Document xzw4gZezZONJ1oa31DGY3o0Ey

CWA FOCUSED COMPLIANCE INSPECTION REPORT U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 5 Purpose: Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process Facility: Milwaukee Metro Sewerage District (MMSD), Jones Island Biosolids Dewatering and Drying Facility NPDES Permit Number: WI-0036820-04 Date of Inspection: June 4, 2021 MMSD Representatives: Sid Arora, Contract Compliance Assistant Manager Patrick Obenauf, Contract Compliance Manager Steve Unger, Contract Administrator EPA Inspector: Dean Maraldo, EPA Region 5 Inspector; (312) 353-2098; maraldo.dean@epa.gov Wisconsin Department of Natural Resources Representatives: Frederick Hegeman, Wastewater Engineer Jacob Wedesky, Wastewater Engineer Report Prepared by: Dean Maraldo, EPA Region 5 Maraldo, Digitally signed by Maraldo, Dean EPA Inspector Signature: _D__e_a_n__________D17_a:t1e_9:_:2301_2-_10.5_0'60_.00_'9__________ Approver Name & Title: Ryan Bahr, Chief, Section 2, Water Enforcement and Compliance Assurance Branch Digitally signed by RYAN RYAN BAHR BAHR Date: 2021.06.09 Approver Signature/Date _______________1_7:_25_:2_1_-0_5'_00_' ____________ Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 [This page intentionally left blank] Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 TABLE OF CONTENTS I. Introduction .................................................................................................................................. 1 II. Background................................................................................................................................... 4 III. Inspection Activity summary........................................................................................................ 4 IV. Closing Conference ...................................................................................................................... 6 V. Documents Received .................................................................................................................... 6 LIST OF APPENDICES Appendix A: Aerial Image of MMSD's Jones Island Facility Appendix B: Facility Presentation "503 Compliance Update" Appendix C: March 2021 Monthly Report Appendix D: Photo Log Appendix E: Documents Received Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 [This page intentionally left blank] Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 I. INTRODUCTION On March 14, 2017, I, along with scientists from EPA's Office of Research and Development (ORD), and inspectors from EPA Region 7, conducted a biosolids inspection at the Milwaukee Metro Sewerage District Combined's (MMSD), Jones Island EQ Biosolids Dewatering and Drying Facility ("D&D Facility"). The D&D Facility is owned and operated by MMSD. Veolia Water Milwaukee, LLC, provides operational management and support for the production of EQ biosolids at the D&D Facility (See Appendix A - Facility map). MMSD sells and distributes processed biosolids as EQ biosolids under the product name "Milorganite." Once biosolids meet EQ requirements, they generally are not subject to further regulation under 40 CFR 503. As a result, 40 CFR 503 regulations include monitoring requirements to ensure EQ biosolids are safe for distribution to the public. EPA assessed MMSD's compliance with 40 CFR Part 503 and the National Pollutant Discharge Elimination System (NPDES) permit for the D&D Facility. During the March 14, 2017 inspection, EPA identified the following areas of concern: Heat drying temperature monitoring issues. MMSD did not measure the temperature of the sewage sludge particles or the wet-bulb temperature of the gas in contact with sewage sludge, as required under 40 CFR Part 503 (Appendix B (B)(2). Instead, MMSD measured temperature approximately 19 feet away from dryer furnace outlet along dryer discharge screw chute. Location of compliance sampling for fecal coliform and moisture content. Fecal coliform samples were collected from the process distribution pile, not at the point of bagging or at the time of load out into trains or trucks for offsite shipping. 40 CFR Part 503.32(a)(7) Class A-- Alternative 5 requires either the density of fecal coliform in the sewage sludge shall be less than 1000 Most Probable Number per gram of total solids (dry weight basis), or the density of Salmonella, sp. bacteria in the sewage sludge shall be less than three Most Probable Number per four grams of total solids (dry weight basis) at the time the sewage sludge is used or disposed, at the time the sewage sludge is prepared for sale or given away in a bag or other container for application to the land, or at the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in 503.10(b), (c), (e), or (f). Product moisture samples were collected after temporary storage in silos, not at the point of bagging. 40 CFR Part 503.33(3) requires one of the vector attraction reduction requirements in 503.33 (b)(1) through (b)(8) shall be met when sewage sludge is sold or given away in a bag or other container for application to the land. Fecal coliform sample preservation and holding time issues. MMSD stored fecal coliform samples at room temperature until the end of the month, when all samples were analyzed. Fecal coliform samples were not refrigerated to <10C and not analyzed within the standard holding time of 8 hours. The purpose of the announced June 4, 2021 inspection was to follow up on MMSD's actions to address the above areas of concern and assess MMSD's compliance with 40 CFR Part 503 and the NPDES permit for the D&D Facility. MMSD raised some concerns regarding COVID-19 and the face-to-face time needed to conduct the mainly indoor inspection of the D&D Facility. To address these concerns and limit face-to-face inspection efforts to only the physical inspection of the D&D Facility, we agreed to hold a pre-inspection teleconference on June 3, 2021, to discuss MMSD's efforts to address the above-referenced areas of concern. MMSD also presented a summary of recent biosolids compliance monitoring information (See 1 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix B "503 Compliance Update"). During the teleconference, MMSD described its new fecal coliform preservation and holding time protocols to address concerns raised during the March 2017 inspection. MMSD now refrigerates samples and analyzes samples within required holding times for fecal coliform. MMSD also described its new temperature monitoring system, including new temperature probes in each dryer and recycling bin. MMSD now utilizes two compliance methods to demonstrate Class-A biosolids compliance at any given time, including 40 CFR Part 503 Dryer Discharge Temperature method (Primary) and Recycle Bin Discharge Temperature method (40 CFR Part 503 Time and Temperature method )(Secondary). MMSD describes the Class-A biosolids system overview and compliance methodology as follows (March 2021 Monthly Report, Appendix C): The drying system consists of twelve Dryers, three Recycle Bins and several product conveyors. The dryers are laid out in two groups - North Side Dryers (1-6) and South Side Dryers (7-8). A recycling bin is at the end of each group of six dryers. The third recycle bin acts as redundant and can serve either side of dryers. From the recycle bin, most pellets return to the dryers. The remaining pellets go to classification and product screening. Figure 1 (below) represents a typical day of biosolids processing with 8 dryers operating (4 Dryers on the North Side and 4 Dryers on the South Side) with Recycle Bins 1 and 2 routing dried product either back to the Dryers or allowing it to go to Classification and Screening through automatic slide gates. The dry mass values on Figure 1 represent annual averages as monitored over the years. Figure 1 also shows the approximate location of the temperature monitoring devices at the discharge end of each dryer and at the discharge end of the recycle bins. [40 CFR Part 503] Alternative 5-503.32(a)(7) and Appendix B.B.2 (Heat Drying) is used as the Primary means to demonstrate compliance with 503 Regulation for Class A. In this method, dryer discharge product temperatures for all in-production dryers stay above 176F. Automatic controls in each dryer recycle all product leaving the dryer back to the inlet of the dryers if a discharge temperature falls below 180F. [40 CFR Part 503] Alternative 1-503.32(a)(3) (Time Temperature) is used as the secondary means to demonstrate compliance. This method is only used when the primary method does not demonstrate compliance. In this method, we continuously monitor the recycle bin discharge temperature and determine detention time of the product through the recycle bin. The District continuously calculates a required temperature by using 40 CFR Part 503(a)(3) Equation 2 for the current detention time. Comparison between the measured recycle bin discharge temperature and the required temperature determines compliance with this method. If a 15-minute dryer discharge product temperature is below 176F at any individual dryer discharge, then the District will use recycling bin time and temperature to demonstrate pathogen reduction. Use of time and temperature will continue until 40 minutes after all in-drum product temperatures are higher than the required temperature. 40 minutes is the worst-case product travel time from the dryer farthest from the recycling bin to the outlet of the recycling bin. If time and temperature does not show compliance, then the gates between the recycle bin and classification & screening will automatically CLOSE. In this configuration, all product will return to the dryers. These gates are reopened when time and temperature show compliance or Dryer discharge temperature show continuous compliance for at least 40 minutes. Figure 2 (below) shows overall compliance strategy to demonstrate compliance with 503 Class A. 2 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 3 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 According to MMSD, since implementing the new temperature monitoring system, dryer temperatures consistently meet the Dryer Discharge Temperature requirements. Before the pre-inspection teleconference, Wisconsin Department of Natural Resources ("WDNR") inspector Fred Hegeman provided monthly compliance reports for the D&D Facility for April 2020 thru March 2021. According to the reports, final biosolids product met temperature (40 CFR Part 503 (Appendix B (B)(2)), fecal coliform (40 CFR Part 503.32(a)(7)), and moisture content (40 CFR Part 503.33(3)) requirements. II. BACKGROUND MMSD is authorized to discharge treated wastewater from the Jones Island Water Reclamation Facility to Lake Michigan, Milwaukee Harbor, and tributary streams in Milwaukee County under NPDES permit number WI-0036820-04 ("Permit"). The Permit also includes land application requirements for EQ biosolids produced at the D&D Facility. The Facility's Operations Department is responsible for operating the D&D Facility and for compliance with the Permit. MMSD is responsible for conducting monitoring activities and reporting monitoring results to the WDNR and EPA. MMSD's Jones Island Water Reclamation Facility (JIWRF) began operating in 1925. MMSD began producing Milorganite at the JIWR Facility in 1926. The current sludge D&D Facility is located within the JIWR Facility and began operation since 1994. The D&D Facility treats sludge from the JIWR Facility and MMSD's South Shore Water Reclamation Facility. Milorganite is produced at the D&D Facility from sludge collected at the two facilities. Milorganite is marketed as commercial fertilizer and sold in bags at retail stores or shipped via rail and truck to commercial customers in the USA, Canada, and elsewhere. III. INSPECTION ACTIVITY SUMMARY The June 4, 2021 inspection consisted of the following activities: Inspection opening conference; Physical inspection of the D&D Facility; and Closing conference and area of concern review. This report summarizes the results of the inspection. The list of attendees is included below. Note that numerous representatives attended on behalf of MMSD, and below I list only the MMSD representatives with key roles in leading the physical inspection or responding to questions: MMSD: Sid Arora, Contract Compliance Assistant Manager Patrick Obenauf, Contract Compliance Manager Steve Unger, Contract Administrator Tom Cox, Operator (Veolia Water Milwaukee) Zach Ream, Operator (Veolia Water Milwaukee) EPA Region 5: Dean Maraldo, Inspector/Enforcement Officer WDNR: Frederick Hegeman, Wastewater Engineer Jacob Wedesky, Wastewater Engineer 4 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 III. A. Opening Conference I arrived at the MMSD Jones Island Water Reclamation Facility Operations Building at 8:45 am on June 4, 2021. I met WDNR engineers Frederick Hegeman and Jacob Wedesky and the MMSD representatives listed above and began the inspection opening conference with introductions at 8:57 am. Due to COVID19 concerns, all participants wore face masks. I presented my EPA-issued Inspector credentials to Patrick Obenauf (MMSD). I discussed the intent and scope of the inspection. I mentioned my plans to take photographs during the inspection, focusing on the new temperature monitoring system and asked if there were any potential confidential business information concerns. Patrick Obenauf said they would have no concerns about taking photographs but asked to confirm before taking each photograph. I agreed, and no concerns were raised with any of the photographs taken during the inspection. Before starting the physical inspection, I asked the MMSD representatives if the new fecal coliform preservation and holding time protocols mentioned during the pre-inspection teleconference were available in written form, such as a standard operating procedure or memo. Sid Arora said they would relay the request to the laboratory manager. III. B. Physical Facility Inspection - D&D Facility We started the physical inspection of the D&D Facility at 9:04 am. Photographs referenced below are included in the Photo Log (Appendix D). Sid Arora, Patrick Obenauf, and Steve Unger led portions of the tour. To minimize concerns regarding COVID-19, we agreed to focus the inspection on the new temperature monitoring system. We began with an overview of the south side dryers (Photograph MMSD0001), then stopped at the three recycle bins (30-ton capacity each) which collect treated material from the dryers and directs material either back to recycling or to classification and screening. The recycle bins are now equipped with temperature probes to monitor for the secondary means to demonstrate compliance (Time and Temperature) as described on page 3, above, and in Appendix C. Sid Arora mentioned that MMSD installed three temperature probes per bin for redundancy (Photograph MMSD0002). Next, we stopped at the product samplers station. Steve Unger explained that the sampler collects an aliquot for every four tons of material over 24 hours. This sampling location is known as WPDES Permit Sampling Point (Outfall) 006 - Jones Island EQ Sludge - PRODUCTION. We walked to the south side dryer area and observed Dryer #1S, which was out of service at the time of inspection. Since the dryer was out of service, we were able to look inside the dryer and observe one of two new temperature probes (Photograph MMSD0004). Patrick Obenauf mentioned that each dryer has two new temperature probes on opposites sides of the dryer to measure temperature and each probe has a unique control signal. Photograph MMSD0005 captures the same probe from outside of Dryer #1S. I asked for copies of the specifications for the new temperature probes. Steve Unger said they would pull together the probe specifications and follow up after the inspection. On the way to the operation control center, we stopped at the former temperature compliance monitoring location, approximately 19 feet away from the dryer furnace outlet along the dryer discharge screw chute (Photograph MMSD0006). Patrick Obenauf confirmed that the location is no longer used for 40 CFR Part 503 compliance monitoring. The last stop in the D&D Facility was the operations control center (Photograph MMSD0007). The center is where operators monitor the treatment and control process, including the temperature monitoring system. Photograph MMSD0009 captures a control screen that monitors the temperature and status of all 12 dryers. Fred Hegeman asked the two operations control center operators, Zach Ream and Tom Cox, how the new temperature monitoring system is working. The operators described how the system improved control over drum temperature. Referring to the new temperature monitoring system, operator Zach Ream added that "monitoring is easier now" and "it's awesome." 5 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 On the way out of the D&D Facility, I asked Sid Arora if they've experienced any compliance issues since implementing the new temperature monitoring system. Sid Arora said they've had no compliance issues. At the request of Fred Hegeman, Steve Unger led the group past the silos to observe the silo load-out facility. On the second floor of the load-out facility, we observed the belt conveyer which transports Milorganite product from the silos to the load-out facility. Photograph MMSD0010 captures the belt conveyor and product autosampler. Steve Unger identified the product autosampler location as WPDES Permit Sampling Point (Outfall) 008 - Jones Island EQ Sludge - SHIPPING. Steve Unger added that all finished Milorganite material, except for some special orders, is now loaded out to two offsite bagging facilities on Jones Island at Kinder Morgan and Spring Valley facilities, where compliance samples are collected at WPDES Permit Sampling Points (Outfall) 009 - Jones Island EQ Sludge - BAGGING. We completed the physical inspection at 10:14 am. IV. CLOSING CONFERENCE I began the closing conference at the Jones Island Water Reclamation Facility office at 10:20 am with the WDNR and MMSD representatives in attendance. I mentioned that I did not observe any preliminary areas of concern, and added that areas of concern may be identified after reviewing information collected as part of the inspection. I asked the group if they had any questions. There were no questions. However, Steve Unger mentioned that the new temperature monitoring system and strategy was "overall a good thing for us." I asked if MMSD could provide the two items requested earlier in the inspection (fecal sampling procedures and temperature probe specifications) within one week. Patrick Obenauf agreed with the requested timeframe. I provided the group with an estimated timeframe for completing the inspection report, and we concluded the closing conference at 10:25 am. I departed the Jones Island Water Reclamation Facility at 10:30 am on June 4, 2021. V. DOCUMENTS RECEIVED Documents received after the inspection (included in Appendix E): MMSD LAB-031 Quantification of Fecal Coliform and Total Coliform Bacteria in Biosolids by MPN REV.0.4 (1/4/2021) Milorganite Fecal Coliform Chain of Custody Form Thermowell and Bosset Fitting Data Form Wireless Transmitter Equipment Data Form Specific resource included by reference: Milwaukee Metropolitan Sewerage District Combined WPDES Permit# WI-0036820-04; issued by WDNR on March 27, 2019; expiration date March 31, 2024. 6 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix A: Aerial Image of MMSD Jones Island Facility Google Earth aerial image of the Facility, dated June 18, 2015. Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 [This page intentionally left blank] Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix B: Facility Presentation "503 Compliance Update" Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 503 Compliance Update EPA WDNR WDNR Visit June 2021 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 1 Presentation Outline Overview of the drying system MMSD 503 Regulation Compliance Plan Dryer Discharge Temperature Mode- Controls Strategy Recycle Bin Temp Mode- Controls Strategy Construction Sequence Operations Summary 2019-Present Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 2 Recycle Feed to dryer in Dry Tons/Day (Typica Mass) 180 Recycle Product returning from Recycle Bin, Dry Tons/Day (Typical Mass) 502 Sludge Cake Feed to dryer, Dry Tons/Day (Typical Mass) 18 180 Dryer7 Drying and Recycle System Schematic 18 18 18 180 180 Dryer8 Dryer9 Dryer10 Dryer11 Dryer12 574 502 Redundant 0 Recycle Bin and Recycle Train 502 Temperature Monitoring Device Gate to Classification RECYCLE BIN 1 RECYCLE BIN 3 RECYCLE BIN 2 72 To Classification & Screening of Milorganite 72 Dryer1 Dryer2 Dryer3 Dryer4 Clea1n8W0ater Act June 4, 2021 Focused 18 Complia1n8c0e Inspection - Milorganite1B8i0osolids 18 Process 18 180 18 Dryer5 Dryer6 South Dryers and recycle system are Mirror Image of the North Appendix B, page 3 Dryer Temps for all in-service dryers per side Biosolids 503 Reg Compliance Plan IN Compliance >176F Time Temp Method IN Compliance for > 40 Mins & Ave Dryer Temps for all in service Dryers >176 IN Compliance (Gate to classificatio n stay OPEN) TimeTemp Condition Met? IN Compliance (OPEN Gate to classification) Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Close the gate to Classification and Recycle all material Condition Met with Recycle mass <25 tons Store In Day Tank Landfill Segregate Product Available room in recycle System Appendix B, page 4 503 Regulation Compliance Strategy We can use any one of the compliance methods to demonstrate CLASS-A compliance in any given time: Dryer Discharge Temperature (Primary Method) Recycle Bin Discharge Temp (Time Temperature)(Secondary Method) Helminth Ova & Virus Testing (Emergency Method) Only Few States Including WI Allow this. Product Produced by this method will stay in WI Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 5 Primary Method- Dryer Temperature WPDES Permit Requirements Dryer Drum Product Temp for all dryers In-Production >176 on continuous basis IN-Production: Dryer IN Service and NOT in ADDBACK Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Dryer Drum Product Temperature Appendix B, page 6 DRYER Temperature MODE for North or South Side This is the Primary Method to demonstrate compliance This Mode is Active per Side (North or South) when: Drum Temperatures > 176F for all Inservice Dryers which are not in Addback If a Dryer is in Addback there is no product leaving the system, hence is not included to determine the Active Mode per side. Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Dryer Drum Temp Appendix B, page 7 Auto Add Back Mode ACTIVE Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Drum Temp Monitoring Discharge Screw Temp Monitoring Appendix B, page 8 Product Mapping Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 9 Dryer Temperature Study Report Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Dry Bulb Air Temps are more conservative measurements as compared to Product Temps Appendix B, page 10 Drum Temp Probes Up Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 11 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 12 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 13 Primary (P) and Secondary (S) Temperature Sensors During normal operation (P) is used for compliance demonstration and nothing is displayed next to drum temperature. Normal operation is defined as when the difference between temperatures measured from Primary and Secondary sensors ( T) is less than 10F. If T is greater than 10F, letters (P) and (S) will be displayed next to the drum temperature. Sensor being used will be highlighted Red and the other sensor will be Flashing Yellow highlight. For example, PS indicates that sensor (S) is being used and (P) needs repair. Hence operator should put in the work request for sensor (P). Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 14 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 15 Alarms and Warnings Normal Operation Warning Alarm Add-Back Mode ACTIVE ALARM When Add-Back ACTIVE Dryer Discharge Screw Starts IF Dryer Drum Temperature HMI Drum Temperature Data Display Discharge Screw Temperature 180F 176F < T < 180F Blue Text Yellow <180F "ACTIVE" 176F 180F for 5 min OR > 200F FLASHING RED Blue Text > 220F Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 16 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 17 Secondary Means of Demonstrating Compliance with 503 Regulation Alternative I: Time-temperature Regime Meet the Established relation between Detention Time and Product Temperature Alternative 2: Biosolids Treated In A High Ph-high Temperature Process Alternative 3: Biosolids Treated In Other Processes Alternative 4: Biosolids Treated In Unknown Processes Alternative 5: Biosolids Treated In Processes To Further Reduce Pathogens Such As Heat Drying Alternative 6: Biosolids Treated In A Process Equivalent To A PFRP Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 18 Evaluation of Time Temperature Method 3 Recycle Bins with capacity of 30 tons each Product discharging the recycle bin approx. 160F Retention time in each recycle bin approx. 20 minutes Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 19 TRACER Study Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 20 Recycle Bin-Time Temperature 3 Temp Probes Installed in each Recycle Bin Using Existing Parameters monitored in HMI added calculation for Retention Time in Recycle Bin Used Safety Factor in Retention Time Calculation based on Continual evaluation of Tracer Study Automatic closure of discharge gate and recycle all material when time temperature requirements are not met Operator verify visually and document gate closed Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 21 Recycle Bin Display Data Recycle Bin Tonnage and T (Required- Actual Bin Temperatures) display YELLOW, if minimum requirements for time-temperature are not being met. Out of Service Bin Shown in Gray Gate Requested Position Actual Gate Position Actual Bin Mass Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 22 Condition for Switching Compliance Mode - Dryer Temp to Recycle Bin Temp 1. In-service dryer Drum T 176 F and add-back fails to engage for that dryer for 15 seconds 2. If Operator MANUALLY takes in-service dryer out of add back mode (manually starts discharge screw) and drum T 176F Dryers Getting too full Temperature Rising Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 23 Recycle Bin Temp MODE for North or South Side This Mode is Active per Side (North or South) when any Drum Temperature <176F for all Inservice Dryers which are not in Addback Permit Conditions: Measured Recycle Bin Discharge Temperature should be > Required Temperature AND The detention time through the bin should be 20 minutes or greater. "Required Temperature": Calculated based on the Detention Time in the Recycle bin. Higher the Detention Time in the Bin lower the required temperature and vice versa. Recycle Bin Discharge Temp > Required Temperature then gate to Classification is OPEN (Auto) Recycle Bin Discharge Temp < Required Temperature then gate to Classification is CLOSED(Auto) (OPERATORS VERIFY THAT GATES ARE CLOSED) Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 24 Alarms and Warnings Normal Operation ALARM & Gates to Warning Alarm Classification Closes Outlet Gate Reopens HMI Data Blue Text Yellow FLASHING RED Blue Residence time Bin Temp - Req Temp = Temp Delta ( T) 3F 1F T < 3F 20 min OR < 1 F > 20 min AND 3F * NOTE: OPERATOR MUST PHYSICALLY VERIFY AND DOCUMENT THAT GATES TO CLASSIFICATION ARE CLOSED FOR THE NON-COMPLIANT BIN. Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process Appendix B, page 25 June 4, 2021 Condition for Switching Compliance ModeRecycle Bin Temp to Dryer Temp When in Recycle Bin Mode for North or South Side and the Dryer Drum Temperatures for all in-production dryers for that side become greater than 176F, a countdown timer is displayed on HMI. When the timer countdowns 40 minutes, the compliance mode is switched to Dryer Compliance Mode. Why 40 minutes? Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 26 Construction Sequence Activity Completion Date Dryer Drums Tested Accutech wireless transmitter for continuous temperature monitoring 7/26/2018 Installed first thermowell and temperature sensor (RTD) with wireless transmitter 10/16/2018 Installed thermowells and RTD with wireless transmitters in all 12 dryer drums 2/28/2019 Installed and tested two redundant RTDs with wireless transmitter 7/9/2019 Completion adding a dedicated power supply for each RTD receiver radio 10/8/2019 Ready to test second RTD installed in Dryers 6 and 12 10/25/2019 Completed installation of redundant RTDs in all 12 dryers 11/19/2019 Recycle Bins Installed and tested first hardwired RTD at a recycle bin 9/24/2018 Completed recycle bin tracer testing to establish residence time 10/22/2018 Installed and collecting data from two hardwired RTDs in each of three recycle bins 11/15/2018 Installed a third hardwired RTD in two active recycle bins 1/24/2019 Installed a third hardwired RTD in redundant recycle bin 4/5/2019 Completed rebuilding all 6 recycle bin outlet gates with SS material to ensure proper ope8r/a3ti1o/n2019 Installed and tested 6 inductive sensors to confirm recycle bin outlet gates "closed" 9/17/2019 Milorganite Temperature Monitoring and Compliance Programming Completed initial PLC programming to control processes to ensure compliance 12/21/2018 Revised control program to use dryer drum temperature as primary compliance measure 3/1/2019 Completed and tested programming to record compliance and place data to historian 3/22/2019 Installed compliance monitor in operator control room (HMI Screen) 4/5/2019 Programmed automatic addback at each dryer to recycle product if temp. <176 F 4/26/2019 Implemented full operation of compliance program for Milorganite production 4/26/2019 Generated first monthly compliance report from Hach WIMS 5/3/2019 Added 20 min. minimum residence time to time-temperature compliance program 9/5/2019 Added 15 sec. delay when switching to time-temperature mode from dryer mode 9/20/2019 Completed programming for redundant RTDs at all 12 dryer drums 10/31/2019 Completed FATs for all compliance modes 2/14/2020 Training, O&M Manual and Spare Parts Completed initial operator and maintenance training on new system Completed operator training on revised compliance program Transferred first shipment of spare instrument parts to Veolia Anticipate completing second version of O&M manual Clean Water Act FToracnusfeedrrCeodmfpinlialnscheipInmspeencttiofns-paMrieloirngsatnriutemeBnitopsoalritdsstPorVoceeoslsia June 4, 2021 Conducted second training session with Veolia operators, 2 days 11/28/2018 3/19/2019 5/30/2019 10/31/2019 12/10/2019 2/12/2020 Appendix B, page 27 Summary - April 2019 through Present All stored and shipped product complied with Dryer Temp or Time Temp Most of time complied with Dryer Temperature Mode Isolated events in Time Temp Mode Example May 28, 2020 One event - had to send product from day tank back to drying system May 31, 2021 Communication failure caused gate control issue No events where we had to send product to landfill Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 28 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 29 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix B, page 30 Appendix C: March 2021 Monthly Report Milorganite Fertilizer 503 Regulation Class A Compliance Monitoring Report Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Milorganite Fertilizer 503 Regulation Class A Compliance Monitoring Report March 2021 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 1 Table of Contents Section 1: Milorganite Solids and Fecal Coliform Results at Various Outfalls Section 2: Drying System Temperature Monitoring Dryer Recycle 2.1 System Overview and Compliance Methodology 2.2 Operations Notes for March 2021 2.3 Dryer Discharge Product Temperature Monitoring 2.4 Time Temperature Monitoring Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 2 Section 1: Milorganite Solids and Fecal Coliform Results at Various Outfalls Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 3 March 2021 Results Sample Collection Date Outfall 3/9/21 009 3/9/21 009 3/9/21 008 3/2/21 006 3/9/21 006 3/16/21 006 3/23/21 006 3/30/21 006 Sample Location BAGGING - Kinder Morgan BAGGING - Spring Valley SHIPPING PRODUCTION PRODUCTION PRODUCTION PRODUCTION PRODUCTION Fecal Coliform Limit MPN/gTS Sample Results MPN/gTS <1000 <1000 <1000 <1000 <1000 <1000 <1000 <1000 < 0.19 < 0.19 < 0.19 < 0.19 < 0.19 < 0.19 < 0.19 < 0.19 Solids, Total Limit % TS Sample Results % TS 90 95 90 95 90 95 90 96 90 94 90 96 90 96 90 94 Milorganite Production = 3,555 ton/month Milorganite to Kinder Morgan Bagging = 3,574 tons/month Milorganite to Spring Valley Bagging = 332 tons/month Milorganite Shipped = 3,959 tons/month Note: - The results shown above are for grab samples collected at Outfalls 6, 8, 9 as defined in the WPDES Permit WI-0036820-04-0 - For all samples shown in the table above, fecal coliform analyses are started within 8 hrs. of collection, as per EPA Method 1680 - All Milorganite Produced in a month is not necessarily bagged or shipped the same month Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 4 Section 2: Drying System Temperature Monitoring Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 5 Section 2.1: System Overview and Compliance Methodology The drying system consists of twelve Dryers, three Recycle Bins and several product conveyors. The dryers are laid out in two groups - North Side Dryers (1-6) and South Side Dryers (7-8). A recycling bin is at the end of each group of six dryers. The third recycle bin acts is redundant can serve either side of dryers. From the recycle bin, most pellets return to the dryers. The remaining pellets go to classification and product screening. Figure 1 represents a typical day of biosolids processing with 8 dryers operating (4 Dryers on the North Side and 4 Dryers on the South Side) with Recycle Bins 1 and 2 routing dried product either back to the Dryers or allowing it to go to Classification and Screening through automatic slide gates. The dry mass values on Figure 1 represent annual averages as monitored over the years. Figure 1 also shows the approximate location of the temperature monitoring devices at the discharge end of each dryer and at the discharge end of the recycle bins. Alternative 5-503.32(a)(7) and Appendix B.B.2 (Heat Drying) is used as the Primary means to demonstrate compliance with 503 Regulation for Class A. In this method, dryer discharge product temperatures for all in-production dryers stay above 176F. Automatic controls in each dryer recycle all product leaving the dryer back to the inlet of the dryers if a discharge temperature falls below 180F. Alternative 1-503.32(a)(3) (Time Temperature) is used as the secondary means to demonstrate compliance. This method is only used when the primary method does not demonstrate compliance. In this method, we continuously monitor the recycle bin discharge temperature and determine detention time of the product through the recycle bin. The District continuously calculates a required temperature by using 40 CFR Part 503(a)(3) Equation 2 for the current detention time. Comparison between the measured recycle bin discharge temperature and the required temperature determines compliance with this method. If a 15-minute dryer discharge product temperature is below 176F at any individual dryer discharge, then the District will use recycling bin time and temperature to demonstrate pathogen reduction. Use of time and temperature will continue until 40 minutes after all in-drum product temperatures are higher than the required temperature. 40 minutes is the worst-case product travel time from the dryer farthest from the recycling bin to the outlet of the recycling bin. If time and temperature does not show compliance, then the gates between the recycle bin and classification & screening will automatically CLOSE. In this configuration, all product will return Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 6 to the dryers. These gates are reopened when time and temperature show compliance or Dryer discharge temperature show continuous compliance for at least 40 minutes. Figure 2 shows overall compliance strategy to demonstrate compliance with 503 Class A. Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 7 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 8 Section 2.2 Operations Notes- March 2021 Dryer discharge product temperatures for all in-production South Side Dryers (Dryers 1-6) were greater than 176F for the entire month, except on March 3, 2021 at 04:29 hours for Dryer 1, and on March 14, 2021 at 05:01 hours for Dryer 3. Dryer discharge product temperatures for all in-production North Side Dryers (Dryers 7-12) were greater than 176F for the entire month. DRYER 1 - March 3, 2021, 04:29 hours At 04:29 hours on March 3, 2021 Dryer 1 was in add back mode due to product temperature less than 176F. The dryer was in add back mode for a prolonged time and eventually became too full. Hence the Operator manually took Dryer 1 out of add back mode. To take the dryer out of add back mode, the Operator manually turned on the discharge screw. At that time, the Dryer 1 discharge product temperature was below 176F, therefore the system controls for South Side Dryers immediately shifted to the Time Temperature mode for compliance demonstration. While in Time Temperature mode, the Recycle Bin discharge temperature and detention time did not meet the required conditions of Time Temperature. Hence the gates to classification and screening were automatically closed and all product was recycled back to the South Side Dryers. Additionally, Operators visually verified that no product was going to classification - the gates to classification were closed. About 1 hour later, Dryer 1 was in compliance and compliance strategy switched back to dryer discharge product temperature mode. Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 9 DRYER 3 - March 14, 2021, 05:01 hours At 05:01 hours on March 14, 2021 Dryer 3 was in add back mode due to product temperature less than 176F. It was in add back mode for a prolonged time and eventually became too full. Hence the Operator took Dryer 3 out of add back mode. To take the dryer out of add back mode, the Operator turned on the discharge screw. At that time, the Dryer 3 discharge product temperature was below 176F, therefore the system controls for South Side Dryers immediately shifted to the Time Temperature mode for compliance demonstration. When the south dryers first shifted to Time Temperature mode, the Recycle Bin discharge temperature and detention time did indeed meet the required conditions of Time Temperature. Hence the gates to classification and screening were initially left open as shown on Table #3. However, shortly after the shift to Time Temperature mode, the Recycle Bin temperature dropped and no longer met the required conditions of Time Temperature. Hence the gates to classification and screening automatically closed and all product was recycled back to the South Side Dryers. At this time, Operators visually verified that no product was going to classification while the gates to classification were closed. About 1 hour later, Dryer 3 was in compliance and compliance strategy switched back to dryer discharge temperature mode. Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 10 Section 2.3. Dryer Discharge Product Temperature Monitoring Graph 1: South Side Dryer Discharge Product Temperature Monitoring Graph 2: North Side Dryer Discharge Product Temperature Monitoring Table 1: South Side Dryers Daily Minimum Discharge Product Temperatures Table 2: North Side Dryers Daily Minimum Discharge Product Temperatures Notes for Graphs 1 and 2 1. Temperature data is presented on these graphs as 15-minute average when the dryer is in production. 2. Temperatures are measured at end of heated zone of each dryer by a resistance temperature detector (RTD) thermometer located in a thermowell on the interior wall of dryer drum. 3. Dryer discharge temperatures are measured continuously and are recorded in reporting database as a 15-minute average. 4. If any dryer temperature drops below 176F, the system control shifts to time temperature control and the data is presented in the Time-Temperature Mode Table. Notes for Tables 1 and 2 1. Data represents the daily minimum 15-minute average temperatures when the dryer was in production. 2. Blank spaces represent that the dryer was out of service the entire day. Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 11 Graph #1 - Dryer Discharge Temperature - South Dryers - March 2021 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 12 Graph #2 - Dryer Discharge Temperature - North Dryers - March 2021 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 13 Table #1 Daily Minimum Discharge Product Temperature - South Dryers - March 2021 Date 03/01/21 03/02/21 03/03/21 03/04/21 03/05/21 03/06/21 03/07/21 03/08/21 03/09/21 03/10/21 03/11/21 03/12/21 03/13/21 03/14/21 03/15/21 03/16/21 03/17/21 03/18/21 03/19/21 03/20/21 03/21/21 03/22/21 03/23/21 03/24/21 03/25/21 03/26/21 03/27/21 03/28/21 03/29/21 03/30/21 03/31/21 Dryer #1 168.90 205.39 202.98 203.68 190.54 191.99 217.11 204.96 201.10 208.39 203.92 186.87 193.59 185.60 194.37 193.61 217.72 180.99 183.51 193.74 199.48 198.37 194.98 197.37 189.45 Daily Minimum Discharge Product Temperature Dryer #2 Dryer #3 Dryer #4 Dryer #5 227.30 205.62 205.93 213.85 185.81 192.83 181.85 193.44 190.54 201.82 191.42 202.30 198.77 199.01 203.72 187.11 202.87 205.25 198.87 200.32 210.28 210.35 187.70 214.09 206.36 198.58 205.29 199.70 199.50 214.73 196.69 198.92 182.23 191.58 187.54 184.97 190.89 187.93 183.90 192.99 170.78 184.93 195.55 190.09 204.95 186.15 192.32 210.03 217.58 201.37 190.67 187.00 199.93 195.16 206.05 187.87 196.46 186.34 197.69 184.24 193.40 190.38 187.45 181.09 187.67 192.35 194.49 191.67 195.09 203.81 186.87 181.25 206.66 183.12 189.70 189.27 203.23 198.23 194.63 183.07 191.03 193.17 204.81 182.29 195.66 191.94 203.40 194.51 189.56 190.62 195.81 183.71 193.25 191.05 208.92 199.67 199.28 185.61 197.43 202.53 185.21 183.85 209.19 185.05 209.14 198.21 182.77 203.68 187.71 182.05 190.88 Dryer #6 213.41 196.88 195.95 193.22 190.16 196.66 197.18 203.53 185.97 191.25 186.70 191.70 182.34 189.97 186.40 194.95 193.30 184.48 199.70 188.09 200.64 183.63 183.34 3693 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 14 Table #2 Daily Minimum Discharge Product Temperature - North Dryers - March 2021 Daily Minimum Discharge Product Temperature Date Dryer #7 Dryer #8 Dryer #9 Dryer #10 Dryer #11 Dryer #12 3699 03/01/21 193.75 221.39 215.84 221.29 209.46 212.32 0.00 03/02/21 203.10 217.72 212.96 212.39 203.67 0.00 03/03/21 196.99 185.00 183.28 192.20 199.14 0.00 03/04/21 188.73 196.51 211.49 202.81 204.39 0.00 03/05/21 203.12 186.21 202.83 203.69 208.29 0.00 03/06/21 191.73 191.34 202.68 190.82 206.03 0.00 03/07/21 192.66 209.01 201.76 206.91 206.58 0.00 03/08/21 198.11 220.71 201.80 218.14 204.83 0.00 03/09/21 185.12 210.76 192.31 190.29 203.64 0.00 03/10/21 189.54 197.21 202.52 217.47 210.02 0.00 03/11/21 186.06 212.22 203.62 218.75 198.27 0.00 03/12/21 185.93 201.55 203.22 218.31 200.37 0.00 03/13/21 185.94 193.50 203.62 199.85 198.76 0.00 03/14/21 197.27 202.20 196.44 195.87 203.04 0.00 03/15/21 203.66 220.13 200.40 210.95 0.00 03/16/21 206.72 225.18 208.72 215.40 0.00 03/17/21 199.96 227.77 202.72 216.28 0.00 03/18/21 187.50 181.61 190.81 190.79 0.00 03/19/21 185.52 192.54 199.87 204.42 0.00 03/20/21 191.56 195.16 200.24 187.13 0.00 03/21/21 198.84 185.62 189.31 197.45 0.00 03/22/21 189.90 201.64 198.94 182.47 0.00 03/23/21 185.31 195.66 195.33 204.06 0.00 03/24/21 194.64 211.18 201.71 206.45 0.00 03/25/21 195.05 211.34 197.09 207.83 0.00 03/26/21 193.17 211.12 184.25 185.28 0.00 03/27/21 209.01 221.78 211.05 199.58 0.00 03/28/21 206.73 186.80 211.56 211.95 0.00 03/29/21 182.93 191.56 184.11 190.59 0.00 03/30/21 187.65 193.84 192.05 187.39 0.00 03/31/21 185.94 185.32 196.32 192.79 0.00 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 15 Section 2.4 Time Temperature Monitoring Table 3: South Side Time-Temperature Mode Temperatures Table 4: North Side Time-Temperature Mode Temperatures Notes for Tables 3 and 4 1. Recycle bin discharge temperature is measured continuously and is reported on this table as a 15-minute average. 2. Time temperature control is active only if any dryer discharge temperature per side is less than 176F. 3. No values in the table (blank table) represents that the dryer recycle system never went to Time Temperate Mode for the month 4. Once the time temperature control is active, it stays active for a minimum of 40 minutes. 5. Recycle bin discharge temperature is measured using RTD probes located in a thermowell on the interior wall of each recycle bin. 6. The required temperature is calculated with 40 CFR 503(a)(3) Equation 2 7. If the recycle bin discharge temperature is less than the required temperature, then gates to classification close and all product is recycled back to the dryers. 8. If the recycle bin discharge temperature is greater than required temperature, then gates to classification stay open and some product goes to classification and the remaining product is recycled back to the dryers. Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 16 Table #3 dd("D",3,A1, Date/Time 03/03/21 04:30 03/14/203/03/21 04:45 03/14/203/03/21 05:00 21 05:15 03/03/21 05:15 21 05:30 03/14/21 05:00 21 05:15 03/14/21 05:15 03/03/21 03/14/21 05:30 03/03/21 03/14/21 05:45 03/03/21 03/14/21 06:00 03/14/21 03/14/21 06:15 none Time-Temperature Mode - South Dryers - March 2021 South Dryers (Recycle Bin #1 or Bin #3) Required Recycle Bin Gates to Temp. Discharge Temp Classifica#on 160.14 153..03 CLOSED Recycle Bin Discharge To: All Recycled to Dryers 159.67 152.46 CLOSED All Recycled to Dryers 159.42 153.77 CLOSED All Recycled to Dryers 159.13 157.67 CLOSED All Recycled to Dryers 159.56 162.56 OPENED Classifica#on & Recycled to Dryers 159.50 160.28 CLOSED All Recycled to Dryers 159.15 156.78 CLOSED All Recycled to Dryers 158.85 158.66 CLOSED All Recycled to Dryers 158.69 158.42 CLOSED All Recycled to Dryers 158.43 157.82 CLOSED All Recycled to Dryers Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 17 Table #4 Date/Time none none none none none none Time-Temperature Mode - North Dryers - March 2021 North Dryers (Recycle Bin #2 or Bin #3) Required Recycle Bin Gates to Recycle Bin Temp. Discharge Temp Classifica#on Discharge To: . x Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendic C, page 18 Appendix D: Photo Log Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Milwaukee Metro Sewerage District (MMSD) Jones Island Biosolids Dewatering and Drying Facility EPA Inspection June 4, 2021 All photos taken by Dean Maraldo, Inspector, U.S. EPA Camera: Ricoh WG-4 1: MMSD0001 Description: Overview of the south side dryers. Location: MMSD D&D Facility Camera Direction: 46 Date/Time: June 4, 2021; 09:06 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix D, page 1 2: MMSD0002 Description: new temperature probes (3) in recycling bin #3. Location: MMSD D&D Facility Camera Direction: 349 Date/Time: June 4, 2021; 09:13 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix D, page 2 3: MMSD0003 Description: Product composite sampler. Location: MMSD D&D Facility (WPDES Permit Sampling Point (Outfall) 006 - Jones Island EQ Sludge - PRODUCTION). Camera Direction: 70 Date/Time: June 4, 2021; 09:24 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix D, page 3 4: MMSD0004 Description: One of two new temperature probes installed within the Dryer #1S. Location: MMSD D&D Facility Camera Direction: 198 Date/Time: June 4, 2021; 09:32 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix D, page 4 5: MMSD0005 Description: The same probe shown in Photograph MMSD0004, viewed from outside of Dryer #1S. Location: MMSD D&D Facility Camera Direction: 105 Date/Time: June 4, 2021; 09:34 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix D, page 5 6: MMSD0006 Description: The former temperature compliance monitoring location (vicinity of steel plate on the screw chute), measured approximately 19 feet away from dryer furnace outlet along dryer discharge screw chute. Location: MMSD D&D Facility Camera Direction: 262 Date/Time: June 4, 2021; 09:40 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix D, page 6 7: MMSD0007 Description: D&D Facility operations control center. Location: MMSD D&D Facility Camera Direction: 240 Date/Time: June 4, 2021; 09:46 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix D, page 7 8: MMSD0009 Description: Close up view of dryer temperature control screen. Location: MMSD D&D Facility Camera Direction: 251 Date/Time: June 4, 2021; 09:47 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix D, page 8 9: MMSD0010 Description: Silo load out belt conveyor and product auto sampler. Location: MMSD Silo Load Out Facility Camera Direction: 232 Date/Time: June 4, 2021; 10:05 Clean Water Act Focused Compliance Inspection - Milorganite Biosolids Process June 4, 2021 Appendix D, page 9 Appendix E: Documents Received MMSD LAB-031 Quantification of Fecal Coliform and Total Coliform Bacteria in Biosolids by MPN REV.0.4 (1/4/2021) Thermowell and Bosset Fitting Data Form Wireless Transmitter Equipment Data Form Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 1 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 2 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 3 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 4 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 5 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 6 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 7 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 8 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 9 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 10 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 11 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 12 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 13 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 14 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 15 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 16 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 17 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 18 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 19 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 20 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 21 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 22 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 23 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 24 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 25 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 26 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 27 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 28 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 29 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 30 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 31 Fecal Coliform via EPA 1680 % Total Solids LIMS Placeholder Type (grab, comp) Preservative Preserved Time Milorganite Fecal Coliform VWM-MMSD Sample Chain of Custody Sample Location: Jones Island Milorganite Production, Shipping, and Bagging Sample Date: ______________ Analyses Requested Sample Time(s) # of Bottles Source Code 978/1 Sample ID *Milorganite Production 978/1 *Milorganite Production 978/5 *Milorganite Shipping 978/5 *Milorganite Shipping 978/4 *Miloragnite Bagging 978/4 *Milorganite Bagging XX X XX X XX X Grab Grab Grab Grab Grab Grab (comp. only) None None None None None None Start Time End Time *Microbiological samples must be collected after 4am and received by the lab no later than 9am* Remarks (any unusual conditions must be recorded here and supervisor informed): VWM Sample Custody Relinquished by: Date Time Received by: For Laboratory Use Only LIMS # pH verified Date Time Sample Courier Custody Received by: *Microbiological samples must be refrigerated upon collection and transported on ice* Date Time Relinquished by: Date Time On Ice? Y / N MMSD Lab Sample Custody Received by: Date Time On Ice? Y / N Relinquished by: Date Time If not received on ice, sample temperature on receipt in lab: __________C Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Version 4; Revised 11/18/20 Appendix E, page 32 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 33 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 34 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 35 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 36 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 37 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 38 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 39 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 40 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 41 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 42 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 43 Clean Water Act Focused Compliance Inspection Milorganite Biosolids Process June 4, 2021 Appendix E, page 44