Document XOmQyg0GwMJnQnrDnNnOqZaYJ

Interoffice Communication to From B. E. Leach M. J. Allen Date March 20, 1984 Subject OXYCHLORINATION REACTOR CATALYST SAMPLING DURING MARCH 1984 TURNAROUND Catalyst samples from the Oxychlorination reactors at the Lake Charles VCM Plant were taken during the March 1984 turnaround prior to removal and disposal. In the past, the used oxy catalyst samples have been analyzed by R. J. Convers to determine the major causes of the catalyst deterioration. In continuing with this program, I have enclosed the oxy catalyst samples along with some plant operating data including hot spot temperatures and reduced pressure drops for the past run. Note, these catalyst samples are from the first run of the new oxygen-based oxychlorination unit (as opposed to the old air-based oxy). All samples are labeled with the reactor number, tube location (center or side), and height from the bottom of the tube sheet from which the samples were taken. The attached drawing gives a schematic of the three reactors with the approximate location of each sample. For each reactor, one tube near the center of the reactor and one tube near the edge of the reactor was sampled. Four samples were obtained from each of these tubes. Also, samples of the 2" raschig rings from the top of each reactor were taken. Also attached are the physical observations of the reactors during the sampling procedure. If you have any questions or need further information, contact me at ETN 640-5128. Process Engineer br cc: RAC-JWW-RB-MLA-MCM-PLF-DLD-PE VVC 000008044 OBSERVATIONS 1) The raschig rings on the top of R-301 were charred (sample Y), as usual. The charring, however, was only on the surface of the rings and did not include plugging of the rings with coke fines. 2) The raschig rings on the top of R-302 and R-303 (samples Z and AA) were <- slightly discolored but were not plugged with any sort of catalyst fines or carryover. 3) The catalyst in the upper portion of the tubes in R-301 was difficult to remove indicating the catalyst may have fused together. However, the catalyst in R-302 and R-303 came out very easily. 4) Catalyst samples were obtained by ramming a welding rod up through the bottom of each tube. This procedure may account for some of the powdering of the catalyst. The catalyst material was then caught in a plastic beaker as it fell down through the tube. The height of the sample was then measured. 0008045 PLANT OPERATING DATA End of Month June July Aug. Sept. Oct. Nov. Dec. Jan. Feb. End of Month June July Aug. Sept. Oct. Nov. Dec. Jan. Feb. Reduced Pressure Drop 2.4 2.4 2.3 2.5 2.8 3.4 3.9 4.8 6.2 R-301 Depth of Hot Spot Temperature (inches from top) 57 60 63 70 77 82 87 100 97 Reduced Pressure Drop 2.5 2.9 2.7 2.8 2.9 3.0 3.1 2.9 2.9 R-302 Depth of Hot Spot Temperature (inches from top) 39 50 67 67 74 74 77 75 77 Hot Spot Temperature C 249 252 255 247 253 258 249 263 266 Hot Spot Temperature C 253 256 256 251 259 267 262 267 271 0000080*0 WC End of Month June July Aug. Sept. Oct. Nov. Dec. Jan. Feb. Reduced Pressure Drop 2.2 2.4 2.2 2.3 2.4 2.5 2.8 2.7 2.7 R-303 Depth of Hot Spot Temperature (inches from top) 47 47 50 47 47 47 47 47 49 Hot Spot Temperature C 241 242 244 241 245 252 251 251 250 VVC 000008047 IL -9 J Z - % -W b o c^_ k- ~&- <T* V, i^^S2 e \ \ A ' o^\ l %V O <i ^ Cw \s e 5 cb ^^ 4^-*' ^ -- tf\ o Cu Qr&L \fNt- ^ * n & IK life ^S-% ICN f <SP * V -` tCk i ' ^<s t ^o O Vw cr* <jo c' Si CC&Vj.ili)U-'b=r -- -jai-i^.z: VVC 000008048 MARCH 1984 TURNAROUND DAY SHIFT vvc 00000804-9 Line No. 1000 1010 1020 103 0 1040 1050 1060 1070 1080 1090 3000 3010 3020 3030 Barry Bernard Employee tDoAJfc Employee No. Barry Bernard 0310 Larry Ogea 03 05 Glen Parker 0306 Harold Shoemaker 1001 Carl Powell Walter Hamraon ^ / James Meche is Nick Farris *^1------------- ------ 1002 1003 1004 1005 Andrew Buller"^ 1006 Keith Rover 1007 i Darryl Darbonne 1163 Ward Johnson 0\ 1^ 1164 Mark Talbott ^ Thomas Wilson ^ 1165 1166 Craft Code LF NW NW PF PF PF PF WL HF HF WL WL WL WL Rate Code 1 2 2 2 2 2 2 2 4 4 2 2 2 2 we 000008050 Line No. Emolovee Leon Cole EmDlovee No. Graft Code Rate Code 1100 1110 1120 1130 1140 1150 1160 1170 Leon Cole 0101 John Doucet 0103 Arvel Feemster 0104 Elridge Oquain 1008 Billy Stark 11 Asa Hoffpauir Louis King Bennie Gill ^ ^ <, l| A tt 1 1^ 4> 1009 1010 1011 1012 Lionel Guillory 1013 John Freeman -x" 1014 Ronald Orphey 1015 LC 1 LC 1 (2nd Week) TM 2 CP 2 CP 2 HE 4 HC 4 HC 4 Catalyst Loaders (2nd Week) 1210 1220 1230 1240 1250 1260 1270 1280 1290 13 00 1310 1320 1330 Phillis Breaux ^ David Feemster ^ Timothy Guillory*^ Ronald Jones ^ 1016 1017 1018 |\ 1019 Wayne Latimer Raymond Lavan Clifton Leday f .i /* 1 i 1020 1021 1022 Shirley Ledee / Curtis Lemoine'''^ 1023 1024 Patricia Manuel 1025 Tana Pike / 1026 Jeff Robinson ^ Donna Swaggart ^ & 1027 1028 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 vvc 000008051 Leon Cole (Cont.) Line No. EmDlovee EmDlovee No. 1340 1350 1360 1370 1380 13 90 1400 1410 1420 1430 1440 1450 1460 1470 Sherry Thompson 1029 103 0 Sheila Castille Ronald Guillory / Gary Jackson / /^ ^i * 1031 1032 1033 1034 Monica Miller^ melissa Moerbe ^ Thomas Riley / 1035 1036 1037 1038 Troy Ryder ' Alan Schwalbe ^ 103 9 1040 -TyM-hxlu Joseph Voussine ^ /f u. 1041 1042 yd -^ Craft Code Rate Code CW 5 GW 6 CW 6 CW 6 CW 6 CW 6 CW 6 CW 6 CW 6 CW 6 CW 6 CW 6 CW 6 CW 6 VVC 000008052 James Davis Line No. Enrolovee 1480 1490 1500 1510 1520 153 0 /James D, Davis Ed Moerbe ^ Lawrence Simon / Judson Obrien lommy Fletcher'^ 0 Dwight Stanley s' EmDlovee No. 0201 0204 0206 1043 1044 1045 Craft Code Rate Code LM 1 MW 2 MW 2 MW 2 HM 4 HM 4 VVC 000003053 Garland Linscombe Line No. 1550 1560 1570 1580 1590 1600 1610 1620 163 0 1640 1650 1660 1670 Employee 'yeuGr Garland Linscombe y Luke Dartez y Nelson Fontenot y Richard Arnold Mike Hoffpauir Jimmy Thibodeaux Douglas Brown Coy Stine James Hogan Max Adams wi Mark Denton ^ Jerry Duhon ^ John Landers Employee No. 03 03 03 09 03 02 1046 1047 1048 1049 1050 1051 1052 1053 1054 1055 Craft Code Rate Code LF 1 WL 2 PF 2 PF 2 PF 2 PF 2 WL 2 WL 2 WL 2 AM 2 HF 4 HF 4 HF 4 VVC 000008054 Russell Oquinn Line No. Emulovee Employee No. 1680 1690 1700 1710 1720 1730 Russell Oquinn 0205 James Cochran 0202 Jesse Coleman James Stine R,T. Edwards 1056 ^ 1057 T 1058 Paul Tramonte / 1059 Craft Code Rate Code LM 1 MW 2 MW 2 MW 2 HM 4 HM 4 vvc 000008055 Bob Shirley (Column Cleaners) (4th Day) Line No. Employee "pout Employee No. 1740 Bob Shirley 1750 1760 j Dale Hoffpauir 1770 ** K David Lamberth 1780 1790 1800 ( Lewis Moreno 1 Edward Pankiewiez ^Craig Richardson # 0404 1060 1061 1062 5-/U/1063 1064 1065 Craft Code Rate Code LB l CC 4 cc 4 cc 4 cc 4 cc 4 cc 4 VVC 000008056 Donald Vincent Line No. Employee *yo Employee No, 1810 1820 1830 1840 1850 1860 1870 1880 1890 1900 1910 1920 193 0 1940 Donald Vincent 0401 Phillip Bellow-^// Marvin Goss fi 0408 1066 1067 James Marburger . J Mark Clement 0 1068 1069 Charlie Fontenot ^ 1070 Louis Martin 1071 Larry Stanley David Meche ^ O'? n.-ft' # 1072 1073 Jerry Webb 1074 1075 Larry Trahan / 1076 Jimmy Smith --- 1077 1950 Gary Cobb 1078 Craft Code Rate Code LB 1 LB 1 BM 2 BM 2 BM 2 BM 2 BM 2 BM 2 BM 2 BM 2 BM 2 RG 2 RG 2 EO 2 HB 4 VVC 00008057 Phillip Leger Line No, Employee Emnlovee No. 1960 1970 1980 1990 2000 2010 2020 203 0 2040 2050 Homer Moseley Phillip Leger y Will Berzas Jesse Gautreaux s / Jimmy Bonnett y/}\ Patrick Conner Lester Logue George Olsen ./ ---- ^ Kenward Stine Danny McKinney. 0501 0503 0504 1 0502 ' 1079 1080 1081 1082 1083 1084 Craft Code Rate Code NW 1 LL 1 EL 2 EL 2 EL 2 EL 2 EL 2 EL 2 EL 2 EL 3 VVC 000008058 Jim Cook Line No, Emolovee Emolovee No, 2060 2070 2080 2090 2100 2110 2120 2130 2140 2150 2160 2170 Jim Cook 0601 Thomas Barton 0602 Darryl Derouen 0604 Hubert Fullerton * 0607 Richard Going 0605 Kermit Ryder Robert Landers .. -- ^ " Charles Hasting^^ 0606 0609 1085 Jody Miller/^ f/ 1086 Robert Rollins Leon Talbott il'W 3 Gregory Thompson ^ 1087 1088 1089 Craft Code Rate Code LN 1 IN 2 NW 2 IN 2 IN 2 IN 2 NW 3 IN 2 IN 2 IN 2 IN 2 IN 2 vvc 000008059 MARCH 1984 TURNAROUND NIGHT SHIFT 000003060 Johnny Burk Line No. --------------- Employee ----------- Do** Employee No, 2180 2190 2200 2210 2220 2230 2240 2250 2260 2270 2280 2290 2300 2310 2320 Johnny Burk Richard Lee Earl Robinson Davis Dennis ^ 0403 0407 1090 f^l091 Rogers Olivier William Dickerson Gilbert Perkins Robbie Robinson Donald Walton "" Homer White ? ft Thomas Perkins - O.C. Perkins Alva Perkins^ ,i 4< Ruston Benoits * Cecil Buller 1092 1093 1094 1095 1096 1097 1098 1099 1100 1101 1102 Graft Code Rate Code LB 1 LB 1 BM 2 BM 2 BM 2 BM 2 BM 2 BM 2 BM 2 BM 2 BM 2 RG 2 RG 2 EO 2 HB 4 vvc 000008061 Freddie Guillory Line No. Employee 2330 2340 2350 2360 2370 2380 2390 2400 2410 2420 Freddie Guillory Joe Adams Harvey Istre Raymond Prince Terry Cobb Tom Duraso v-Raymond Durousseau Fred Shillow ^ Fred Comeaux ^ ^ Curtis Leday*^ Employee No. & 0105 0102 0203 1103 7 1104 1105 1106 1 y 1107 1108 1109 Craft Code Rate Code LC 1 LC 1 TM 2 CP 2 CP 2 HC 4 HC 4 HS 5 HE 5 HE 5 (2nd Week) V m..* 'V**1 2430 2440 2450 2460 2470 2480 2490 2500 2510 2520 253 0 2540 2550 2560 Gilbert Adams ^ Roland Darbonne Mark Feemster Junious Guillory <y Paul Guillory; ^ David Heddins Katheryn Pettus y Randy Thibodeaux ' yCarl Trent Kenneth Trent ^ Doug Addison Vivian Babino Bertha Benoit Joseph Buller X 1110 1111 1112 1113 1114 1115 1116 1117 1118 1119 1120 1121 1122 1123 CW 5 cw 5 CW 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 5 cw 6 cw 6 cw 6 cw 6 VVC 000008062 Freddie Guillory (Cont.) Line No. 2570 2580 2590 2600 2610 2620 2630 2640 2650 2660 2670 2680 2690 Emnlovee Emolovee No,, Dennis Derouen ^ Christina Deville / 1124 1125 Trov Dubroc Brent Fetzer / Donald Guillory S S' Ivory Harris ^ 9 1126 i 1127 1128 1129 Tab Key S Clinton Lee ^ 113 0 \^y 1131 David Parker . 1132 Geraldine Rogers Elizabeth RolLo ^ 1133 1134 Leah Stoddard Bill Williamson ^ Aij) 1135 1136 Craft Code Rate Code CW 6 cw 6 CW 6 cw 6 cw 6 cw 6 cw 6 cw 6 cw 6 cw 6 cw 6 cw 6 cw 6 vvc 000008063 Larry Thompson Line No. Enrolovee Employee No, 1540 2700 2710 2720 2730 2740 2750 2760 2770 2780 Tom Hooper Larry Thompson Leonard Turner ^ Doug Owens X" Kenneth Moreland ^ Robert Hebert ^ TM Edgar Sonnier Connie Guidry ^ ^ Curtis Koonce I^ / J Mark Theriot 0301 0307 1137 1138 113 9 1140 1141 1142 1143 1144 Craft Code Rate Code TS 7 LF 1 PF 2 PF 2 PF 2 PF 2 PF 2 WL 2 HF 4 HF 4 VVC 000008064 Nelson Trent Column Cleaners 3rd Night Line No, Enrol ovee jilt Enrolovpfl No. 2790 2800 2810 2820 2830 2840 2850 Nelson Trent Alvin Anderson Mike Estes ^ Michael Nassar ^ David Rasmus s a James Thibodeaux^ / Steven Turner / / 0405 1145 1 1146 1147 1148 1149 1150 Craft Code Rate LB 1 CC 4 cc 4 CC 4 cc 4 cc 4 cc 4 H'1' ^ <<!// VVC 000008065 Line No. Enrolovee Kenneth Vincent dff Emolovee No. 2860 2870 2880 2890 2900 2910 2920 2930 2940 2950 2960 Kenneth Vincent Paul Vincent ^ 03 08 1151 Greg Fontenot - 1152 Phil Gillard Albert Blaha ^ 4 ' * 1153 1154 Thomas Benoit 1155 Henry Monticello S 1156 Timmy Hooper Clayton Gray John Shipp ^ fj /Jfh 1158 ^ 1159 Patrick Winey ^ 1160 Craft Code Rate Code LF 1 PF 2 PF 2 PF 2 PF 2 WL 2 WL 2 WL 2 HF 4 HF 4 HF 4 vvc 000008066 Line No,, Employee 2970 2980 Gordon Lyons Robert Trahan Electricians Employee No, 1161 1162 Craft Code Rate Code EL 2 HL 4 VVC 000008067 u> * Uj \ o uOo U, -X1 > T -sfl O - fru> U i \ sq r~ -4> <o o 0* s I 30 K wo *r9* \A Cv su S' o \ u. <A %- y V Vj a C S -<. *< Vcj f wa \ !b v Ui Jl> v ty o UI c S' *0 * c (A o P )h co e >cj- T 0 >z 4 S* Mt ift >- ?0 / cw n tl al OJ * s ft ft * c * G \ 4\ (A t- r* ft & % r* M '-v r/ it/o iW Q tv t / f j z w r v f < tA r^ %o UJ <S U| Nft NT Ui 8\ < >o (A h> to o u \s* "'Cl ? -4 r 0 \ V s\ N. c* \ V >0 \ ft 01 ^* >* N> O W 5^ * x> o tNfc o n n $> r Cj yo o n ta n <? 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