Document nmZkDBw7EL3JE6a9gXMOKq9dz
Report Prepared by: Report Approved by:
NPDES Pretreatment Compliance Sampling Inspection Report
Matco Tools 160 Chautauqua Avenue Lakewood, New York
March 18-19, 2021
ROBERT
Digitally signed by ROBERT
MORRELL
_M__O_R_R__E_L_L________Da_te_: 2_02_1.0_5_.13_0_9:0_2:_51_-0_4'_00_' _
Robert Morrell, Geologist
Monitoring Operations Section
Date: ________________
Digitally signed by PHILIP
PHILIP COCUZZA COCUZZA
________________Da_te_: 2_02_1._05_.1_3 0_6:_08_:0_6 -_04_'0_0' __ Philip Cocuzza, Chief Monitoring Operations Section
Date: ________________
Matco Tools
Inspection Dates: March 18-19, 2021
Page 2 of 6
Matco Tools
Inspection Dates: March 18-19, 2021
1.0 OBJECTIVE
On March 18-19, 2021, at the request of the Water Compliance Branch, the United States Environmental Protection Agency (USEPA) conducted a National Pollutant Discharge Elimination System (NPDES) Pretreatment Compliance Sampling Inspection (CSI) at Matco Tools in Lakewood, New York. The objective of the CSI was to gather information necessary to determine compliance with the requirements and limitations of 40 CFR Part 433 (Metal Finishing Point Source Category).
2.0 KEY PARTICIPANTS
Listed below are key inspection participants and contact information, grouped by organization.
U.S. Environmental Protection Agency Robert Morrell, Geologist, Lead Inspector Morrell.robert@epa.gov, 732-906-6804 Neal Johansen, Physical Scientist Johansen.neal@epa.gov, 732-321-6691
Matco Tools Kurt Eckberg, Maintenance Supervisor Kurt.eckberg@matcotools.com, 716-763-8525, Ext 2241
3.0 FACILITY DESCRIPTION
3.1 General Information
Matco Tools is located at 160 Chautauqua Avenue in Lakewood, New York. The facility, which has been operating since 1980, is a manufacturer of professional tool boxes for auto mechanics. The company is categorized as Standard Industrial Classification (SIC) Code 3499 (Fabricated Metal Products). Matco Tools employs approximately 100 people. There are two 10-hour shifts that operate from 4:00 am until 12:00 midnight, six days per week.
3.2 Process Information
Incoming steel (sheet and coiled) is sent to the shearing department, where the steel is cut to size. The sheared steel sheets are then sent to the case cell, where the drawers and tool box shells are formed by punching, stamping, and spot welding. The drawers and tool box shells are then placed on moving overhead hangers. The parts on the hangers are conveyed to an aqueous cleaning line, where the cleaning, zirconium coating, and sealing operations occur. This improves the powder coating performance and assists in corrosion protection of the steel substrate. The cleaning and degreasing begin with a first stage hot water rinse, followed by a second stage alkaline cleaner. The third and fourth stages consist of city water rinses. In the
Page 3 of 6
Matco Tools
Inspection Dates: March 18-19, 2021
fifth stage, a zirconium coating is applied. In the sixth stage, the parts are sprayed with a sealer solution. The seventh and final stage consists of a reverse osmosis water rinse.
The parts then pass through the dry-off oven. After cooling, the parts are conveyed to the powder coat booth, where the powder coating is applied. The parts then pass through the curing oven, which is maintained at 350oF. The heat causes the powder coating to fuse into a smooth finish. After cooling, the parts are removed from the hangers for assembly. Casters, locks, handles, and other accessories are attached to the tool boxes during the assembly process. The accessories are purchased from outside suppliers. The final product is inspected, packaged, and shipped to the distributor.
The water used in the aqueous cleaning line is provided by the Jamestown Municipal Authority. The water is treated in a reverse osmosis unit for the final stage rinse. The first stage hot water rinse and the second stage alkaline cleaner are collected and reused. The fifth stage zirconium coating and the sixth stage sealer solution are also collected and reused continually. Wastewaters from the third stage, fourth stage, and seventh stage rinses are collected in a tank, which overflows to a wastewater trench. The wastewater from the trench is discharged to the South and Central Chautauqua Lake Sewer District in Celeron, New York. The alkaline cleaning solution, zirconium coating, and sealer solution are replaced approximately once per year and are discharged to the South and Central Chautauqua Lake Sewer District. Average process wastewater flow is approximately 13,000 gallons per day.
3.3 Facility Self-Monitoring Information
Wastewater samples are collected twice per year at the wastewater trench by facility personnel. Samples are analyzed for the parameters listed in 40 CFR Section 433.15 and the local POTW parameters (oil and grease, iron, mercury, and pH). Grab samples of the final discharge are collected for four consecutive days. Samples are analyzed by Eurofins TestAmerica of Amherst, New York.
4.0 EPA SAMPLING/INSPECTION ACTIVITIES
4.1 Sampling Activities
An automatic composite sampler was set up at the effluent location to collect an aliquot of the effluent wastewater every 15 minutes for 24 hours. After 24 hours, the automatic composite sampler was disassembled and a 500-ml plastic jar was filled for the analysis of metals (cadmium, chromium, copper, lead, nickel, silver, zinc, iron, and mercury). A grab composite sample was also collected by filling one-fourth of the sample containers four times during the 24-hour survey. The grab composite sample was analyzed for TTO non-volatile organics and cyanide. Four grab samples for TTO volatile organics were also collected during the 24-hour survey. The four grab samples were composited in the EPA laboratory.
Page 4 of 6
Matco Tools
Inspection Dates: March 18-19, 2021
A fifth grab sample was also collected for oil and grease. Total residual chlorine and pH were analyzed in the field and recorded in the field notebook.
All sample containers, preservation techniques, and holding times were in accordance with U.S. EPA requirements specified in 40 CFR Part 136. All samples were placed in a cooler with wet ice and transported to the U.S. EPA Region 2 Laboratory in Edison, New Jersey.
Split samples were collected and given to the facility representative.
5.0 ANALYTICAL RESULTS
Parameter
Total Residual Chlorine (mg/l) pH (su)
Cadmium (mg/l) Chromium (mg/l)
Copper (mg/l) Lead (mg/l) Nickel (mg/l) Silver (mg/l) Zinc (mg/l) Iron (mg/l) Mercury (mg/l) Total Cyanide (mg/l) TTO (mg/l) Oil and Grease (mg/l)
Matco Tools Pretreatment CSI
March 18-19, 2021
Discharge to
Daily Maximum
POTW
Pretreatment Standards
for Existing Sources -
Metal Finishing Point
Source Category (40 CFR
Section 433.15)
0.00
--
8.44
5.0 minimum
Not detected
0.69
Not detected
2.77
0.0205
3.38
Not detected
0.69
Not detected
3.98
Not detected
0.43
Not detected
2.61
Not detected
--
Not detected
--
Not detected
1.20
Not detected
2.13
Not detected
--
Local Discharge Limit - Daily Maximum
-6.0 - 9.0
0.4 1.0 3.0 0.5 1.0 0.2 1.0 5.0 0.2 --100
6.0 FINDINGS
6.1 Sampling Result Findings
Based on the EPA analytical results for the samples that were collected on March 18-19, 2021, Matco Tools was in compliance with the effluent guidelines and pretreatment standards for existing sources in the Metal Finishing Point Source Category (40 CFR Part 433). The facility was also in compliance with the non-approved pretreatment limits established by the South and Central Chautauqua Lake Sewer District.
Page 5 of 6
Matco Tools
7.0 ATTACHMENTS
Photograph (#1) Laboratory Data Report Chain of Custody / Field Data Form
Inspection Dates: March 18-19, 2021
Photo #1: View of effluent sampling location.
Page 6 of 6
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
2890 Woodbridge Avenue Edison , New Jersey 08837
732-906-6886 Phone 732-906-6165 Fax
April 14, 2021
Philip Cocuzza Monitoring & Assessment Branch LSASD/MAB Edison, NJ 08837
RE: Matco Tools - 2103014 Enclosed are the results of analyses for samples received by the laboratory on 03/19/2021. The signature below reflects the laboratory's approval of the reported results. If you have any questions concerning this report, please refer to Project Number 2103014 and contact the laboratory. Sincerely,
James Ferretti Acting Chief, LSASD/LB
Project Narrative:
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014
The National Environmental Laboratory Accreditation Conference Institute (TNI) is a voluntary environmental laboratory accreditation association of State and Federal agencies. TNI established and promoted a National Environmental Laboratory Accreditation Program (NELAP) that provides a uniform set of standards for the generation of environmental data that are of known and defensible quality. The EPA Region 2 Laboratory is NELAP accredited. The Laboratory tests that are accredited have met all the requirements established under the TNI Standards.
Condition Comments
None
Comment(s):
The "Sample Analysis Date and Time" is included in the results section for any analyte with a prescribed holding time of 72 hours or less.
Data Qualifier(s):
U- The analyte was not detected at or above the Reporting Limit. J- The identification of the analyte is acceptable; the reported value is an estimate. K- The identification of the analyte is acceptable; the reported value may be biased high. L- The identification of the analyte is acceptable; the reported value may be biased low. NJ- There is presumptive evidence that the analyte is present; the analyte is reported as a tentative identification. The reported value is an estimate.
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 1 of 26
Reporting Limit(s):
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014
The Laboratory was able to achieve the standard laboratory reporting limits, where applicable, for each analyte requested except for the following analyte(s):
NVOA GCMS The reporting level of 5.00 ug/L was raised to 10 ug/L for the following analyte(s): Pentachlorophenol for the following samples: 2103014-01 The reporting level of 5.00 ug/L was raised to 30 ug/L for the following analyte(s): 2,4-Dinitrophenol, 4,6-Dinitro-2-Methylphenol for the following samples: 2103014-01
SUMMARY REPORT FOR SAMPLES
Field ID Effluent-Grab Composite Composite Effluent-Grab # 1-4 Trip Blank Effluent-Grab # 5 Effluent-24-Hr Composite
Laboratory ID 2103014-01 2103014-06 2103014-07 2103014-08 2103014-09
Matrix Aqueous Aqueous Aqueous Aqueous Aqueous
Date Sampled 03/19/2021 07:42 03/22/2021 00:01 03/18/2021 10:22 03/18/2021 11:06 03/19/2021 07:45
Date Received 03/19/2021 17:08 03/19/2021 17:08 03/19/2021 17:08 03/19/2021 17:08 03/19/2021 17:08
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 2 of 26
Analysis 624.1 VOA EPA-NPDES 625.1 SVOA NPDES Cyanide, Total Mercury Metals ICP TAL NPDES/DW Oil & Grease
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014
SUMMARY REPORT FOR METHODS
Method EPA 624.1 SOP C-89 Rev 3.6 EPA 625.1 SOP C-90 Rev 3.8 EPA 335.4 SOP C-28 Rev 2.7 EPA 245.1 SOP C-110 Rev 2.7 EPA 200.7 SOP C-109 Rev 3.6 EPA 1664A SOP C-126 Rev 1.6
Certification
NELAP NELAP NELAP NELAP NELAP NELAP
Matrix
Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 3 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014
Analyte
Field ID: Effluent-Grab Composite NVOA GCMS Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2103014-01
Date and Time of Analysis*
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
30.0
ug/L B103041
---
U
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U
30.0
ug/L B103041
---
U
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 4 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014
Analyte
Field ID: Effluent-Grab Composite NVOA GCMS 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene Sanitary Cyanide, Total
Field ID: Composite Effluent-Grab # 1-4 VOA GCMS Chloromethane
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2103014-01
Date and Time of Analysis*
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U L
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
10.0
ug/L B103041
---
U L
5.00
ug/L B103041
---
U
5.00
ug/L B103041
---
U
10.0
ug/L B103042
Sample ID: 2103014-06
---
U
5.00
ug/L B103040
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 5 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014
Analyte
Field ID: Composite Effluent-Grab # 1-4 VOA GCMS Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2103014-06
Date and Time of Analysis*
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 6 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014
Analyte
Result
Qualifier
Reporting Limit
Units
Batch
Date and Time of Analysis*
Field ID: Composite Effluent-Grab # 1-4 VOA GCMS 1,2-Dichlorobenzene
Field ID: Trip Blank VOA GCMS Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene
Sample ID: 2103014-06
---
U
5.00
ug/L B103040
Sample ID: 2103014-07
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 7 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014
Analyte
Field ID: Trip Blank VOA GCMS Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Field ID: Effluent-Grab # 5 GC - Sanitary Oil & Grease
Field ID: Effluent-24-Hr Composite Metals ICP Cadmium Chromium Copper Lead Nickel Silver Zinc Mercury CVAA Mercury
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2103014-07
Date and Time of Analysis*
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
---
U
5.00
ug/L B103040
Sample ID: 2103014-08
---
U
5.70
mg/L B104012
Sample ID: 2103014-09
---
U
3.00
ug/L B103052
---
U
5.00
ug/L B103052
20.5
10.0
ug/L B103052
---
U
8.00
ug/L B103052
---
U
20.0
ug/L B103052
---
U
5.00
ug/L B103052
---
U
20.0
ug/L B103052
---
U
0.050
ug/L B104002
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 8 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014
VOA GCMS - Quality Control
Analyte
Batch B103040
Blank (B103040-BLK1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
ND
ug/L
100.0
ND
ug/L
100.0
ND
ug/L
100.0
99.8
60-140
95.9
60-140
97.1
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 9 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 VOA GCMS - Quality Control
Analyte
Batch B103040
LCS (B103040-BS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
78.6
ug/L
50.00
157
19-205
77.0
ug/L
50.00
154
5-195
70.7
ug/L
50.00
141
15-185
61.2
ug/L
50.00
122
40-160
61.0
ug/L
50.00
122
50-150
61.3
ug/L
50.00
123
50-150
53.3
ug/L
50.00
107
60-140
54.9
ug/L
50.00
110
70-129
56.8
ug/L
50.00
114
70-130
54.9
ug/L
50.00
110
70-130
53.3
ug/L
50.00
107
70-135
53.3
ug/L
50.00
107
70-130
54.2
ug/L
50.00
108
70-130
50.4
ug/L
50.00
101
70-130
50.0
ug/L
50.00
99.9
65-135
53.4
ug/L
50.00
107
65-135
51.9
ug/L
50.00
104
35-165
48.6
ug/L
50.00
97.2
65-135
46.9
ug/L
50.00
93.8
25-175
50.9
ug/L
50.00
102
70-130
52.1
ug/L
50.00
104
50-150
52.3
ug/L
50.00
105
70-130
54.2
ug/L
50.00
108
70-130
52.0
ug/L
50.00
104
70-135
54.7
ug/L
50.00
109
65-135
52.3
ug/L
50.00
105
60-140
49.9
ug/L
50.00
99.7
70-130
48.8
ug/L
50.00
97.7
60-140
53.8
ug/L
50.00
108
70-130
54.3
ug/L
50.00
109
65-135
53.8
ug/L
50.00
108
65-135
99.7
ug/L
100.0
99.7
60-140
97.8
ug/L
100.0
97.8
60-140
94.1
ug/L
100.0
94.1
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 10 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 VOA GCMS - Quality Control
Analyte
Batch B103040
LCS Dup (B103040-BSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
85.0
ug/L
50.00
170
19-205
7.77
20
81.9
ug/L
50.00
164
5-195
6.22
20
75.7
ug/L
50.00
151
15-185
6.86
20
66.6
ug/L
50.00
133
40-160
8.58
20
67.0
ug/L
50.00
134
50-150
9.27
20
66.3
ug/L
50.00
133
50-150
7.79
20
56.2
ug/L
50.00
112
60-140
5.22
20
55.7
ug/L
50.00
111
70-129
1.45
20
61.7
ug/L
50.00
123
70-130
8.17
20
58.7
ug/L
50.00
117
70-130
6.78
20
56.3
ug/L
50.00
113
70-135
5.46
20
56.8
ug/L
50.00
114
70-130
6.40
20
58.1
ug/L
50.00
116
70-130
6.91
20
52.7
ug/L
50.00
105
70-130
4.46
20
51.8
ug/L
50.00
104
65-135
3.73
20
55.8
ug/L
50.00
112
65-135
4.29
20
54.1
ug/L
50.00
108
35-165
4.22
20
50.2
ug/L
50.00
100
65-135
3.22
20
48.5
ug/L
50.00
97.0
25-175
3.29
20
52.7
ug/L
50.00
105
70-130
3.59
20
53.7
ug/L
50.00
107
50-150
3.10
20
53.7
ug/L
50.00
107
70-130
2.64
20
56.0
ug/L
50.00
112
70-130
3.28
20
54.0
ug/L
50.00
108
70-135
3.90
20
56.6
ug/L
50.00
113
65-135
3.45
20
54.5
ug/L
50.00
109
60-140
4.03
20
51.3
ug/L
50.00
103
70-130
2.87
20
51.1
ug/L
50.00
102
60-140
4.54
20
55.2
ug/L
50.00
110
70-130
2.48
20
56.5
ug/L
50.00
113
65-135
4.03
20
56.1
ug/L
50.00
112
65-135
4.31
20
99.0
ug/L
100.0
99.0
60-140
98.7
ug/L
100.0
98.7
60-140
95.1
ug/L
100.0
95.1
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 11 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 VOA GCMS - Quality Control
Analyte
Batch B103040
Matrix Spike (B103040-MS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2103014-06
45.7
ug/L
48.5
ug/L
46.5
ug/L
46.7
ug/L
49.2
ug/L
51.5
ug/L
50.7
ug/L
49.5
ug/L
52.1
ug/L
50.3
ug/L
49.9
ug/L
50.0
ug/L
51.2
ug/L
48.1
ug/L
49.2
ug/L
49.8
ug/L
48.8
ug/L
48.2
ug/L
50.1
ug/L
49.1
ug/L
49.7
ug/L
49.8
ug/L
49.7
ug/L
49.5
ug/L
50.4
ug/L
50.8
ug/L
50.2
ug/L
50.2
ug/L
52.3
ug/L
51.2
ug/L
51.7
ug/L
99.0
ug/L
99.4
ug/L
99.7
ug/L
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
50.00
0.00
100.0 100.0 100.0
91.3
19-273
96.9
49-251
93.0
21-242
93.4
14-230
98.3
50-150
103
52-234
101
69-221
98.9
40-160
104
54-156
101
59-155
99.7
51-138
100
52-162
102
70-140
96.3
49-155
98.4
37-151
99.5
70-157
97.7
74-210
96.4
35-155
100
80-227
98.2
47-150
99.5
17-183
99.6
52-150
99.3
64-148
99.0
53-149
101
37-160
102
37-162
100
45-169
100
46-157
105
59-156
102
18-190
103
18-190
99.0
60-140
99.4
60-140
99.7
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 12 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 VOA GCMS - Quality Control
Analyte
Batch B103040
Matrix Spike Dup (B103040-MSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2103014-06
47.8
ug/L
50.00
0.00
95.5
19-273
4.47
28
47.5
ug/L
50.00
0.00
95.0
49-251
2.02
28
49.3
ug/L
50.00
0.00
98.6
21-242
5.82
28
49.3
ug/L
50.00
0.00
98.6
14-230
5.48
28
47.0
ug/L
50.00
0.00
94.0
50-150
4.53
28
51.2
ug/L
50.00
0.00
102
52-234
0.545
28
52.5
ug/L
50.00
0.00
105
69-221
3.53
28
51.5
ug/L
50.00
0.00
103
40-160
4.06
28
53.4
ug/L
50.00
0.00
107
54-156
2.52
28
53.0
ug/L
50.00
0.00
106
59-155
5.19
28
52.6
ug/L
50.00
0.00
105
51-138
5.44
28
50.8
ug/L
50.00
0.00
102
52-162
1.43
28
50.5
ug/L
50.00
0.00
101
70-140
1.42
28
50.2
ug/L
50.00
0.00
100
49-155
4.17
28
50.1
ug/L
50.00
0.00
100
37-151
1.73
28
49.2
ug/L
50.00
0.00
98.4
70-157
1.15
28
49.5
ug/L
50.00
0.00
99.0
74-210
1.34
28
49.2
ug/L
50.00
0.00
98.4
35-155
2.09
28
51.7
ug/L
50.00
0.00
103
80-227
3.18
28
50.1
ug/L
50.00
0.00
100
47-150
1.96
28
51.2
ug/L
50.00
0.00
102
17-183
2.93
28
51.2
ug/L
50.00
0.00
102
52-150
2.79
28
48.4
ug/L
50.00
0.00
96.7
64-148
2.67
28
52.2
ug/L
50.00
0.00
104
53-149
5.39
28
51.6
ug/L
50.00
0.00
103
37-160
2.34
28
51.6
ug/L
50.00
0.00
103
37-162
1.52
28
52.0
ug/L
50.00
0.00
104
45-169
3.58
28
51.6
ug/L
50.00
0.00
103
46-157
2.77
28
53.6
ug/L
50.00
0.00
107
59-156
2.62
28
53.5
ug/L
50.00
0.00
107
18-190
4.41
28
53.2
ug/L
50.00
0.00
106
18-190
2.74
28
99.3
ug/L
100.0
99.3
60-140
98.6
ug/L
100.0
98.6
60-140
98.9
ug/L
100.0
98.9
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 13 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B103041
Blank (B103041-BLK1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
RPD Limit
Page 14 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 NVOA GCMS - Quality Control
Analyte
Batch B103041
Blank (B103041-BLK1) Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
LCS (B103041-BS1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
40.1
ug/L
50.00
ND
ug/L
50.00
38.8
ug/L
50.00
37.0
ug/L
50.00
37.7
ug/L
50.00
50.3
ug/L
50.00
51.5
ug/L
50.00
48.7
5.00 ug/L
50.00
49.0
5.00 ug/L
50.00
50.8
5.00 ug/L
50.00
50.9
5.00 ug/L
50.00
48.1
5.00 ug/L
50.00
51.9
5.00 ug/L
50.00
53.2
5.00 ug/L
50.00
51.9
5.00 ug/L
50.00
80.1
60-140
31.6
60-140
77.7
60-140
74.1
60-140
75.4
60-140
101
60-140
103
60-140
97.3
47-145
98.0
33-145
102
27-133
102
33-143
96.2
17-163
104
24-159
106
35-219
104
11-162
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 15 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B103041
LCS (B103041-BS1) Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene
52.8
5.00 ug/L
50.00
51.2
5.00 ug/L
50.00
50.5
5.00 ug/L
50.00
41.6
5.00 ug/L
50.00
52.5
5.00 ug/L
50.00
41.8
5.00 ug/L
50.00
49.9
5.00 ug/L
50.00
39.3
5.00 ug/L
50.00
52.8
5.00 ug/L
50.00
49.1
5.00 ug/L
50.00
47.6
5.00 ug/L
50.00
48.4
5.00 ug/L
50.00
59.2
5.00 ug/L
50.00
50.7
5.00 ug/L
50.00
47.1
5.00 ug/L
50.00
44.3
5.00 ug/L
50.00
48.5
5.00 ug/L
50.00
58.6
5.00 ug/L
50.00
47.1
5.00 ug/L
50.00
44.7
5.00 ug/L
50.00
53.5
5.00 ug/L
50.00
42.5
5.00 ug/L
50.00
31.2
5.00 ug/L
50.00
44.9
5.00 ug/L
50.00
43.8
5.00 ug/L
50.00
39.2
5.00 ug/L
50.00
53.8
5.00 ug/L
50.00
43.1
5.00 ug/L
50.00
40.7
5.00 ug/L
50.00
39.2
5.00 ug/L
50.00
33.1
5.00 ug/L
50.00
50.8
5.00 ug/L
50.00
50.9
5.00 ug/L
50.00
46.6
5.00 ug/L
50.00
35.3
5.00 ug/L
50.00
106
17-168
102
33-227
101
26-137
83.3
59-121
105
39-171
83.7
21-133
99.8
54-120
78.7
44-142
106
37-144
98.2
39-135
95.1
32-120
96.7
39-139
118
50-158
101
21-191
94.2
60-120
88.6
23-134
97.0
29-182
117
38-262
94.2
17-181
89.4
53-127
107
22-147
84.9
25-158
62.3
9-132
89.9
33-184
87.6
12-158
78.5
36-166
108
8-158
86.2
38-152
81.4
60-115
78.4
31-114
66.2
28-120
102
1-120
102
4-146
93.3
35-152
70.5
24-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
RPD Limit
Page 16 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 NVOA GCMS - Quality Control
Analyte
Batch B103041
LCS (B103041-BS1) Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
LCS Dup (B103041-BSD1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
43.2
5.00 ug/L
50.00
34.2
5.00 ug/L
50.00
49.0
5.00 ug/L
50.00
46.2
5.00 ug/L
50.00
28.3
5.00 ug/L
50.00
43.6
5.00 ug/L
50.00
52.6
5.00 ug/L
50.00
55.8
5.00 ug/L
50.00
20.7
5.00 ug/L
50.00
48.9
5.00 ug/L
50.00
40.3
ug/L
50.00
19.0
ug/L
50.00
38.1
ug/L
50.00
35.3
ug/L
50.00
51.6
ug/L
50.00
45.2
ug/L
50.00
49.7
ug/L
50.00
50.0
5.00 ug/L
50.00
50.1
5.00 ug/L
50.00
51.7
5.00 ug/L
50.00
53.3
5.00 ug/L
50.00
49.3
5.00 ug/L
50.00
53.5
5.00 ug/L
50.00
54.9
5.00 ug/L
50.00
53.4
5.00 ug/L
50.00
54.9
5.00 ug/L
50.00
53.9
5.00 ug/L
50.00
50.4
5.00 ug/L
50.00
43.5
5.00 ug/L
50.00
53.9
5.00 ug/L
50.00
39.1
5.00 ug/L
50.00
50.8
5.00 ug/L
50.00
37.0
5.00 ug/L
50.00
86.3
15-76
68.4
40-120
98.1
21-196
92.3
35-180
56.6
17-127
87.3
43-230
105
79-139
112
14-176
41.4
5-120
97.8
52-120
80.5
60-140
38.0
60-140
76.2
60-140
70.7
60-140
103
60-140
90.3
60-140
99.4
60-140
100
47-145
2.80
30
100
33-145
2.12
30
103
27-133
1.66
30
107
33-143
4.72
30
98.7
17-163
2.50
30
107
24-159
2.90
30
110
35-219
3.09
30
107
11-162
2.85
30
110
17-168
3.88
30
108
33-227
5.06
30
101
26-137
0.258
30
87.0
59-121
4.35
30
108
39-171
2.71
30
78.3
21-133
6.69
30
102
54-120
1.67
30
73.9
44-142
6.21
30
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 17 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike Level
Source Result
%REC
%REC Limits
Batch B103041
LCS Dup (B103041-BSD1) 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol
52.4
5.00 ug/L
50.00
46.6
5.00 ug/L
50.00
42.6
5.00 ug/L
50.00
48.9
5.00 ug/L
50.00
59.3
5.00 ug/L
50.00
45.0
5.00 ug/L
50.00
47.5
5.00 ug/L
50.00
39.6
5.00 ug/L
50.00
44.8
5.00 ug/L
50.00
61.6
5.00 ug/L
50.00
44.1
5.00 ug/L
50.00
46.8
5.00 ug/L
50.00
52.6
5.00 ug/L
50.00
43.1
5.00 ug/L
50.00
29.4
5.00 ug/L
50.00
44.4
5.00 ug/L
50.00
41.4
5.00 ug/L
50.00
37.7
5.00 ug/L
50.00
54.8
5.00 ug/L
50.00
43.6
5.00 ug/L
50.00
42.5
5.00 ug/L
50.00
40.8
5.00 ug/L
50.00
34.0
5.00 ug/L
50.00
51.5
5.00 ug/L
50.00
52.6
5.00 ug/L
50.00
47.5
5.00 ug/L
50.00
33.6
5.00 ug/L
50.00
39.8
5.00 ug/L
50.00
32.1
5.00 ug/L
50.00
49.6
5.00 ug/L
50.00
43.1
5.00 ug/L
50.00
24.8
5.00 ug/L
50.00
43.6
5.00 ug/L
50.00
53.8
5.00 ug/L
50.00
54.3
5.00 ug/L
50.00
105
37-144
93.1
39-135
85.1
32-120
97.8
39-139
119
50-158
89.9
21-191
95.0
60-120
79.3
23-134
89.5
29-182
123
38-262
88.2
17-181
93.5
53-127
105
22-147
86.2
25-158
58.7
9-132
88.7
33-184
82.8
12-158
75.3
36-166
110
8-158
87.2
38-152
85.0
60-115
81.7
31-114
68.0
28-120
103
1-120
105
4-146
95.0
35-152
67.3
24-120
79.6
15-76
64.2
40-120
99.2
21-196
86.2
35-180
49.5
17-127
87.2
43-230
108
79-139
109
14-176
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
RPD
0.779 5.25 11.1 1.09 0.321 12.0 0.930 11.1 8.04 4.94 6.58 4.44 1.68 1.47 5.91 1.30 5.61 4.11 1.82 1.11 4.23 4.02 2.71 1.35 3.36 1.81 4.70 8.05 6.25 1.18 6.81 13.3 0.0459 2.33 2.82
RPD Limit
30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30
Page 18 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 NVOA GCMS - Quality Control
Analyte
Batch B103041
LCS Dup (B103041-BSD1) Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
Matrix Spike (B103041-MS1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
17.9
5.00 ug/L
50.00
48.1
5.00 ug/L
50.00
38.3
ug/L
50.00
16.4
ug/L
50.00
38.0
ug/L
50.00
35.6
ug/L
50.00
51.3
ug/L
50.00
46.3
ug/L
50.00
51.6
ug/L
50.00
35.8
5-120
14.5
30
96.3
52-120
1.57
30
76.5
60-140
32.8
60-140
75.9
60-140
71.1
60-140
103
60-140
92.7
60-140
103
60-140
Source: 2103014-01
45.0
5.21 ug/L
44.8
5.21 ug/L
54.5
5.21 ug/L
52.9
5.21 ug/L
51.2
5.21 ug/L
52.0
5.21 ug/L
43.0
5.21 ug/L
54.1
5.21 ug/L
52.9
5.21 ug/L
43.3
5.21 ug/L
58.2
5.21 ug/L
60.0
5.21 ug/L
45.6
5.21 ug/L
44.1
5.21 ug/L
56.4
5.21 ug/L
46.7
5.21 ug/L
46.1
5.21 ug/L
45.1
5.21 ug/L
43.7
5.21 ug/L
60.1
5.21 ug/L
44.1
5.21 ug/L
79.6
5.21 ug/L
48.2
5.21 ug/L
40.1
5.21 ug/L
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
86.4
47-145
86.1
33-145
105
27-133
102
33-143
98.3
17-163
99.9
24-159
82.6
35-219
104
11-162
102
17-168
83.2
33-227
112
26-137
115
59-121
87.5
39-171
84.7
21-133
108
54-120
89.7
44-142
88.6
37-144
86.5
39-135
83.9
32-120
115
39-139
84.7
50-158
153
21-191
92.5
60-120
77.0
23-134
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 19 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B103041
Matrix Spike (B103041-MS1) 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10
Source: 2103014-01
45.8
5.21 ug/L
2.54
5.21 ug/L
66.8
5.21 ug/L
59.6
5.21 ug/L
38.5
5.21 ug/L
62.6
5.21 ug/L
20.6
5.21 ug/L
44.0
5.21 ug/L
40.9
5.21 ug/L
37.4
5.21 ug/L
48.6
5.21 ug/L
48.8
5.21 ug/L
53.8
5.21 ug/L
58.5
5.21 ug/L
42.8
5.21 ug/L
52.7
5.21 ug/L
46.5
5.21 ug/L
60.0
5.21 ug/L
45.3
5.21 ug/L
43.3
5.21 ug/L
41.6
5.21 ug/L
45.5
5.21 ug/L
44.1
5.21 ug/L
21.1
5.21 ug/L
43.1
5.21 ug/L
59.5
5.21 ug/L
76.3
5.21 ug/L
18.7
5.21 ug/L
58.3
5.21 ug/L
26.6
ug/L
17.0
ug/L
42.3
ug/L
42.3
ug/L
42.1
ug/L
49.6
ug/L
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08
ND
52.08 52.08 52.08 52.08 52.08 52.08
87.9
29-182
4.88
38-262
128
17-181
115
53-127
73.9
22-147
120
25-158
39.5
9-132
84.4
33-184
78.6
12-158
71.9
36-166
93.3
8-158
93.8
38-152
103
61-106
112
31-114
82.1
28-120
101
1-120
89.3
4-146
115
35-152
87.0
24-120
83.2
15-76
79.9
40-120
87.3
21-196
84.6
35-180
40.4
17-127
82.7
43-230
114
79-139
146
14-176
35.9
5-120
112
52-120
51.0
60-140
32.6
60-140
81.3
60-140
81.2
60-140
80.8
60-140
95.2
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
RPD Limit
Page 20 of 26
Analyte
Batch B103041 Matrix Spike (B103041-MS1)
Surrogate: Chrysene-D12
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 NVOA GCMS - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2103014-01
50.3
ug/L
52.08
96.7
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 21 of 26
Analyte
Batch B104012 Blank (B104012-BLK1)
Oil & Grease
LCS (B104012-BS1) Oil & Grease
LCS Dup (B104012-BSD1) Oil & Grease
Matrix Spike (B104012-MS1) Oil & Grease
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 GC - Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 mg/L
34.3
5.00 mg/L
40.00
86
78-114
34.8
5.00 mg/L
40.00
87
78-114
1
20
Source: 2103014-08
51.0
5.00 mg/L
49.38
4.90
93
78-114
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 22 of 26
Analyte
Batch B103052
Blank (B103052-BLK1) Cadmium Chromium Copper Lead Nickel Silver Zinc
LCS (B103052-BS1) Cadmium Chromium Copper Lead Nickel Silver Zinc
LCS Dup (B103052-BSD1) Cadmium Chromium Copper Lead Nickel Silver Zinc
Matrix Spike (B103052-MS1) Cadmium Chromium Copper Lead Nickel Silver Zinc
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 Metals ICP - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
3.00 ug/L
--- U
5.00 ug/L
--- U
10.0 ug/L
--- U
8.00 ug/L
--- U
20.0 ug/L
--- U
5.00 ug/L
--- U
20.0 ug/L
204
3.00 ug/L
200.0
205
5.00 ug/L
200.0
202
10.0 ug/L
200.0
205
8.00 ug/L
200.0
205
20.0 ug/L
200.0
203
5.00 ug/L
200.0
200
20.0 ug/L
200.0
102
85-115
103
85-115
101
85-115
103
85-115
102
85-115
102
85-115
100
85-115
203
3.00 ug/L
200.0
204
5.00 ug/L
200.0
201
10.0 ug/L
200.0
203
8.00 ug/L
200.0
204
20.0 ug/L
200.0
203
5.00 ug/L
200.0
198
20.0 ug/L
200.0
102
85-115
0.398
20
102
85-115
0.611
20
101
85-115
0.357
20
101
85-115
1.22
20
102
85-115
0.515
20
101
85-115
0.394
20
99.1
85-115
1.03
20
Source: 2103014-09
201
3.00 ug/L
205
5.00 ug/L
233
10.0 ug/L
199
8.00 ug/L
212
20.0 ug/L
207
5.00 ug/L
209
20.0 ug/L
200.0
ND
200.0
ND
200.0
20.5
200.0
ND
200.0
10.6
200.0
1.53
200.0
10.4
100
80-120
102
80-120
106
80-120
99.5
80-120
101
80-120
103
80-120
99.5
80-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 23 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 Metals ICP - Quality Control
Analyte
Batch B103052
Matrix Spike Dup (B103052-MSD1) Cadmium Chromium Copper Lead Nickel Silver Zinc
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2103014-09
208
15.0 ug/L
200.0
ND
104
80-120
3.84
10
210
25.0 ug/L
200.0
ND
105
80-120
2.60
10
230
50.0 ug/L
200.0
20.5
105
80-120
1.33
10
203
40.0 ug/L
200.0
ND
102
80-120
2.08
10
218
100 ug/L
200.0
10.6
104
80-120
2.47
10
210
25.0 ug/L
200.0
1.53
104
80-120
1.35
10
215
100 ug/L
200.0
10.4
102
80-120
2.57
10
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 24 of 26
Analyte
Batch B104002 Blank (B104002-BLK1)
Mercury
Blank (B104002-BLK2) Mercury
LCS (B104002-BS1) Mercury
LCS (B104002-BS2) Mercury
LCS Dup (B104002-BSD1) Mercury
LCS Dup (B104002-BSD2) Mercury
Matrix Spike (B104002-MS3) Mercury
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 Mercury CVAA - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
0.050 ug/L
--- U
0.050 ug/L
0.957
0.050 ug/L
1.000
95.7
85-115
0.990
0.050 ug/L
1.000
99.0
85-115
0.961
0.050 ug/L
1.000
96.1
85-115
0.417
20
0.967
0.050 ug/L
1.000
96.7
85-115
2.35
20
Source: 2103014-09
1.03
0.050 ug/L
1.000
ND
103
80-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 25 of 26
Analyte
Batch B103042 Blank (B103042-BLK1)
Cyanide, Total
Blank (B103042-BLK2) Cyanide, Total
LCS (B103042-BS1) Cyanide, Total
LCS Dup (B103042-BSD1) Cyanide, Total
Matrix Spike (B103042-MS1) Cyanide, Total
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Matco Tools - 2103014
Project Number: 2103014 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
10.0 ug/L
--- U
10.0 ug/L
315
10.0 ug/L
340.0
93
90-110
317
10.0 ug/L
340.0
93
90-110
0.6
20
Source: 2103014-01
537
10.0 ug/L
500.0
ND
107
90-110
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 4/14/2021
Page 26 of 26
