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September 2nd, 1987
Mr. Dick Znidarsic Technical Director Chardon Rubber
Subject: Low Temperature Testing of Chardon Rubber Compounds
Dear Dick;
Samples supplied by Chardon Rubber were tested to determine their low temperature properties. Compound BX58J-26301 was reported to be a PVC compound containing no NBR rubber. Compound BX58J-26302 was reported to be the same compound with NBR rubber added. The Gehman low temperature test run
showed the all PVC control compound to have better low tem perature properties by a slight margin. The low temperature brittleness test showed the NBR bearing compound to perform
the best of the two compounds.
Dick, we believe the compression/deflection test to come
closest to reproducing the type of results you reported from
Nissan.
The hardness of the compound containing NBR was
lower initially, but became harder than its counterpart at
lower temperatures. The compression/deflection test reports
the load necessary to deflect a sample a predetermined per
centage. For your purposes we ran the test at room temper
ature, -25 deg. C, -35 deg. C, and at -40 deg. C.
Examination of the test results indicate that this data re
flects the findings you described in our last meeting. The
nitrile bearing compound does require higher loads to com
press it the same amount than the non-nitrile bearing com
pound.
At room temperature there is no noticeable
difference between the two recipes. At -25 deg. C, the two
recipes are still relatively close in low temperature prop
erties. However, at -35 deg. C, the NBR containing compound
stiffens up considerably more than the non-NBR bearing com
pound. The NBR/PVC compound appears to be approximately
twice as stiff as the PVC control at -35 and -45 deg. C.
CHARDO 01800
As a result of the data reported in this correspondence, we
have initiated a program to study the effects of employing
lower
ACN
polymers
in PVC/NBR. alloys on
compression/deflection test results. We will report our
findings to you at a later date. Please let us know if we
can be of any further help in your development effort.
Sincerely,
(\VJUJ "Srv&JJb
BCC: J R Purdon D E Miller J R Frazier
K M Kline J M Campo L A Cobb
Michael Stockdale Customer Technical Service Goodyear Chemical Division
CHARDO 01801
CHARDON RUBBER LOW TEMPERATURE TESTING
BX58J
26301 26302
GERMAN LOW TEMP. T{ 2) T ( 5} T< 10) T(100)
TORSION (DEG . C)
-14.
-9.
-26. -21.
-31. -26.
-43. -38.
BRITTLE TEMP. (C)
-43.5 -49.5
COMPRESSION/DEFLECTION INITIAL TEST - FIRST CYCLE
PSI g 10%
99. 50.
PSI @ 20%
115. 125.
PSI 8 30% PSI g 40%
247. 460.
235. 413.
HARDNESS A
55. 52.
COMPRESSION/MODULUS FINAL TEST THIRD CYCLE
PSI g 10%
89. 50.
PSI g 20%
97. 110.
PSI g 30%
190. 226.
PSI g 40%
495 . 436.
INCHES SET
.011 .012
COMPRESSION/MODULUS PSI g 10% PSI @ 20% PSI g 30% PSI g 40% HARDNESS A
TESTED 8 140. 450. 1000. 2140.
83.
--25C, INITIAL TEST 200. 550. 1120. 1850.
84.
(FIRST CYCLE)
COMPRES SION/MODULUS TESTED 8 --25C, FINAL TEST 3RD CYCLE
PSI @ 10%
225. 360.
PSI 8 20%
650. 950.
PSI g 30%
1675. 2080.
PSI @ 40%
3650 . 3350.
INCHES SET
.061 .061
COMPRESSION/MODULUS TESTED 8 --35C, INITIAL TEST
PSI @ 10%
140. 325 .
PSI g 20%
450. 740.
PSI @ 30%
820. 1340.
PSI g 40%
1355. 2005.
HARDNESS A
86. 89.
(FIRST RUN)
COMPRESSION/MODULUS TESTED 8 -35C, THIRD CYCLE FINAL TEST
PSI 8 10%
130 - 380.
PSI 8 20%
355. 935.
PSI @ 30%
1120. 2000.
PSI 8 40%
1892. 3125.
INCHES SET
.025 .053
CHARDO 01802
CHARDON RUBBER LOW TEMPERATURE TESTING
BX58J
26301 26302
COMPRESSION/MODULUS TESTED g
PSI 0 10%
385.
PSI @ 20%
950.
PSI 6 30%
1750.
PSI 40%
3200.
HARDNESS A
91.
-40C, INITIAL TEST
1460. 26S0. 3940. 5520. 93.
(FIRST RUN)
COMPRESSION/MODULUS PSI @ 10% PSI @ 20% PSI @ 30% PSI g 40% INCHES SET
TESTED g 960. 2350. 4025. 6450. .105
-40C, FINAL
2000. 4100. 6550. 9100. .086
TEST THIRD
CYCLE
CHARDO 01803