Document YZREYOY4kjDd25Xdw6xkje38
Dept, A-246 - Operating Instructions
Transformer Pyratiol A-13B3B
'
.
45$ Arcelor 1250 - 55/. TTCB
To make l4,000 gal, batch A-13B3B in #2 mix tank.
.
1 Take 1 - 16 oz. sample of Unox Epoxide 201 for assay.
2 ~ Unload 8,000 gal. car of TTCB to #2 mix tank (approx,. 12*
In tank).
.
3 - Pump 1260 from #8 storage to 256" in #2 mix tank. .
4 ~ Add 1 - bag attapulgus earth.
5 - Agitate with air and mechanical agitator and circulate by passing press for 3 hours.
6 - Circulate thru press for 1 hour and take 1 - 5 pt. bottle for check analysis - gravity - index - chlorides & moisture.
7 - Continue circulating thru press for 3 hours.
.
8 - Blow and clean press.
, .
9 - Correct gravity and index (Gr. 1.563 - 1.571) (Index 1.6075 -
1,6085). Mix should be on low side with above measure
ments. Gravity will be raised about .001 and index will
be raised about .0004 by the addition of 1 inch of 1260,
If gravity or index or both are high, resample for gravity
and index analysis. Moisture can be reduced by blowing
. with air. Chlorides can be. reduced, by. additional earth .
treatment.
. .
.
10 - When all check analysis are in specs add Unox Epoxide 201, (Ihis must be calculated from the assay).,
11 - Circulate again by passing press for 3 hours.
12 - Put thru-, press 1 hour and take final samples. 3 - 5 pt.
. bottles.
.
13 - After an additional 3 hours thru press - blow and .clean press.
ghw 9/12/63
R. C. Smith
PCB-ARCH-EXT0374511
Dept. A-246 - Operating Instructions
Transformer Pyranol A-I3B3B 45^ Apoclor 1260 - 55/ TTCB
To make 14,000 sal. batch A-13B3B in #2 mix tank.
1 - Take 1 - 16 02. cample of Unox Epoxide 201 for* assay. .
2 - Unload 8,000 gal. car* of TTCB to #2 mix tank (approx. 12* in tank).
3 - Pump 1260 from #3 storage to 256T' in #2 mix tank.
4 ~ Acid 1 ~ bag attapralgus earth.
5 - Agitate with air and mechanical agitator and circulate by passing press for 3 hours.
6 - Circulate thru press for 1 hour and take 1 - 5 pt. bottle for check analysis - gravity ~ index - chlorides & moisture.
7 - Continue circulating thru press for 3 hours.
8 ~ Blow and clean press.
.
9 - Correct gravity and index (Gr. 1.563 - 1.571) (Index 1,6075 1.6085). Mix should be on low side with above measure ments. Gravity will be raised about .001 and index will be raised about .0004 by the addition of 1 inch of 1260. If gravity or index or both are high, resample for gravity and index analysis. Moisture can be reduced by blowing
. with air. Chlorides can be reduced by additional earth
treatment.
10 - When all check analysis are in specs add Unox Epoxide 201. (This must be calculated from the assay),
11 - Circulate again by passing press for 3 hour's.
12 - Put thru press 1 hour and take final samples. 3-5 pt. bottles.
13 - After an additional 3 hours thru press - blow and clean press.
9/12/63
R. 0. Smith
PCB-ARCH-EXT0374512
Dept, A-246 - Operating Instructions
Transformer* Pyronol A-13B3B
45# Arcelor 1260 - 55/ TTCB
.
To make 14, 000 gal,, batch A-13B3B in #2 mix tank,
1 - Take 1 - l6 02* saraple of Unox Epoxide 201 for assay,
2 - Unload 8/000 gal* car of TTCB to $2 mix tank {approx. 12' in tank),
3 - Pump 1260 from 0 storage to 256 in #2 mix tank.
4 - Add 1 - bag att&pulgus earth,
5 - Agitate with air and mechanical agitator and circulate by passing press for 3 hours,
6 - Circulate thru press for 1 hour and take 1 - 5 pt, bottle for check analysis - gravity - index - chlorides 8t moisture.
7 - Continue circulating thru press for 3 hours.
8 - Blow and clean press.
9 - Correct gravity and index (Gr. 1.563 - 1.571) (index 1.6075 1,6085). Mix should be on low side with above measuremeats. Gravity will be raised about .001 and index will be raised about .0004 by the addition of 1 inch of 1260*
If gravity or index or both are high, resample for gravity and index analysis. Moisture can be reduced by blowing with air. Chlorides can be reduced by additional earth
treatment.
10 - When all check analysis are in specs add Unox Epoxide 201,
(Ibis must be calculated from the assay),
.
11 - Circulate again by passing press for 3 hours.
12 - Put thru press 1 hour and take final samples. 3-5 Pt. .
bottles,
.
.
13 - After an additional 3 hours thru press ** blow and clean press.
ghw 9/12/63
R. C. Smith
PCB-ARCH-EXT0374513
'Oc.pi;> A--g46 - Operating Instructions
Transformer Pyr&nol A-13B3B Arcolos*' 1260 - 55/ TTCB
To make 14,000 gal, batch A-13B3B in #2 mix tank,
1 - Take X - 16 os, .eansple of,. Unox .Epoxide 201 for assay.
2 - Unload 6,000 gal, car of TTC3 to $2 mix tank (approx, 12*
in tank).
-
Pun?) 1260 from 8 storage to 256 *' in /2 mix tank.
.
4 Add.1 ~ bag afctapulgus earth.
5 Agitate with air and mechanical agitator and circulate by passing press? for 3 hours.
OC'
Circulate thru press for 1 horn1 and. take 1-5 pt, bottle
for check analysis- gravity - index - chlorides &. moisture.
7
Continue circulating thru press for 3 hours.
.
B Blow and clean press.
c> Correct.gravity and index (Cr. 1.563 - 1.571) (Index 1*5075 -
1,6085)* Mix should be on low side with above measure
ments.' Gravity will be raised about .001 and index will
be raised about .0004 by the addition of 1 inch of 1260.
If gravity or index or both arc high, resample for gravity
. and Index, analysis. Moisture car. be reduced by blowing
with air, Chlorides.can be reduced by additional earth
. .. treatment,
" .
IQ - blien all check analysis are in specs add Unox Epoxide 201. (This .must be calculated from the- assay),
21 - Circulate again by passing press far 3 hours.
.
12 Tut thru press:. 1' hour and taka final samples. 3-5 pt, bottles.
s;> After an additional 3 hours thru press - blow and clear, press.
rfV* y*
9/12/53
n. a. smith
PCB-ARCH-EXT0374514
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PCB-ARCH-EXT0374515