Document pekOMj3yneL401qeanDvbN3nB

Report Prepared by: Report Approved by: NPDES Pretreatment Compliance Sampling Inspection Report Sportsfield Specialties, Inc. (SSI) 41155 State Highway 10 Delhi, New York 13753 40 CFR Parts 403 & 433.17 & IU Permit Inspection Date: November 15, 2022 THUAN TRAN Digitally signed by THUAN TRAN _________________D_ate_: 2_0_23_.0_1.1_0_1_2:0_7:_03_-_05_'00_' Thuan Tran, Physical Scientist Date: _____________________________ Digitally signed by PHILIP PHILIP COCUZZA COCUZZA _________________D_ate_: _20_23_.0_1._10_1_2:1_2_:43_-_05_'0_0' Phil Cocuzza, Chief Monitoring Operations Section Date: ________________ Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Parts 403 & 433.17, & IU Permit 1.0 OBJECTIVE Insp. Date: November 15, 2022 On November 15, 2022, the United States Environmental Protection Agency (USEPA) conducted a Pretreatment Compliance Sampling Inspection (CSI) at Sportsfield Specialties, Inc. (SSI). The objective of the Pretreatment CSI was to gather information necessary to determine if the facility is in compliance with the requirements and limitations of the Federal General Pretreatment Regulations for Existing and New Sources of Pollution in 40 CFR Part 403 and the Federal Metal Finishing Point Source Category for Pretreatment Standards for New Sources in 40 CFR Part 433.17, as well as, their issued Industrial User Permit from the Village of Stamford which expires on August 31, 2023. 2.0 KEY PARTICIPANTS Listed below are key inspection participants and contact information, grouped by organization. U.S. Environmental Protection Agency Thuan Tran, Lead Inspector 732-321-4455, email: tran.thuan@epa.gov Robert Morrell, Geologist Sportsfield Specialties, Inc. (SSI) Ivan Gielskie, Maintenance Manager 607-746-1402, email: igielskie@sportsfield.com Jonathan Kemp, Director of Operations Kathleen Souzzo, PE, PLLC - A NYS Certified WBE Engineering Firm (Contractor) Casey Corrigan, Assistant Manager 315-941-0219, email: ccorrigan@kspepllc.com 3.0 FACILITY DESCRIPTION 3.1 General Information Sportsfield Specialties, Inc. (SSI) has two manufacturing warehouses that perform metal finishing operation. The main building is located at 41155 State Highway 10, Delhi, New York (NY) and started in 2003. The second building was constructed and completed at the end of 2019 and is located at 40995 State Highway 10, Delhi, NY. Sportsfield Specialties, Inc. manufactures specialized sporting infrastructure and equipment, such as football goal posts, soccer goals, protective netting systems, team benches, track & field equipment, dugouts, etc. The facility is categorized under Standard Industrial Classification (SIC) 3949 Sporting and Athletic Goods, Not Elsewhere Classified and the North American Industry Classification System (NAICS) 339920 - Sporting and Athletic Goods Manufacturing. Page 2 of 7 Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Parts 403 & 433.17, & IU Permit Insp. Date: November 15, 2022 To product specialized sporting infrastructure and equipment, raw materials are received and stored at the two manufacturing locations depending on the sizes of the stock material. Major manufacturing equipment at the facilities consist of Benders, Press, Welding, Washroom (cleaning and etching), and Painting (powder coating). The production of specialized equipment generates process wastewater that is pretreated by an on-site Alar Waste Treatment System. The pretreated process wastewater is contained in an aerated storage tank until enough accumulates to be transported for further treatment. Gray's Countryside Septic Service located at 51 Union Street, Walton, NY serves as the septic hauler. Approximately 3,000 gallons of pretreated wastewater are trucked to the Village of Stamford WWTP per event. 3.2 Process Information The manufacturing operation is similar at both locations. In the old warehouse, raw material (aluminum and steel) in the forms of sheet and cylindrical tubes go through the process of machining (milling, sanding and/or bending) followed by the process of forming (shear, laser cut, and/or punch). The bare parts are moved to the staging area in preparation for welding. After welding, some parts may go through the process of grinding, sanding, and/or deburring to smooth rough edges. From the welding process and some side operations, the bare parts are moved into the washroom for cleaning. Bare parts are washed with well water and detergent/chemical etcher to remove dirt, grease, oil, and/or oxide from their surface. The parts are dried in a heat oven. After the parts have cooled down to ambient temperature, the surface is spray painted and allowed to dry. The coated parts are visually inspected before moving onto the assembly area. Once the parts are assembled into specialized equipment/infrastructures, they are moved to the shipping area. In the new building, larger bare parts, such as football goal posts, baseball dugouts, etc., go through machining, welding, blasting, and sanding to smooth the rough edges. The bare parts continue to the washroom where well water is mixed with detergent/chemical etcher to clean and etch the surface. The large parts are moved to the heat oven for drying. Once the large parts have cooled down, they go to the spray paint booth where they are powder coated. Finally, the parts move to the heat oven where the paint is baked on the surface of the bare parts. From the heat oven, the parts are moved to the assembly area and/or shipped out as large parts and assembled at the site. Well water mixed with detergent and chemical etchers is used to wash and clean parts in the washrooms at the warehouses. Process wastewater generated from the washroom in the old warehouse flows into the floor drain and is collected in a pit. Physical separation is allowed to settle out heavy matters, while the wastewater continues to a separate holding compartment. From the holding compartment, the accumulated process wastewater is pumped into a 500-gallon tote once every week or two (2) and trucked to the new warehouse. The 500-gallon tote of process wastewater discharges onto the washroom floor of the new building. The process wastewater flows into the floor drain and is pumped to the Alar Waste Treatment System in the cylindrical treatment tank. In the treatment tank, pH is adjusted with acid and/or caustic and a cationic polymer is added to promote flocculation, while Page 3 of 7 Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Parts 403 & 433.17, & IU Permit Insp. Date: November 15, 2022 constantly mixing. From the treatment tank, the wastewater is pumped to the vacuum filtration unit as a batch while additional polymer is added at the head of the unit. The filtrate is conveyed into a holding tank where a defoaming agent is added. The pretreated process wastewater is pumped into a mobile storage tank outside the building based on the water level in the holding tank. The mobile storage tank is trucked to the old warehouse where the pretreated wastewater is pumped into the pretreated effluent storage tank. Aeration is provided in the storage tank to keep the pretreated effluent homogenized. Depending on the manufacturing operation at the two locations, it could take months before the storage tank reaches a level that requires a septic hauler to truck the pretreated effluent to the POTW. Solids removed from the washroom pit in the old warehouse and from the vacuum filtration unit are trucked and disposed of at a solid waste facility once per month. 3.3 Facility Self-Monitoring Information Sample containers with and without preservatives, and the chain of custody are provided by Phoenix Environmental Laboratories, Inc. The laboratory is located at 587 East Middle Turnpike in Manchester, Connecticut. Samples are collected by the facility's personnel from the spigot for metals, cyanide (T), and total toxic organics (TTO). The samples are carried or shipped via UPS/FedEx to the laboratory for analysis. 4.0 EPA SAMPLING/INSPECTION ACTIVITIES 4.1 Sampling Activities Grab samples were collected from the spigot attached to the storage tank. Samples were collected and analyzed for metals (cadmium, chromium, copper, lead, nickel, silver, zinc, barium and magnesium), cyanide (T), total toxic organics (TTO), oil & grease (O&G), phosphorus (T), total suspended solids (TSS) and 5-day biochemical oxygen demand (BOD5). TTO consists of volatile organic analytes (VOAs), non-volatile organic analytes (NVOAs), pesticides and polychlorinated biphenyls (PCBs). On-site grab samples were collected and analyzed for pH, temperature, and total residual chlorine (TRC). All sample containers, preservation techniques and holding times were in accordance with US EPA requirements specified in 40 CFR Part 136. Signed and dated custody seals were placed across the lids and along the sides of the sample containers. The custody sealed sample containers were placed inside plastic sample bags and sealed. All samples were shipped on ice to the USEPA Laboratory in Edison, New Jersey for analysis. Chain of custody was maintained for all samples. USEPA Laboratory Analytical Data Package is attached with the report. The average daily flow value is calculated based on the hauling record over a certain period of months and divided by the number of operational days. During the inspection, it was Page 4 of 7 Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Parts 403 & 433.17, & IU Permit Insp. Date: November 15, 2022 anticipated that about 3,000 gallons of the pretreated wastewater is hauled by Gary's Countryside Septic Service to the Village of Stamford Wastewater Treatment Plant (WWTP). Split samples were collected and given to the facility representative. 4.2 Inspection Activities A Pretreatment Compliance Sampling Inspection (CSI) at Sportsfield Specialties, Inc. was conducted on November 15, 2022. Inspector's credential was presented, and business card was provided during the opening conference. It was explained that the purpose of the Pretreatment CSI with supporting on-site activities was to determine if the facility is in compliance with the Federal Pretreatment Regulations for New and Existing Sources (40 CFFR Part 403), Metal Finishing Categorical for Pretreatment Standards for New Sources (40 CFR Part 433.17) and their issued Industrial User Permit by the Village of Stamford. The supporting on-site activities consist of collecting samples of the pretreated effluent, observing and evaluating the monitoring location, determining the presence or absence of chlorine in the pretreated effluent at the monitoring location, observing and evaluating the facility's sample protocol, observing and evaluating the process waste streams to the pretreated effluent storage tank, tour of the manufacturing process and where process wastewater is generated, review and evaluate the June 2022 Semi-Annual report which include sampling and laboratory information, as well as, interviewing the facility's representatives. During the closing conference, the facility representatives were briefed on the inspection activities. On-site sample results and concerns discovered or observed during the inspection were communicated to the facility's representatives so that they understand their responsibilities to comply with the Federal General Pretreatment Regulations for New and Existing Sources, the Federal Metal Finishing Category for Pretreatment Standards for New Sources as well as their issued Industrial User Permit by the Village of Stamford. 4.3 Deviations and/or Environmental Conditions The facility representatives indicated that the aerator in the storage tank must be shut-off before samples can be collected from the spigot. Once all the samples are collected, the aerator can be turned on to maintain a homogenized waste stream. To be consistent with the facility Standard Operating Procedures (SOPs), the aerator was turned off prior to collecting compliance samples during the EPA sampling inspection. The process of shutting down the aerator and turning it back on after sample collection is not consistent with the process of maintaining a homogenized waste stream. A residual chlorine sample was collected and analyzed of the pretreated effluent to ensure that proper sample preservations are taken into account and sample integrity is followed in accordance with the approved analytical methods in 40 CFR Part 136. Page 5 of 7 Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Parts 403 & 433.17, & IU Permit 5.0 ANALYTICAL RESULTS Insp. Date: November 15, 2022 Sportsfield Specialties, Inc. - Pretreated Effluent November 15, 2022 Parameter Units 40 CFR Part 433.17 Stamford (V) Daily Max. Monthly Avg. IU Permit Metals: Cadmium mg/l 0.11 0.07 ---- Chromium mg/l 2.77 1.71 ---- Copper mg/l 3.38 2.07 ---- Lead mg/l 0.69 0.43 ---- Nickel mg/l 3.98 2.38 ---- Silver mg/l 0.43 0.24 ---- Zinc mg/l 2.61 1.48 < 10 Barium mg/l ---- ---- < 5.0 Magnesium mg/l ---- ---- < 20 Cyanide, Total mg/l 1.20 0.65 ---- TTO mg/l 2.13 ---- ---- VOAs mg/l ---- ---- ---- NVOAs mg/l ---- ---- ---- Pesticides mg/l ---- ---- ---- PCBs mg/l ---- ---- ---- Oil & Grease mg/l No amount that will cause ---- interference or pass-through pH SU >/= 5.0 6.0 - 9.0 Temperature C (F) </= 40C (104F) ---- Flow GPD ---- </= 3,000 gpd; </= 6,000/wk Phosphorus, T mg/l ---- < 650 TSS mg/l ---- < 600 BOD5 mg/l ---- < 500 Notes: U- The analyte was not detected at or above the Reporting Limit. J- The identification of the analyte is acceptable; the reported value is an estimate. L- The identification of the analyte is acceptable; the reported value may be biased low. K- The identification of the analyte is acceptable; the reported value may be biased high. EPA U U 0.018 U U U 0.03 U 2.5 0.026 U L J U J U L J U J U J U L 6.84 18 3,000 0.753 25 161 Result K 6.0 FINDINGS 6.1 Sampling Result Findings The EPA analytical results obtained during this inspection are within the acceptable limits. 6.2 Inspection Findings In addition to the analytical data, an inspection of the facility operations was conducted as discussed in Section 4.2 above. Page 6 of 7 Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Parts 403 & 433.17, & IU Permit 7.0 ATTACHMENTS Insp. Date: November 15, 2022 Attachment #1. Sportsfield Specialties, Inc. consists of two manufacturing warehouses. Attachment #2. The production layout in the old warehouse is located at 41155 NY-10. Attachment #3. The production layout in the new warehouse is located at 40995 NY-10. Attachment #4. Wash water from the old warehouse is trucked to the new warehouse. Attachment #5. Wash water is combined & is treated by the Alar Waste Treatment System. Attachment #6. Process wastewater flow starts from the washrooms to the storage tank. Attachment #7. USEPA Chain of Custody for Samples was submitted to the USEPA Lab. Attachment #8. USEPA Analytical Data Package was received on 12/07/2022. 8.0 PHOTOGRAPHS Photo #1. Pretreated effluent is contained in the storage tank with aeration. Photo #2. Compliance samples were collected from the spigot attached to the storage tank. Photo #3. Pretreated effluent from the storage tank is pumped onto the septic hauler. Photo #4. The Alar Waste Treatment System receives and treats process wastewater. Photo #5. Solids from the vacuum filtration unit are collected in the tote bag. Photo #6. A defoaming agent is added to the filtrate in the holding tank. Page 7 of 7 Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Part 403 & 433.17, & IU Permit Insp. Date: November 15, 2022 7.0 Attachments Attachment #1. Sportsfield Specialties, Inc. consists of two manufacturing warehouses. ION OF WASHBAY ALL TREATED WASTEWATER ALL WAST AND HAULED FROM THIS FACILITY. WA DOE OLD FACLITY (NY-1). SEEl---# C-2 FOR BUILDING LAYOUT. SENIC) S ASHING. LOWER T. RAW RTHER ACCESS RD CONNECTING BUILDINGS. HAUL WATER ON FLAT BED TRUCK WITH I 2 500 GALLON PLASTIC TOTES (USUALLY ONCE A WEEK) APPROXIMATE LOCATION OF WASHBAY. J---'11 ALAR FILTER IS INSTALLED AT THIS WASHBAY. SEE PAGE C-3 AND C-5. BUILDING (NY-2). SEE C-3 FOR BUILDING LAYOUT. APPROXIMATE LOCATION OF WELL FOR BUILDING. WATER IS UNTREATED AND IS NON-POTABLE (USED ONLY FOR WASHING METALS AND BATHROOMS) r ,.. 1 C-1 .... ...ii PRODUCTION PROCESS 1" = 150' GRAPHIC SCALE FLOW DIAGRAM 150 0 150 300 450 600 ,,. ' .. z0 N N 0 (.) :::) _J en _J a_ ww w _J I a_ I- <( . 8 - 'l 0 ij >- '.::i ZJ UC 0 w> ITT w IwTT a '.:j 8 :e ru " 0 mvu0 J rigu <J ITTWJ m oc[ xvw u J O al N ,r:i C (I) C J - w "-i,f s "- 0 ru gJ 0 , o C -w "' 0u -< ITT J c o~ v r-.. 0 0 0 (/) n st --'2. - "' "1 (/) 0 (/) 0 _J (!) 0 L,._ I 0 - z II N N - f- Q N N - Of- 0 W<( -0, ::e N CL >-' >-' ci [D >-' [D z CL o_ 0 L,._ 0 w [D 0 w f- w "' z- w _J z Cl z 3' 3w' (w-.,) w en f- <( <( (.) <( w CL w 5 0 CL w :r: 0 (/) 0 0 CL o_ (/) z 0 o_ enz CL (/) 0 0 w(/) 0 5 w CL w f<( 0 0 z X ffi <5 i.?5oo .o.,5 e ;C'D.:ii'i:i;:i _"wo - s, 0" l!)IIJ w6wcO co,. "'ffi iti e"o" gg :::i:z!e!a a5 z" u 80 <N .... :i (J).i.!.',;8;: Oo c t5 ,i"c C5 Cww 0 " eiz 8 ouui eNzo oe "" rewu " " o<o"O II 0z- .. (wI) F .<-..J 0...... i 0w .z)_ CL (I) IC) C I ...J I..C..).. w i 0::: 0 CL (I) 0::: (/) z < g CL C - Ci: :::J 0 (I) - < 0::: 0 LL. C 1 .. ... Attachment #2. The production layout in the old warehouse is located at 41155 NY-10. Attachment #3. The production layout in the new warehouse is located at 40995 NY-10. Attachment #4. Wash water from the old warehouse is trucked to the new warehouse. Attachment #5. The wash water is combined and is treated by the Alar Waste Treatment System. Attachment #6. Process wastewater flow starts in the washrooms to the storage tank. Attachment #7. The Chain of Custody for Samples was received by the USEPA Laboratory in Edison, NJ on Wednesday, 11/16, 2022. Attachment #8. USEPA Analytical Data Package was received on Wednesday, 12/07/2022. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory 2890 Woodbridge Avenue Edison , New Jersey 08837 732-906-6886 Phone 732-906-6165 Fax December 07, 2022 Philip Cocuzza Monitoring & Assessment Branch LSASD/MAB Edison, NJ 08837 RE: Sportsfield Specialties, Inc. - 2211012 Enclosed are the results of analyses for samples received by the laboratory on 11/16/2022. The signature below reflects the laboratory's approval of the reported results. If you have any questions concerning this report, please refer to Project Number 2211012 and contact the laboratory. Sincerely, John R. Bourbon Chief, LSASD/LB Project Narrative: UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 The National Environmental Laboratory Accreditation Conference Institute (TNI) is a voluntary environmental laboratory accreditation association of State and Federal agencies. TNI established and promoted a National Environmental Laboratory Accreditation Program (NELAP) that provides a uniform set of standards for the generation of environmental data that are of known and defensible quality. The EPA Region 2 Laboratory is NELAP accredited. The Laboratory tests that are accredited have met all the requirements established under the TNI Standards. Condition Comments None Comment(s): Pesticide/PCB analysis: Analysis indicated the stationary phase of the front and back columns were severely affected by the sample matrix. The end of the sequence standards, surrogate recoveries and sample and corresponding MS/MSD pairs spike recoveries were also severely affected. No visible target compounds were detected in the sample. VOA analysis: Foaming initailly caused analytical issues at the instrument at normal volume purge. Final data used was 10X for effluent sample outside hold in order to have better final reporting limit (50 ug/L). All data is J qualified as a result. SVOA analysis: Sample matrix caused extraction issues that also affected final reporting of analytes. Data is qualified accordingly for effluent sample. Data Qualifier(s): U- The analyte was not detected at or above the Reporting Limit. J- The identification of the analyte is acceptable; the reported value is an estimate. K- The identification of the analyte is acceptable; the reported value may be biased high. L- The identification of the analyte is acceptable; the reported value may be biased low. NJ- There is presumptive evidence that the analyte is present; the analyte is reported as a tentative identification. The reported value is an estimate. U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 1 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Reporting Limit(s): The Laboratory was able to achieve the standard laboratory reporting limits, where applicable, for each analyte requested except for the following analyte(s): NVOA GCMS The reporting level of 5.00 ug/L was raised to 10 ug/L for the following analyte(s): 4,6-Dinitro-2-Methylphenol, Pentachlorophenol for the following samples: 2211012-02 The reporting level of 5.00 ug/L was raised to 30 ug/L for the following analyte(s): 2,4-Dinitrophenol for the following samples: 2211012-02 SUMMARY REPORT FOR SAMPLES Field ID TRIP BLANK Pretreated Effluent Laboratory ID 2211012-01 2211012-02 Matrix Aqueous Aqueous Date Sampled 11/14/2022 09:28 11/15/2022 10:00 Date Received 11/16/2022 13:30 11/16/2022 13:30 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 2 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Analysis 608.3 Pesticides/PCBs-NPDES 624.1 VOA EPA-NPDES 625.1 SVOA NPDES Biochemical Oxygen Demand Cyanide, Total Metals ICP TAL NPDES/DW Oil & Grease Phosphorus Residue, Non-Filterable SUMMARY REPORT FOR METHODS Method EPA 608.3 SOP C-91 Rev 4.3 EPA 624.1 SOP C-89 Rev 3.6 EPA 625.1 SOP C-90 Rev 3.8 SM 5210B SOP C-21 Rev 2.7 EPA 335.4 SOP C-28 Rev 2.7 EPA 200.7 SOP C-109 Rev 3.6 EPA 1664A SOP C-126 Rev 1.6 EPA 365.1 SOP C-68 Rev 2.7 SM 2540D SOP C-33 Rev 3.7 Certification NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP Matrix Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 3 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Analyte Field ID: TRIP BLANK VOA GCMS Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene Result Qualifier Reporting Limit Units Batch Sample ID: 2211012-01 Date and Time of Analysis* --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 4 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Analyte Result Qualifier Reporting Limit Units Batch Date and Time of Analysis* Field ID: TRIP BLANK VOA GCMS 1,4-Dichlorobenzene 1,2-Dichlorobenzene Field ID: Pretreated Effluent VOA GCMS Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Sample ID: 2211012-01 --- U J 5.00 ug/L B211150 --- U J 5.00 ug/L B211150 Sample ID: 2211012-02 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 5 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Analyte Field ID: Pretreated Effluent VOA GCMS Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene NVOA GCMS Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol Result Qualifier Reporting Limit Units Batch Sample ID: 2211012-02 Date and Time of Analysis* --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U J 50.0 ug/L B211150 --- U L 4.90 ug/L B211125 --- U L 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U L 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U L 4.90 ug/L B211125 --- U J 29.4 ug/L B211125 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 6 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Analyte Field ID: Pretreated Effluent NVOA GCMS 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Result Qualifier Reporting Limit Units Batch Sample ID: 2211012-02 Date and Time of Analysis* --- U L 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U L 4.90 ug/L B211125 --- U J 9.80 ug/L B211125 --- U 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U L 4.90 ug/L B211125 --- U L 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U J 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U J 9.80 ug/L B211125 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 7 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Analyte Field ID: Pretreated Effluent NVOA GCMS Phenol Pyrene Pest/PCBs GC alpha-BHC gamma-BHC (Lindane) beta-BHC delta-BHC Heptachlor Aldrin Heptachlor epoxide Endosulfan I 4,4'-DDE Dieldrin Endrin 4,4'-DDD Endosulfan II 4,4'-DDT Endrin aldehyde Endosulfan sulfate Toxaphene Chlordane Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Result Qualifier Reporting Limit Units Batch Sample ID: 2211012-02 Date and Time of Analysis* --- U L 4.90 ug/L B211125 --- U 4.90 ug/L B211125 --- U J 0.002 ug/L B211133 --- U J 0.002 ug/L B211133 --- U J 0.002 ug/L B211133 --- U J 0.002 ug/L B211133 --- U J 0.002 ug/L B211133 --- U J 0.002 ug/L B211133 --- U J 0.002 ug/L B211133 --- U J 0.002 ug/L B211133 --- U J 0.004 ug/L B211133 --- U J 0.004 ug/L B211133 --- U J 0.004 ug/L B211133 --- U J 0.004 ug/L B211133 --- U J 0.004 ug/L B211133 --- U J 0.004 ug/L B211133 --- U J 0.004 ug/L B211133 --- U J 0.004 ug/L B211133 --- U J 0.167 ug/L B211133 --- U J 0.056 ug/L B211133 --- U J 0.028 ug/L B211133 --- U J 0.056 ug/L B211133 --- U J 0.028 ug/L B211133 --- U J 0.028 ug/L B211133 --- U J 0.028 ug/L B211133 --- U J 0.028 ug/L B211133 --- U J 0.028 ug/L B211133 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 8 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Analyte Field ID: Pretreated Effluent GC - Sanitary Oil & Grease Metals ICP Barium Cadmium Chromium Copper Lead Magnesium Nickel Silver Zinc Sanitary Biochemical Oxygen Demand Cyanide, Total Phosphorus Total Suspended Solids Result Qualifier Reporting Limit Units Batch Sample ID: 2211012-02 Date and Time of Analysis* --- U L 5.80 mg/L B212014 --- U 100 ug/L B211134 --- U 3.00 ug/L B211134 --- U 5.00 ug/L B211134 17.5 10.0 ug/L B211134 --- U 8.00 ug/L B211134 2500 500 ug/L B211134 --- U 20.0 ug/L B211134 --- U 5.00 ug/L B211134 30.3 20.0 ug/L B211134 161 26.4 0.753 25.0 2.00 mg/L B211129 11/22/2022 08:51 K 10.0 ug/L B211124 0.0500 mg/L B211139 10.0 mg/L B211128 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 9 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 VOA GCMS - Quality Control Analyte Batch B211150 Blank (B211150-BLK1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L 103 ug/L 100.0 ND ug/L 100.0 ND ug/L 100.0 103 60-140 90.2 60-140 84.1 60-140 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 10 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 VOA GCMS - Quality Control Analyte Batch B211150 LCS (B211150-BS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit 34.2 5.00 ug/L 50.00 39.9 5.00 ug/L 50.00 42.9 5.00 ug/L 50.00 34.0 5.00 ug/L 50.00 44.8 5.00 ug/L 50.00 45.5 5.00 ug/L 50.00 37.7 5.00 ug/L 50.00 38.2 5.00 ug/L 50.00 46.9 5.00 ug/L 50.00 39.6 5.00 ug/L 50.00 44.9 5.00 ug/L 50.00 47.3 5.00 ug/L 50.00 46.6 5.00 ug/L 50.00 41.4 5.00 ug/L 50.00 41.3 5.00 ug/L 50.00 42.7 5.00 ug/L 50.00 36.8 5.00 ug/L 50.00 41.9 5.00 ug/L 50.00 39.7 5.00 ug/L 50.00 41.9 5.00 ug/L 50.00 43.2 5.00 ug/L 50.00 41.0 5.00 ug/L 50.00 43.9 5.00 ug/L 50.00 43.7 5.00 ug/L 50.00 42.0 5.00 ug/L 50.00 42.9 5.00 ug/L 50.00 44.1 5.00 ug/L 50.00 40.2 5.00 ug/L 50.00 45.4 5.00 ug/L 50.00 44.9 5.00 ug/L 50.00 45.5 5.00 ug/L 50.00 102 ug/L 100.0 91.1 ug/L 100.0 83.5 ug/L 100.0 68.4 19-205 79.8 5-195 85.8 15-185 67.9 40-160 89.5 50-150 91.0 50-150 75.4 60-140 76.4 60-140 93.9 70-130 79.2 70-130 89.8 70-135 94.6 70-130 93.3 70-130 82.8 70-130 82.7 65-135 85.3 65-135 73.6 35-165 83.7 65-135 79.5 25-175 83.7 70-130 86.5 50-150 82.0 70-130 87.8 70-130 87.3 70-135 83.9 65-135 85.9 60-140 88.2 70-130 80.3 60-140 90.8 70-130 89.8 65-135 91.0 65-135 102 60-140 91.1 60-140 83.5 60-140 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 11 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 VOA GCMS - Quality Control Analyte Batch B211150 LCS Dup (B211150-BSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit 36.0 5.00 ug/L 50.00 39.6 5.00 ug/L 50.00 45.9 5.00 ug/L 50.00 36.5 5.00 ug/L 50.00 47.3 5.00 ug/L 50.00 48.6 5.00 ug/L 50.00 40.0 5.00 ug/L 50.00 41.2 5.00 ug/L 50.00 50.9 5.00 ug/L 50.00 42.6 5.00 ug/L 50.00 48.6 5.00 ug/L 50.00 50.8 5.00 ug/L 50.00 49.6 5.00 ug/L 50.00 44.6 5.00 ug/L 50.00 43.5 5.00 ug/L 50.00 45.8 5.00 ug/L 50.00 39.8 5.00 ug/L 50.00 44.9 5.00 ug/L 50.00 42.8 5.00 ug/L 50.00 44.9 5.00 ug/L 50.00 46.1 5.00 ug/L 50.00 43.4 5.00 ug/L 50.00 46.4 5.00 ug/L 50.00 46.0 5.00 ug/L 50.00 44.1 5.00 ug/L 50.00 45.1 5.00 ug/L 50.00 47.2 5.00 ug/L 50.00 42.7 5.00 ug/L 50.00 48.4 5.00 ug/L 50.00 47.5 5.00 ug/L 50.00 47.7 5.00 ug/L 50.00 103 ug/L 100.0 90.6 ug/L 100.0 81.2 ug/L 100.0 71.9 19-205 4.99 20 79.2 5-195 0.729 20 91.7 15-185 6.64 20 73.0 40-160 7.13 20 94.6 50-150 5.56 20 97.1 50-150 6.46 20 80.0 60-140 5.84 20 82.5 60-140 7.73 20 102 70-130 8.17 20 85.1 70-130 7.13 20 97.2 70-135 8.00 20 102 70-130 7.22 20 99.2 70-130 6.17 20 89.1 70-130 7.33 20 87.1 65-135 5.21 20 91.7 65-135 7.16 20 79.6 35-165 7.73 20 89.8 65-135 6.99 20 85.6 25-175 7.39 20 89.9 70-130 7.07 20 92.2 50-150 6.40 20 86.9 70-130 5.85 20 92.7 70-130 5.45 20 92.0 70-135 5.22 20 88.3 65-135 5.06 20 90.2 60-140 4.93 20 94.5 70-130 6.94 20 85.5 60-140 6.20 20 96.8 70-130 6.33 20 95.1 65-135 5.67 20 95.3 65-135 4.66 20 103 60-140 90.6 60-140 81.2 60-140 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 12 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 VOA GCMS - Quality Control Analyte Batch B211150 Matrix Spike (B211150-MS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit Source: 2211012-02RE2 34.5 5.00 ug/L 40.5 5.00 ug/L 43.5 5.00 ug/L 39.9 5.00 ug/L 46.2 5.00 ug/L 47.4 5.00 ug/L 41.8 5.00 ug/L 41.3 5.00 ug/L 49.2 5.00 ug/L 43.7 5.00 ug/L 50.4 5.00 ug/L 51.4 5.00 ug/L 51.0 5.00 ug/L 45.4 5.00 ug/L 45.7 5.00 ug/L 46.9 5.00 ug/L 41.3 5.00 ug/L 46.7 5.00 ug/L 44.8 5.00 ug/L 47.7 5.00 ug/L 45.8 5.00 ug/L 46.7 5.00 ug/L 48.5 5.00 ug/L 47.4 5.00 ug/L 47.2 5.00 ug/L 47.0 5.00 ug/L 49.0 5.00 ug/L 45.3 5.00 ug/L 51.7 5.00 ug/L 51.1 5.00 ug/L 51.2 5.00 ug/L 104 ug/L 92.9 ug/L 84.3 ug/L 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 100.0 100.0 100.0 69.0 19-273 81.0 49-251 86.9 21-242 79.8 14-230 92.5 17-181 94.7 52-234 83.7 69-221 82.6 40-160 98.4 54-156 87.4 59-155 101 51-138 103 52-162 102 70-140 90.7 49-155 91.4 37-151 93.8 70-157 82.6 74-210 93.5 35-155 89.5 80-227 95.4 47-150 91.5 17-183 93.4 52-150 97.0 64-148 94.7 53-149 94.5 37-160 94.1 37-162 98.0 45-169 90.7 46-157 103 59-156 102 18-190 102 18-190 104 60-140 92.9 60-140 84.3 60-140 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 13 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 VOA GCMS - Quality Control Analyte Batch B211150 Matrix Spike Dup (B211150-MSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit Source: 2211012-02RE2 32.8 5.00 ug/L 50.00 ND 65.5 19-273 5.20 28 37.9 5.00 ug/L 50.00 ND 75.8 49-251 6.66 28 42.8 5.00 ug/L 50.00 ND 85.6 21-242 1.48 28 37.7 5.00 ug/L 50.00 ND 75.5 14-230 5.57 28 44.2 5.00 ug/L 50.00 ND 88.5 17-181 4.44 28 44.0 5.00 ug/L 50.00 ND 88.0 52-234 7.35 28 39.8 5.00 ug/L 50.00 ND 79.6 69-221 4.92 28 39.3 5.00 ug/L 50.00 ND 78.5 40-160 5.06 28 46.1 5.00 ug/L 50.00 ND 92.2 54-156 6.57 28 41.5 5.00 ug/L 50.00 ND 83.0 59-155 5.16 28 47.7 5.00 ug/L 50.00 ND 95.4 51-138 5.56 28 48.6 5.00 ug/L 50.00 ND 97.3 52-162 5.46 28 47.8 5.00 ug/L 50.00 ND 95.5 70-140 6.48 28 43.7 5.00 ug/L 50.00 ND 87.5 49-155 3.66 28 43.9 5.00 ug/L 50.00 ND 87.8 37-151 4.06 28 45.6 5.00 ug/L 50.00 ND 91.2 70-157 2.77 28 39.9 5.00 ug/L 50.00 ND 79.7 74-210 3.50 28 45.1 5.00 ug/L 50.00 ND 90.1 35-155 3.64 28 43.6 5.00 ug/L 50.00 ND 87.2 80-227 2.56 28 46.1 5.00 ug/L 50.00 ND 92.1 47-150 3.46 28 44.7 5.00 ug/L 50.00 ND 89.4 17-183 2.32 28 44.7 5.00 ug/L 50.00 ND 89.5 52-150 4.27 28 46.3 5.00 ug/L 50.00 ND 92.6 64-148 4.66 28 46.0 5.00 ug/L 50.00 ND 92.1 53-149 2.81 28 45.5 5.00 ug/L 50.00 ND 90.9 37-160 3.86 28 45.1 5.00 ug/L 50.00 ND 90.3 37-162 4.14 28 48.1 5.00 ug/L 50.00 ND 96.2 45-169 1.90 28 44.4 5.00 ug/L 50.00 ND 88.9 46-157 1.96 28 50.0 5.00 ug/L 50.00 ND 100 59-156 3.22 28 49.6 5.00 ug/L 50.00 ND 99.3 18-190 2.92 28 49.6 5.00 ug/L 50.00 ND 99.1 18-190 3.20 28 103 ug/L 100.0 103 60-140 93.2 ug/L 100.0 93.2 60-140 83.7 ug/L 100.0 83.7 60-140 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 14 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 NVOA GCMS - Quality Control Analyte Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD Batch B211125 Blank (B211125-BLK1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 RPD Limit Page 15 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 NVOA GCMS - Quality Control Analyte Batch B211125 Blank (B211125-BLK1) Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12 LCS (B211125-BS1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L --- U 5.00 ug/L ND ug/L 50.00 ND ug/L 50.00 ND ug/L 50.00 ND ug/L 50.00 ND ug/L 50.00 ND ug/L 50.00 ND ug/L 50.00 36.7 5.00 ug/L 50.00 35.6 5.00 ug/L 50.00 33.9 5.00 ug/L 50.00 34.2 5.00 ug/L 50.00 36.2 5.00 ug/L 50.00 38.3 5.00 ug/L 50.00 38.8 5.00 ug/L 50.00 37.7 5.00 ug/L 50.00 43.5 60-140 17.8 60-140 36.6 60-140 34.4 60-140 40.1 60-140 56.1 60-140 50.5 60-140 73.4 47-145 71.2 33-145 67.8 27-133 68.5 33-143 72.4 17-163 76.5 24-159 77.7 35-219 75.3 11-162 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 16 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 NVOA GCMS - Quality Control Analyte Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD Batch B211125 LCS (B211125-BS1) Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene 32.0 5.00 ug/L 50.00 37.4 5.00 ug/L 50.00 35.2 5.00 ug/L 50.00 31.2 5.00 ug/L 50.00 39.4 5.00 ug/L 50.00 30.7 5.00 ug/L 50.00 34.7 5.00 ug/L 50.00 29.2 5.00 ug/L 50.00 33.9 5.00 ug/L 50.00 32.1 5.00 ug/L 50.00 32.2 5.00 ug/L 50.00 35.4 5.00 ug/L 50.00 42.4 5.00 ug/L 50.00 32.9 5.00 ug/L 50.00 33.6 5.00 ug/L 50.00 27.8 5.00 ug/L 50.00 32.7 5.00 ug/L 50.00 39.8 5.00 ug/L 50.00 38.3 5.00 ug/L 50.00 33.1 5.00 ug/L 50.00 35.1 5.00 ug/L 50.00 30.3 5.00 ug/L 50.00 20.1 5.00 ug/L 50.00 31.3 5.00 ug/L 50.00 29.8 5.00 ug/L 50.00 29.1 5.00 ug/L 50.00 39.8 5.00 ug/L 50.00 38.2 5.00 ug/L 50.00 33.1 5.00 ug/L 50.00 32.4 5.00 ug/L 50.00 34.5 5.00 ug/L 50.00 36.2 5.00 ug/L 50.00 39.5 5.00 ug/L 50.00 32.8 5.00 ug/L 50.00 27.9 5.00 ug/L 50.00 63.9 17-168 74.8 33-227 70.5 26-137 62.4 59-121 78.9 39-171 61.5 21-133 69.4 54-120 58.4 44-142 67.8 37-144 64.2 39-135 64.4 32-120 70.7 39-139 84.7 50-158 65.8 21-191 67.1 60-120 55.5 23-134 65.4 29-182 79.7 38-262 76.6 17-181 66.2 53-127 70.3 22-147 60.6 25-158 40.2 9-132 62.6 33-184 59.6 12-158 58.1 36-166 79.5 8-158 76.3 38-152 66.1 60-115 64.7 31-114 69.0 28-120 72.4 1-120 78.9 4-146 65.6 35-152 55.7 24-120 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 RPD Limit Page 17 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 NVOA GCMS - Quality Control Analyte Batch B211125 LCS (B211125-BS1) Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12 LCS Dup (B211125-BSD1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit 37.2 5.00 ug/L 50.00 27.0 5.00 ug/L 50.00 34.5 5.00 ug/L 50.00 34.1 5.00 ug/L 50.00 18.8 5.00 ug/L 50.00 31.1 5.00 ug/L 50.00 38.3 5.00 ug/L 50.00 34.6 5.00 ug/L 50.00 12.9 5.00 ug/L 50.00 35.6 5.00 ug/L 50.00 27.4 ug/L 50.00 11.0 ug/L 50.00 26.1 ug/L 50.00 25.1 ug/L 50.00 29.4 ug/L 50.00 41.3 ug/L 50.00 29.2 ug/L 50.00 33.9 5.00 ug/L 50.00 33.0 5.00 ug/L 50.00 34.6 5.00 ug/L 50.00 36.9 5.00 ug/L 50.00 37.0 5.00 ug/L 50.00 39.8 5.00 ug/L 50.00 38.5 5.00 ug/L 50.00 38.6 5.00 ug/L 50.00 34.6 5.00 ug/L 50.00 37.2 5.00 ug/L 50.00 35.6 5.00 ug/L 50.00 34.4 5.00 ug/L 50.00 38.3 5.00 ug/L 50.00 29.5 5.00 ug/L 50.00 35.9 5.00 ug/L 50.00 28.5 5.00 ug/L 50.00 74.4 15-76 54.0 40-120 69.0 21-196 68.3 35-180 37.6 17-127 62.2 43-230 76.6 79-139 69.2 14-176 25.8 5-120 71.2 52-120 54.8 60-140 22.1 60-140 52.3 60-140 50.1 60-140 58.8 60-140 82.7 60-140 58.3 60-140 67.9 47-145 7.81 30 66.0 33-145 7.61 30 69.1 27-133 1.93 30 73.7 33-143 7.37 30 74.1 17-163 2.27 30 79.5 24-159 3.79 30 77.0 35-219 0.957 30 77.2 11-162 2.44 30 69.1 17-168 7.85 30 74.4 33-227 0.456 30 71.3 26-137 1.10 30 68.7 59-121 9.67 30 76.5 39-171 3.01 30 58.9 21-133 4.22 30 71.8 54-120 3.37 30 57.0 44-142 2.46 30 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 18 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 NVOA GCMS - Quality Control Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits Batch B211125 LCS Dup (B211125-BSD1) 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol 32.4 5.00 ug/L 50.00 31.4 5.00 ug/L 50.00 29.4 5.00 ug/L 50.00 38.2 5.00 ug/L 50.00 38.9 5.00 ug/L 50.00 26.6 5.00 ug/L 50.00 31.9 5.00 ug/L 50.00 28.5 5.00 ug/L 50.00 32.4 5.00 ug/L 50.00 43.1 5.00 ug/L 50.00 40.3 5.00 ug/L 50.00 35.7 5.00 ug/L 50.00 33.5 5.00 ug/L 50.00 34.5 5.00 ug/L 50.00 16.6 5.00 ug/L 50.00 31.1 5.00 ug/L 50.00 30.4 5.00 ug/L 50.00 27.5 5.00 ug/L 50.00 43.6 5.00 ug/L 50.00 38.3 5.00 ug/L 50.00 35.1 5.00 ug/L 50.00 34.5 5.00 ug/L 50.00 32.5 5.00 ug/L 50.00 37.2 5.00 ug/L 50.00 42.4 5.00 ug/L 50.00 35.0 5.00 ug/L 50.00 26.6 5.00 ug/L 50.00 35.7 5.00 ug/L 50.00 28.3 5.00 ug/L 50.00 34.6 5.00 ug/L 50.00 33.0 5.00 ug/L 50.00 19.3 5.00 ug/L 50.00 32.1 5.00 ug/L 50.00 41.0 5.00 ug/L 50.00 36.2 5.00 ug/L 50.00 64.9 37-144 62.8 39-135 58.9 32-120 76.5 39-139 77.7 50-158 53.2 21-191 63.8 60-120 57.0 23-134 64.9 29-182 86.2 38-262 80.6 17-181 71.3 53-127 66.9 22-147 69.0 25-158 33.2 9-132 62.2 33-184 60.7 12-158 55.0 36-166 87.3 8-158 76.6 38-152 70.2 60-115 69.1 31-114 65.0 28-120 74.3 1-120 84.7 4-146 70.1 35-152 53.2 24-120 71.4 15-76 56.6 40-120 69.1 21-196 65.9 35-180 38.5 17-127 64.2 43-230 81.9 79-139 72.3 14-176 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 RPD 4.37 2.24 8.96 7.80 8.59 21.0 5.10 2.52 0.859 7.86 5.14 7.51 4.87 12.9 19.1 0.673 1.86 5.51 9.31 0.340 5.96 6.52 5.94 2.65 7.11 6.64 4.59 4.09 4.81 0.203 3.52 2.47 3.10 6.76 4.47 RPD Limit 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Page 19 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 NVOA GCMS - Quality Control Analyte Batch B211125 LCS Dup (B211125-BSD1) Phenol Pyrene Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12 Matrix Spike (B211125-MS1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit 13.0 5.00 ug/L 50.00 36.3 5.00 ug/L 50.00 28.4 ug/L 50.00 11.3 ug/L 50.00 25.1 ug/L 50.00 23.6 ug/L 50.00 29.0 ug/L 50.00 42.0 ug/L 50.00 31.5 ug/L 50.00 26.0 5-120 1.08 30 72.6 52-120 1.98 30 56.8 60-140 22.6 60-140 50.1 60-140 47.1 60-140 57.9 60-140 84.1 60-140 63.0 60-140 Source: 2211012-02 29.0 4.95 ug/L 30.3 4.95 ug/L 43.9 4.95 ug/L 38.3 4.95 ug/L 38.0 4.95 ug/L 38.2 4.95 ug/L 46.0 4.95 ug/L 36.3 4.95 ug/L 37.3 4.95 ug/L 44.9 4.95 ug/L 36.7 4.95 ug/L 47.7 4.95 ug/L 46.5 4.95 ug/L 18.4 4.95 ug/L 45.7 4.95 ug/L 16.6 4.95 ug/L 28.8 4.95 ug/L 31.8 4.95 ug/L 38.5 4.95 ug/L 47.3 4.95 ug/L 36.0 4.95 ug/L 4.99 4.95 ug/L 26.7 4.95 ug/L 23.8 4.95 ug/L 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 58.6 47-145 61.3 33-145 88.6 27-133 77.4 33-143 76.7 17-163 77.2 24-159 93.0 35-219 73.4 11-162 75.3 17-168 90.6 33-227 74.1 26-137 96.3 59-121 94.0 39-171 37.1 21-133 92.3 54-120 33.5 44-142 58.1 37-144 64.3 39-135 77.7 32-120 95.6 39-139 72.7 50-158 10.1 21-191 53.9 60-120 48.1 23-134 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 20 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 NVOA GCMS - Quality Control Analyte Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD Batch B211125 Matrix Spike (B211125-MS1) 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Source: 2211012-02 21.9 4.95 ug/L 7.50 4.95 ug/L 11.3 4.95 ug/L 48.4 4.95 ug/L 31.2 4.95 ug/L 46.6 4.95 ug/L 14.3 4.95 ug/L 23.9 4.95 ug/L 14.4 4.95 ug/L 13.6 4.95 ug/L 54.0 4.95 ug/L 34.6 4.95 ug/L 52.7 4.95 ug/L 47.3 4.95 ug/L 27.4 4.95 ug/L 44.9 4.95 ug/L 47.0 4.95 ug/L 44.6 4.95 ug/L 13.7 4.95 ug/L 2.01 4.95 ug/L 7.84 4.95 ug/L 19.8 4.95 ug/L 20.0 4.95 ug/L 3.50 4.95 ug/L 18.6 4.95 ug/L 50.0 4.95 ug/L 27.2 4.95 ug/L 16.8 4.95 ug/L 35.6 4.95 ug/L 14.1 ug/L 14.9 ug/L 16.2 ug/L 15.6 ug/L 25.5 ug/L 55.3 ug/L 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 3.48 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 ND 49.50 49.50 49.50 49.50 49.50 49.50 44.1 29-182 15.2 38-262 22.9 17-181 97.7 53-127 63.0 22-147 94.2 25-158 28.8 9-132 48.2 33-184 29.0 12-158 27.5 36-166 102 8-158 69.9 38-152 106 61-106 95.6 31-114 55.4 28-120 90.8 1-120 95.0 4-146 90.1 35-152 27.8 24-120 4.06 15-76 15.8 40-120 39.9 21-196 40.3 35-180 7.08 17-127 37.6 43-230 101 79-139 55.0 14-176 33.9 5-120 71.9 52-120 28.4 60-140 30.1 60-140 32.8 60-140 31.4 60-140 51.6 60-140 112 60-140 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 RPD Limit Page 21 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 NVOA GCMS - Quality Control Analyte Batch B211125 Matrix Spike (B211125-MS1) Surrogate: Chrysene-D12 Matrix Spike Dup (B211125-MSD1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD Source: 2211012-02 32.6 ug/L Source: 2211012-02 33.6 5.00 ug/L 35.2 5.00 ug/L 48.1 5.00 ug/L 40.3 5.00 ug/L 41.0 5.00 ug/L 41.5 5.00 ug/L 48.1 5.00 ug/L 39.4 5.00 ug/L 39.7 5.00 ug/L 47.3 5.00 ug/L 39.6 5.00 ug/L 53.9 5.00 ug/L 48.5 5.00 ug/L 24.6 5.00 ug/L 50.0 5.00 ug/L 21.0 5.00 ug/L 47.2 5.00 ug/L 51.2 5.00 ug/L 52.5 5.00 ug/L 53.2 5.00 ug/L 40.7 5.00 ug/L 9.00 5.00 ug/L 32.3 5.00 ug/L 36.7 5.00 ug/L 37.1 5.00 ug/L 8.09 5.00 ug/L 20.2 5.00 ug/L 51.8 5.00 ug/L 47.8 5.00 ug/L 52.7 5.00 ug/L --- U 5.00 ug/L 29.8 5.00 ug/L 49.50 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 50.00 ND 65.8 60-140 67.1 47-145 14.6 70.3 33-145 14.8 96.3 27-133 9.30 80.5 33-143 5.00 82.1 17-163 7.77 82.9 24-159 8.11 96.1 35-219 4.34 78.8 11-162 8.19 79.5 17-168 6.42 94.5 33-227 5.19 79.2 26-137 7.73 108 59-121 12.3 97.0 39-171 4.18 49.2 21-133 29.1 100 54-120 9.02 42.1 44-142 23.7 94.3 37-144 48.5 102 39-135 46.5 105 32-120 30.8 106 39-139 11.7 81.5 50-158 12.3 18.0 21-191 57.3 64.6 60-120 19.0 73.4 23-134 42.6 74.1 29-182 51.6 16.2 38-262 7.50 40.4 17-181 56.2 104 53-127 6.87 95.5 22-147 42.0 105 25-158 12.2 9-132 59.6 33-184 22.1 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 RPD Limit 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 Page 22 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 NVOA GCMS - Quality Control Analyte Batch B211125 Matrix Spike Dup (B211125-MSD1) Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12 Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit Source: 2211012-02 21.7 5.00 ug/L 50.00 ND 43.5 12-158 40.9 24 19.7 5.00 ug/L 50.00 ND 39.4 36-166 36.4 24 55.3 5.00 ug/L 50.00 3.48 104 8-158 2.27 24 32.1 5.00 ug/L 50.00 ND 64.2 38-152 7.48 24 56.0 5.00 ug/L 50.00 ND 112 61-106 6.14 24 42.6 5.00 ug/L 50.00 ND 85.1 31-114 10.5 24 16.8 5.00 ug/L 50.00 ND 33.6 28-120 48.1 24 45.0 5.00 ug/L 50.00 ND 90.0 1-120 0.154 24 51.0 5.00 ug/L 50.00 ND 102 4-146 8.04 24 50.8 5.00 ug/L 50.00 ND 102 35-152 13.0 24 18.8 5.00 ug/L 50.00 ND 37.5 24-120 30.9 24 2.50 5.00 ug/L 50.00 ND 5.00 15-76 21.7 24 15.4 5.00 ug/L 50.00 ND 30.9 40-120 65.3 24 28.2 5.00 ug/L 50.00 ND 56.4 21-196 35.1 24 26.9 5.00 ug/L 50.00 ND 53.7 35-180 29.5 24 12.6 5.00 ug/L 50.00 ND 25.2 17-127 113 24 27.8 5.00 ug/L 50.00 ND 55.6 43-230 39.6 24 54.5 5.00 ug/L 50.00 ND 109 79-139 8.65 24 42.7 5.00 ug/L 50.00 ND 85.5 14-176 44.3 24 20.0 5.00 ug/L 50.00 ND 40.0 5-120 17.3 24 38.2 5.00 ug/L 50.00 ND 76.4 52-120 7.09 24 23.0 ug/L 50.00 46.1 60-140 17.8 ug/L 50.00 35.5 60-140 22.6 ug/L 50.00 45.3 60-140 21.5 ug/L 50.00 43.0 60-140 42.8 ug/L 50.00 85.7 60-140 64.1 ug/L 50.00 128 60-140 35.4 ug/L 50.00 70.8 60-140 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 23 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Pest/PCBs GC - Quality Control Analyte Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD Batch B211133 Blank (B211133-BLK1) alpha-BHC alpha-BHC [2C] gamma-BHC (Lindane) gamma-BHC (Lindane) [2C] beta-BHC beta-BHC [2C] delta-BHC delta-BHC [2C] Heptachlor Heptachlor [2C] Aldrin Aldrin [2C] Heptachlor epoxide Heptachlor epoxide [2C] gamma-Chlordane gamma-Chlordane [2C] alpha-Chlordane alpha-Chlordane [2C] Endosulfan I Endosulfan I [2C] 4,4'-DDE 4,4'-DDE [2C] Dieldrin Dieldrin [2C] Endrin Endrin [2C] 4,4'-DDD 4,4'-DDD [2C] Endosulfan II Endosulfan II [2C] 4,4'-DDT 4,4'-DDT [2C] Endrin aldehyde Endrin aldehyde [2C] Methoxychlor --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.002 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.005 ug/L --- U 0.025 ug/L U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 RPD Limit Page 24 of 38 Analyte Batch B211133 Blank (B211133-BLK1) Methoxychlor [2C] Endosulfan sulfate Endosulfan sulfate [2C] Endrin ketone Endrin ketone [2C] Toxaphene Toxaphene [2C] Chlordane Chlordane [2C] tech-Chlordane tech-Chlordane [2C] Aroclor 1016 Aroclor 1016 [2C] Aroclor 1221 Aroclor 1221 [2C] Aroclor 1232 Aroclor 1232 [2C] Aroclor 1242 Aroclor 1242 [2C] Aroclor 1248 Aroclor 1248 [2C] Aroclor 1254 Aroclor 1254 [2C] Aroclor 1260 Aroclor 1260 [2C] Aroclor 1262 Aroclor 1262 [2C] Aroclor 1268 Aroclor 1268 [2C] Surrogate: TCMX Surrogate: TCMX [2C] Surrogate: DCB Surrogate: DCB [2C] UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Pest/PCBs GC - Quality Control Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U 0.034 --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U 0.0378 0.0387 0.0373 0.0367 0.025 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.188 ug/L 0.188 ug/L 0.062 ug/L 0.062 ug/L 0.062 ug/L 0.062 ug/L 0.031 ug/L 0.031 ug/L 0.062 ug/L 0.062 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L ug/L ug/L ug/L ug/L 0.06000 0.06000 0.06000 0.06000 63.0 23-101 64.4 23-101 62.2 25-107 61.2 25-107 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 25 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Pest/PCBs GC - Quality Control Analyte Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD Batch B211133 LCS (B211133-BS1) alpha-BHC alpha-BHC [2C] gamma-BHC (Lindane) gamma-BHC (Lindane) [2C] beta-BHC beta-BHC [2C] delta-BHC delta-BHC [2C] Heptachlor Heptachlor [2C] Aldrin Aldrin [2C] Heptachlor epoxide Heptachlor epoxide [2C] gamma-Chlordane gamma-Chlordane [2C] alpha-Chlordane alpha-Chlordane [2C] Endosulfan I Endosulfan I [2C] 4,4'-DDE 4,4'-DDE [2C] Dieldrin Dieldrin [2C] Endrin Endrin [2C] 4,4'-DDD 4,4'-DDD [2C] Endosulfan II Endosulfan II [2C] 4,4'-DDT 4,4'-DDT [2C] Endrin aldehyde Endrin aldehyde [2C] Methoxychlor 0.02 0.002 ug/L 0.02000 0.01 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.01 0.002 ug/L 0.02000 0.01 0.002 ug/L 0.02000 0.01 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.01 0.002 ug/L 0.02000 0.01 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.01 0.002 ug/L 0.02000 0.02 0.002 ug/L 0.02000 0.03 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.05 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.04 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.03 0.005 ug/L 0.04000 0.18 0.025 ug/L 0.2000 76.3 37-140 73.1 37-140 80.1 32-140 73.6 32-140 74.5 17-147 72.2 17-147 86.1 19-140 84.1 19-140 62.5 34-140 59.1 34-140 78.4 42-140 77.6 42-140 81.6 37-142 78.1 37-142 83.2 45-140 75.6 45-140 81.5 45-140 75.8 45-140 73.3 45-153 77.9 45-153 85.5 30-145 82.1 30-145 86.7 36-146 83.9 36-146 120 30-147 86.9 30-147 88.0 31-141 81.7 31-141 79.4 50-202 75.8 50-202 86.3 25-160 80.7 25-160 81.7 10-154 78.8 10-154 90.0 29-167 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 RPD Limit Page 26 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Pest/PCBs GC - Quality Control Analyte Batch B211133 LCS (B211133-BS1) Methoxychlor [2C] Endosulfan sulfate Endosulfan sulfate [2C] Endrin ketone Endrin ketone [2C] Surrogate: TCMX Surrogate: TCMX [2C] Surrogate: DCB Surrogate: DCB [2C] LCS (B211133-BS2) Aroclor 1016 Aroclor 1016 [2C] Aroclor 1260 Aroclor 1260 [2C] Surrogate: TCMX Surrogate: TCMX [2C] Surrogate: DCB Surrogate: DCB [2C] LCS Dup (B211133-BSD1) alpha-BHC alpha-BHC [2C] gamma-BHC (Lindane) gamma-BHC (Lindane) [2C] beta-BHC beta-BHC [2C] delta-BHC delta-BHC [2C] Heptachlor Heptachlor [2C] Aldrin Aldrin [2C] Heptachlor epoxide Heptachlor epoxide [2C] Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit 0.16 0.03 0.03 0.03 0.03 0.0373 0.0404 0.0376 0.0369 0.17 0.17 0.17 0.16 0.0348 0.0347 0.0366 0.0347 0.02 0.01 0.02 0.01 0.02 0.01 0.02 0.02 0.01 0.01 0.02 0.02 0.02 0.01 0.025 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L ug/L ug/L ug/L ug/L 0.2000 0.04000 0.04000 0.04000 0.04000 0.06000 0.06000 0.06000 0.06000 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L ug/L ug/L ug/L ug/L 0.2500 0.2500 0.2500 0.2500 0.06000 0.06000 0.06000 0.06000 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 79.9 29-167 85.3 26-144 83.1 26-144 73.6 23-168 78.6 23-168 62.2 23-101 67.3 23-101 62.7 25-107 61.6 25-107 68.0 50-140 69.3 50-140 67.0 8-140 64.8 8-140 58.0 23-101 57.9 23-101 61.0 25-107 57.8 25-107 83.6 37-140 9.13 36 71.9 37-140 1.64 36 82.1 32-140 2.36 39 71.6 32-140 2.69 39 80.9 17-147 8.21 44 69.6 17-147 3.56 44 84.4 19-140 1.93 52 80.0 19-140 4.88 52 59.0 34-140 5.89 43 55.9 34-140 5.51 43 77.9 42-140 0.582 35 78.5 42-140 1.10 35 80.0 37-142 1.97 26 74.1 37-142 5.23 26 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 27 of 38 Analyte Batch B211133 LCS Dup (B211133-BSD1) gamma-Chlordane gamma-Chlordane [2C] alpha-Chlordane alpha-Chlordane [2C] Endosulfan I Endosulfan I [2C] 4,4'-DDE 4,4'-DDE [2C] Dieldrin Dieldrin [2C] Endrin Endrin [2C] 4,4'-DDD 4,4'-DDD [2C] Endosulfan II Endosulfan II [2C] 4,4'-DDT 4,4'-DDT [2C] Endrin aldehyde Endrin aldehyde [2C] Methoxychlor Methoxychlor [2C] Endosulfan sulfate Endosulfan sulfate [2C] Endrin ketone Endrin ketone [2C] Surrogate: TCMX Surrogate: TCMX [2C] Surrogate: DCB Surrogate: DCB [2C] UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Pest/PCBs GC - Quality Control Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit 0.02 0.01 0.02 0.01 0.01 0.01 0.03 0.03 0.03 0.03 0.05 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.17 0.15 0.03 0.03 0.03 0.03 0.0394 0.0409 0.0361 0.0357 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.002 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.025 ug/L 0.025 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L 0.005 ug/L ug/L ug/L ug/L ug/L 0.02000 0.02000 0.02000 0.02000 0.02000 0.02000 0.04000 0.04000 0.04000 0.04000 0.04000 0.04000 0.04000 0.04000 0.04000 0.04000 0.04000 0.04000 0.04000 0.04000 0.2000 0.2000 0.04000 0.04000 0.04000 0.04000 0.06000 0.06000 0.06000 0.06000 81.4 45-140 2.16 35 71.1 45-140 6.16 35 79.9 45-140 2.06 35 71.6 45-140 5.74 35 70.2 45-153 4.28 28 73.6 45-153 5.67 28 81.7 30-145 4.60 35 77.4 30-145 5.80 35 83.8 36-146 3.37 49 79.6 36-146 5.21 49 117 30-147 2.51 48 82.4 30-147 5.26 48 85.2 31-141 3.33 39 77.6 31-141 5.11 39 77.0 50-202 3.11 53 72.3 50-202 4.69 53 83.3 25-160 3.59 42 76.6 25-160 5.15 42 79.7 10-154 2.49 30 74.7 10-154 5.29 30 85.7 29-167 4.92 30 75.0 29-167 6.30 30 82.6 26-144 3.24 38 79.3 26-144 4.68 38 73.3 23-168 0.473 30 74.6 23-168 5.18 30 65.7 23-101 68.1 23-101 60.2 25-107 59.5 25-107 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 28 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Pest/PCBs GC - Quality Control Analyte Batch B211133 LCS Dup (B211133-BSD2) Aroclor 1016 Aroclor 1016 [2C] Aroclor 1260 Aroclor 1260 [2C] Surrogate: TCMX Surrogate: TCMX [2C] Surrogate: DCB Surrogate: DCB [2C] Matrix Spike (B211133-MS1) alpha-BHC alpha-BHC [2C] gamma-BHC (Lindane) gamma-BHC (Lindane) [2C] beta-BHC beta-BHC [2C] delta-BHC delta-BHC [2C] Heptachlor Heptachlor [2C] Aldrin Aldrin [2C] Heptachlor epoxide Heptachlor epoxide [2C] gamma-Chlordane gamma-Chlordane [2C] alpha-Chlordane alpha-Chlordane [2C] Endosulfan I Endosulfan I [2C] 4,4'-DDE 4,4'-DDE [2C] Dieldrin Dieldrin [2C] Endrin Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit 0.17 0.17 0.18 0.16 0.0381 0.0334 0.0359 0.0360 0.031 ug/L 0.031 ug/L 0.031 ug/L 0.031 ug/L ug/L ug/L ug/L ug/L 0.2500 0.2500 0.2500 0.2500 0.06000 0.06000 0.06000 0.06000 67.6 50-140 0.632 36 68.2 50-140 1.68 36 72.7 8-140 8.16 38 63.7 8-140 1.61 38 63.6 23-101 55.7 23-101 59.8 25-107 60.0 25-107 Source: 2211012-02 0.006 0.002 ug/L 0.005 0.002 ug/L 0.006 0.002 ug/L 0.006 0.002 ug/L 0.008 0.002 ug/L 0.006 0.002 ug/L 0.01 0.002 ug/L --- U 0.002 ug/L 0.02 0.002 ug/L 0.008 0.002 ug/L 0.005 0.002 ug/L 0.002 0.002 ug/L 0.009 0.002 ug/L 0.006 0.002 ug/L 0.006 0.002 ug/L 0.006 0.002 ug/L --- U 0.002 ug/L 0.004 0.002 ug/L 0.005 0.002 ug/L 0.007 0.002 ug/L 0.009 0.004 ug/L 0.009 0.004 ug/L 0.01 0.004 ug/L 0.01 0.004 ug/L 0.02 0.004 ug/L 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.01786 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.03571 ND 34.2 37-140 29.8 37-140 33.9 32-140 33.0 32-140 44.7 17-147 33.0 17-147 78.2 19-140 19-140 93.4 34-140 44.7 34-140 28.2 42-140 12.4 42-140 48.6 37-142 34.7 37-142 35.9 45-140 34.2 45-140 45-140 24.0 45-140 26.1 45-153 37.6 45-153 26.1 30-145 25.0 30-145 34.8 36-146 29.3 36-146 48.0 30-147 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 29 of 38 Analyte Batch B211133 Matrix Spike (B211133-MS1) Endrin [2C] 4,4'-DDD 4,4'-DDD [2C] Endosulfan II Endosulfan II [2C] 4,4'-DDT 4,4'-DDT [2C] Endrin aldehyde Endrin aldehyde [2C] Methoxychlor Methoxychlor [2C] Endosulfan sulfate Endosulfan sulfate [2C] Endrin ketone Endrin ketone [2C] Surrogate: TCMX Surrogate: TCMX [2C] Surrogate: DCB Surrogate: DCB [2C] Matrix Spike (B211133-MS2) Aroclor 1016 Aroclor 1016 [2C] Aroclor 1260 Aroclor 1260 [2C] Surrogate: TCMX Surrogate: TCMX [2C] Surrogate: DCB Surrogate: DCB [2C] UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Pest/PCBs GC - Quality Control Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit Source: 2211012-02 0.01 0.004 ug/L 0.008 0.004 ug/L 0.008 0.004 ug/L 0.008 0.004 ug/L 0.009 0.004 ug/L 0.006 0.004 ug/L 0.006 0.004 ug/L 0.003 0.004 ug/L 0.005 0.004 ug/L 0.04 0.022 ug/L 0.02 0.022 ug/L 0.004 0.004 ug/L 0.002 0.004 ug/L --- U 0.004 ug/L --- U 0.004 ug/L 0.0205 ug/L 0.0138 ug/L 0.00687 ug/L 0.00618 ug/L Source: 2211012-02 --- U 0.028 ug/L --- U 0.028 ug/L 0.06 0.028 ug/L 0.05 0.028 ug/L 0.0199 ug/L 0.0135 ug/L 0.00334 ug/L 0.00594 ug/L 0.03571 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.1786 ND 0.1786 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.03571 ND 0.05357 0.05357 0.05357 0.05357 0.2222 ND 0.2222 ND 0.2222 ND 0.2222 ND 0.05333 0.05333 0.05333 0.05333 34.7 30-147 23.3 31-141 23.1 31-141 23.6 50-202 24.8 50-202 17.6 25-160 16.0 25-160 7.98 10-154 13.7 10-154 22.3 29-167 13.8 29-167 10.7 26-144 5.18 26-144 23-168 23-168 38.2 23-101 25.8 23-101 12.8 25-107 11.5 25-107 50-140 50-140 27.8 8-140 20.4 8-140 37.4 23-101 25.3 23-101 6.27 25-107 11.1 25-107 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 30 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Pest/PCBs GC - Quality Control Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits Batch B211133 Matrix Spike Dup (B211133-MSD1) alpha-BHC alpha-BHC [2C] gamma-BHC (Lindane) gamma-BHC (Lindane) [2C] beta-BHC beta-BHC [2C] delta-BHC delta-BHC [2C] Heptachlor Heptachlor [2C] Aldrin Aldrin [2C] Heptachlor epoxide Heptachlor epoxide [2C] gamma-Chlordane gamma-Chlordane [2C] alpha-Chlordane alpha-Chlordane [2C] Endosulfan I Endosulfan I [2C] 4,4'-DDE 4,4'-DDE [2C] Dieldrin Dieldrin [2C] Endrin Endrin [2C] 4,4'-DDD 4,4'-DDD [2C] Endosulfan II Endosulfan II [2C] 4,4'-DDT 4,4'-DDT [2C] Endrin aldehyde Endrin aldehyde [2C] Methoxychlor Source: 2211012-02 0.008 0.002 ug/L 0.006 0.002 ug/L 0.007 0.002 ug/L 0.005 0.002 ug/L 0.009 0.002 ug/L 0.006 0.002 ug/L 0.01 0.002 ug/L --- U 0.002 ug/L 0.02 0.002 ug/L 0.008 0.002 ug/L 0.005 0.002 ug/L 0.004 0.002 ug/L 0.008 0.002 ug/L 0.008 0.002 ug/L 0.006 0.002 ug/L 0.006 0.002 ug/L --- U 0.002 ug/L 0.005 0.002 ug/L 0.004 0.002 ug/L 0.006 0.002 ug/L 0.009 0.004 ug/L 0.008 0.004 ug/L 0.01 0.004 ug/L 0.01 0.004 ug/L 0.02 0.004 ug/L 0.01 0.004 ug/L 0.007 0.004 ug/L 0.007 0.004 ug/L 0.008 0.004 ug/L 0.007 0.004 ug/L 0.005 0.004 ug/L 0.004 0.004 ug/L 0.002 0.004 ug/L 0.004 0.004 ug/L 0.03 0.022 ug/L 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.01794 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.03587 ND 0.1794 ND 42.8 37-140 32.8 37-140 39.9 32-140 27.6 32-140 52.0 17-147 34.1 17-147 83.2 19-140 19-140 106 34-140 45.7 34-140 28.3 42-140 24.7 42-140 46.8 37-142 46.5 37-142 35.7 45-140 31.6 45-140 45-140 25.9 45-140 25.0 45-153 34.9 45-153 25.4 30-145 23.6 30-145 33.3 36-146 30.9 36-146 45.2 30-147 34.1 30-147 19.0 31-141 18.4 31-141 21.0 50-202 18.5 50-202 13.2 25-160 12.2 25-160 6.37 10-154 10.9 10-154 18.1 29-167 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 RPD 22.2 9.61 16.3 18.0 15.0 3.24 6.20 12.6 2.36 0.266 66.2 3.90 29.0 0.586 8.04 7.69 4.54 7.44 2.78 5.88 4.47 5.42 5.96 1.86 20.2 22.6 11.3 28.9 28.2 27.4 22.3 23.0 20.5 RPD Limit 36 36 39 39 44 44 52 52 43 43 35 35 26 26 35 35 35 35 28 28 35 35 49 49 48 48 39 39 53 53 42 42 30 30 30 Page 31 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Pest/PCBs GC - Quality Control Analyte Batch B211133 Matrix Spike Dup (B211133-MSD1) Methoxychlor [2C] Endosulfan sulfate Endosulfan sulfate [2C] Endrin ketone Endrin ketone [2C] Surrogate: TCMX Surrogate: TCMX [2C] Surrogate: DCB Surrogate: DCB [2C] Matrix Spike Dup (B211133-MSD2) Aroclor 1016 Aroclor 1016 [2C] Aroclor 1260 Aroclor 1260 [2C] Surrogate: TCMX Surrogate: TCMX [2C] Surrogate: DCB Surrogate: DCB [2C] Batch S211050 Performance Mix (S211050-PEM1) 4,4'-DDE 4,4'-DDE [2C] Endrin Endrin [2C] 4,4'-DDD 4,4'-DDD [2C] 4,4'-DDT 4,4'-DDT [2C] Endrin aldehyde Endrin aldehyde [2C] Endrin ketone Endrin ketone [2C] Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit Source: 2211012-02 0.02 0.022 ug/L 0.1794 ND 11.3 29-167 19.9 30 0.003 0.004 ug/L 0.03587 ND 7.80 26-144 31.3 38 0.002 0.004 ug/L 0.03587 ND 26-144 38 0.005 0.004 ug/L 0.03587 ND 14.8 23-168 30 0.004 0.004 ug/L 0.03587 ND 11.3 23-168 30 0.0243 0.0142 0.00446 0.00477 ug/L 0.05381 ug/L 0.05381 ug/L 0.05381 ug/L 0.05381 45.2 23-101 26.4 23-101 8.29 25-107 8.86 25-107 Source: 2211012-02 --- U 0.028 ug/L 0.2232 ND 50-140 36 --- U 0.028 ug/L 0.2232 ND 50-140 36 0.05 0.028 ug/L 0.2232 ND 21.8 8-140 24.1 38 0.05 0.028 ug/L 0.2232 ND 23.6 8-140 14.8 38 0.0190 0.0122 0.00326 0.00436 ug/L 0.05357 ug/L 0.05357 ug/L 0.05357 ug/L 0.05357 35.5 23-101 22.7 23-101 6.08 25-107 8.15 25-107 1.33 ug/L 0-200 1.01 ug/L 0-200 127 ug/L 100.0 127 0-200 102 ug/L 100.0 102 0-200 2.25 ug/L 0-200 2.28 ug/L 0-200 96.6 ug/L 100.0 96.6 0-200 99.3 ug/L 100.0 99.3 0-200 4.13 ug/L 0-200 2.51 ug/L 0-200 5.08 ug/L 0-200 4.39 ug/L 0-200 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 32 of 38 Analyte Batch B212014 Blank (B212014-BLK1) Oil & Grease LCS (B212014-BS1) Oil & Grease LCS Dup (B212014-BSD1) Oil & Grease Matrix Spike (B212014-MS1) Oil & Grease UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 GC - Sanitary - Quality Control Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit --- U 5.00 mg/L 31.8 5.00 mg/L 40.00 80 78-114 34.5 5.00 mg/L 40.00 86 78-114 8 20 Source: 2211012-02 29.9 5.00 mg/L 47.06 1.40 61 78-114 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 33 of 38 Analyte Batch B211134 Blank (B211134-BLK1) Barium Cadmium Chromium Copper Lead Magnesium Nickel Silver Zinc LCS (B211134-BS1) Barium Cadmium Chromium Copper Lead Magnesium Nickel Silver Zinc LCS Dup (B211134-BSD1) Barium Cadmium Chromium Copper Lead Magnesium Nickel Silver Zinc UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Metals ICP - Quality Control Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit --- U --- U --- U --- U --- U --- U --- U --- U --- U 199 194 196 194 196 4830 195 194 193 204 199 201 200 198 4980 200 199 197 100 ug/L 3.00 ug/L 5.00 ug/L 10.0 ug/L 8.00 ug/L 500 ug/L 20.0 ug/L 5.00 ug/L 20.0 ug/L 100 ug/L 3.00 ug/L 5.00 ug/L 10.0 ug/L 8.00 ug/L 500 ug/L 20.0 ug/L 5.00 ug/L 20.0 ug/L 200.0 200.0 200.0 200.0 200.0 5000 200.0 200.0 200.0 100 ug/L 3.00 ug/L 5.00 ug/L 10.0 ug/L 8.00 ug/L 500 ug/L 20.0 ug/L 5.00 ug/L 20.0 ug/L 200.0 200.0 200.0 200.0 200.0 5000 200.0 200.0 200.0 99.6 85-115 96.8 85-115 97.8 85-115 97.0 85-115 97.9 85-115 96.7 85-115 97.6 85-115 96.9 85-115 96.4 85-115 102 85-115 2.54 20 99.3 85-115 2.58 20 100 85-115 2.65 20 99.8 85-115 2.86 20 99.1 85-115 1.24 20 99.7 85-115 3.03 20 100 85-115 2.62 20 99.3 85-115 2.50 20 98.3 85-115 1.93 20 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 34 of 38 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Metals ICP - Quality Control Analyte Batch B211134 Matrix Spike (B211134-MS1) Barium Cadmium Chromium Copper Lead Magnesium Nickel Silver Zinc Matrix Spike Dup (B211134-MSD1) Barium Cadmium Chromium Copper Lead Magnesium Nickel Silver Zinc Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit Source: 2211012-02 245 100 ug/L 190 3.00 ug/L 200 5.00 ug/L 234 10.0 ug/L 196 8.00 ug/L 7100 500 ug/L 203 20.0 ug/L 204 5.00 ug/L 223 20.0 ug/L Source: 2211012-02 245 500 ug/L 195 15.0 ug/L 199 25.0 ug/L 229 50.0 ug/L 195 40.0 ug/L 7360 2500 ug/L 209 100 ug/L 196 25.0 ug/L 227 100 ug/L 200.0 44.4 200.0 ND 200.0 1.68 200.0 17.5 200.0 ND 5000 2500 200.0 9.12 200.0 ND 200.0 30.3 101 80-120 94.9 80-120 99.0 80-120 108 80-120 97.8 80-120 91.9 80-120 97.1 80-120 102 80-120 96.2 80-120 200.0 44.4 100 80-120 0.0285 10 200.0 ND 97.4 80-120 2.60 10 200.0 ND 99.7 80-120 0.130 10 200.0 17.5 106 80-120 2.11 10 200.0 ND 97.4 80-120 0.338 10 5000 2500 97.2 80-120 3.67 10 200.0 ND 104 80-120 2.65 10 200.0 ND 98.2 80-120 3.72 10 200.0 30.3 98.2 80-120 1.79 10 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 35 of 38 Analyte Batch B211124 Blank (B211124-BLK1) Cyanide, Total Blank (B211124-BLK2) Cyanide, Total LCS (B211124-BS1) Cyanide, Total LCS Dup (B211124-BSD1) Cyanide, Total Matrix Spike (B211124-MS1) Cyanide, Total Batch B211128 Blank (B211128-BLK1) Residue, Non-Filterable Blank (B211128-BLK2) Residue, Non-Filterable LCS (B211128-BS1) Residue, Non-Filterable LCS Dup (B211128-BSD1) Residue, Non-Filterable UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Sanitary - Quality Control Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit --- U 10.0 ug/L --- U 10.0 ug/L 721 10.0 ug/L 796.0 91 90-110 717 10.0 ug/L 796.0 90 90-110 0.6 20 Source: 2211012-02 852 10.0 ug/L 500.0 26.4 165 90-110 --- U 10.0 mg/L --- U 10.0 mg/L 59.0 10.0 mg/L 55.10 56.0 10.0 mg/L 55.10 107 85-115 102 85-115 5.22 20 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 36 of 38 Analyte Batch B211128 Duplicate (B211128-DUP1) Residue, Non-Filterable Batch B211129 Blank (B211129-BLK1) Biochemical Oxygen Demand LCS (B211129-BS1) Biochemical Oxygen Demand LCS (B211129-BS2) Biochemical Oxygen Demand LCS (B211129-BS3) Biochemical Oxygen Demand Batch B211139 Blank (B211139-BLK1) Phosphorus Blank (B211139-BLK2) Phosphorus LCS (B211139-BS1) Phosphorus UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Sanitary - Quality Control Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit Source: 2211012-02 27.0 10.0 mg/L 25.0 7.69 20 --- U 2.00 mg/L 196 mg/L 198.0 172 mg/L 198.0 186 mg/L 198.0 99.1 84.6-115.4 87.0 84.6-115.4 93.8 84.6-115.4 --- U 0.0500 mg/L --- U 0.0500 mg/L 8.32 0.250 mg/L 8.450 98 90-110 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 37 of 38 Analyte Batch B211139 LCS Dup (B211139-BSD1) Phosphorus Matrix Spike (B211139-MS1) Phosphorus UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory Final Report Project: Sportsfield Specialties, Inc. - 2211012 Project Number: 2211012 Sanitary - Quality Control Result Reporting Limit Units Spike Source %REC Level Result %REC Limits RPD RPD Limit 8.52 0.250 mg/L 8.450 101 90-110 2 20 Source: 2211012-02 1.68 0.0500 mg/L 1.000 0.753 93 90-110 U.S.E.P.A Region 2 Laboratory NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 12/7/2022 Page 38 of 38 Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Part 403 & 433.17, & IU Permit Insp. Date: November 15, 2022 8.0 Photographs Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Part 403 & 433.17, & IU Permit Insp. Date: November 15, 2022 Photo #1. Pretreated process wastewater is stored in the aerated storage tank. Photo #2. Compliance samples were collected from the spigot attached to the storage tank. Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Part 403 & 433.17, & IU Permit Insp. Date: November 15, 2022 Photo #3. Pretreated effluent is transported by the septic hauler to the POTW for treatment. Photo #4. Generated process wash water is treated through the Alar Waste Treatment System. Sportsfield Specialties, Inc., Delhi, NY 13753 40 CFR Part 403 & 433.17, & IU Permit Insp. Date: November 15, 2022 Photo #5. Accumulated solids from the vacuum filtration unit are collected in the tote bag. Photo #6. Defoaming agent is added to the filtrate in the holding tank.