at the i laboratory by next day air. "Personal" Samples i Personal samples were collected by attaching the cassette in the breathing zone of the individual performing the work for the duration of the test. The sampling pump was worn on the individual's belt. .Homogeneous Sampling Area The residence was composed of a number of rooms. While the removal activities were actually being performed in the bathroom, the adjacent kitchen was the necessary access point to the bathroom. Consequently, the kitchen (130ft2) and bathroom (about 45ft2) were considered one homogeneous sampling area (HSA) of about 175ft2. The total volume of this homogeneous sampling area (HSA) was approximately 1,400ft3. Access to other parts of the residence were -j prohibited by the closing of doors and windows and the establishment of a dual layer critical barrier between the kitchen and living room. . j "Average Room Air* Samples To determine the "average room air' concentration, four (4) random locations were selected in. the bathroom and four (4) random locations were selected in the kitchen. A sampling pump and cassette was placed in each of the eight (8) locations for the duration of the test. "Background Air" Samples for TEM Analysis .i Prior to conducting the test, the room was sampled to verify cleanliness. Ten (10) samples were collected (five inside the HSA and five outside the residence) following a modified AHERA i Protocol. Three (3) blanks were also reserved. Analysis was performed by transmission electron microscopy (TEM) following AHERA Protocol. Prior of conducting the background test, the horizontal surfaces ofthe bathroom and kitchen were wet wiped. Since this was an actual residence, utilization of "aggressive leaf blower" techniques was judged impractical. Consequently, samples were collected under static conditions. This static collection of samples is what modifies the technique from AHERA. Complete Removal -1970 Vintage Congoleum VAT - Residential Bathroom June 27,2002 Page 3 Air was drawn through a 25mm, conductive cowl cassette with an 0.45 micron mixed cellulose ester (MCE) filter for collecting airborne fibers. The cassette was connected to a dedicated Gast high volume pump. The pump was used to maintain a flow rate of 10 liters per minute (Ipm). A BGI rotameter was used to calibrate the pumps prior to, during, and post sample collection. The rotameter was calibrated against a primary standard. Boelter & Yates, Inc NOTES The samples were sealed, labeled and shipped to the laboratory for analysis. Samples were signed, placed in an overnight shipping container, sealed, tracked by Airborne, and arrived at the laboratory by next day air. PCM Light Microscopy Analysis Samples were analyzed in accordance with NIOSH Method 7400. Total fiber counts were determined by phase contrast microscopy (PCM) in accordance with the NIOSH Manual of Analytical Methods, Fourth Edition, dated 8/15/94, A Rules. Values for PCM analysis are provided in the Appendix A and Appendix 6 spreadsheets. The only fibers which are counted are those which are longer than 5 microns and have a length to width ratio equal to or greater than 3:1. PCM analysis counts all fibers meeting the specified dimensions. The analysis is not specific for asbestos but is the method specified to be used in the OSHA regulations. . The PCM laboratory reports are presented in Appendix C. Fiber Type Determination bv Electron Microscopy Air samples were subsequently analyzed in accordance with NIOSH Method 7402. Specific fiber types were determined by transmission electron microscopy (TEM) in accordance with the NIOSH Manual of Analytical Methods, Fourth Edition, dated 8/15/94, ASBESTOS by TEM. Values for TEM analysis are provided in the Appendix A and Appendix B spreadsheets. The only fibers which are counted are those which are longer than 5 microns and have a length to width ratio equal to or greaterthan 3:1. The specific fiber types were determined as a "fraction of optically visible asbestos fibers on the filter". The TEM laboratory reports are presented in Appendix C. AHERA Electron Microscopy Analysis AHERA Protocol transmission electron microscopy (TEM) analysis was performed on all background samples to verify the cleanliness of the HSA prior to beginning the test. The sample analysis was performed as described in the Federal Register Vol. 52, No. 210, the Asbestos Hazard Emergency Response Act (AHERA Protocol). Small squares were cut from each filter, processed appropriately, placed onto 200 mesh copper screens (grids) and transferred to a modified Jaffe Wick Washer containing acetone solvent. After the appropriate processing time, the grids were examined with a JEOL1200EX or 100CX TEM. Grid openings from each sample were scanned at 20.000X. When fibers or structures of various shapes were encountered, they were assessed for morphological characteristics and crystalline structure with selected area electron diffraction (SAED). Complete Removal -1970 Vintage Congoleum VAT - Residential Bathroom June 27,2002 Page 4 The TEM laboratory reports are presented in Appendix D. PLM Light Microscopy Analysis Bulk samples were analyzed for asbestos by Polarized Light Microscopy (PLM) in accordance with guidelines set forth in the EPA Method for Determination of Asbestos in Bulk Building Materials, U.S. EPA/600/R-93-116 (7/93 Edition). Boelter & Yates, Inc. NOTES v The PLM laboratory reports are presented in Appendix E. Statistical Comparisons Data was formatted in spreadsheets for analysis. Statistical functions were performed including maximum, average, minimum, standard deviation, and variance. The spreadsheets in Appendices A and B presents the data and summarize the statistical analyses performed. Laboratory Accreditation The samples were shipped to and analyzed by R. J. Lee Group, Inc. in their Monroeville, Pennsylvania laboratory. R. J. Lee is accredited for TEM analysis by the National Institute of Standards and Technology (NIST) under the National Voluntary Laboratory Accreditation Program (NVLAP) as Lab #101208. R. J. Lee is also accredited for PCM analysis by the American Industrial Hygiene Association (AIHA) as Lab #8204. Video Recording The entire process was video recorded. A Sony Digital Handycam DCR-TRV11 was used to record the activities from various vantage points in the bathroom. Complete Removal - 1970 Vintage Congoleum VAT - Residential Bathroor.; June 27, 2002 Page 5 DISCUSSION OF FINDINGS Residential Setting Testing was performed in an actual bathroom located in a residence at 225 Fremont Avenue in Seaside Heights, New Jersey. The bathroom is an area of about 45ft2 (360ft3) with a configuration as shown in Figure 1. The bathroom is located just ofF the kitchen of the residence(see Figure 2). Access to the bathroom is through the kitchen and consequently the kitchen and bathroom were established as the homogeneous sampling area (see Figure 3). Figure 2 - View from kitchen to bathroom An airtight critical barrier was constructed of a double layer of 6 mil polyethylene sheeting to physically separate the kitchen from the livingroom. One layer was constructed on the kitchen side and one layer was constructed on the living room side. Access to the kitchen was gained through the rear porch. Figure 1 - Bathroom configuration Porch Soulh Qidroow Mh MM* Bedfoocn North BMraoa KKchtn Uvtnfl Room Porch Figure 3 - HSA for the test. All other openings such as doors and windows were closed. The critical barrier is visible in the view from the bathroom to the kitchen shown in Figure 4. Background Sampling Results Figure 4 - Critical barrier from kitchen to living room. Prior to conducting any tests, horizontal surfaces in the homogeneous sampling area were systematically wet wiped. Following the cleaning, a series of background samples 2 3 Complete Removal -1970 Vintage Congoleum VAT - Residential Bathroom June 27,2002 Page 6 1 were analyzed from five (5) area sampling locations inside the homogeneous sampling area in accordance with a modified AHERA protocol. 1 Background samples were collected under "static'' conditions with analysis by AHERA TEM in Boelter & Yates, Inc. accordance with AHERA Protocol. NOTES / Results of the Pre-Test Background sampling are shown in the following Table I: u Aggressive Air AHERA Method .r*.* STATISTICAL AHERA TEM (s/mm3) NIOSH 7400 PCM (f/cc) -1 FUNCTION - Background for S/29 Background for 5/29 MAXIMUM AVERAGE MINIMUM STAND. DEV. <15.3 <15.3 <15.3 0.0 0.011 0.006 0.005 0.002 COUNT 55 1 The levels met the AHERA Clearance Criteria of an average of less than seventy structures per millimeter squared (<70 s/mm2) for the 5 samples analyzed and the homogeneous sampling 3 areas was considered clean. Results are shown in the spreadsheet presented in Appendix B. Results of the Durino-Test. Outdoor Area Background sampling are shown in the following Table II: STATISTICAL NIOSH 7402 TEM (asbestos f/cc) NIOSH 7400 PCM (total f/cc) FUNCTION Background on 5/22 PM - Background on 5/22 PM - MAXIMUM AVERAGE MINMUM STAND. DEV. COUNT 0 <0.01 0 <0.01 0 <0.01 0.0 0.0 55 The results indicate that roof and siding removal and replacement activities across the street during the previous week did not adversely impact on the outdoor air quality around the residence where testing was being performed. Consequently, the outdoor air was not an influencing factor in the indoor tests. Results are shown in the spreadsheet presented in Appendix .B. Complete Removal -1970 Vintage Congoleum VAT - Residential Bathroom June 27, 2002 Page 7 A mosaic of tiles were installed in the bathroom (see Figure 5) as a result of a previous test. All are 1970's vintage vinyl asbestos tiles (VATs) as manufactured by Congoleum Corporation. The existing original bathroom tile is shown with its corresponding bulk sample in Figure 6. The tile known as Supertile "Libra" VAT with stock number VA-938 was bulk sampled (i.d. MFM-0502401) and analyzed. The asbestos content of this VAT was determined to be 0.0% chrysotile. Another style (See Figure 7) known as Congoleum Aztec is orange with a star pattern. This tile had been previously bulk sampled (i.d. MFM-0698-004) and analyzed. The asbestos content of the Aztec tile was determined to be 0.02% chrysotile. Figure 7 - Congoleum Aztec vinyl asbestos tile. A third style (See Figure 8) known as Congoleum Ventura has a hexagonal pattern in three different colors. This tile had been previously bulk sampled (i.d. MFM-0698-007) and analyzed. The asbestos content of the Ventura tile was determined to be 0.0% chrysotile. Figure 8 - Congoleum Ventura vinyl asbestos tile. See Appendix E for bulk sample data. Complete Removal -1970 Vintage Congoleum VAT - Residential Bathroom June 27, 2002 Page 8 Tile Removal Test The particular test being performed was a complete removal of the existing tile as would be typical for a repair activity. The bathroom had approximately 40ft2 of tiled area as shown in Figure 9. Mr. Wynder was to remove all the tile from this area. oelter & Yates, Inc. I OT E S During the test, there was no deliberate air movement into or out of the residence. No doors or windows were opened during the testing nor was any mechanical ventilation operated before, during or after any of the test cycles. Since this is an actual residence, however, it is likely that there is a natural ventilation rate due to building envelop leakage. This would represent an actual exposure while performing the tasks. Figure 9 - Area selected for partial removal Mr. Scott Wynder, the professional flooring installer, was asked to perform the activities using typical pre-1970's techniques, tools and methods. The removal was performed entirely by hand using a 6" wide flat blade scraper and af wide wood chisel. Personal and average room air samplers were started prior to beginning the testing. The samplers were stopped after completion of the testing. The samplers were operated for the period of time indicated. During the test cycle, no one left or entered the homogeneous sampling area. During the sampling event, similar procedures were followed as described in Table III: STEP 1 2 3 4 5 6 7 TABLE III-SEQUENCE ACTIVITY Scope project; prepare and stage tools Remove bathroom fixtures Plug the waste piping Remove the baseboard Remove the tile using a fiat blade or chisel Remove high spots of mastic Clean tools and clean debris PHOTO Figure 10 . Figure 12 Figure 13 Figure 14 Complete Removal -1970 Vintage Congoleum VAT - Residential Bathroom June 27, 2002 Page 9 Figure 10 - Existing VAT. Original tile is on the right and the partial installation tile is on the left. Figure 10 shows the bathroom floor before the test began. The variety of tile types is the product of the partial installation test performed the week earlier. A new Armstrong S- 750 mastic (see Figure 12) was used for the Figure 11 - Mastic used to adhere N.O.S. tiles. partial installation. This mastic was allowed to cure for one week and thus obtain maximum adhesion strength. Figure 11 shows removal of a section of original tile from under the vanity. Mr. Wynder is using a 1" wide wood chisel for this task. Figure 12 - Original floor tile removal using a 1" wide wood chisel. Figure 13 - Floor area after complete removal. Area of original mastic is at the top and the area of "new" mastic is at the bottom. Figure 13 shows the "finished floor" after all the tile has been removed. In all, about 40ft2 of tiles were removed. Figure 14 shows a bucket of the tile and mastic scraps that were created during the removal activities. Figure 14 - Removed VAT in bucket. Complete Removal -1970 Vintage Congoleum VAT - Residential Bathroom June 27,2002 Page 10 Sampling Results During Test Results of 8-hr Time Weighted Average (TWA) Permissible Exposure Limit (PEL! sampling is shown in the following table: STATISTICAL FUNCTION S/29/01 - PCM Total f/cc by NIOSH 7400 - Personal Samples - - Average Room Air S/29/01 - TEM Asbestos f/cc by NIOSH 7402 - Personal Samples - Average Room Air- Boelter & Yates, Inc. NOTES MAXIMUM AVERAGE MINIMUM STAND. DEV. COUNT 0.001 0.001 0.001 0.000 2 0.006 0.003 0.001 0.002 8 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 28 All sample results indicate that while there were some total fiber concentrations as detected by PCM NIOSH 7400, there were no asbestos fibers detected when the samples were analyzed by TEM NIOSH 7402. Clearly, the results are well below the current OSHA 8-hr Time Weighted Average (TWA) Permissible Exposure Limit of 0.1 f/cc. The Appendix A spreadsheets summarized in the above tables are also depicted graphically in the Appendix A. Complete Removal -1970 Vintage Congoleum VAT - Residential Bathroom June 27,2002 Page 11 CONCLUSIONS An approximately 40 square foot area of bathroom tile was entirely removed while testing for the fiber release from 1970's vintage Congoleum Corporation vinyl asbestos tile (VAT). The entire installation process was demonstrated including removing the fixtures, lifting the tiles, and scraping the adhesive. Eight (8) room air samples and two (2) long term personal samples were collected during the process during each test. The process as tested took slightly less than 60 minutes to perform. Boelter & Yates, Inc. NOTES All sample results show the total airborne concentrations of total fibers to be well below the current OSHA 8-hrTime Weighted Average (TWA) Permissible Exposure Limit (PEL) of 0.1 f/cc. Furthermore, all samples showed zero (0) asbestos fibers when analyzed by definitive analytical techniques. Respectfully submitted, BOELTER & YATES, INC. Reviewed by, Enclosures u r APPENDIX A Compilation Spreadsheets and Graphs NIOSH 7400 and NIOSH 7402 TESTING RESULTS f l L [ L i i f oooooooo oooooooo OOOOO OOOOO 8i8 00000060' 8o 8o liisi" d6dod OOOOO" NN m N JO p 0000000 o' o o' o o' O O d eoooooaoooc gOgOSOJOJOfi o o 0 o' o 5OdoO?oO?oOgOog" NNNNNNNNOONNNN lAinininninnioo 00 to 10 i ti n n{ * k,* O5*A?00- uitiiuiiLiujiiiuiui 55555555 20O20QS0OIS0Q 05I50Q3" L 99 1- n o 009 ?8S?i? 8 5? 5 5 3 5555 <wl> tunS cuSd 0uS. vS CM CM *4 W W S CM CM L M88N8N 8888 NNN 8888888 CM CM CM CM CM CM CM s' s' s' S'S'S'S' >WUJ--) UD<"I ss-ss-ss- 5* S' 5* 2222 22**2*2&2&2&2 *> >> 1^:SaVaOfcVcpVcLcCtaCiwrOcwcOwciUr1aO1QOi: l.SJ2fii2 j3-?o-?-o9'j5`o&oo.eavaao ,oaao >00000000000 lOUMMtaifllOIOIOIOIAttlOtO 88 IBsSS isiiife |2S<|5f?S>Uo Congoleum Test #5 ~ Full Removal - Bathroom IAI31 Aq (oo/* sojsoqse) uo!*e4*ueouoo W to 1-- LO o O Top oo lAIOd Aq (oo/j. |B*oi) uo!*B4*ueouoo CM If) t-- 10 O d^d0 oo lAIOd Aq (oo/j. |B}oi) uoiiBjjuaouoo Congoleum Test #5 -- Full Removal - Bathroom Random Area - 8hr TWA MBiBB Personal 8-hr TWA Personal 8-hr TWA I/M3J. Aq (oo/j. sojseqse) uo.qej)udouoo U5 CM od IoT) 1 1 Congoleum- Test #5 Full RemovalBathroom 03 (D I E <D s (0 i (/) f L Random Area ( APPENDIX B Compilation Spreadsheets and Graphs PRE-TEST BACKGROUND RESULTS and DURING TEST OUTDOOR AREA BACKGROUND RESULTS EEEEE 11111 ci co co co n ui 10 to u> vi ^T"TT-T" VVVVV N N fv fv s N NN NN i * i NNNOOlO NN OO z o P U. it OF 2rl 30 sgg3 Oy-t-t-tq OOOO 0 0 0*0* Ml 10 Ml U) r- o o o o 00000 odddo 00000 oodoo Ml Ml Ml (A Ml ggggg odddo Ml Ml Ml O O M) OOOOO OOOOO odddo i 5 ! ooooo nd idAdodood CM CM CM CM CM s! CONOCO CO CO CO Ml CO CM CM CM CM CM CM CM CM CM CM * UJ 2 r- t~ t- r- uzjuiw5. teil 015 SSS'g'6 p; O' Ui <t-ns2g Si SSSiSS?55 cccctrcco: jjj <<<<<mmcD t- d Cl ^` lLO. 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S|8ss ?d ^ VJ V 2 88 8 8 a 2a s o & o 4J J *fdst.'st iuii m/tr/s :*in lAftlti BoeKer i'Vates JUK SAMPLE ANALYSIS DATJJUCHAN OFCUSTOOY 0AT6 phojktwoj imA-liTT COUGCTEDBV: ANALYZED TURNAROUND THE: SHI 12HR 24KR ft >K* L*L IMTUDM. f-k'ol ___ 01 0% 6* 05 1_ Oft o7 08 MWU TYK _ MomwucAisfsao.oi ocmm liEMHIMflil *ft h' ACTMTY mUTOK tm Hi&rtzk /vv>/"_______ Wtirt*rCWW- if /If U KitdtJ'iW -Ilf f&l M i\I7t fk* HSR km -1 1 S /r ^ . i 1 --. 1 HULneu. am uuuas bee ta <ibY Safe*M(Am <n> fca**-* | ftMlM MM ! wmi MM An am u* ml TM DM VM am ' KM IM MM Mu' tfalwtf uanotari | *mSt i I HE w s? tp 76::l (10 r oi jUL w ft po w |f0 _ 0* 1130 JB5 ?s VO'i |K> 1730 .1! 7<t W M_ |I0 JBL 35wj ft U tiT lip oL > _ AT -OR ___MMIW iinnfi ItzL ft ft ft K> R) |io VO l|6 li Ml J6 i -- -- mmm -- Mia MW |Mw| i wj ororr aujii rrt/rc/c'*1*1 RJ LeeGroup, Inc. 350 Hochberg Road Monroeville, PA 15146 Tel: (724)325-1776 Fax: (724) 733-1799 The Materials Characterization Specialists June 7, 2002 Mr. Fred W. Boelter Boelter & Yates, Inc. 1300 Higgins Road Suite 301 Park Ridge, IL 60068-5772 RE: TEM Asbestos Results for Samples as Shown on the Test Report RJ Lee Group, Inc. Job No.: ATH206309 Client Purchase Order No.: 1941A-7237 Dear Mr. Boelter: Enclosed are the results from the transmission electron microscopy (TEM) asbestos analysis of the above referenced samples using the counting rules established by the NIOSH Method 7402, Issue #2, 8/15/94. The samples and volume information were provided by Boelter & Yates, Inc. personnel. The analysis for asbestos fibers consisted of fiber morphology, visual selected area electron diffraction (SAED) and elemental chemical analysis by energy dispersive spectroscopy (EDS), supplemented by the measurement and interpretation of micrographs of several selected area electron diffraction patterns (SAED). The samples were analyzed at a magnification of 1000X., Particles meeting the definition of a fiber > 5pm in length , > 0.25pm in diameter and having a length to width aspect ratio 3:1 were classified as chrysotile or amphibole. The electron microscope used for the analysis was a JEOL1200 EX equipped with Gresham PEDX system. The Test Report lists each sample identification number, filter area, volume, area analyzed, asbestos fiber counts (fg), analytical sensitivity, concentration of asbestos in fibers per cubic centimeters (f/cc). Total Fibers (Fs), and Fiber Ratio (fs/Fs). . RJ Lee Group, Inc. is accredited by the National Voluntary Laboratory Accreditation Program (NVLAP) for selected test methods for airborne asbestos fiber analysis (TEM), asbestos fiber analysis (PLM), New York State Department of Health Environmental Laboratory Approval Program (ELAP), and by the American Industrial Hygiene Association (AIHA). This test report only relates to the items tested. NVLAP accreditation does not imply endorsement by NVLAP or any agency of the U.S. Government. The report shall not be reproduced except in full. Monroeville, PA San Leandro, CA Washington, DC fttsco, WA www.rjlg.com Mr. Boelter Page 2 ATH206309 June 7, 2002 These results are submitted pursuant to RJ Lee Group's current terms and conditions of sale, including the company's standard warranty and limitation of liability provisions and no responsibility or liability is assumed for the manner in which the results are used or interpreted. Unless notified in writing to return the samples covered by this report, RJ Lee Group will store die samples for a period of thirty (30) clays before discarding. A shipping and handling fee will be assessed for the return of any samples. If you have any questions, feel free to call me. Very truly yours. Kimberly A. Allison Manager - TEM Analysis KAA/slb Enclosures 3 Test Report Asbestos C oncentrations and F ib e r R atios N IO S H 7402 A nalysis P ro je c t A T H 206309 3 Q s CJ CM CM CM CM CJ CM CM C! CM CM CM CM s C: Cc t c: c < O a; O o o O o u4> JD 11 f T C/> O 00 in o *n On V"> to q co ^ co o cm in o v) so in in o r^' o ^ s t2 oc KO 'am I tPo 4o) **--' < U *#** * t}- Tj- Tj- 8 8 8 8 8CTs Os Os Os Os - Os o o OS ooo VVVV V o V v* *vo *wo d v *3 2? s:s >..2 *<^e3F 0C0O sTf Oos oo d TT Tf Tfr 8 88Os Os Oo OS OS ooO od m n d qqqqqo III dd dddddddddddd JJ *3 E J3 oooooo dddddddddddddd g 11 co r-* *1 = co CrCOOo COCOO' o COCOO' CocOo o CCOOO' cOCoO' d COCOO' o CCOOO' o CoCOO* d CCOOO' d CCOOO' o CoCOO COCOO' 3 o o o1-H oM4 tH o o 8 d 1 s u C00s O00s 1 s 3 5 S* td O o cr 00 CO 00 CO *n 00 CO wo 00 CO m oo CO in 00 CO m 00 CO m 00 co <n 00 CO n 00 CO in 00 CO m 00 CO *n 00 CO m oo CO S& tt. u 43 E ^ 04 O I! s s sU c 'H.i .a e < S i < mo -4 i; o <: 0o0 < s 4 CoM 4 U W *n n in in n in in in *n in in n Q-l I 62 o 2 I1 5 rrs so C" cs cm Or-s g CM CM Os CM co rf 04 co CO CO CO CO n co CO cCo*' 55 5505 oCM Os r*% CM Os o** CM Os " CM Os O' CM os CM OS CM C\ O `2 '> a *o a 3 M *a o a >s C CO o *23 o a ^ o^ 2R *2 1 i C .1 gS CM w J<t oc s O <Q t) CQ -S cu co b* *3 <2 g (3 C Oc of g a -g *1 < 3 O \a 9> *5> g .2 w *c3 = i ISS"'ri . ^ a V) >v`- o. 5 >i =o5.5#: E^'a <S *>o **-ao rS | 3w * 2a S01 S E_ ao g *1 ^MU fat U '3 O1T U* 2 CM CM CO V cC 3 cu *a co so G O w a i> a) h4-^ sl> *5 o u 4) ] * APPENDIX D AHERA TEM Laboratory Reports CgJ m S <0 cSCoJ ci i i > * Q < < rt H C| H H s<o sco Q3 O^' ^Oi O Ifl < H H &ts * O *o 45->L* a^" o 8 3 ss |!| - ^ c K rSa >K-5 3o3 t; O a <u K 5 2 e A C*4 q b-i I V V S' I sgfc 8 $C3O CSQ ^ u 8 2 cOr' g *| $s j . S A 0 I<8 5 03 TC>O I s -s8 m o = R n-H 2 >< CU3 boc *cL ill ss ssa s5 c g c o v*j r> j| 8 8 J 8 J 8 J n o o o* 8O* o n 3 M 111 8 o o ? V fv* tv- ^ V 8888 O O S *"> N a_ _ ^NO in M CH 9 = ?9 9 111O O O Q to m n b u Cl. so k SMo 0f0i 00 i cit o Ljptopstr AID SAMPU ANAITSS DATAKtUUiWN OF CUSTODY SHEEty , Bodict iYates WfBTOEJECTNSO.jV\-t>Z ______ 72V7 COUICIffiBY: \iAiUNlMlVYTZCH)M, V. Wgfc-fWV ** TUHMROtJNO TIME' 6KR tjiw 124HR sMMfnn. vTmtKi VOUMWQtraHUCMBK. si - ? Mih Svd* iCf`frartttHiM - f,tdtWM- Jivtfit 6i KtttkJ? W.*ic& \ Sc,05 ____ KMttw-..Si mm1 ' 11________ H B.KMOf- It. \_-- i 1-- 1 21 , /TO.------------- ------------ 1 ACTWtY P*9_L<rf i- KBWMOfl tm fcRhDIk.' Ihtta Mta W til 02. 14f{ 0? . 1417 tS ton r> ____ J1____ S-ltt-K*' 11. bt v ,frl> /Oil i wW i? 1? 17 lift 130 4 hM IM 7A 2.0 to U ** ** MJ w Si: Man IM um: R ...RJI WZ.e 2.4 ` 6 2.0 *4 j ! sfr &L Tfl/ MM IMnaaM IfVCUMfcM* {TEWWrf i i Rra nra* Mwl WTR |---------- . [li____________ ----------------------------------- 1--------------------- -- ImtflSaJS" >mi|ii r imi aa w hRM at Ma C M atm** * mm t cmm> n mm* at mu a--im u *rw Ml* U) M*a MR fnuMMNMiM Wtfk Wtfc laMtaMMkSKialalCtlltKiMaMMwM. ua . (Mat OucMRk tta hM mamtUMraa*a*a aanaMnk 14 M(/t M*WkHtaaa*aaataL tMlltMteUttarc^ kMMliW MM titanMil "MkCMiflc MkMMl*.**:C1.Y;tt.oa. it MMNIK W*42te jbRfflw: V-Tfl' flZT >****:_ baakTMe. jkaliMartil.... iy*r.. MUkat. MMfe. C*#M!___ tmaHjMMCMewiaujMi I ^ -<r> CO 3 ; 'tCO"" g_ ^ n ? g>r- ii ton CO NN CO CO <N C4 ^ MQ? N\*v0<. *S<*hv0. S5o< Q*\ <*3\ 4) 5 15 * Q U^ . s S5 &3 5Ss f Jo? o 2 o O*-u^ C 7oJ Ill I 05 03 02 O te a e 13 uo & C3 c * 2 O Vv l-J P? &* o g s S i*n * 8 0. s S' ne5o o S t3o -s tS 00 fe N 8T 5 Jt5 <Oo' ,*N 5 |4 tl 1 siJ5 3 "> 00 s tj g 05 ^3 43 Co 6K K 2o JD GC. cu < ^ a* ao co a o oo* o ? o CS o .3 O0tQt. 2 1 a a S fi I I 35 a I 5 VSV 888 -* ~ Ot * <N VCOH vWo s s c_q _m 0om mo ocq A r> r> n ^2 sc sc Ov n\ ^On n N 8N S .S Boeltcr tYates ANALYSIS OATAiOWN OF CUSTODY date COUOTHTBY: PROJECT HO.: M lt~ 1197 nmwmrote shris ANALYZBW '14HR SAWUONO. HIK TYPE WM3WWEAM IS UCAT10N 06 _ frr fid-irur- 1 67 frt IV _5 Wf M lo EyT _4_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ EkTi iv. : ..J ^r _________ 3 Ext S/ 13_ _ _ _ _ _ K?W!B ----<* t> ?! A0TMTT AESJHATCII rcre 1 ;- - - - - /V- - - - - - - - - - - - %- - - - - - - - - - - - - - - tala t*& i'-Bfcb-fcM-flf. rt*o It 14 _____ 07 H4 M oft' 1467 JCn r*nta MM iji MM Hit Mb PS 3JL. Rn..- 2,0 I M IMWf TMm Vml w 2i ttfc 2.X --jjLj*tfi inmpxmEiaeiE^i isnar?nifjOTf^isn (Mnfebf (tatwd initaM iMnW (TW4) Nr~Tai s=a Efil BES3 t___ 5 -BfiWdw-fi .____ . -- ! -r -ftlU.U__________ -Z 1 1 ------------ T"!------------------------------ 1 i i Zj "1 .jf! i i * NOTES: ttmUaf AM ad j ; MhNl MUX NtMCX a u OmM K9 to**** m MnM W . MUM 8 Mn C M*QbMM mi It *VM* M MkA ** It MM* C miarpMum U tXMA M twiN AM fnXAkNftttft) MXtXIM NOTE l**ta<*<NtfkXiU>ueEI>rM<MAn4<Mtf. UXt-UmNOMMa Tin--MWK|iiitrt<ww>MiltWBian;o Miftiitoi <i;hi l lniiialw:oaw<CTaMi4iMMnmf Ai TKhni>WM.<>Mn*,'Otr>;Ot.2,<e.<t*arNi fcifrr, l.Vfcfa. NNjIWIp^ Cwwry Bn/Toc___ PtMMNMtowrtR. OMOtM:. ton** IWIlK ivfrtyi- if*#. tmwv_ OiWBh: oMnMSMivonauKWMac RJ LeeGroup, Inc. 350 Hochberg Road Monroeville, PA 15146 Tel: (724)325-1776 Fax: (724)733-1799 June 4, 2002 The Materials Characterization Specialists Mr. Fred W. Boelter Boelter & Yates, Inc. 1300 Higgins Road Suite 301 Park Ridge, IL 60068-5772 RE: TEM Asbestos Results for Samples as Shown on the Test Report RJ Lee Group Job No.: ATH20S302 Client Purchase Order No.: 1941A-7237 Dear Mr. Boelter: Enclosed are the results from the transmission electron microscopy (TEM) asbestos analysis of the above referenced samples. The samples and volume information were provided by Boelter & Yates, Inc. personnel. As per your request, counting rules as described by the AHERA Method published in the Federal Register, 40 CFR, Part 763, October 30,1987 were used for the analysis.* The Test Report lists each sample identification number, area analyzed, sample volume, structure counts, analytical sensitivity, and the concentration of asbestos. Copies of the count sheets are presented in Appendix A. Each count sheet contains sample information pertaining to structure identification, dimensions, magnification, filter size and type. RJ Lee Group, Inc. is accredited by the National Voluntary Laboratory Accreditation Program (NVLAP) for selected test methods for airborne asbestos fiber analysis (TEM), asbestos fiber analysis (PLM), New York State Department of Health Environmental Laboratory Approval Program (ELAP), and by the American Industrial Hygiene Association (AIHA). This test report only relates to the items tested. NVLAP accreditation does not imply endorsement by NVLAP or any agency of the U.S. Government. The report shall not be reproduced except in full. These results are submitted pursuant to RJ Lee Group's current terms and conditions of sale, including the company's standard warranty and limitation of liability provisions and no responsibility or liability is assumed for the manner in which the results are used or interpreted. Unless notified in writing to return the samples covered by this report, RJ Lee Group will store the samples for a period of thirty (30) days before discarding. A shipping and handling fee will be assessed for the return of any samples. If you have any questions, feel free to call me. Very truly yours. KAA/slb Enclosures Received 8 samples Monroeville, PA San Leandro, CA Washington, DC Rasco, WA www.rifg.com 1 g v) s' C! CO VO C2 v C VO2 CN $ VO 3 ***** 8 s S 8a CO` o 0t}0 f- VTOf VTOf to sa o d d o VVVVV Cc Og '1 oa c6 * CO * CO * CO * CO * to <3 er to to to to to w wVVVVV cn M s s s\o \o to > to ;*5aoa5 o o o TT o o *t o o o CO uaa CO fO fO fO to v-i to to 3 ooooo I I I ooooo Test Report T otal Asbestos S tructure C oncentration CO CO CO CO to ito VO to SO to to to VO < 5S z dd s CO s to dr- SB 8 1 CNCNCNCNCO-sess tototototototouo QOOOOOOOOOOOOOOO COCOCOCOCOCOCOCO sj? 8 to **< CN CO i g s 2 s I B B t;1 s? BEB H *7 t-< o C *04 Q o Q O Q O Q o Q O Q O Q o o o m m m P5 m CQ U co >A A iA >A A <n IO >A o as 2| O2 o 3* CN r0*0- CO 0r0- COO o roo VO 00 r- r*C-* CorOo- 0rc^o\ CN CN CN CN CN 2 CO vo on fC'' ot>\ o Jc0O 01 X tin ;S ;|j *5ta>3 CO T3 VO -a it o in iV. <--c ? o * aSa,f S O o 8 o -- oaor. PS icnr> CoN *w5l CN *--< o *5> C^O ~g Da S'rS1" 2t <t*j ^B *^21 E |a * f< g< g o *3 *o o o aj -- u oj i a. i 0 (j 3 oo g- 1 S ' 1^ ^ wU* Z <j C a 9 8 og <u s I-} "VIU FIBER COUNT SHEET B = Bundle C = Cluster M = Matrix Appendix A i Client Name Boelter & Yates, Inc. Project Number ATH205302 RJL Sample # 0127872HT Client Sample # 5-BGD-TEM-01 Microscope 2000 FX Accelerating Volt 120 Kv Magnification 21000 X Analyst BF EDS Disk I Structure Field Fiber <5 pun 5 pm Type______ Morph 10 -1 2 0 31X 40 j 50 60 NSD NSD Nonasbestos NSD NSD NSD Nonasbestos RJ LeeGroup , Inc Count Sheet RJL QA Number Grid Openings Total Asbestos Total Non-Asbestos Filter Volume Grid Opening Area Amphibole EDS Photo SAED Type X NONE XX HQ20733 7 0 -2 CE 385 mm2 1230.0 Liters 0.0093 mm2 Comment i J NSD - No Structures Detected Page: 1 of 1 RJ Lee Group ,Inc Count Sheet Client Name Boelter & Yates, Inc. Project Number ATH205302 RJL Sample # 0127873HT Client Sample # 5-BGD-TEM-02 Microscope 2000 FX Accelerating Volt 120 Kv Magnification 21000 X Analyst BF EDS Disk Structure Field Fiber <5 pm S5pm Type Morph 10 20 30 40 5 1X 60 70 NSD NSD NSD NSD Nonasbestos NSD NSD RJL QA Number Grid Openings Total Asbestos Total Non-Asbestos Filter Volume Grid Opening Area Amphibole EDS Photo SAED Type XX HQ20733 7 0 1 CE 385 mm2 1250.0 Liters 0.0093 mm2 Comment NSD - No Structures Detected Page: 1 of I RJ Lee Group ,Inc Count Sheet Client Name Boelter & Yates, Inc. Project Number ATH205302 RJL Sample # 0127876HT Client Sample # 5-BGD-TEM-05 Microscope 2000 FX Accelerating Volt 120 Kv Magnification 21000 X Analyst BF EDS Disk Structure Field Fiber <5 pm a5|im Type Morph 10 20 30 40 50 60 70 NSD NSD NSD NSD NSD NSD NSD RJL QA Number Grid Openings Total Asbestos Total Non-Asbestos Filter Volume Grid Opening Area EDS Photo SAED Amphibole Type HQ20733 7 0 0 CE 385 mm2 1300.0 Liters 0.0093 mm2 Comment NSD - No Structures Detected Page: 1 of 1 "1 ,3 -J Client Name Boelter & Yates, Inc. Project Number ATH205302 RJL Sample # 0127875HT Client Sample # 5-BGD-TEM-04 Microscope 2000 FX Accelerating Volt 120 Kv Magnification 21000 X Analyst BF EDS Disk I Structure Field Fiber <5 pm S5|im Type Morph 10 1-~I\ 20 30 40 50 60 70 NSD NSD NSD NSD NSD NSD NSD RJ Lee Group , Inc Count Sheet RJL QA Number Grid Openings Total Asbestos Total Non-Asbestos Filter Volume Grid Opening Area Amphibole EDS Photo SAED Type__________ HQ20733 7 0 0 CE 385 mm2 1280.0 Liters 0.0093 mm2 Comment NSD - No Structures Detected Page: I of 1 ?! Client Name Boelter & Yates, Inc. Project Number ATH205302 RJL Sample # 0127876HT ill Client Sample # 5-BGD-TEM-05 Microscope 2000 FX Accelerating Volt 120 Kv - 1tl Magnification 21000X Analyst BF EDS Disk Structure Field Fiber < 5 um S 5 pm Type Morph 0 NSD 0 NSD 0 NSD 0 NSD 0 NSD 0 NSD 0 NSD RJ Lee Group ,111c Count Sheet RJL QA Number Grid Openings Total Asbestos Total Non-Asbestos Filter Volume Grid Opening Area Amphibole EDS Photo SAED Type HQ20733 7 0 0 CE 385 mm 2 1300.0 Liters 0.0093 mm2 Comment NSD; No Structures Detected Page: 1 of 1 APPENDIX E PLM Bulk Sample f Supertile J Capella TM Vinyl asbestos tile Everyone loves brick. And V understandably so. It never I tires the eye, and its robust i good looks go with practically B any decor. Imagine brick red Capella in a country kitchen, and a no-nonsense boy's room, a E book-lined den. or an informal living room ... In fact, anywhere. ! Supertile Libra Vinyl asbestos tile Libra... a lovely balance between pattern and texture in an all new tile. Random embossing traces a marbelized background, and the result-is a look of luxury and the prettiest play of light and shadow. Over-all patterns such as Libra are perfect for every room in your home. VA935 VA036 YA938 W.tnut VA03S 8 4 ] I i ( J SI g o Cf <Cof Cf Cf Cf H && u? ni J CO si I 03 8 $ I 'i ooor on< 10 10 << o> c0u 03 cow m 5-` Ocu m cOu CQ O0 03 POU n H I* o iII S0 o' flu 1 15 *s 8888 <S 5 $ t1 o QS 2 3 o MO ow w o wo o tT %u a Q Z Q Z Q Z Q Z Q Z Q 2 I I I I | CO i o SI c (& Zj 4 <0 2 tS gQ ? fl * .e5 1> -fff 5 ii >cSu* 010000 g<o Of 00 g 2 g S O CO5 T fl 2g o <S2 foe 22 o gto o 2 S aS4. soo g 8 bJ .. <aon *4a3 cSgof "OjsC> _a3, .. J<OcrCo. t7*oa3s sg Black Mastic Page2 o f 3 ]' ] ef o 4i 8 t U3 d ca] <2 COM a 5 '1 I o ch A Z ~ W Q* o s2 o| iS o--}; sO w <M VO cm Col oOf OCM 10 s* OT I 5 5 0) S ft.CL. o CL, o o a. o 3 CU O 03 CD m" OQ E-" (5 5& * 888 8 oM M o o wO 2 c i o 3 > z U A H r., a s 1 o>0 zd 0c 1 Cl Cl <8 ? J < $ 2 a- 32 o z Q Z Q Z az a z az 3 333 82 S i 810 10 o T4 ? ii g1 oo 5 'S H8 S 2vO o fil o S 1 > 95 i^ il ** * S uCU a cccoi 08vo* cu ffi C00O0> <O8of U a. S oi 00 8 VO Of SJ a 10 8 <8o Cf o aa 03 ^cO3 00 8 82 ?n/oj/c nicv- JQ^PIA 4 M3UJJCIN :0l T<T/-tr7/ le^lldo ;UJCj_f RJ Lee Group, In c .__________________ AIH A Accreditation No. 460 NVLAP Accreditation No. 101208-0 Laboratory Report (c o m .) RJLee Group Job No: AOH20558C PaeJ uJ 3 5*1 J 1i .J J /fa/?*#0 W Bodter& Yates, he. BULK SAMPLE SUMMARY-LABORATORY ANALYSIS REQUEST tensMwtYK,tov UMKahrM^ktewi --> `0 -^OntiBfeTiaSit llSps. .; A." IlilMht.- ^^wifftM^hlWMfiMatiMflii ,- >-'LHWfi titam kfcuad '. * ( ra. dew tMpbl. USA. n# I. *w ^fbl 4*rt .'* >WSiw"1v .' " *u5*bS " ~->-,-*lll4i',.W',' -?l ^- " . av^HpNnnp utWvTO \'i '? " .r.'W'. * wnp, .vfattmfi; WW.;: Tw*of; Cootfoa' taw -WNSO) - Fril Xii */, uhdl S^trev'iy -M Mft^yC bf ^n*cU" /z1* GjAyi^w, 7gj<r+ilt '*ii*i Mu* 7T w/-mUUl 4flL li'' CrftHtl t"wlr<-vf A^edfW)'*f4o3 . Alt? l ftV) TOT ___4ft! .\ f / ft ww r*wO -flLUtl 7Ci/Q7./$ `i)CO ji^sri j*aqnw -01 &,L\-ZL ttL lc=l'.a0 <uc-J Boefter&vaiesima BULK SAMPLE SUMMARY* LABORATORY ANALYSIS BEQUEST , '- :-'D.- CMMCwiife- --- . flight `"'V..5! -'*w> -.,r.;.: ^ M, .-I. \ i .-...~y~ ;''' '.' ' - : aT*,Tfn>--piihtawimtwi :. W * /ms) ^r?; wS/jif-7;*^?_** * 'r,';.;~ ;" *'" <Mr.- ::1 WfI w/ 4<W^ # 4#" ^Or Tfp**e CsMW MM iniem YnM \\ v/ u#*k'`WL> r X 1 >< s XV // s_______ \/ f X\ vS^ V \N iMrannuiisuKrftmamt n*,.*# ffi.Kpnlk*itHM. DiwtiWiUfMiwIal HOWISO: net <ttMMdiiiariMilfiamk tmail ^ r aillll 7A (rt^ isai*. j MArniPM *rtl CC / * n"r < .*.7 j iPnnrlrv`UJOJ J ] j COMPLETE REMOVAL 1370 VINTAGE CONGOLEUM t VINYL ASBESTOS TILE J RESIDENTIAL BATHROOM ] i ] ] ] ] ] June 27, 2002 BYI Project #1941A-7237 Boelter & Yates environmental engineers and scientists