Document gEDxV7LOx8RkVLqkeexyg0VDL
Report Prepared by: Report Approved by:
NPDES Pretreatment Compliance Sampling Inspection Report
Hyatt Ball Company Ltd. 1 School Street Fort Edward, New York
NYP004952
February 9, 2023
ROBERT
Digitally signed by ROBERT
MORRELL
_M_O__R_R__E_L_L________Da_te_: 2_02_3_.04_.0_6 _11_:24_:4_9_-0_4'0_0'_
Robert Morrell, Geologist
Monitoring Operations Section
Date: ________________
Digitally signed by PHILIP
PHILIP COCUZZA COCUZZA ________________D_a_te:_2_02_3._04_.06_1_0:_21_:1_5 -_04_'0_0'_ Philip Cocuzza, Supervisor Monitoring Operations Section
Date: ________________
Hyatt Ball Company Ltd.
Inspection Date: February 9, 2023
Page 2 of 11
Hyatt Ball Company Ltd.
Inspection Date: February 9, 2023
1.0 OBJECTIVE
On February 9, 2023, at the request of the Water Compliance Branch, the United States Environmental Protection Agency (USEPA) conducted a National Pollutant Discharge Elimination System (NPDES) Pretreatment Compliance Sampling Inspection (CSI) at Hyatt Ball Company in Fort Edward, New York. The objective of the CSI was to gather information necessary to determine compliance with the general pretreatment requirements of 40 CFR Part 403 and the effluent guidelines and standards in 40 CFR Part 414 Subpart E (Thermosetting Resins).
2.0 KEY PARTICIPANTS
Listed below are key inspection participants and contact information, grouped by organization.
U.S. Environmental Protection Agency Robert Morrell, Geologist, Lead Inspector Morrell.robert@epa.gov, 732-906-6804 Thuan Tran, Physical Scientist Tran.thuan@epa.gov, 732-321-4455 Molly Hillenbrand, Life Scientist Hillenbrand.molly@epa.gov, 732-321-4452
Hyatt Ball Company Ltd. Robert A. Simpson, President Ra.simpson@hyattball.com, 518-747-0272 Ray McCasland, Operations Manager, Retired
3.0 FACILITY DESCRIPTION
3.1 General Information
Hyatt Ball Company is located at 1 School Street in Fort Edward, New York. The facility is a manufacturer of phenolic resin balls. The company is categorized as Standard Industrial Classification (SIC) Code 2821 (Plastic Materials, Synthetic Resins, and Nonvulcanizable Elastomers). The facility uses a batch manufacturing process, which varies from four to six batches per year, depending on market demand. There are currently two full-time employees and one part-time employee. Hyatt Ball is also a reseller of other industrial balls that are manufactured elsewhere.
Hyatt Ball Company was formerly known as Albany Hyatt Billiard Ball Company, which was founded in the early 1900's by John Wesley Hyatt, who invented celluloid as an alternative to ivory. The company eventually was purchased and moved operations to Fort Edward in 1987 as a manufacturer of billiard balls. Two years later, the company began manufacturing industrial balls and became known as Hyatt Ball Company.
Page 3 of 11
Hyatt Ball Company Ltd. 3.2 Process Information
Inspection Date: February 9, 2023
There are two reactors that are used in the phenolic resin batch manufacturing process. Kettle 4 is a small reactor with a capacity of approximately 10 gallons. Kettle 3 is a large reactor with a capacity of approximately 40 gallons. There are two other reactors on site that have been out of service for many years. For each batch, a mixture of formaldehyde, sodium hydroxide, and phenol is heated and mixed in the reactor. After the reaction is complete, the finished resin is poured into molds and heated in the oven to 170 o F. After cooling, the final product is removed from the molds and packaged for shipping. Approximately 60 pounds of resin are produced in a single batch from Kettle 4. Approximately 360 pounds of resin are produced in a single batch from Kettle 3.
All process wastewater is collected in a 100-gallon receiving tank. During mixing, a vacuum line extracts the distillate vapors. The vapors pass through condenser coils and the distillate liquid flows into the 100-gallon receiving tank. Approximately 3-4 gallons of distillate are generated for each batch in the small reactor. Approximately 30-34 gallons of distillate are generated for each batch in the large reactor. After each batch is completed, the reactor is cleaned with heated water and sodium hydroxide. The reactor rinse water drains into the 100-gallon receiving tank.
Rubber ball grinding operations were discontinued in 2022. There is presently no wastewater generated from this source. Prior to 2022, most of the process wastewater was generated from grinding operations. Wastewater from the reactors is now the sole source of process wastewater. Approximately 700 gallons are generated in a calendar year.
In the past, Hyatt Ball would discharge its process wastewaters to the Washington County Sewer District. At the present time, Hyatt Ball plans to ship the wastewater in the 100-gallon receiving tank to a TSDF (treatment, storage, and disposal facility).
3.3 Facility Self-Monitoring Information
In the past, Hyatt Ball personnel have collected pretreatment wastewater samples from the resin manufacturing and grinding process wastewater streams. These grab samples were collected twice per year for pollutants listed in 40 CFR Section 414.111. In addition, samples were collected for pH. Flow was also recorded for each batch discharge. Samples were analyzed by Adirondack Environmental Services in Albany, New York.
4.0 EPA SAMPLING/INSPECTION ACTIVITIES
4.1 Sampling Activities
A grab sample was collected from the receiving tank by opening a tap on the discharge line. The wastewater was allowed to flow for several minutes before filling the sample containers.
Page 4 of 11
Hyatt Ball Company Ltd.
Inspection Date: February 9, 2023
This sample was analyzed for cyanide, metals (lead, zinc), non-volatile organics, and volatile organics. Total residual chlorine and pH were analyzed in the field.
All sample containers, preservation techniques, and holding times were in accordance with U.S. EPA requirements specified in 40 CFR Part 136. All samples were placed in a cooler with wet ice and transported to the U.S. EPA Region 2 Laboratory in Edison, New Jersey.
Split samples were collected and given to the facility representative.
5.0 ANALYTICAL RESULTS
Hyatt Ball Company Pretreatment CSI
February 9, 2023
Parameter
Receiving Pretreatment Standards for New and
Tank
Existing Sources - Daily Maximum (40
CFR Section 414.111)
Total Residual Chlorine (mg/l)
0.09
--
pH (su)
12.63
5.0 - 12.5 (range)
Phenol (ug/l)
171,000 L
--
Lead (ug/l)
22.1
690
Zinc (ug/l)
481
2,610
Total Cyanide (ug/l)
Not detected
1,200
L - The reported value may be biased low.
*Only analytes detected at or above the reporting limit are listed in the above table. A complete list of analytes may be found in the attached Laboratory Data Report.
6.0 FINDINGS
6.1 Sampling Result Findings
Phenol was the only organic compound detected in the receiving tank wastewater. However, it is not listed as a toxic pollutant in 40 CFR Section 414.11. Analytical results indicate that all parameters listed in 40 CFR Section 414.111 did not exceed daily maximum discharge limitations for new and existing sources.
The pH of the wastewater in the receiving tank was 12.63, which is greater than 12.5. Because the wastewater is aqueous and has a pH greater than or equal to 12.5, it exhibits the RCRA characteristic of corrosivity (40 CFR Section 261.22).
Hyatt Ball Company has indicated that it plans to ship its receiving tank wastewater to a TSDF. It is recommended that the TSDF collect samples to characterize the wastewater prior to shipping to ensure compliance with RCRA and DOT regulations. Because the wastewater exhibits the RCRA characteristic of corrosivity, it currently must be shipped as a RCRA
Page 5 of 11
Hyatt Ball Company Ltd.
Inspection Date: February 9, 2023
D002 hazardous waste. Another option would be to treat the wastewater on site using elementary neutralization to make it non-hazardous with respect to corrosivity.
7.0 ATTACHMENTS
Photographs (#1 - #5) Laboratory Data Report Chain of Custody / Field Data Form
Page 6 of 11
Hyatt Ball Company Ltd.
Inspection Date: February 9, 2023
Photo #1: View of Kettle 4, the small reactor.
Page 7 of 11
Hyatt Ball Company Ltd.
Inspection Date: February 9, 2023
Photo #2: View of Kettle 3, the large reactor.
Page 8 of 11
Hyatt Ball Company Ltd. Photo #3: View of the oven.
Inspection Date: February 9, 2023
Page 9 of 11
Hyatt Ball Company Ltd. Photo #4: View of the receiving tank.
Inspection Date: February 9, 2023
Page 10 of 11
Hyatt Ball Company Ltd.
Inspection Date: February 9, 2023
Photo #5: View of the tap on the discharge line where samples were collected.
Page 11 of 11
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
2890 Woodbridge Avenue Edison , New Jersey 08837
732-906-6886 Phone 732-906-6165 Fax
February 28, 2023
Bob Morrell Monitoring & Assessment Branch LSASD/MAB Edison, NJ 08837
RE: Hyatt Ball Company - 2302011 Enclosed are the results of analyses for samples received by the laboratory on 02/09/2023. The signature below reflects the laboratory's approval of the reported results. If you have any questions concerning this report, please refer to Project Number 2302011 and contact the laboratory. Sincerely,
John R. Bourbon Chief, LSASD/LB
Project Narrative:
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011
The National Environmental Laboratory Accreditation Conference Institute (TNI) is a voluntary environmental laboratory accreditation association of State and Federal agencies. TNI established and promoted a National Environmental Laboratory Accreditation Program (NELAP) that provides a uniform set of standards for the generation of environmental data that are of known and defensible quality. The EPA Region 2 Laboratory is NELAP accredited. The Laboratory tests that are accredited have met all the requirements established under the TNI Standards.
Condition Comments
None
Comment(s): SVOA:
Due to the nature of the matrix, surrogate recoveries were out of the acceptance limit in sample, MS, and MSD. Majority of the target analytes recovery were out of the acceptance limit in MS/MSD. Due to the above problems, all target compounds in the sample were fagged with "L".
The "Sample Analysis Date and Time" is included in the results section for any analyte with a prescribed holding time of 72 hours or less.
Data Qualifier(s):
U- The analyte was not detected at or above the Reporting Limit. J- The identification of the analyte is acceptable; the reported value is an estimate. K- The identification of the analyte is acceptable; the reported value may be biased high. L- The identification of the analyte is acceptable; the reported value may be biased low. NJ- There is presumptive evidence that the analyte is present; the analyte is reported as a tentative identification. The reported value is an estimate.
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 1 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011
Reporting Limit(s):
The Laboratory was able to achieve the standard laboratory reporting limits, where applicable, for each analyte requested except for the following analyte(s):
NVOA GCMS
The reporting level of 5.00 ug/L was raised to 30 ug/L for the following analyte(s): 4,6-Dinitro-2-Methylphenol, Pentachlorophenol for the following samples: 2302011-02 The reporting level of 5.00 ug/L was raised to 50 ug/L for the following analyte(s): 2,4-Dinitrophenol for the following samples: 2302011-02
SUMMARY REPORT FOR SAMPLES
Field ID Trip Blank Receiving Tank-Grab
Laboratory ID 2302011-01 2302011-02
Matrix Aqueous Aqueous
Date Sampled 02/09/2023 12:10 02/09/2023 12:46
Date Received 02/09/2023 18:00 02/09/2023 18:00
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 2 of 26
Analysis 624.1 VOA EPA-NPDES 625.1 SVOA NPDES Cyanide, Total Metals ICP TAL NPDES/DW
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011
SUMMARY REPORT FOR METHODS
Method EPA 624.1 SOP C-89 Rev 3.7 EPA 625.1 SOP C-90 Rev 3.9 EPA 335.4 SOP C-28 Rev 2.8 EPA 200.7 SOP C-109 Rev 3.7
Certification
NELAP NELAP NELAP NELAP
Matrix
Aqueous Aqueous Aqueous Aqueous
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 3 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011
Analyte
Field ID: Trip Blank VOA GCMS Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2302011-01
Date and Time of Analysis*
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 4 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011
Analyte
Result
Qualifier
Reporting Limit
Units
Batch
Date and Time of Analysis*
Field ID: Trip Blank VOA GCMS 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Field ID: Receiving Tank-Grab VOA GCMS Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene
Sample ID: 2302011-01
---
U
5.00
ug/L B302038
---
U
5.00
ug/L B302038
Sample ID: 2302011-02
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 5 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011
Analyte
Field ID: Receiving Tank-Grab VOA GCMS Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene NVOA GCMS Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2302011-02
Date and Time of Analysis*
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U L
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U
50.0
ug/L B302038
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U J
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
51.0
ug/L B302020
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 6 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011
Analyte
Field ID: Receiving Tank-Grab NVOA GCMS 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2302011-02
Date and Time of Analysis*
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
30.6
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U J
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U L
5.10
ug/L B302020
---
U J
5.10
ug/L B302020
---
U L
30.6
ug/L B302020
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 7 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011
Analyte
Field ID: Receiving Tank-Grab NVOA GCMS Phenol Pyrene Metals ICP Lead Zinc Sanitary Cyanide, Total
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2302011-02
Date and Time of Analysis*
171000
L
---
U L
22.1 481
25500 5.10
8.00 20.0
ug/L ug/L
B302020 B302020
ug/L B302068 ug/L B302068
---
U L
10.0
ug/L B302069
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 8 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011
VOA GCMS - Quality Control
Analyte
Batch B302038
Blank (B302038-BLK1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
ND
ug/L
100.0
ND
ug/L
100.0
102
ug/L
100.0
98.7
60-140
98.8
60-140
102
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 9 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 VOA GCMS - Quality Control
Analyte
Batch B302038
LCS (B302038-BS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
53.0
5.00 ug/L
50.00
44.7
5.00 ug/L
50.00
46.4
5.00 ug/L
50.00
48.6
5.00 ug/L
50.00
52.5
5.00 ug/L
50.00
48.6
5.00 ug/L
50.00
45.9
5.00 ug/L
50.00
48.1
5.00 ug/L
50.00
50.6
5.00 ug/L
50.00
47.0
5.00 ug/L
50.00
47.0
5.00 ug/L
50.00
47.5
5.00 ug/L
50.00
46.8
5.00 ug/L
50.00
46.6
5.00 ug/L
50.00
46.5
5.00 ug/L
50.00
46.5
5.00 ug/L
50.00
46.5
5.00 ug/L
50.00
46.3
5.00 ug/L
50.00
46.7
5.00 ug/L
50.00
46.5
5.00 ug/L
50.00
48.9
5.00 ug/L
50.00
45.3
5.00 ug/L
50.00
45.6
5.00 ug/L
50.00
46.5
5.00 ug/L
50.00
45.6
5.00 ug/L
50.00
47.2
5.00 ug/L
50.00
46.4
5.00 ug/L
50.00
46.5
5.00 ug/L
50.00
45.3
5.00 ug/L
50.00
45.0
5.00 ug/L
50.00
45.4
5.00 ug/L
50.00
97.6
ug/L
100.0
100
ug/L
100.0
99.6
ug/L
100.0
106
19-205
89.4
5-195
92.7
15-185
97.3
40-160
105
50-150
97.2
50-150
91.8
60-140
96.3
60-140
101
70-130
93.9
70-130
94.1
70-135
95.1
70-130
93.6
70-130
93.3
70-130
93.0
65-135
93.1
65-135
93.0
35-165
92.7
65-135
93.4
25-175
93.0
70-130
97.9
50-150
90.6
70-130
91.2
70-130
93.0
70-135
91.1
65-135
94.4
60-140
92.8
70-130
92.9
60-140
90.6
70-130
90.0
65-135
90.7
65-135
97.6
60-140
100
60-140
99.6
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 10 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 VOA GCMS - Quality Control
Analyte
Batch B302038
LCS Dup (B302038-BSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
52.1
5.00 ug/L
50.00
44.4
5.00 ug/L
50.00
46.5
5.00 ug/L
50.00
48.1
5.00 ug/L
50.00
50.4
5.00 ug/L
50.00
48.1
5.00 ug/L
50.00
44.1
5.00 ug/L
50.00
48.1
5.00 ug/L
50.00
49.2
5.00 ug/L
50.00
45.6
5.00 ug/L
50.00
45.6
5.00 ug/L
50.00
46.2
5.00 ug/L
50.00
45.8
5.00 ug/L
50.00
45.7
5.00 ug/L
50.00
45.6
5.00 ug/L
50.00
45.8
5.00 ug/L
50.00
45.2
5.00 ug/L
50.00
45.4
5.00 ug/L
50.00
45.9
5.00 ug/L
50.00
45.6
5.00 ug/L
50.00
48.2
5.00 ug/L
50.00
44.0
5.00 ug/L
50.00
43.6
5.00 ug/L
50.00
44.8
5.00 ug/L
50.00
43.5
5.00 ug/L
50.00
45.3
5.00 ug/L
50.00
44.7
5.00 ug/L
50.00
45.3
5.00 ug/L
50.00
44.0
5.00 ug/L
50.00
43.1
5.00 ug/L
50.00
43.7
5.00 ug/L
50.00
98.8
ug/L
100.0
101
ug/L
100.0
99.1
ug/L
100.0
104
19-205
1.79
20
88.7
5-195
0.719
20
93.1
15-185
0.344
20
96.2
40-160
1.18
20
101
50-150
3.95
20
96.1
50-150
1.10
20
88.2
60-140
4.02
20
96.2
60-140 0.0831
20
98.4
70-130
2.85
20
91.2
70-130
3.00
20
91.1
70-135
3.20
20
92.4
70-130
2.84
20
91.6
70-130
2.20
20
91.4
70-130
2.06
20
91.2
65-135
2.04
20
91.5
65-135
1.67
20
90.5
35-165
2.70
20
90.7
65-135
2.12
20
91.7
25-175
1.84
20
91.2
70-130
1.93
20
96.5
50-150
1.44
20
88.1
70-130
2.82
20
87.2
70-130
4.42
20
89.7
70-135
3.61
20
87.0
65-135
4.65
20
90.6
60-140
4.04
20
89.4
70-130
3.73
20
90.6
60-140
2.51
20
87.9
70-130
3.02
20
86.2
65-135
4.34
20
87.4
65-135
3.73
20
98.8
60-140
101
60-140
99.1
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 11 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 VOA GCMS - Quality Control
Analyte
Batch B302038
Matrix Spike (B302038-MS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2302011-02
55.3
5.00 ug/L
45.3
5.00 ug/L
43.8
5.00 ug/L
48.2
5.00 ug/L
49.9
5.00 ug/L
48.6
5.00 ug/L
44.0
5.00 ug/L
44.4
5.00 ug/L
48.3
5.00 ug/L
45.4
5.00 ug/L
45.7
5.00 ug/L
45.5
5.00 ug/L
45.0
5.00 ug/L
44.5
5.00 ug/L
45.1
5.00 ug/L
79.9
5.00 ug/L
44.7
5.00 ug/L
44.0
5.00 ug/L
43.6
5.00 ug/L
44.8
5.00 ug/L
46.3
5.00 ug/L
41.4
5.00 ug/L
43.8
5.00 ug/L
43.0
5.00 ug/L
43.3
5.00 ug/L
45.3
5.00 ug/L
42.8
5.00 ug/L
--- U
5.00 ug/L
46.0
5.00 ug/L
45.3
5.00 ug/L
45.7
5.00 ug/L
97.8
ug/L
99.3
ug/L
98.7
ug/L
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
100.0 100.0 100.0
111
19-273
90.7
49-251
87.5
21-242
96.4
14-230
99.8
17-181
97.2
52-234
88.0
69-221
88.7
40-160
96.5
54-156
90.8
59-155
91.4
51-138
91.0
52-162
89.9
70-140
89.0
49-155
90.2
37-151
160
70-157
89.3
74-210
88.1
35-155
87.2
80-227
89.5
47-150
92.6
17-183
82.9
52-150
87.6
64-148
86.0
53-149
86.6
37-160
90.7
37-162
85.5
45-169
46-157
92.0
59-156
90.7
18-190
91.4
18-190
97.8
60-140
99.3
60-140
98.7
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 12 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 VOA GCMS - Quality Control
Analyte
Batch B302038
Matrix Spike Dup (B302038-MSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2302011-02
59.6
5.00 ug/L
50.00
ND
119
19-273
7.46
28
48.9
5.00 ug/L
50.00
ND
97.8
49-251
7.58
28
49.5
5.00 ug/L
50.00
ND
98.9
21-242
12.2
28
52.2
5.00 ug/L
50.00
ND
104
14-230
8.07
28
53.1
5.00 ug/L
50.00
ND
106
17-181
6.12
28
51.6
5.00 ug/L
50.00
ND
103
52-234
6.09
28
47.2
5.00 ug/L
50.00
ND
94.4
69-221
6.93
28
51.6
5.00 ug/L
50.00
ND
103
40-160
15.0
28
51.0
5.00 ug/L
50.00
ND
102
54-156
5.60
28
48.2
5.00 ug/L
50.00
ND
96.3
59-155
5.84
28
48.7
5.00 ug/L
50.00
ND
97.5
51-138
6.48
28
48.7
5.00 ug/L
50.00
ND
97.3
52-162
6.69
28
48.5
5.00 ug/L
50.00
ND
97.0
70-140
7.62
28
48.3
5.00 ug/L
50.00
ND
96.5
49-155
8.08
28
47.9
5.00 ug/L
50.00
ND
95.8
37-151
6.09
28
87.5
5.00 ug/L
50.00
ND
175
70-157
9.13
28
47.5
5.00 ug/L
50.00
ND
95.0
74-210
6.12
28
47.0
5.00 ug/L
50.00
ND
94.0
35-155
6.48
28
46.7
5.00 ug/L
50.00
ND
93.4
80-227
6.93
28
47.6
5.00 ug/L
50.00
ND
95.3
47-150
6.23
28
49.9
5.00 ug/L
50.00
ND
99.9
17-183
7.54
28
44.7
5.00 ug/L
50.00
ND
89.3
52-150
7.53
28
46.0
5.00 ug/L
50.00
ND
91.9
64-148
4.81
28
46.7
5.00 ug/L
50.00
ND
93.5
53-149
8.31
28
47.0
5.00 ug/L
50.00
ND
93.9
37-160
8.11
28
48.4
5.00 ug/L
50.00
ND
96.9
37-162
6.61
28
47.9
5.00 ug/L
50.00
ND
95.8
45-169
11.4
28
--- U
5.00 ug/L
50.00
ND
46-157
28
49.0
5.00 ug/L
50.00
ND
98.0
59-156
6.25
28
48.8
5.00 ug/L
50.00
ND
97.6
18-190
7.39
28
49.9
5.00 ug/L
50.00
ND
99.9
18-190
8.89
28
98.0
ug/L
100.0
98.0
60-140
99.4
ug/L
100.0
99.4
60-140
101
ug/L
100.0
101
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 13 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B302020
Blank (B302020-BLK2) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
RPD Limit
Page 14 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 NVOA GCMS - Quality Control
Analyte
Batch B302020
Blank (B302020-BLK2) Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
LCS (B302020-BS2) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
35.2
ug/L
50.00
ND
ug/L
50.00
38.0
ug/L
50.00
37.1
ug/L
50.00
35.1
ug/L
50.00
ND
ug/L
50.00
54.3
ug/L
50.00
44.0
5.00 ug/L
50.00
42.1
5.00 ug/L
50.00
43.4
5.00 ug/L
50.00
41.0
5.00 ug/L
50.00
45.1
5.00 ug/L
50.00
48.3
5.00 ug/L
50.00
47.5
5.00 ug/L
50.00
45.7
5.00 ug/L
50.00
70.4
60-140
35.7
60-140
76.0
60-140
74.2
60-140
70.2
60-140
54.9
60-140
109
60-140
88.0
47-145
84.3
33-145
86.8
27-133
82.0
33-143
90.2
17-163
96.6
24-159
95.0
35-219
91.3
11-162
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 15 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B302020
LCS (B302020-BS2) Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene
40.4
5.00 ug/L
50.00
46.3
5.00 ug/L
50.00
45.2
5.00 ug/L
50.00
43.3
5.00 ug/L
50.00
47.6
5.00 ug/L
50.00
35.2
5.00 ug/L
50.00
44.9
5.00 ug/L
50.00
31.6
5.00 ug/L
50.00
41.2
5.00 ug/L
50.00
38.9
5.00 ug/L
50.00
21.2
5.00 ug/L
50.00
47.2
5.00 ug/L
50.00
46.7
5.00 ug/L
50.00
36.8
5.00 ug/L
50.00
40.6
5.00 ug/L
50.00
32.5
5.00 ug/L
50.00
39.3
5.00 ug/L
50.00
45.3
5.00 ug/L
50.00
47.2
5.00 ug/L
50.00
44.4
5.00 ug/L
50.00
41.9
5.00 ug/L
50.00
43.4
5.00 ug/L
50.00
21.6
5.00 ug/L
50.00
39.4
5.00 ug/L
50.00
34.0
5.00 ug/L
50.00
34.2
5.00 ug/L
50.00
52.2
5.00 ug/L
50.00
52.1
5.00 ug/L
50.00
44.5
5.00 ug/L
50.00
44.5
5.00 ug/L
50.00
42.0
5.00 ug/L
50.00
48.5
5.00 ug/L
50.00
50.1
5.00 ug/L
50.00
43.2
5.00 ug/L
50.00
29.0
5.00 ug/L
50.00
80.7
17-168
92.6
33-227
90.4
26-137
86.6
59-121
95.1
39-171
70.3
21-133
89.9
54-120
63.2
44-142
82.5
37-144
77.8
39-135
42.3
32-120
94.5
39-139
93.4
50-158
73.5
21-191
81.1
60-120
65.0
23-134
78.6
29-182
90.7
38-262
94.3
17-181
88.8
53-127
83.9
22-147
86.8
25-158
43.3
9-132
78.8
33-184
68.0
12-158
68.5
36-166
104
8-158
104
38-152
89.0
60-115
89.0
31-114
84.0
28-120
97.0
1-120
100
4-146
86.4
35-152
57.9
24-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
RPD Limit
Page 16 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 NVOA GCMS - Quality Control
Analyte
Batch B302020
LCS (B302020-BS2) Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
LCS Dup (B302020-BSD2) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
40.5
5.00 ug/L
50.00
27.6
5.00 ug/L
50.00
45.5
5.00 ug/L
50.00
38.4
5.00 ug/L
50.00
22.1
5.00 ug/L
50.00
38.3
5.00 ug/L
50.00
51.9
5.00 ug/L
50.00
40.1
5.00 ug/L
50.00
15.1
5.00 ug/L
50.00
44.9
5.00 ug/L
50.00
27.8
ug/L
50.00
14.5
ug/L
50.00
35.2
ug/L
50.00
33.4
ug/L
50.00
39.4
ug/L
50.00
33.5
ug/L
50.00
40.8
ug/L
50.00
40.4
5.00 ug/L
50.00
39.0
5.00 ug/L
50.00
44.4
5.00 ug/L
50.00
42.1
5.00 ug/L
50.00
45.3
5.00 ug/L
50.00
48.6
5.00 ug/L
50.00
48.3
5.00 ug/L
50.00
46.4
5.00 ug/L
50.00
41.7
5.00 ug/L
50.00
46.9
5.00 ug/L
50.00
46.3
5.00 ug/L
50.00
43.6
5.00 ug/L
50.00
48.8
5.00 ug/L
50.00
34.4
5.00 ug/L
50.00
45.9
5.00 ug/L
50.00
31.0
5.00 ug/L
50.00
81.0
15-76
55.1
40-120
91.0
21-196
76.8
35-180
44.2
17-127
76.6
43-230
104
79-139
80.2
14-176
30.3
5-120
89.8
52-120
55.6
60-140
29.0
60-140
70.4
60-140
66.9
60-140
78.8
60-140
66.9
60-140
81.7
60-140
80.9
47-145
8.36
30
77.9
33-145
7.87
30
88.9
27-133
2.41
30
84.1
33-143
2.55
30
90.6
17-163
0.443
30
97.1
24-159
0.558
30
96.6
35-219
1.59
30
92.8
11-162
1.63
30
83.5
17-168
3.36
30
93.8
33-227
1.24
30
92.5
26-137
2.34
30
87.1
59-121
0.575
30
97.6
39-171
2.55
30
68.9
21-133
2.07
30
91.8
54-120
2.11
30
61.9
44-142
2.11
30
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 17 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike Level
Source Result
%REC
%REC Limits
Batch B302020
LCS Dup (B302020-BSD2) 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol
39.6
5.00 ug/L
50.00
39.2
5.00 ug/L
50.00
13.9
5.00 ug/L
50.00
49.7
5.00 ug/L
50.00
45.5
5.00 ug/L
50.00
35.1
5.00 ug/L
50.00
37.6
5.00 ug/L
50.00
35.7
5.00 ug/L
50.00
41.2
5.00 ug/L
50.00
43.2
5.00 ug/L
50.00
50.2
5.00 ug/L
50.00
46.1
5.00 ug/L
50.00
39.5
5.00 ug/L
50.00
44.4
5.00 ug/L
50.00
19.8
5.00 ug/L
50.00
39.4
5.00 ug/L
50.00
38.2
5.00 ug/L
50.00
34.3
5.00 ug/L
50.00
54.4
5.00 ug/L
50.00
50.5
5.00 ug/L
50.00
44.3
5.00 ug/L
50.00
45.0
5.00 ug/L
50.00
37.2
5.00 ug/L
50.00
50.7
5.00 ug/L
50.00
51.0
5.00 ug/L
50.00
44.6
5.00 ug/L
50.00
27.5
5.00 ug/L
50.00
36.9
5.00 ug/L
50.00
27.7
5.00 ug/L
50.00
45.5
5.00 ug/L
50.00
38.5
5.00 ug/L
50.00
25.9
5.00 ug/L
50.00
39.1
5.00 ug/L
50.00
51.5
5.00 ug/L
50.00
42.0
5.00 ug/L
50.00
79.3
37-144
78.5
39-135
27.7
32-120
99.5
39-139
90.9
50-158
70.3
21-191
75.1
60-120
71.3
23-134
82.4
29-182
86.4
38-262
100
17-181
92.3
53-127
78.9
22-147
88.9
25-158
39.7
9-132
78.8
33-184
76.3
12-158
68.7
36-166
109
8-158
101
38-152
88.7
60-115
90.0
31-114
74.4
28-120
101
1-120
102
4-146
89.3
35-152
54.9
24-120
73.7
15-76
55.4
40-120
91.1
21-196
77.0
35-180
51.8
17-127
78.1
43-230
103
79-139
84.0
14-176
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
RPD
3.96 0.845 41.7 5.18 2.65 4.48 7.68 9.27 4.72 4.77 6.27 3.87 6.07 2.41 8.78 0.0254 11.6 0.321 4.11 3.08 0.338 1.05 12.2 4.49 1.82 3.26 5.32 9.38 0.434 0.110 0.260 15.8 1.96 0.832 4.68
RPD Limit
30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30
Page 18 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 NVOA GCMS - Quality Control
Analyte
Batch B302020
LCS Dup (B302020-BSD2) Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
Matrix Spike (B302020-MS1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
17.0
5.00 ug/L
50.00
46.0
5.00 ug/L
50.00
31.2
ug/L
50.00
15.6
ug/L
50.00
33.3
ug/L
50.00
31.7
ug/L
50.00
37.5
ug/L
50.00
32.9
ug/L
50.00
40.1
ug/L
50.00
33.9
5-120
11.4
30
91.9
52-120
2.27
30
62.5
60-140
31.2
60-140
66.6
60-140
63.4
60-140
75.1
60-140
65.8
60-140
80.1
60-140
Source: 2302011-02
17.5
5.49 ug/L
17.1
5.49 ug/L
17.5
5.49 ug/L
21.7
5.49 ug/L
16.5
5.49 ug/L
23.5
5.49 ug/L
12.1
5.49 ug/L
22.0
5.49 ug/L
22.4
5.49 ug/L
15.5
5.49 ug/L
17.4
5.49 ug/L
19.5
5.49 ug/L
14.7
5.49 ug/L
17.9
5.49 ug/L
18.1
5.49 ug/L
17.4
5.49 ug/L
13.3
5.49 ug/L
14.2
5.49 ug/L
19.7
5.49 ug/L
22.8
5.49 ug/L
20.0
5.49 ug/L
20.2
5.49 ug/L
17.5
5.49 ug/L
--- U
5.49 ug/L
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
31.9
47-145
31.1
33-145
31.9
27-133
39.4
33-143
30.0
17-163
42.8
24-159
21.9
35-219
40.0
11-162
40.8
17-168
28.2
33-227
31.6
26-137
35.4
59-121
26.8
39-171
32.7
21-133
33.0
54-120
31.6
44-142
24.1
37-144
25.8
39-135
35.8
32-120
41.4
39-139
36.3
50-158
36.7
21-191
31.8
60-120
23-134
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 19 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B302020
Matrix Spike (B302020-MS1) 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10
Source: 2302011-02
--- U
5.49 ug/L
--- U
5.49 ug/L
16.5
5.49 ug/L
18.4
5.49 ug/L
261
5.49 ug/L
19.3
5.49 ug/L
13.7
5.49 ug/L
--- U
5.49 ug/L
143
5.49 ug/L
--- U
5.49 ug/L
32.2
5.49 ug/L
21.0
5.49 ug/L
19.0
5.49 ug/L
20.2
5.49 ug/L
17.9
5.49 ug/L
19.0
5.49 ug/L
29.5
5.49 ug/L
17.9
5.49 ug/L
15.5
5.49 ug/L
20.4
5.49 ug/L
14.1
5.49 ug/L
21.9
5.49 ug/L
13.7
5.49 ug/L
--- U
5.49 ug/L
--- U
5.49 ug/L
4.96
5.49 ug/L
13.2
5.49 ug/L
--- U
5.49 ug/L
17.0
5.49 ug/L
ND
ug/L
ND
ug/L
19.4
ug/L
18.9
ug/L
13.0
ug/L
14.8
ug/L
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
ND
54.95
1370
54.95
ND
54.95 54.95 54.95 54.95 54.95 54.95
29-182
38-262
29.9
17-181
33.5
53-127
475
22-147
35.1
25-158
24.9
9-132
33-184
260
12-158
36-166
58.5
8-158
38.1
38-152
34.6
61-106
36.7
31-114
32.5
28-120
34.6
1-120
53.6
4-146
32.6
35-152
28.2
24-120
37.1
15-76
25.6
40-120
39.8
21-196
24.9
35-180
17-127
43-230
9.02
79-139
24.0
14-176
NR
5-120
30.9
52-120
60-140
60-140
35.4
60-140
34.5
60-140
23.7
60-140
27.0
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
RPD Limit
Page 20 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 NVOA GCMS - Quality Control
Analyte
Batch B302020
Matrix Spike (B302020-MS1) Surrogate: Chrysene-D12
Matrix Spike Dup (B302020-MSD1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Source: 2302011-02
23.7
ug/L
Source: 2302011-02
22.2
5.56 ug/L
21.2
5.56 ug/L
23.7
5.56 ug/L
27.0
5.56 ug/L
20.3
5.56 ug/L
28.6
5.56 ug/L
15.1
5.56 ug/L
27.8
5.56 ug/L
27.8
5.56 ug/L
19.3
5.56 ug/L
21.9
5.56 ug/L
26.8
5.56 ug/L
18.5
5.56 ug/L
16.2
5.56 ug/L
24.9
5.56 ug/L
13.7
5.56 ug/L
13.7
5.56 ug/L
13.1
5.56 ug/L
19.7
5.56 ug/L
29.7
5.56 ug/L
24.7
5.56 ug/L
19.1
5.56 ug/L
20.7
5.56 ug/L
2.81
5.56 ug/L
--- U
5.56 ug/L
--- U
5.56 ug/L
19.0
5.56 ug/L
25.2
5.56 ug/L
273
5.56 ug/L
26.2
5.56 ug/L
14.3
5.56 ug/L
--- U
5.56 ug/L
54.95
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
43.2
60-140
39.9
47-145
23.5
38.2
33-145
21.7
42.7
27-133
30.2
48.6
33-143
21.8
36.5
17-163
20.6
51.6
24-159
19.7
27.2
35-219
22.5
50.0
11-162
23.3
50.1
17-168
21.4
34.8
33-227
22.0
39.4
26-137
23.2
48.3
59-121
31.9
33.2
39-171
22.4
29.1
21-133
10.3
44.8
54-120
31.4
24.7
44-142
23.3
24.6
37-144
3.24
23.6
39-135
7.72
35.5
32-120
0.263
53.4
39-139
26.4
44.4
50-158
21.1
34.4
21-191
5.59
37.3
60-120
17.1
5.06
23-134
29-182
38-262
34.1
17-181
14.2
45.4
53-127
31.4
492
22-147
4.56
47.1
25-158
30.3
25.8
9-132
4.65
33-184
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
RPD Limit
24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24
Page 21 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 NVOA GCMS - Quality Control
Analyte
Batch B302020
Matrix Spike Dup (B302020-MSD1) Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2302011-02
152
5.56 ug/L
55.56
ND
274
12-158
6.36
24
--- U
5.56 ug/L
55.56
ND
36-166
24
38.1
5.56 ug/L
55.56
ND
68.6
8-158
16.9
24
26.8
5.56 ug/L
55.56
ND
48.2
38-152
24.4
24
25.8
5.56 ug/L
55.56
ND
46.5
61-106
30.4
24
26.5
5.56 ug/L
55.56
ND
47.7
31-114
27.2
24
21.4
5.56 ug/L
55.56
ND
38.5
28-120
18.0
24
25.9
5.56 ug/L
55.56
ND
46.6
1-120
30.7
24
35.2
5.56 ug/L
55.56
ND
63.3
4-146
17.7
24
22.9
5.56 ug/L
55.56
ND
41.2
35-152
24.4
24
10.3
5.56 ug/L
55.56
ND
18.5
24-120
40.2
24
19.7
5.56 ug/L
55.56
ND
35.4
15-76
3.42
24
5.50
5.56 ug/L
55.56
ND
9.90
40-120
87.6
24
27.7
5.56 ug/L
55.56
ND
49.8
21-196
23.5
24
--- U
5.56 ug/L
55.56
ND
35-180
24
--- U
5.56 ug/L
55.56
ND
17-127
24
--- U
5.56 ug/L
55.56
ND
43-230
24
7.12
5.56 ug/L
55.56
ND
12.8
79-139
35.9
24
14.7
5.56 ug/L
55.56
ND
26.5
14-176
11.2
24
1040
5.56 ug/L
55.56
1370
NR
5-120
24
21.6
5.56 ug/L
55.56
ND
38.9
52-120
24.1
24
ND
ug/L
55.56
60-140
ND
ug/L
55.56
60-140
18.2
ug/L
55.56
32.8
60-140
16.8
ug/L
55.56
30.2
60-140
13.5
ug/L
55.56
24.2
60-140
19.4
ug/L
55.56
34.8
60-140
30.1
ug/L
55.56
54.2
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 22 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 Metals ICP - Quality Control
Analyte
Batch B302068
Blank (B302068-BLK1) Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
LCS (B302068-BS1) Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Chromium Cobalt
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U --- U
4500 193 187 198 194 188 194
4450 196 195
100 ug/L 20.0 ug/L 8.00 ug/L 100 ug/L 3.00 ug/L 3.00 ug/L 500 ug/L 5.00 ug/L 20.0 ug/L 10.0 ug/L 50.0 ug/L 8.00 ug/L 500 ug/L 5.00 ug/L 10.0 ug/L 20.0 ug/L 500 ug/L 20.0 ug/L 5.00 ug/L 1000 ug/L 20.0 ug/L 20.0 ug/L 20.0 ug/L
100 ug/L 20.0 ug/L 8.00 ug/L 100 ug/L 3.00 ug/L 10.0 ug/L 3.00 ug/L 500 ug/L 5.00 ug/L 20.0 ug/L
5000 200.0 200.0 200.0 200.0 200.0 200.0 5000 200.0 200.0
90.1
85-115
96.6
85-115
93.4
85-115
98.9
85-115
97.2
85-115
94.1
85-115
97.1
85-115
89.0
85-115
97.8
85-115
97.5
85-115
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 23 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 Metals ICP - Quality Control
Analyte
Batch B302068
LCS (B302068-BS1) Copper Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc
LCS Dup (B302068-BSD1) Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
194 4470
196 4450
193 195 196 4470 190 195 4340 201 192 198 196 197 192
4550 193 188 199 196 189 195
4500 196 196 195
4520 195
4510 194 195
10.0 ug/L 50.0 ug/L 8.00 ug/L 500 ug/L 5.00 ug/L 10.0 ug/L 20.0 ug/L 500 ug/L 20.0 ug/L 5.00 ug/L 1000 ug/L 10.0 ug/L 20.0 ug/L 10.0 ug/L 10.0 ug/L 20.0 ug/L 20.0 ug/L
200.0 5000 200.0 5000 200.0 200.0 200.0 5000 200.0 200.0 5000 200.0 200.0 200.0 200.0 200.0 200.0
100 ug/L 20.0 ug/L 8.00 ug/L 100 ug/L 3.00 ug/L 10.0 ug/L 3.00 ug/L 500 ug/L 5.00 ug/L 20.0 ug/L 10.0 ug/L 50.0 ug/L 8.00 ug/L 500 ug/L 5.00 ug/L 10.0 ug/L
5000 200.0 200.0 200.0 200.0 200.0 200.0 5000 200.0 200.0 200.0 5000 200.0 5000 200.0 200.0
97.1
85-115
89.3
85-115
97.8
85-115
89.0
85-115
96.7
85-115
97.5
85-115
98.0
85-115
89.5
85-115
95.1
85-115
97.3
85-115
86.8
85-115
101
85-115
96.1
85-115
99.0
85-115
97.9
85-115
98.4
85-115
96.0
85-115
91.1
85-115
1.12
20
96.7
85-115 0.0310
20
93.8
85-115
0.438
20
99.5
85-115
0.564
20
97.9
85-115
0.620
20
94.5
85-115
0.493
20
97.4
85-115
0.396
20
90.0
85-115
1.10
20
98.2
85-115
0.378
20
97.9
85-115
0.415
20
97.4
85-115
0.375
20
90.3
85-115
1.09
20
97.7
85-115 0.0870
20
90.1
85-115
1.28
20
97.1
85-115
0.382
20
97.4
85-115 0.0308
20
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 24 of 26
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 Metals ICP - Quality Control
Analyte
Batch B302068 LCS Dup (B302068-BSD1)
Nickel Potassium Selenium Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc
Matrix Spike (B302068-MS1) Lead Zinc
Matrix Spike Dup (B302068-MSD1) Lead Zinc
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
196 4530
194 197 4390 203 191 200 196 197 193
20.0 ug/L 500 ug/L 20.0 ug/L 5.00 ug/L 1000 ug/L 10.0 ug/L 20.0 ug/L 10.0 ug/L 10.0 ug/L 20.0 ug/L 20.0 ug/L
200.0 5000 200.0 200.0 5000 200.0 200.0 200.0 200.0 200.0 200.0
98.2
85-115
0.204
20
90.6
85-115
1.18
20
97.0
85-115
1.96
20
98.7
85-115
1.36
20
87.8
85-115
1.21
20
101
85-115
0.609
20
95.4
85-115
0.663
20
99.8
85-115
0.734
20
98.2
85-115
0.331
20
98.7
85-115
0.315
20
96.6
85-115
0.639
20
Source: 2302011-02
205
8.00 ug/L
669
20.0 ug/L
200.0
22.1
200.0
481
91.7
80-120
93.8
80-120
Source: 2302011-02
224
40.0 ug/L
200.0
22.1
101
80-120
8.66
10
717
100 ug/L
200.0
481
118
80-120
6.88
10
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 25 of 26
Analyte
Batch B302069 Blank (B302069-BLK1)
Cyanide, Total
Blank (B302069-BLK2) Cyanide, Total
LCS (B302069-BS1) Cyanide, Total
LCS Dup (B302069-BSD1) Cyanide, Total
Matrix Spike (B302069-MS1) Cyanide, Total
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Hyatt Ball Company - 2302011
Project Number: 2302011 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
10.0 ug/L
--- U
10.0 ug/L
770
10.0 ug/L
796.0
97
90-110
743
10.0 ug/L
796.0
93
90-110
4
20
Source: 2302011-02
--- U
10.0 ug/L
500.0
ND
90-110
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 2/28/2023
Page 26 of 26
"'-~-L.
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- Page __ of _,_ pages
SURVEY NAME & LOCALITY
", PROGRAM: SF D
".L .w,
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SITEID
'V"~r"
__
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PROJECT LEADER PROGRAM RESULTS CODE
_., .~ ,._,. _
RCRAD
RCRAENFD 0307
NPDESD B304
SDWAD C215
AM 0
B224
CM 0
A305
TSCA D
L306
00 D
B253
FIFRA 0
CRIMINAL ENF D
DESCRIPTION & INSTRUCTIONS
~ CHECK IF ESTIMATED CONCENTRATIONS,
-I SPLIT
LIMITS
~ SAMPLE ~----'
--------------------------------
INCLUDING LOCATION, SPECIAL REPORTING
__ ~
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Collection Time (24hr clock)
(circle)
11/1/1/1/11/1/
Begin:
End
Collection Date
mm/dd/yy
0012345678910
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Preservative Added & Checked
O=ice
7=FAS
1=H2S04 pH<2
8=ZnAc
2=HN03 pH<2
9=NaOH pH>12
3=HCI pH<2
10=NH4CI
4=Na2S203
5=NaOH pH>9
6=Ascorbic Acid
A=aqueous B=aqueous C=soil D=sediment ,E=sludge
atrlx: (chlorinated)
F=multiphasic G=solvent H=biota I=oil J=other
Survey Complete? Y
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Relinquished By~ Relinquished By: Relinquished By:
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revised 10/25/2004
