Document jK7pymEwd9ELpydNYyXdax9Z

UKAS ISO/IEC 17025 Accredited Testing Laboratory No. 4279 Element Materials Technology Environmental UK Limited trading as Element and Element Ireland Unit C5, Emery Court, The Embankment Business Park, Stockport, SK4 3GL Element, Unit C6, Emery Court, The Embankment Business Park, Heaton Mersey, Stockport, SK4 3GL Your Element Contact: E Site Specific Protocol (SSP) Commissioned by AGC Chemicals Europe Ltd Installation Name & Address AGC Chemicals Europe Ltd PO Box 4 York House Hillhouse International Thornton Cleveleys FY5 4QD A4 L168 Lubricant Oven EPR Permit: EPR/BU5453IY/V004 Dates of the Proposed Monitoring Campaign 9th - 12th May 2023 SSP Reference Number EMT-SSP-05959 Release Point References A5 ARK Inlet A5 ARK Outlet Report Written by Report Date & Version 2nd May 2023, Version 1 Report Approved by Signature of Report Approver (Element) Name of Client I confirm that I have read and understood the sampling protocol contained in this report, that the sampling location complies with the requirements of all relevant legislation, and I am happy for the sampling to proceed. Date of Client Approval Signature of Client (for SSP Approval) EL-LS-OP-SE-X-EWB 002 UK SSP (Version BF) EMT-SSP-05959 - AGC Chemicals Europe Ltd (May 2023) SSP Part 1 CONTACT DETAILS, MONITORING DATES & PERSONNEL This SSP (Site Specific Protocol) will be updated, if required to include feedback from each visit. Operator Contact Details Operator Name Site Location Full Installation Address AGC Chemicals Europe Ltd Lancashire PO Box 4 York House Hillhouse International Thornton Cleveleys FY5 4QD EPR Permit Contact Name Telephone Number Fax Number Mobile Phone Number Email Address Monitoring Dates Dates of Previous Campaign Job No. of Previous Campaign Planned Dates of Campaign EPR/BU5453IY/V004 Primary Site Contact - 9th March 2023 EMT05518 9th - 12th May 2023 Analysis Laboratories (with short name reference as referenced in Part 2 of the SSP) Element Stockport (EET) Element Deeside (ELD) i2 Analytical Ltd ISO17025 Accreditation Number: 4279 ISO17025 Accreditation Number: 4225 ISO17025 Accreditation Number: Alternative Site Contact - (If the Planned Dates of the Campaign change at late notice, the SSP will not be re-issued. The final test report will detail the actual monitoring dates.) Stack Emissions Monitoring Personnel where SCM = Site Campaign Manager Position Name SCM Team Leader Technician MCERTS Accreditation MCERTS Number & Expiry Date Technical Endorsements Element Site Campaign Manager Contact Details Name Mobile Phone Number Email Address Further Notes on Stack Emissions Monitoring Personnel There may be, in exceptional circumstances, a need to change the personnel who will be performing the monitoring. If this was to occur, the sampling team sent to site will hold all the necessary MCERTS Technical Endorsements for the required tests. As this scenario would most likely happen at late notice, the SSP will not be re-issued. The names of the monitoring personnel will be available to the client on the day of sampling (or before if required for inductions / site security / permits to work). The names of the monitoring personnel along with their personal MCERTS accreditation details will also be detailed in the final test report. AGC Chemicals Europe Ltd Lancashire EL-LS-OP-SE-X-EWB 002 UK SSP (Version BF) 2 of 9 SSP Reference: EMT-SSP-05959, Version 1 EPR Permit: EPR/BU5453IY/V004 SSP Part 2 DETAILS OF MONITORING: STACK AND LOCATION DETAILS Release Point Reference A4 L168 Lubricant Oven Sampling Location and Stack Photos Operating & Process Information Type of Process Batch or Continuous Process Feedstock / Fuel Type Load / Throughput / Continuous Rating of Plant Expected Velocity, Temperature & Moisture Details of Abatement System Details of any CEMS Installed (including DCS) Process Details Required Reference Conditions 1 Reference Conditions 2 Sampling Location Details Stack Type / Shape Diameter / Dimensions (m) Access Platform Type and Location Orientation of Duct Sample Port Size / Diameter Sample Port Depth (cm) Sample Ports Correctly Located? Number of Sampling Lines Available Number of Sampling Lines to be Used Number of Sample Points to be Used (per line) Total Number of Sample Points to be Used EN 15259 / Homogeneity Representative Point/s Details Oven Continuous Process Oven Normal Load 14.6 m/s | 107 C | 0.1 % v/v N/A N/A Operating conditions to be Provided by Site Contact 273K, 101.3kPa, without correction for water vapour content. N/A Value Circular 0.25 On Ground On Ground Horizontal Hole 0 Yes 1 1 1 1 - Outside - no shelter N/A Details Availability of Utilities Power 240V Lighting Yes Water Yes EA Technical Guidance Note M1 / EN 15259 Platform Requirements Value Sufficient working area to manipulate probe and operate the measuring instruments Yes Platform has 2 levels of handrails (approx. 0.5m & 1.0m high) Yes Platform has vertical base boards (approx. 0.25m high) Yes Platform has chains / self closing gates at top of ladders Yes There are no obstructions present which hamper insertion of sampling equipment Yes Safe Access Available Yes Easy Access Available Yes Sampling Platform / Improvement Recommendations: The sampling location meets all the requirements specified in EA Guidance Note M1 and EN 15259, and therefore there are no improvement recommendations. Sampling Plane Validation Criteria Requirement Lowest Differential Pressure (Pa) Ratio of Gas Velocities (:1) Maximum Angle of Swirl () No Local Negative Flow Value 140 1.0 0 Yes Compliant Yes Yes Yes Yes AGC Chemicals Europe Ltd Lancashire EL-LS-OP-SE-X-EWB 002 UK SSP (Version BF) 3 of 9 SSP Reference: EMT-SSP-05959, Version 1 EPR Permit: EPR/BU5453IY/V004 SSP Part 2 DETAILS OF MONITORING: SAMPLING METHOD INFORMATION Release Point Reference A4 L168 Lubricant Oven In the "Units" column, = Reference Conditions 1, = Reference Conditions 2 (continued) Determi na nd Hydrogen Fluoride PFOA Water Vapour Vel oc i ty Number of Runs | Blanks Uni ts Emi s s i on Limit Expected Emi s s i on PERIODIC SAMPLING: MANUAL METHODS Projected Standard Element Absorption Media / LOD Reference Technical Analysis Technique Method Procedure Ana l ys i s Lab | ISO17025 Status Sa mpl e Duration (mi ns ) Sa mpl e Fl owra te (ACTUAL) (l /mi n) Sa mpl e Vol ume (REF) (m) Projected Status MU of (%) Testing 10 1 mg/m N/A 10 1 mg/m N/A 10 0 % v/v N/A 1 0 m/s N/A 59.0 0.045 CEN/TS 17340 CAT-TP-10 NaOH / IC EET MCERTS 60 - 0.045 EN 1911 CAT-TP-11 C3H8O EET MCERTS 60 0.10 0.10 EN 14790 CAT-TP-05 Gravimetric EET MCERTS 60 14.6 3.0 EN ISO 16911-1 CAT-TP-41 Pressure & Temp EET MCERTS N/A 10 0.550 15% MCERTS 10 0.550 15% MCERTS 10 N/A 5% MCERTS N/A N/A 10% MCERTS Velocity Profile - Source: Previous Testing Campaign P Pt Pa 1 139.5 Line A Temp C 107.2 Velocity m/s 14.65 Monitoring Objectives / Unusual Occurrences / Comments / Health & Safety / Expected Deviations from Standard Reference Methods 1 Perform testing, as requested by the customer, for a number of prescribed pollutants. There are no emission limits set for any of the pollutants at this time AGC Chemicals Europe Ltd Lancashire EL-LS-OP-SE-X-EWB 002 UK SSP (Version BF) 4 of 9 SSP Reference: EMT-SSP-05959, Version 1 EPR Permit: EPR/BU5453IY/V004 SSP Part 2 DETAILS OF MONITORING: STACK AND LOCATION DETAILS Release Point Reference A5 ARK Inlet Sampling Location and Stack Photos Operating & Process Information Type of Process Batch or Continuous Process Feedstock / Fuel Type Load / Throughput / Continuous Rating of Plant Expected Velocity, Temperature & Moisture Details of Abatement System Details of any CEMS Installed (including DCS) Process Details Required Reference Conditions 1 Reference Conditions 2 Sampling Location Details Stack Type / Shape Diameter / Dimensions (m) Access Platform Type and Location Orientation of Duct Sample Port Size / Diameter Sample Port Depth (cm) Sample Ports Correctly Located? Number of Sampling Lines Available Number of Sampling Lines to be Used Number of Sample Points to be Used (per line) Total Number of Sample Points to be Used EN 15259 / Homogeneity Representative Point/s Details Pre-Scrubber Batch PTFE Parts TBC on day of testing 5.3 m/s | 68.7 C | 0.8 % v/v ARK Plant None Operating conditions to be Provided by Site Contact 273K, 101.3kPa, without correction for water vapour content. N/A Value Circular 0.79 Stairs On Roof Horizontal 5" Flange 10 Yes 1 1 1 1 - Details Outside - shelter in the adjacent building N/A Availability of Utilities Power 110V Lighting No Water No EA Technical Guidance Note M1 / EN 15259 Platform Requirements Value Sufficient working area to manipulate probe and operate the measuring instruments Yes Platform has 2 levels of handrails (approx. 0.5m & 1.0m high) Yes Platform has vertical base boards (approx. 0.25m high) Yes Platform has chains / self closing gates at top of ladders N/A There are no obstructions present which hamper insertion of sampling equipment Yes Safe Access Available Yes Easy Access Available Yes Sampling Platform / Improvement Recommendations: The sampling location meets all the requirements specified in EA Guidance Note M1 and EN 15259, and therefore there are no improvement recommendations. Sampling Plane Validation Criteria Requirement Lowest Differential Pressure (Pa) Ratio of Gas Velocities (:1) Maximum Angle of Swirl () No Local Negative Flow Value 13 1.4 7 Yes Compliant Yes Yes Yes Yes AGC Chemicals Europe Ltd Lancashire EL-LS-OP-SE-X-EWB 002 UK SSP (Version BF) 5 of 9 SSP Reference: EMT-SSP-05959, Version 1 EPR Permit: EPR/BU5453IY/V004 Determi na nd SAA 1000 PFOA Water Vapour Vel oc i ty SSP Part 2 DETAILS OF MONITORING: SAMPLING METHOD INFORMATION Release Point Reference A5 ARK Inlet In the "Units" column, = Reference Conditions 1, = Reference Conditions 2 (continued) Number of Runs | Blanks Uni ts Emi s s i on Limit Expected Emi s s i on PERIODIC SAMPLING: MANUAL METHODS Projected Standard Element Absorption Media / LOD Reference Technical Analysis Technique Method Procedure Ana l ys i s Lab | ISO17025 Status Sa mpl e Duration (mi ns ) Sa mpl e Fl owra te (ACTUAL) (l /mi n) Sa mpl e Vol ume (REF) (m) Projected Status MU of (%) Testing 2 1 mg/m N/A 2 1 mg/m N/A 4 0 % v/v N/A 2 0 m/s N/A 41.0 0.006 EN 1911 CAT-TP-11 10% DMSO EET MCERTS 240 0.10 0.006 EN 1911 CAT-TP-11 50% Methanol EET MCERTS 240 1.0 0.10 EN 14790 CAT-TP-05 Gravimetric EET MCERTS 240 2.8 3.0 EN ISO 16911-1 CAT-TP-41 Pressure & Temp EET MCERTS 5 10 2.216 15% MCERTS 10 2.216 15% MCERTS 10 N/A 5% MCERTS N/A N/A 10% MCERTS Velocity Profile - Source: Previous Testing Campaign Line A P Temp Velocity Pt Pa C m/s 1 16.8 68.6 4.86 2 13.4 68.7 4.35 3 25.4 68.7 5.98 4 24.6 68.7 5.89 Monitoring Objectives / Unusual Occurrences / Comments / Health & Safety / Expected Deviations from Standard Reference Methods 1 Perform testing of an investigative nature under trial operation 2 A5 ARK Inlet and Outlet to be tested similtaneously AGC Chemicals Europe Ltd Lancashire EL-LS-OP-SE-X-EWB 002 UK SSP (Version BF) 6 of 9 SSP Reference: EMT-SSP-05959, Version 1 EPR Permit: EPR/BU5453IY/V004 SSP Part 2 DETAILS OF MONITORING: STACK AND LOCATION DETAILS Release Point Reference A5 ARK Outlet Sampling Location and Stack Photos Operating & Process Information Type of Process Batch or Continuous Process Feedstock / Fuel Type Load / Throughput / Continuous Rating of Plant Expected Velocity, Temperature & Moisture Details of Abatement System Details of any CEMS Installed (including DCS) Process Details Required Reference Conditions 1 Reference Conditions 2 Sampling Location Details Stack Type / Shape Diameter / Dimensions (m) Access Platform Type and Location Orientation of Duct Sample Port Size / Diameter Sample Port Depth (cm) Sample Ports Correctly Located? Number of Sampling Lines Available Number of Sampling Lines to be Used Number of Sample Points to be Used (per line) Total Number of Sample Points to be Used EN 15259 / Homogeneity Representative Point/s Details Post-Scrubber Batch PTFE Parts TBC on day of testing 5 m/s | 38.3 C | 7.9 % v/v Scrubber None Operating conditions to be Provided by Site Contact 273K, 101.3kPa, without correction for water vapour content. N/A Value Circular 0.73 Ladder Permanent Vertical 5" Flange 10 Yes 2 2 1 1 - Outside - no shelter N/A Details Availability of Utilities Power 110V Lighting No Water Yes EA Technical Guidance Note M1 / EN 15259 Platform Requirements Value Sufficient working area to manipulate probe and operate the measuring instruments Yes Platform has 2 levels of handrails (approx. 0.5m & 1.0m high) Yes Platform has vertical base boards (approx. 0.25m high) Yes Platform has chains / self closing gates at top of ladders Yes There are no obstructions present which hamper insertion of sampling equipment Yes Safe Access Available Yes Easy Access Available Yes Sampling Platform / Improvement Recommendations: The sampling location meets all the requirements specified in EA Guidance Note M1 and EN 15259, and therefore there are no improvement recommendations. Sampling Plane Validation Criteria Requirement Lowest Differential Pressure (Pa) Ratio of Gas Velocities (:1) Maximum Angle of Swirl () No Local Negative Flow Value 16 1.3 NM Yes Compliant Yes Yes No Yes AGC Chemicals Europe Ltd Lancashire EL-LS-OP-SE-X-EWB 002 UK SSP (Version BF) 7 of 9 SSP Reference: EMT-SSP-05959, Version 1 EPR Permit: EPR/BU5453IY/V004 Determi na nd SAA 1000 PFOA Water Vapour Vel oc i ty SSP Part 2 DETAILS OF MONITORING: SAMPLING METHOD INFORMATION Release Point Reference A5 ARK Outlet In the "Units" column, = Reference Conditions 1, = Reference Conditions 2 (continued) Number of Runs | Blanks Uni ts Emi s s i on Limit Expected Emi s s i on PERIODIC SAMPLING: MANUAL METHODS Projected Standard Element Absorption Media / LOD Reference Technical Analysis Technique Method Procedure Ana l ys i s Lab | ISO17025 Status Sa mpl e Duration (mi ns ) Sa mpl e Fl owra te (ACTUAL) (l /mi n) Sa mpl e Vol ume (REF) (m) Projected Status MU of (%) Testing 2 1 mg/m N/A 2 1 mg/m N/A 4 0 % v/v N/A 2 0 m/s N/A 41.0 0.006 EN 1911 CAT-TP-11 10% DMSO EET MCERTS 240 0.10 0.006 EN 1911 CAT-TP-11 50% Methanol EET MCERTS 240 1.00 0.100 EN 14790 CAT-TP-05 Gravimetric EET MCERTS 240 2.80 3.000 EN ISO 16911-1 CAT-TP-41 Pressure & Temp EET MCERTS 5 10 2.387 15% MCERTS 10 2.387 15% MCERTS 10 N/A 5% MCERTS N/A N/A 10% MCERTS Velocity Profile - Source: Previous Testing Campaign P Pt Pa 1 24.7 2 19.8 Line A Temp Velocity P C m/s Pa 38.2 5.71 17.0 38.3 5.11 15.7 Line B Temp C 38.4 38.4 Velocity m/s 4.73 4.55 Monitoring Objectives / Unusual Occurrences / Comments / Health & Safety / Expected Deviations from Standard Reference Methods 1 Perform testing, as requested by the customer, for a number of prescribed pollutants. There are no emission limits set for any of the pollutants at this time 2 Perform testing of the required parameters simultaneous with the ARK inlet AGC Chemicals Europe Ltd Lancashire EL-LS-OP-SE-X-EWB 002 UK SSP (Version BF) 8 of 9 SSP Reference: EMT-SSP-05959, Version 1 EPR Permit: EPR/BU5453IY/V004 SSP Part 3 DEVIATIONS FROM THE SSP THAT MAY HAVE OCCURED ON SITE DURING THE SAMPLING CAMPAIGN Make a note of any deviations from this SSP below: (Deviations may include: modification to a sampling duration, removal of a test, change to the number of sampling runs etc.) At the end of the sampling campaign, the Team Leader must select one of the statements below and complete the required boxes: (1) I certify that all testing performed for this sampling campaign followed the testing programme as detailed in this SSP, and no deviations (unless specified in the original SSP and approved by the client) were required. Signature of Team Leader Date of Signature (tick) (2) It was necessary to deviate from the testing programme as detailed in this SSP. All deviations are listed above. The client was informed of the deviations and was happy for the testing to proceed / continue on this basis. (A client signature MUST be obtained for Contract Review purposes) Signature of Team Leader Date of Signature (tick) Signature of Client Date of Signature AGC Chemicals Europe Ltd Lancashire EL-LS-OP-SE-X-EWB 002 UK SSP (Version BF) 9 of 9 SSP Reference: EMT-SSP-05959, Version 1 EPR Permit: EPR/BU5453IY/V004