Document NezYrZ0Kw9YO067DYvXpVLjY8

1972 discontinued product U.S. DEPARTMENT OF LABOR Occupational Safety and Health Administration Fotrn Approved OMB No. 44 - R ] J87 MATERIAL SAFETY DATA SHEET SECTION 1 MANUFACTURER'S NAME EMERGENCY TELEPHONE NO Johns-Manville Corp. Subsidiaries 303/979-1000 Ext. ADDRESS (Number, Street, City, State, and ZIP Codej Ken-Caryl ftancn. Denver. CO 80217 CHEMICAL NAME AND SYNONYMS CHEMICAL FAMILY {TRADE NAME AND SYNONYMS NA ______B01 Insulatine Cement FORMULA NA 3119 SECTION II - HAZARDOUS INGREDIENTS PAINTS, PRESERVATIVES. & SOLVENTS TLV % (Units) ALLOYS AND METALLIC COATINGS PIGMENTS BASE METAL 0 ' TLV 4 (Units) I CATALYST VEHICLE SOLVENTS ADDITIVES ALLOYS METALLIC COATINGS FILLER METAL PLUS COATING OR CORE FLUX OTHERS r. J J: is? OTHERS HAZARDOUS MIXTURES OF OTHER LIQUIDS. SOLIDS. OR GASES Asbestos Fiber Natural Diatomaceous Earth Other - *See attachment 1 o TLV % 1 (Units) 15 * : 20 ... 15 ; mppcf 70:mppcf || !i BOILING POINT (F.) VAPOR PRESSURE (mm Hg.) VAPOR DENSITY (AIR3 1) SOLUBILITY IN WATER APPEARANCE AND ODOR SECTION III - PHYSICAL DATA NA NA NA Slight SPECIFIC GRAVITY (H20=1) PERCENT. VOLATILE BY VOLUME 4%) EVAPORATION RATE ( .. . =1) Grev Dowder - no odor SECTION IV FLASH POINT (Method used) FIRE AND EXPLOSION HAZARD DATA FLAMMABLE LIMITS EXTINGUISHING MEDIA Non-rfl-amma. b- le SPECIAL FIRE FIGHTING PROCEDURES 0.5 NA NA UNUSUAL FIRE AND EXPLOSION HAZARDS PAGE (1) (Continued on reverse side) Form OSHA-20 Rtv. May 72 CRMC-Thermo&Cement-000001 SECTION V HEALTH HAZARD DATA miUSHOLD LIMIT VALUf t r r ects oT"ove"re x"posu"re _ Section Expos ure_.tCL..excessive_amQunls disease. IT_______________________ of airborne dust may cause pulmonary ' EMERGENCY AND FIRST AID PROCEDURES STABILITY UNSTABLE SECTION VI - REACTIVITY DATA CONDITIONS TO AVOID STABLE X INCOMPATABILITY (Materials to avoid) None in Designed use. HA7ARDOUS DECOMPOSITION PRODUCTS NA HAZARDOUS POLYMERIZATION MAY OCCUR WILL NOT OCCUR CONDITIONS TO AVOID SECTION VII - SPILL OR LEAK PROCEDURES STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED Vacuum clean or damp sweep WASTE; DISPOSAL METHOD L.Disp_Q.S-_in closed containers . SECTION VIII - SPECIAL PROTECTION INFORMATION TP i RATO ft Y PROTECTION {Spcuh' tifH )' vi ntilation LOCAL EXHAUST MECHANICAL H,enfrail SPECIAL OTHER PROTECTIVE GLOVES Ttif R PROTECTIVE EQUIPMI N1 3 EYE PROTECTION SECTION IX - SPECIAL PRECAUTIONS , PRECAUTIONS TO BE TAKEN IN HANDLING AND STORING i OTHER PRECAUTIONS mg dusts. d oc AE '' While the information and recommendations set forth herein are believed to be accurate as of the date hereof, Form osha-20 JOHNS-MANVILLE CORPORATION MAKES NO WARRANTY WITH RESPfecf THERETO AND DISCLAIMS ALL LIABILITY FROM RELIANCE THEREON. CRMC-Thermo&Cement-000002 r - ::'- - Industrial Insulations Waukegan Plant February 12, 1971 D. B. Wingepter - Manville Plant C. L. Mesecve - Finderne . Librarian - Research Center D. P. Chard A. W. Swanson cc: W. K. Hesse - Research J. A. Me Cague File/ MANUFACTURING SPECIFICATION II-4336-1 #301 CEMENT P. B. Wingerter's letter of February 8th serves as approval to cancel the Manufacturing Specification for #301 Cement, II-4336-1. This product has been removed from the line as of 1/1/71 by the Product Manager. Please remove all copies from your files. yr' ' - . C. H. vflZNSEN CHJ/jaa CRMC-Thermo&Cement-000003 FINISHED PSODUCY SPECIFICATION PRODUCT: NO. 301 CEMENT I. MANUFACTURING LOCATION: Waukegan II II. GENERAL DESCRIPTION: This product is a one-coat Hydraulic Setting Insulating and Finishing Cement. III. OUTSIDE SPECIFICATION TO BE MET: (When required) ASTM-C-449-64 SS-C-160 (Type III, Grade F) U. S. Coast Guard certificate of approval 164.009/95/0 IV. PHYSICAL PROPERTIES AND REQUIREMENTS: A. Density (TM-II-433-16) Maximum - 21.0 pcf B. Wet Adhesion (TM-II-433-13) Adhere for minimum of 30 minutes. NOTE: In case of adhesion complaints, the referee Test Method shall be 11-433-17. This test may be performed with cement having 35% to 45% deformation; however, if failure occurs, retesting is required with cement having 8% to 15% deformation for final disposition. C. Dry Coverage (TM-II-433-15 or ASTM-C-166) Minimum - 30.0 Bd. ft./lOO lbs. 1 As t I 1 D. Volume Shrinkage (TM-II-433-19 or ASTM-C-166) -r Maximum - 10.0% ^ , .--------- - --- ----------Jf4_ E. Deformation /(JFM-II-433-"8 or ASTM-C--34-)l Immediately after mixing , Minimum 40.0% 2-1/2 hrs. after mixing 2.0% Maximum 60.0% 10.0% PLEASE RETURN\ i V i-M RESEARCH X-- CHANGE ES --REASON' General Revision LIBRARY (MM) AUTHOR STY FOR CHANGE D.B. Wingerter per Approvals to Proposed FPS dated 4/23/69 SUPERSEDES! DIR. M6R. 8.C. O.C. Page 1, FPS-II-4336.-1. dated 7/28/67 V fchr/X*' SUPR. PROD. PLMT. m/l Q.C. SUPT. PM. LAB. ! P.T. Buche lIlSUID 3/10/70 CRMC-Thermo&Cement-000004 Jehat-Maovlllo FINISHED PRODUCT SPECIFICATION PRODUCT) NO. 301 CEMENT PIVWOH SPEC. NO. PACE NO. II 4336-1 2 of 2 V. TEST FREQUENCY: Property Frequency A. Performaed by Plant 1. Density Test a minimum of once per day when produced. 2. Wet Adhesion Test a minimum of once per day when produced. 3. Dry Coverage Test a minimum of once per week when produced. 4. Volume Shrinkage Test a minimum of once per week when produced. 5. Deformation Test a minimum of once per day when produced. B. Performed by Research 1. Thermal Conductivity (for SS-C-160) Test a minimum of once per year. VI. PACKAGING: Packaged 50 lbs. net per bag in a 3-ply printed valve type paper bag (P.S. 11-9027). Stencil date of cement manufacture on bag in code as follows: eg: 4 188 = Decoded date = 4188 Year 1964 188 Day of year 7/6/64 PLEASE RETURN TO * CINHDAINCGAETES AUTHORITY POR CHANGE REASON: General Revision IIRR4RV ({vM D.B. Wingerter Per Approvals to Proposed FPS dated 4/23/69 SUPERSEDES) DIR. NCR. o.e. .C. New Page \)KiVf n SUPR. 1 PROD. PLNT. MX Q.C. | SUPT. PN. LAB. P.T. Buche | Issued 3/10/70 CRMC-Thermo&Cement-000005 Waukegan IID #301 CEMENT 4336-1 > 1 GENERAL DESCRIPTION This specification describes the manufacture of #301 Cement which is used as a one coat hydraulic setting insulating and finishing cement. Jut* ! II. FORMULA I PURCHASE SPEC. NO. | 1065 1185 1952 ; ------- INGREDIENTS 7M13 Fiber. 4220 Fiber ` Hi Early Portland Cement M&D Clay White Mineral Wool * Celite 392 TOTALS WEIGHT 150# 50 235 450 280 200 1365# PERCENT 11.0 3.7 17.2 33.0 20.5 14.6 10Q.0% * An equivalent uncalcined grade of Celite may be used if necessary. III. OPERATIONAL SEQUENCE 1) Mixing Procedure Step 1 2 bags - White Mineral Wool 3 bags - M&D Clay ' I bag - Hi Early Portland Cement 1 bag - Celite #392 Weight 70# 150 94 50 Step 2 2 bags - White Mineral Wool 2 bags - M&D Clay . 1 bag - 7M13 Fiber 1 bag - Celite #392 ' 70 100 100 50 Step 3 2 bags -- White Mineral Wool 2 bags - M&D Clay 1 bag - Hi Early Portland Cement % bag - 4Z20 Fiber 1 bag - Celite #392 70 100 94 50 50 PLEASE RETURN TO J-M RESEARCH 1 V INOICATES r.-- CHANGE -- AUTHORITY FOR CMAN3E LIBRARY (MM) *Revi*sibn"made~to show packaging changes and 'delete reference to Richmond Wool D. B. WingerterTs letter to C. H. Jensen dated 11/5/70 SUPERSEDES: Page 1 thru 2, same spec, dated 7/21/69 G.O.C. KGK. G.C. OVi it* PP.C-C. o.c. SU?T. punt. ! gWl FiN- i l j |j jj ISSUFR 12/23/70 CRMC-Thermo&Cement-000006 #301 CEMENT ;Waukegan 1JD j: 4336-1 :i 2 l 111 OPERATIONAL SEQUENCE (cont.; j Step 4 2 bags - White Mineral Wool 2 bags - M&D Clay % bag - 7M13 Fiber 1 bag - Celite #392 h bag - Hi Early Portland Cement TOTAL Weight 70# " 100 50 50 47 1365# | IV. MANUFACTURING INSTRUCTIONS 1) After mixer is filled, reverse mixer and mix for five minutes. V. PACKAGING 1) Reverse mixer - draw mix into multi wall valve type bags - 50 lbs. per bag '(paper) or 25 lbs. per bag (plastic). 2) For export shipments, a special waterproof valve type plastic lined burlap bag is used. \ Purchase Spec, Material 11-9027 11-9033 11-9029 Paper Bag for #301 Cement Plastic bag for #301 Cement Waterproof bag for #301 Cement VI 3) Code date per Finished.Product Specification. Code is stamped on top of bag close to valve. %V't .vi. PROCESS COZnTKOL CHECK 1) Take a one bag sample from each lot and submit to laboratory for control tests. ` '* - ---- --' > iv`T l ,, " c ; i ihin;:.; URN TO J-M RESEARCH LIBRARY (MM) Revision made to show packaging changes and delete reference to Richmond Wool D. B. Wingerter's letter to C. H. Jensen dated 11/5/70 Pages 1 thru 2, same spec, dated 7/21/69 V::V, 12/23/70 CRMC-Thermo&Cement-000007 ufi nZ-;-i2.:V:. i iO i'"Mi'i U FAuTLJ RIN G SFECiriCATIOM #301 CEMSET SPEC no. PAGE MO. Waiiliegaa HD j; 4336-1 ii 1 FORMULA. SPEC. 1T0 1065 1185 inGREDIEHTS 7M13 Fiber 4Z20 Fiber Hi Early Strength Cement M & D Clay Richmond Granulated Wool Sealtite Granulated Wool Celite 392 / Totals MPG. SPEC. WT. 'TfJt 150- 11.0 50 3-7 235 17.3 450 33.1 275 20.2 -- 200 14.7 13S0 100.0 ALTEEKATE WT. 150 11.0 50 3.7 235 17.2 450 33.0 -- m 280 20.5 200 14.6 2355 100.0 * An equivalent uncalcined grade of Celite may be used if necessary ** 4T30 or 4zi2 fibre c are approved alternates for 4Z20 II. MANUFACTIJRII5C- PROCEDURE a. Mix in #109 mixer -with mixer reversed b. Charge ingredients as follows: Step 1 1.3 bags - Richmond Granulated Wool 2. .3 bag3 - M & D Clay 3. 1 bag - Hi Early Portland Cement 4. 1 bag - Celite 392 Step 2 5 3 bags - Richmond Granulated Wool 6. 2 bags - M & D Clay 7. 1 bag - TKL3 Fiber 8. 1 bag - Celite 392 75# 150# 94# 5C# 75# 100# 100# 50# c. $ *SP-2 9* 3 bags - Richmond Granulated Wool vj 1C. 2 bags - M & D Clay 11. 1 bag - Hi Early Portland Cement $ 12. bag - 4Z20 Fiber 13. 1 bag - Celite 392 75# 10Q# 94# 50# 5<# Step 4 14. 2 bags - Richmond Granulated Wool 15. 2^38 - M & D Clay -- --------- - 50# 100# 16. 1/2 bag- 7M13 Fiber 50# 17- 1 bag - Celite 392 50# < 18. ^ bag - Hi-Early Portland Cement /> 13S0# 3 jg J-M RESEARCH 3 LIBRARY (MM)CL x"* 'change8 --REAS0N: Show Sealtite Wool as an approved alternate < CSJ AUTHORITY cnr>o FOR CHANGE D. B. Wingerter's letter to C. H. Jensen dated 7/16/69 SUPERSEDES: Page 1, same spec, issued 16/3/68 MGR. 5.C1.C. MGR. O.C. supr. I prod, i purr. JQ.G. j SUPT. [ H(t`. DATE CRMC-Thermo&Cement-000008 AOhnS-i'-'i'jE'/iiW MAMUrAGTLfilNG ! SPECIFICATION i -;) s . tOi GiMEEJ' ; SLANT & Div. ; SPEC NO. 1; j ?AGE NO. Waukegan : X 4336-1 2. _ _ _ .... c. Charge ingredients as follows for a2.tertr.te formula: Alternate Fcwil Step.1 1. 2 begs - Sealtite Granulated Wool 2. 3 bags - M & D Clay 3 1 bag - Hi Early Portland Cement 4. 1 bag - Celite 392 70if 150# 9 5c# Step 2 5- 2 bags " Sealtime Gsamrtated Wool 6. 2 bags - M & D. Clay 7. 1 bag 7M13 Fiber 8. 1 bag Celite 392 m 10c# 10c# 50# Step 3 9. 2 bags - Sealtite Granulated Wool 10. 2. bags " M 2: D Clay 11. 1 bag - Hi Early Portland Cement 12. bag - 4T.30 Fiber 13 - 1 bag - Celite 392 7C# 10c# 9 50if 5 Step 4 14. 2 bags - Sealtite Granulated Wool 15 * 2 bags ~ M & D Clay 16. -a- bag - 7M13 Fiber 17. 1 bag - Celite 392 | 18. t beg " Hi Early Portland Cement .1). PACKAGIECr PROCEDURE 7C# 10c# 50# 50# . jf 136^ 1. Reverse sixer for five minutes. 2. Draw mixture through auger bagger into valve type paper bags until the the net weight per bag is 50 lbs. Adjust setting if necessary to obtain correct weight. Weigh at least one bag per batch. Purchase Spec II--9027^' * Material 301 Cement 3 Cede Cate per Finished Product Specification, Code is stamped on top part of bag close to the valve. 4. For export shipments, a special waterproof valve type bag is used when ordered. P.3, 11-9033.* 5. One sample per day will be checked for wet adhesion and density. One sample per week will be submitted to the Quality Control 'Xaboratory fox*. complete testing. pj:- . ._iO*m INDICATES CHANGE ' -REASON: AUTHORITY FOR CHANGE J-M RESEARCH .LIBRARYShow Sealtite Wool as an approved alternate (MMS. D. B. Wxngsrter's letter to C. H, Jensen elated 7/16/69 SUPERSEDES: Page 2 same spec. issued .10/3/68 M3R, j MGR. | SUPS. KIOf.E ! ELNT. G.Q.C. I o.C. 1 0.0. :W, ! afj j....... il 7/21/69 CRMC-Thermo&Cement-000009 J:nn3-r-i"avi!iS MANUFACTURING SPECIFICATION PRODUCT: PLANT A. DiV. r j SPEC NO. i RASE NO. ;'oi: r-^r.v, ; I FORMULA Spec No. -- -- 1065 1165 -- -- Ingredients m3 Fibre 4T30 Fibre ** Hi-Early Strength Portland Cement M ;s D ClayRichmond Granulated-Wool Celite 392 * Wei gilt 150 50 235 450 275 200 Percent 11.0 3-? ' 17.3 53.1 20rg-- 14.7 TOTAL 1360 lbs 10070 * An equivalent uncalcined grade of Oolite- nay be used if necessary ** 4Z20 or 4Z12 fibres are approved alternates for 4T30 II. MANUFACTURING PROCEDURE a. Mix in #109 mixer with mixer reversed b. Charge ingredients as follows- Step 1 1. 3 bags - Richmond Granulated Wool 2. 3 bags - M & D Clay 3. 1 bag - Hi-Early Portland Cement 4. 1 bag. - Celite 392 75# 150# 9 50# Step 2 . 5. 3 bags - Richmond Granulated Wool 6. 2 bags - M & D Clay ' 7. 1 bag - 7M13 Fibre 8. 1 bag - Celite 392 75# 100# 100# 50# Step 3 9. 3 bags - Richmond Granulated Wool 10. 2 bags - M & 0 Clay 11. 1 bag - Hi-Early Portland Cement 12. i bag - 4T30 Fibre 13- 1 bag - Celite 392 75# 100# 94# 5C# 50# Step 4 14/ 2 bags - Richmond Granulated Wool 15- 2 bags - M 5s D Clay 16. ^ bag - m3 Fibre 17. 1 bag - Celite 392 18. % bag - Hi-Early Portland Cement i$ PLEASE RETURN 1% J-M RESEARCH ^ LIBRARY (MM) L n xX~ ICNHDAICNACTEES --RRErAieSrOuNj.! AUTHORITY FOR CHANGE x - SJww'propecr authority tor change to Richmond Wool D.. B. .Uinartar:s Ut;-taar to D. Zelanko . . . SUPERSEDES: MGR. G.Q.C. MGR. o.c. SUPR. Q.C. Page 1, same spec- Issued <>--68 PRoa' 1 ' PUTT. 1 RES. I SUPT. FIN. LAB. H DATE ISSUED 10-3-68 1 ! i1! 1 i11 CRMC-Thermo&Cement-000010 Johns-..uriVi.is MANUFACTURING SPECIFICATION 1 .J: U L* jT: #30.1 Cement !, n.\/ .............. SFC K0- 1 .. . II auxeGaxi ;! 4336-1 * -. PAGE WO. || x rOHMUIA Spec No. -- -- 1065 1185 -- -- Ingredients 7M13 Fibre 4T30 Fibre Hi-Early Strength Portland Cement M 1 D Clay Richmond Granulated Wool Celite 392 * TOTAL ` Weight 150 50 235 450 275 200 1360 lbs Percent 11. C 3-7 17-3 33.1 20.2 -14.7 100.0 * An ej_ui'/alent uncalcined grade of Celite may be used if necessary ** 4Z20 or 4Z12 fibres are approved alternates for 4T30 II. MANUFACTURING PROCEDURE a. Mix in #109 mixer with sixer reversed b. Charge ingredients as follows- Step 1 1* 3 tags - Richmond Granulated Wool 2. 3 bags - M & D Clay 3. 1 bag - Hi-Early Portland Cement 4. 1 bag - Celite 392 75# 150# 9 5C# Step 2 5. 3 bags - Richmond Granulated Wool 6. 2 bags - M D Clay 7. 1 bag - 7M13 Fibre 8. 1 bag - Celite 392 75# 10Q# 100# 50# Step 3 9- 3 bags - Richmond Granulated Wool 10. 2 bags -M & D Clay 75# 100# 11. 1 bag - Hi-Early Portland Cement L 12. | bag - 4T30 Fibre 9 5 Or 13- 1 bag - Celite 392 ..... .... ____ . . .. 50# Step 4 14. 2 bags - Richmond Granulated Wool 15- 2 bags - M & D Clay 16. | bag - 7M13 Fibre 17. 1 bag - Celite 392 18. \ bag - Hi-Early Portland Cement 50# ^ please return RESEARCH gwIlBRARy (mm) X-- KBS? --REASON: X - To show mixing steps C AUTHORITY FOR CHANGE Memorandum dated 11-9-67, L. Blair and D, B. Wingerter SUPERSEDES; Page 1, same spec* issued 2/5/68 MGR. I MGR. G.Q.C. j Q.C. SUPR. ac. proo. SOPT. PUTT. FIN. RES. LAB. DATE ISSUED 5-5-68 CRMC-Thermo&Cement-000011 Johns-Manvilla MANUFACTURING SPECIFICATION I. FORMULA PRODUCT; #301 Cement jt PUNT L D'V. jjWaukegan IID SPEC MO. PAGE MO. jj 4336-1 i----------------------li 1 Spec. No. -- -- 1065 1185 . Ingredients m3 Fibre 4T30 Fibre ** Hi-Early Strength Portland Cement M & D Clay Sealtite White Wool *** Celite 392 * TOTAL Weif&t 150 50 235 450 280 200 135T Percent 11.0 3-7 17.2 . 33.0 20.5 14.6 100.0 * An equivalent uncalcined grads of Celite say be used if necessary ** 4Z20 or 4Z12 fibres are approved alternates for 4T30 *** Richmond batt scrap is an approved alternate II. mUFACTURDIG PROCEDURE A. Mixing Procedure TI Mix in #109*mixer with mixer reversed 2. Charge ingredients as follows: 1. 2 bags - Sealtite White Wool 2. 3 tegs - M & D Clay 3. lteg - Hi-Early Portland Cement 4. 1 hag - Celite 392 70# 150# chS 5C# Step 2 5. 2 tegs - Sealtite White Wool 6. 2 bags - M & D Clay 7. 1 bag - 7M13 Fibre 8. 1 bag - Celite 392 Step 3 9. 2 bags - Sealtite White Wool 10. 2 bags - M & D Clay 11. 1 teg - Hi-Early Portland Cement 12. teg - 4T30 Fibre 13* 1 teg - Celite 392 7C# 100# 100# 50# 70# io<# 9 50# . 5<# ----- tSEJL 14. 2 tegs - Sealtite White Wool 15. 2 bags - M & D Clay 16. bag - m3 Fibre \17. 1 teg - Celite 392 18. teg - Hi-Early Portland Cement *X ICNHDAICNAGTEES RpEcAASsOoNM: . vX - Show use of Sealtite White Wool 70# 100# 50# 50# 47f 1365# PLEASE RETURN TO AUTHORITY FOR CHANGE SUPERSEDES: S Lane's enactment letter of 6/13/68 J-M RESEARCH Bags 1, same spec, issued 2/5/68 LIBRARY (MM) MGR. G.Q.C. MGR. O.C. SUPS. Q.C. PROS. SUPT. PLOT. m FIN. DATE ISSUED 8/23/68 CRMC-Thermo&Cement-000012 . Form 333-2-A Ptd. In U.S.A. .Johns-Ma. v:!lo MANUFACTURING ! SPECIFICATION pnonccr. ' #301 Cement ""-t" SPEC NO. PAGE NO. '--auix. c 1 :; Ii| 41,30.-3.-0|i I FORT-AULA Spec. No. -- -- 1065 1185 -- Ingredients 7M13 Fibre - 4T30 Fibre * Hi-Early Strength Portland Cement M Si D Clay Richmond Granulated Wool Celite 392 * Weight 150 50 235 450 2T5 200 `ereetr: 11.0 3.7 17.3 33.1 2C.2 14.7 TOTAL 1360 lbs 100.0 * An equivalent uncalcined grade of Celite nay be used if necessary ** bz20 or kZl2 fibres are approved alternates for 4T30 II. MANUFACTURING PROCEDURE a. Mix in #109 mixer with mixer reversed b. Charge ingredients as follows- Step 1 1. 3 bags - Richmond Granulated Wool 2. 3 bags - M & D Clay 3. 1 bag - HUSarly Portland Cement 4. 1 bag - Celite 392 75# 150# 9 50# X /Ap . 'V1 >1 X { s* Step 2 5. 3 bags - Richmond Granulated Wool 6. 2 bags - M & B Clay 7. 1 bag - 7M13 Fibre 8. 1 bag - Celite 392 Step 3 9- 3 bags - Richmond Granulated Wool 10. 2 bags -.M & D Clay 11. 1 bag - Hi-Early Portland Cement 12. j bag - 4T30 Fibre 13- 1 bag - Celite 392 75# 100# 100# 50# 75# ioc# 9 5C# Step 4 ITT Richmond Granulated Wool 15* 2 bags - M & D Clay 16. | bag - m3 Fibre 17. 1 bag - Celite 392 03 18. ^ bag - Hl-Early Portland Cement 3s 50# 100# 50# 5# PLEASE RETURN 13--< >M RESEARCH L i ^KSP-**so* X - To shew nixing steps LIBRARY (MM) N< AtfmoRnY $m FOR CHANGE Memorandum dated 11-9-67, L. Blair and D, B. Wlngerter SUPERSEDES: Page 1, same spec* issued 10-19-66 MGR. G.Q.C. MGS. Q.C. SUPS. Q.a PRoa SUPT. wPtNT. nr*. DATE ISSUED 2-5-68 CRMC-Thermo&Cement-000013 CRMC-Thermo&Cement-000014 . . iii r MANUFACTURING SPECIFICATION I. FORMOIA Spec Bo. X e 1COO 1185 301 Ces3xt . \ V. . f/r\ :\'2 v- spec no. PAGE NO. j 11 4336-1 |1 4 ' : . <c'euv `cT /J Iagredleata Welftfet Percent 5 KsponrteA Perlite Lwnlte Ceeent MAD day Rlebaaad Graimlated Vool Cdlte 392* SOttL 16 282 650 375 iM 1.2 20.6 vr.3 e?.3 3.6 isfe / 3 ii /*. / *ka tvoliilnk end* ocf Cellte H. MMOTACIQRDC PBOCSDCBE a. KLx la #109 alxcr nth b. Qmxam lagredlwfce a follow ' 1. % - 2. k - 3. 11 Gwilrtofl Vool MAD Clay Ionite - CaOlte 392 rl 1/2 10. 3 1 11. 11 02. 1/2 13. 1/3 1%. 3 * 15. 3 16. l -MAD Clajr Perlite - Cellte 392 MMmM Onaelated Vool -MAD day - Perlite - Cellte 392 - HMwnwit Qwu--leteA Wool -MAD day be wed it 100# 9 IT# 15C# 8# IT# & % 1*# 75# 15C# tM vvrx (P.8. ZZ-902T) end then dear off lato 5C# wire type C INDICATES _BF.cn-, X CHANGE -REAS0*11 i SUPERSEDES: KSK GAC. HM. SUP* o& OC. MOO. supt. PINT. PIN. Ml lab. ^TT 8-16-66 PLEASE RETUftR'' 'TO' J-M HtSSl'i LIBKAKV IMMf BATE 9-9-66 CRMC-Thermo&Cement-000015 2 V. V. . Vj A' Jcf.riS-i-ia'iYiiie MANUFACTURING SPECIFICATION I. FORMJIA Spec Bo. 1C00 1183 * -J u J i: 301 Cssccst c\ u;V. j 1 VJaviissan IID SPEC NO. 4336-1 PAGE NO. 1 Ingredients ,. 8-*^ Rapandad Perlite Laenite Ceaent M & D day HichaoMd Grennlatad Wool cellte 392* SOUL Weight 16 282 630 373 Percent 1.0 20.0 47.5 28*5 -IS 100.0 *An eq.uiTaleat encaleined grade of Cellte be wed If OBceuary. H. IftflUFACTOHIHB PBDCBDOHB a. Nix in #109 nlxer vitb b. Charge Ingredients ea fbUove: 4 bags - Blefemad Granulated Wool 4 bags - M ft D day 3. 1 bag - Loanita Cernat 4. 1/3 bag - Cellte 392 3. 4 bags - mafeaoad ftraatflatad Wool 3 begs - M ft D day 1/2 bag - Perlite 8. 1/3 1*8 * Cellte 392 9. 4 bags - Blekasad GrassOated Wool 3 bam - M 4 D day 1 bag - Lawita 1/2 tag - Perlite 1/3 bag - Cellte 392 3 begs - Blehsond oramlated Wool 15. 3 bags - N & 0 day 1 bag - Lonite fOML 10c# 20c# 9 17# 100# 150# 8# ' 17# 10c# 150# 9 a# 16# 75# 150# T3$ far 5 atimtes and than dm off Into $0# win type bags (P.S. XX-9027) j.M \r: x- cKtP -REAS0"** Bailee tM AUTHORITY FOR CHANGE btiee of enamel Bos FP 433-74 dated 4-29-66 SUPERSEDES: sea GJOtJC. HQ& O.C. sunt Q.C. PROD. SUPT. 1, PLNT. ON. RES. US. Lab. 6-11-64 DATE ISSUED 8-16-66 CRMC-Thermo&Cement-000016 MANUFACTURING SPECIFICATION #301 CEKEHT vlV. spec :;o. PAGE NO. jl 4336-1 uV' I. POHMOIA Spec. Ho. Ingredients ` Weight Percent - 1065 1185 - - 7X13 Fibre 4T30 fibre** Hi-Early Strength Portland CeMaat M & D Clay Rlchaond Granulated Wool CeUte 392* 150 11.0 50 3.7 235 17.3 450 33.1 275 20.2 200 14.7 TOTAL 1360 lbs. 100.0 * An equivalent uacalclsed grade of Cellte nay be used if necessary. ** 4220 or 4Z12 fibre* are approved alternate* for 4T30. II. MAMOIACTCRIBO PBOCKDPHK a. Mix in #109 mixer vith Mixer reverted. , b. Charge ingredienta aa follova: 1. 3 baga - Rirhaond Granulated Wool 2. 3 bags - M & 0 Clay 3. 1 bag - Hi-Early Portland Caaot 4. 1 bag - Celite 392 5. 3 baga - Rlchaond Granulated Wool 6. 2 baga - M & D Clay 7. 1 bag - 7X13 fibre 8. 1 bag - CeUte 392 9. 3 KLrhMnnd Granulated Wool 10. 2 MAO Clay 11. l bag - Hi-Early Portland Ceaent 12. 1/2 bag- 4T30 fibre 13. 1 bag - Cellte 392 1*. 2 Biebnoad Granulated Wool 13. 2 hi M *0 Clay 16. 1/2 7NL3 fibre 17. l bag - CeUte 392 18. 1/2 bag- Hi-Early Portland Caaant TOTAL 75# 15<# 94# 50# 75# IOC# 100# 50# 75# 10c# 94# 50# 50# 50# 100# 50# 50# J&L 1360# e. Eeeerae aixer for 5 ainutea and then draw off into 50# valve type paper baga (P.8. U-9027) BSP "REAS0W: Revise Ponmla AUTHORITY ,, FOR change E. C. Lindatrae's letter to C. H. Jenaen dated 6-10-64 SUPERSEDES: PM* 1 NCR. MM. SUM. fnoo. C.QX. OX. O.C. sun. apee. issued 5*28-62 PINT. d.tjgs 1-- FIN. WL lab. 1 DATE ISSUED 6-11-64 CRMC-Thermo&Cement-000017 FORMULA ; Spec. Mo. Ingredients r*'i ** ''"RIB) ! i- 7ia3 Fibre i>Z20 Fibre * 150# 50 | 1065 lli-Early Strength Pci`bland cement 235 Celite #395-A* i P.S. 1185 M&.D Clay i Eatt Scrap Total 2 CO 1*50 250 Ammnn 1335# v-An equivalent uncalcined grade of Celiis amy be used if necessa: aUZ12 Fibre is an approved alternate for UZ2Q. Ho K/liiUFACTURIUG PROCEDURE . a* JQx in #109 mixer tilth mixer revere-.?, ba Charge ingredients as follows: lo 3 tags Ricbnond Eatt Scrap 2. 3 bags M& D Clay 3* 1 bag Ex2arly Portland Ceraeat ko 1 bag Oolite #'3?5~A 5* 3 bag3 Richmond Eatt Scrap 6o 2 bags M & D Clay 7* 1 bag 7ICL3 Fibse 8. 1 bag Cents #395=A 9. 2 bags Richmond Eatt Scrap 10. 2 bags M& D Clay 11a 1 bag Hi^Early Portland Cement 12 l/2 bag iiZ20 fibre 13 1 bag Collie #3?5=A 111* 2 bags Richmond Bait Scrap 15. 2 Bags H & D Clay 16. 1/2 bag 7KL3 fibre 17. 1 bag Celite #395=>A 18. 1/2 bag KiEarly Portland Cement Total 75# 150 9U 50 75 ICO 100 5o 5o 100 9h 50 50 50 100 50 50 hr 1335 lbs `-V 11.2 3.7 17.6 15.0 33.7 _18.8 100.0 CRMC-Thermo&Cement-000018 pass ;:o. l-Oi'kVi .ui SgQG o iJo o i-agrgfJionT&a Woieht AS1rf=l50=>^2) Typs in ) = P.S. 6H85-U 7W13 Fibre % i}220 Fibre ^ Hi-Early Strength Portland Cevsnt ^-Caliti #395=A H &D Clay 3att Scrap . ........ 150# 50 235 200 1*50 250 lin 2 3c7 17,6 15 o0 33,7 13* 3 Total 1335# 100,05? ' - **An equivalent uncalcined grade of Ciite may be used if` necessary* iii, hanufactbhieq procedure A. Kis in #109 mixer with mixer reversed. B0= Charge ingredients as fellows: 1, 3 bags Richmond Batt Scrap 2, 3 bags M & D Clay 3, 1 bag Hi-eariy Portland Cement ho 1 bag Cellto #395=A 5, 3 bags Ricbaand Batt Scrap 6, 2 bags M & 3 Clay 7o 1 bag 7M13 Fibre 8, 1 bag Celite i?395=A 9, 2 bags Richmond Batt Scrap 10, 2 bags M & D Clay 11, 1 bag Hi-Early Portland Cemont 12, 1/2 bag liZ20 Fibre 13, 1 bag Celite #395=A 111, 2 bags Richmond Batt Scrap 15* 2 bags M & D Clay 16. 1/2 bag 7M13 Fibre C 17. 1 bag Celite #395=A 18. 1/2 bag Hi-Early Portland Ceaent 75# 150 9h 50 75 100 100 5o 5o 100 RETURN to 9li 50 J-M RESEARCH 50 5o FILE ROOM 100 5o 5o ii7 ' Total 1335 lbs. Reverse mixer for 5 minutes and then dratr off into 50# bags. ( P.S. 68169) C v INDICATES Bc..en.. X~ CHANGE "REASON: Show use of fibre in place of IiM28 Fibre AUTHORITY / FOR change B.C. Lindstrom1 s letter/bf 7=lU-58 to C,,H. Jensen enpppepnFC* DIR. Q.C. MGR. Q.C. BoP Page 1, same spec. ^leaded 7-26-5L & Cancels Dev* #103 dated 6-5-58 SUPR. PROD. PLNT. 1 -- DATE Q.C. SUPT. FIN. Mo-1. lab. ISSUED WWW CRMC-Thermo&Cement-000019 ,/ '\ , \J ' MANUFACTURING SPECIFICATIONS Gscent -DEPT. -PLANT PRODUCT: 301 Ccscnt DIVISIONtll 133 51*26 PACE NC 1 7. BCUKtfXA Psycho Spec. A2Z& 0150-52) TJpo in ) 6liS54i Ingredients ^%-.iiemT i*1-* i ii m ii t n !! n sirs nfun iiT 73K13 Fibre ttsifht 150^ 1023 Fibre 5o 3L Sarly Strength Portland C errant 235 Ca31ta #395* H !-. D Clay Batt Scrap SCO U5o 25C Jl'WTO- % 11.2 3.7 17.6 15.0 33.7 18.8 itnr *An equivalent uncalcdztod grade of Calita say bo used if noccccary. Ho PATTUFCATURIBG SROCKD;JPS A, l&x in #10? wise? *itU d:;or rfrrsrsad- Bo Chargo Ingradioate as foiled i 3.o 3 baga 355-chsscna Eatt Earan 2o 3 baj a & D Glaser 3 1 bag Hi Syrly Portland Ceaisni ii. 1 bag OeUta 3?5<=A 5, 3 bags Richmond B&tt Scrap 6e 2 bags H%D Clay ? 1 bag 7M13 Fibre 8, 1 bag Cent* 395A 9. 2 bags Richmond Batt Scrap 10. 2 bags HID Clay lie 1 Bag Hi Early Fortland Caaant 12. 1/2 Bag 1^126 Fibre 13. 1 bag Calita 395-A lb. 2 baga Xlebacod Batt Scrap 15. 2 baga M ft B Clay 16. 1/2 bag 7K13 Fibre 17. 1 bag Calita 395-* 18. 1/2 bag Hi Erly Portland Count 75 150 9k So 75 100 100 5o 50 100 9U 50 50 50 100 50 50 U7 1335 Iba. Co Eaearaa Mixer for 5 niauoea and then oraw off into 50? bags. 68169) C*B1B sjtlFJ RETURNTO J-M RESEARCH FILEROOM X-'ch53? -""Aw^orrection per Prod. Prop. 230-120 Rov. B.' ppheinnttk0o11in1-u1.0a.i CRMC-Thermo&Cement-000020 IWANUrMUl UftlNb 4|-fcClNCA'nUNb -PLANT PRODUCT: j C/1T101..0 PAGE NO. "b 3 ASTH CX5CM52) Type HI sues-1! Ingredients . JMs$L 7TH3 Fibre . 3'Ft; libra Hi Early Strength Portland Ceomgeent 200 100 26 : 11.6 5*7 l6ch C15.to #395=A ?>I & I> Clay Bait Scrap . ' 250 56o .. 3.:l.. 171? Il$ ,, 6 32.-7 0 100*0 An oc'iivalGat uncaXeireb grade of Cc-lrlte jnay be used if necessary* IT - EEHIFACimlNO JillFECglg Ac Ex in #10? Riser trith saKor reversed* 3 Charge' inrrodionta so follows? la h lags Batt Scrap 2o 4 'bags H & D Clay 3o 2 bag Oolite 4o 1 teg Hi. Barly Portland Cement ->o 1 bag ?H13 Fibre 6 s 1 bag 4H23 Fibre . { < h bags Batt Scrap 0, 4 batw Ti & O Clay s 2 bags Colit #390^ 10c, 1 bag la Sariy Portland Cement 11c 1 bag 7'A13 Fibre 12 o 5 tag Batt Scrap 13 c 3 bags H & B Clay XJj.o 1 bag GaUte #3>`5>^ 15* 1 bag Hi Early Portland Ceramt 10C# . 200 ? 100 ?k 100 100 100 200 100 94 100 125 150 50 9k C* Sevsroe tslsar and package5 0$ to a bsgo Kota: Use a #450 Cement hag .flat has bean cut doan Cross off the #450 label ar:E write #301 on the bag with crayon J-MRESEARCH FILE ROOM V* INDICATES -REASON: Add to linso A. CHANGE AUTHORITY -- FOR CHANGE G0 I*Gatbttia9s .tetter > 11^54 FILE-HOLDERS tWlc. Lab,- Form 50132-10 PRINTED IN U.S.A. SUPERSEDES: Wonot m\$ pfp, SUPR. QUAL. CONTROL PROD. SUPT. PLANT FINANCE OFFICE MGR. QUAL. CONTROL DIR. QUAL, CONTRi DATE ISSUED h-bli^F CRMC-Thermo&Cement-000021 inanviile jemem; #301 Cement DIVISION- CT-4 PAGE NO. #1 JRMU.'-iA: Spec. No. - ; `. s #4 [' \ X ' Standard Material, .. -sags vrtT 7M-13 Asbestos Fiber ' (352 Cement) 1/2 Eag 50# % 12.5? C-ranulated Batt Scrap 3 Bags 75 18.7 p.s. 61065 High-Early Strength - 67 16.7 I/' Portland Cement A P.S. 61185** M-D Clay - 133 33. i - 395A Celite - 60 15.0 - 4M28 Fiber - 16 4.0 401# 100.0# Note: * - Richmond plant is source. ** _ A3TM-C-150-52 Type 3 xx MANUFACTURING INSTRUCTIONS: .` ( 1. height out or use tag weights of Ingredients and charge Stedman Mixer in the above proportions. 2. Mix for a minimum of three minutes. .* 3. Catch cement in hoist as it comes from Stedman mixer. Lift hoist and transfer cement to tagger by hopper. c 4. Using bagger, put into 50# 3 ply paper bag (P.S. 68l6$). 5. Tie with bag ties. A, C roma aoiil*w MINTED IN U.I.A. ------------- X~-~Change in Formula to shuw use of 1/g bag and bag X '-INDICATE* CHANGE iwasoxx _ change in wording. weignts. AI1TMrt_1TV Letter of E :CT"E'ihdstrora to'-J.TT: McUa^O&^d T/g/56, fonchIno*- Enactment Letter of J.B. McCarty dated 3/12/56. FILE-HOLDEM SUKMIOH : "iron-- ENGR. WKG. same apecirrcau - on dated 2/3/56, COWTROI LAB. iasutd 3/3/34 H HN. OUAL. COMTtO* now. \ v urr. * mpfclHT ` PINAMCK OFFIC1 and DSVittllUti c. fi+t A--/I OUAL. CONTROL DATE OIR. OUAL. CONTROL SSUED mi CRMC-Thermo&Cement-000022 CRMC-Thermo&Cement-000023 AUTHORITY -- FOR CHANGE FILE-HOLDERS SUPERSEDES! FORM 90132-10 PRINTED IN U. 8. A. Product Proposal ^33-PP-l6* CCBTROL- Lab. P.&S. EHD.EHQR. WKB, Sams specification issued 11/25/53* SUPR. QUAU CONTROL SUPT. PLANT FINANCE OFFICE i / MGR. ' QUAU QU4 fXi CONTROL CONT DATE ISSUE DEC 4 1955 CRMC-Thermo&Cement-000024 L. L rtm ooioft'io PRINTED IN U.O.A* -authority FORCHANOC . FILE-HOLDCM Latter of C. (gCWHOL LAB LeOattuta to B.J. ?hS O'Brien dated 11-6-53 WED. SUPR. QUAL. CONTROL Hone* Enter In index and file numberically. SUPERSEDES: DATE I8SU .25 I CRMC-Thermo&Cement-000025 1972 DISCONTINUED PRODUCT U.S. DEPARTMENT OF LABOR Occupational Safety and Health Administration MATERIAL SAFETY DATA SHEET Fotrr Approved OMB No. 44-R 1 J87 SECTION 1 MANUFACTURER'S NAME EMERGENCY TELEPHONE NO. Johns-Manville Corp. & Subsidiaries ADDRESS (Number, Street, City, State, and ZIP Code) Ken-Carvl Ranch. Denver. Colorado 80217 303/978-3118 CHEMICAL NAME AND SYNONYMS Chrysotile Asbestos TRADE NAME AND SYNONYMS 352 Cement CHEMICAL FAMILY Asbestos FORMULA SECTION II - HAZARDOUS INGREDIENTS PAINTS. PRESERVATIVES. & SOLVENTS % TLV (Unit!) ALLOYS AND METALLIC COATINGS PIGMENTS BASE METAL TLV % (Units) CATALYST ALLOYS VEHICLE SOLVENTS ADDITIVES METALLIC COATINGS FILLER METAL PLUS COATING OR CORE FLUX OTHERS L* OTHERS HAZARDOUS MIXTURES OF OTHER LIQUIDS. SOLIDS. OR GASES TLV % (Units) Chrysotile Asbestos Fiber 10 -------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- 1-------- .1 ..... ... . . ____ __ _ ... ......... . _. ____ ____ ___ _J___ 1 *For TLV see attached (29 CFR 1910.1001) SECTION III - PHYSICAL DATA BOILING POINT (F.J VAPOR PRESSURE (mm Mg.) VAPOR DENSITY (AIR1) SOLUBILITY IN WATER NA SPECIFIC GRAVITY (HjO'l) PERCENT. VOLATILE BY VOLUME (%) EVAPORATION RATE ( *H appearance and odor white fibrous dry material - no odor SECTION IV FIRE AND EXPLOSION HAZARD DATA FLASH POINT (Method und) FLAMMABLE LIMITS EXTINGUISHING MEDIA Non-flammable SPECIAL FIRE FIGHTING PROCEDURES UNUSUAL FIRE AND EXPLOSION HAZAROS NA PAGE (1) (Continued on ravers* side) Form OSHA-20 Ittv. May 72 CRMC-Thermo&Cement-000026 SECTION V - HEALTH HAZARD DATA IMHFSHOLDLIMITVALUt See Section II MrsCTSOF OVEREXPOSURE . '" 0verexposure to excessive concentrations of asbestos fiber may cause pulmonary disease. EMERGENCY AND FIRJT AID PROCEDURES Avoid breathing excessive dust when handling, dumping and mixing, _See caution 1 abel on bag. STABILITY UNSTABLE SECTION VI REACTIVITY DATA CONDITIONS TO AVOID STABLE X incompatability (Materials to smii| one in HAZARDOUS DECOMPOSITION PRODUCTS NA HAZARDOUS POLYMERIZATION MAY OCCUR WILL NOT OCCUR designed use. CONDITIONS TO AVOID X SECTION VII SPILL OR LEAK PROCEDURES STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED ' .Vacuum_clean spillage,___Repair broken bags. If sweeping is necessan wet down spillage. Use approved respiratory equipment when required. WASTE DISPOSAL METHOD .Comply_with_40 CFR, Chapter 1, Part 61 SECTION VIII - SPECIAL PROTECTION INFORMATION RESPIRATORY PROTECTION fStnxilv . NIOSH approved - See OSHA 1910.1001 VENTILATION LOCAL EXHAUST . SPECIAL MECHANICAL (General) OTHER PROTECTIVE GLOVES EYE PROTECTION OTHER PROTECTIVE EQUIPMENT SECTION IX - SPECIAL PRECAUTIONS MPREaCiAnUtTaIOiNnS TgO oBoE dTAKhEoNuINseHAkNeOeLIpNGinAgNDpSrTOaRcINtGices. place in"closed containers. 1 .V.acuum c,lean waste and OTHER PRECAUTIONS SEE CAUTION LABEL ON BAG. While the information and recommendations set forth hereiri cpo n so are believed to be accurate as of the date hereof, AvrTM,yS72 ` JOHNS-MANVILLE CORPORATION MAKES NO WARRANTY WITH RESPECT THERETO AND DISCLAIMS ALL LIABILITY FROM RELIANCE THEREON. 20 CRMC-Thermo&Cement-000027 CRMC-Thermo&Cement-000028 CRMC-Thermo&Cement-000029 MEMORANDUM TO: CEMENT PRODUCT FILE FROM: LKB DATE: June 11, 1990 RE: GRADE 7M13 FIBER AND 352 CEMENT Pursuant to a request from Mr. Sold of Gordon & Silber, I called Bob Rushforth with the following question: Was 7M13 grade asbestos fiber marketed commercially as an insulating cement simultaneously with 352 Cement? His response was that the intentions of the Industrial Products Division/Industrial Insulations Division were that 352 Cement was specifically "manufactured" and marketed for use as an insulating product and that 7M13 was specifically marketed for use as an asbestos fiber grade. When the "manufacture" of 352 Cement was discontinued, it was not the intent of IPD/IID that grade 7M13 Cement be substituted for 352 Cement. Subsequent to the discontinuance of 352 Cement, some J-M customers learned that the two products were synonymous and began purchasing 7M13 fiber from the Asbestos Fiber Division to use as a substitute for 352 Cement. Any purchases of 7M13 would have been made through the Asbestos Fiber Division. He was not personally aware of what intentions the Asbestos Fiber Division may have had (or whether, in fact, they had any) in marketing 7M13 Cement as a substitute for 352 Cement. Mr. Rushforth further stated that the above information was available to him through heresay only and that he was not qualified and would not testify to it. CRMC-Thermo&Cement-000030 3. A CRMC-Thermo&Cement-000031 CRMC-Thermo&Cement-000032 / h I N IbHEU HKQUUCI SKtUMUAilUN and So. Xnsulaiii / Cement 4^<3> SJSfflB /' 1 jJj-su* -7, GENERAL PESOSIPTION AW OSS ' ?'7:S Ho* 0352, Ro. 340 No. 352 and So. 364 Insulating Cements are composed of asbestos and other materials with the exception of No. 352 Insulating Cement which is composed .entirely of asbestos. They ar used* whoa mixed witfa water to a plastics oonsistenoy, as surface finishes over hi00k or sheet forms of' insulation to seal joints between -the blocks and to pro-rid a smooth finish or e surfao to which canvas or other materials m.be applied. They are also used for insulating hasting boilers and pipe -fittings. They are used principally by tbs stoaa fitting arid plumbing trade for domes tie heating installations. No. 552 Insulating Cement is also used- industrially as a general finishing cement. They are used where the temperature on the eeaent may be m high as ie000 P,, They ..are also used as admixtures with Portland cement for a finish-coat over | ^pTr'i g. preceding rough coats. 11 ,~`'jL*IvLL -' - 38 !9: MANUFACTURING. PRODUCING. IMP FACTORY STOCKING- POINTS - ' INSULATING CEMENTS No. 0352 Ho. 340 No. 352 Sl&nville ManvllX Manufactured & Stocked W&ukagan Waukegan Pittsburg .JSEPr LMDRATQb^ Wo* 364 Manvilla Waukegan Produced aad Stocked Asbestos Mines Stocked Only 4 Redwood City l Hon ManvilIs W'aukeg&n None COMPOSITION Uniformity in composition of each of the 0meats is desired. It is recognised* however, that compositlon of an individual cement produced at several ;-fstories may not bo uniform because of variations in materials used; therefor uniformity is liiaitad to production at s&eh factory. The cements shall b manufactured or produced in dry form which oan be readily mixed with water for use and applied with trowel in costs approximately .1/415 ia thickness per ooat. They shall be free from lumps and foreign materials Composition snail be-such, that when need as reooamendsd they shall withstand heat to within recaamaa&sd temperature rang without deterioration. They shall be 0aments which will ce capable of being applied in a. finish cost that will show no cracks whieh will impair the efficiency or present an unsatisfactory appearance when allowed to dry in air. So. 0352 and fs. 36h Insulating Cements shall be oosaposed of asbestos a plastie agent, a setting agent and a filler. i\ Pag #1 . ISSUES OR IGIHAL SPEC. EFFECTIVE LAST REVIS 1 OR EFFECTIVE THIS REV IS 108 EFFECT IVE approves ;C.1U ;:-89is 2-39 HIITH 18 u.S.A. ;: - COMPTROLLER CRMC-Thermo&Cement-000033 MNISHfcD PHfUDUCI SKtUMOAi lUrt and fsoo yok Insulatln, Cement; COMPOSmOll (Continued) Ho* 352 Insulating.Cement ghaii be composed oi asbestos. No. 3k0 Insulating Cement shall be composed of asbestos and plastic agent* CONSISTENCY (with water)' ` When mixed with water to a plasties consistency the osments shall be readily workable with trowel or by hand for use as described in paragraph headed "General Description and UaeR. COLOR Uniformity ' in color of each of the several seats as maaufaotarsd or prod iced is desired. It is rooognized, however, that color of an iadfricucl oc-acat p-'odtio&d at several locations may not be uniform baoeuee of variations ir raw ratorisia used. Therefore limitation of uniformity in oolor of a oament to production of east location is aeoeptabla although it is desired that an oversell standard of eclor be adopted. On date of issuance of 'this speoifie&tion colors of the cements w@m as listed below and wore acceptable.- Irlo, 0352 gray at M&nvllle and DTaukegan and gray-whits at Pittsburg . }No. 340 Mo, 352 gray Ro. 364 grayish~brown COVERAGE! The eamenta shall b of auoh densities when produced that whan mixed with water to a plastic consistency;. applied. ana dried. 1QG pounds of the dry cement will cover not less then the areas listed below to a thlokness of 1 inch. Cement Jo *0352 Ko. 34 Bo. 352 Ro. 364 Mia. Coveraga (l8 Thlok) 1? square feet 18 * ^ 8 15 a * 18 a s DSimn (dry) ' Uniformity in density of e&oh of the several 0moats is desired* Density shall fa auoSi that they fcUu. fulfill the ?equIresaents of this specification as "to coverage as stated in foregoing paragraph headed ^Coverage9. ASBESTOS GRADING (No- 352 Insulating Cement, Only) ' Uniformity in asbestos grading is desired. The asbestos grading Of the day osment when produced shall fas suoh that It will ba equal to Q.A.P.A. Grade Class ifio&tion 7U (J.M. Grad $352 or 7M13) end c.a& pound tested is. Quebec Standard Tasting Machine Page .#2 FORM X- n i ms 8918 18 2-39 U.S.A, ISSUED < OR IGIBAL SPEC. EFFECTIVE LAST REV IS I0 EFFECTIVE THIS REV IS 1 OR EFFECT IVE APPROVED t/n #Hf COMPTROLLER CRMC-Thermo&Cement-000034 MNIbHtU FKUUUUI SKtUl- IUAI iu ami ho, joft inmi&tl Cornerit ASBESTOS gating (Continued) shall have results as Indicated baio**. Quebec Standard Test Min. Max. 1/2* 0.0 0.0 Results In. Ounces 4 10 35 Mesh ft >. n n r* Mesh 1.0 & Pan 15.0 0.G 2Ji 14.0 Mia. on Fan . * 38 ADHESIOM The oements, when mixed with water and applied, shall adhere readily to hot or cold metal surfaces?, to pipe, block or sheet insulation and to the preceding layer of th sea cement- APPSA8AHCE ' i'/Sios applied, as rscoa/aended the essaents shB.il form a hard eating aih sill as of nest appearance with ao e-bjcetionable racks and will not curl or warp 'when dry,-, RSSlSTAitCB fO ABRAS1QM The ocsaoirba, when mixed with water and applied as coating, shall .fora a hard ooat which will bo sufficiently resistant to abrasion due to external abuse as normally encountered in roeoamended installations ao that they will not powder* crumble or pull sway, RBS1STAMCS TO HEAT Th cements shall not crack, crumble, softer, or otherwise fail mechanically when subject tc heat within raccstmsndsd temperature rang. SH8IKEA6B - Uniformity In the yoltsae shrinkages of the indivbdum'. absents, in drying and when exposad to heat within recommended temperature rengo* iu desired. Shrinkage in drying cither cold or heated shall not bo largo enough to cause the seraents to sari or pull away,. The shrinkage of th omenta when exposed to herit within reoexamandod rang shall not cause them to poll away frees the surface to h& pro tooted, or impair the efficiency of th cement as caning* ' FACSA&XKG Mos, 0352, 34 352 and 36/4. Insulating Camanta snail to packed to insure acceptance by Qosmon carriers and. to insure safe del ivory to and warehoas ing and handling by the customer M ultimate. user at lowest total cost of packing, shipping !?,m transportatio - The container- shill h-s of such construction and strength as to' present loss of material fcy sS.fti -,g through or by ordinary wear aad handling Is storage and shipment. The package shall- be of goat appe-aranoe, tight- p&oked end securely closed. , Page #5 POSH X-891B 2-39 raiBTEO IB u.S.A. ISSUED /#ORIGlRAt SPEC. EFFECTIVE LAST RE V IS I OR EFFECTIVE THIS RE V IS ION EFFECTIVE A P PR OVE D C0PTR01I-Er CRMC-Thermo&Cement-000035 FINISHED PRODUCT SPECIFICATION ana so. jot*. lnsuiatin Cement , PACKAGING '(Continued) At present the dements are packed in the containers listed below,, These were approved by tha Sales Department prior to date of issuance of this epeoiflcatiojn Th desired net weights per oont&iner are 50 pounds and 100 pounds net for No* 352 Insulating Cement and 100 pounds net for all other oaments (approximate gross weights indicated below)0 Insulating Gameat Ho. 0352 Ho. 3k0 No. 352 No. 364 Container and Shipping Weight Data Manufaoturing Location Containers i Maaville Factory 1 Waukegan s Plain burlap sack 3 1? S3 v. Pittsburg " n t 0 Gross Shipping (Weight (approx.) 102# 102# 101# / Manville Waukegan R fr e S3 3 102# 102# Asbestos Mines Printed jute sack (100$) s paper bag (50#) 101# 51# OO 4 Manville Factory la, Waukegan B Plain burlap sack 3 fl S3 Printed juts sack and printed paper bag at Asbestos shall be printed as per Form No. and Pom Ho. ** respectively. Each saak of cement at all factories shall b@ tagged with appropriate product tagss as follows: ** No * 0332 No. 340 No. 364 :)S:0 be supplied when available Printed Produot fag-Pora Ho. M. 3 Boedeker Comptroller (s FORM X-691B 2-39 PR IKTEO IR U.S.A. Pag 44 ISSUEO 08 1G 1 HA L SPEC. EFFECTIVE LAST REV IS 10* EFFECTIVE THIS REV IS 10* EFFECT IVE COMPTRotUl CRMC-Thermo&Cement-000036 CRMC-Thermo&Cement-000037 CRMC-Thermo&Cement-000038 1973 VOID - DISCONTINUED U.S. DEPARTMENT OF LABOR Occupational Safety and Health Administration PRODUCT Form Approved OMB No. 44 R 1387 II ftIKTERIAL SAFETY DATA SHEET SECTION 1 MANUFACTURER'S NAME Johns-Manville Corp. EMERGENCY TELEPHONE NO. 303/978-3118 address (Number, Street, City, State, and ZIP Code) Ken-Caryl Ranch, Denver, Colorado 80217 CHEMICAL NAM{- AND SYNONYMS Calcium Silicate Thermal Insulation TRADE NAME AND SYNONYMS THERMOBESTOS CHEMICAL FAMILY FORMULA SECTION II - HAZARDOUS INGREDIENTS PAINTS, PRESERVATIVES, & SOLVENTS % TLV (Units) ALLOYS AND METALLIC COATINGS PIGMENTS BASE METAL CATALYST ALLOYS ' VEHICLE SOLVENTS ADDITIVES METALLIC COATINGS filler metal PLUS COATING OR CORE FLUX OTHERS OTHERS HAZARDOUS MIXTURES OF OTHER LIQUIDS. SOLIDS, OR GASES Chrysotile Asbestos Fiber Natural diatomaceous earth *See attached (29 CFR 1910.1001) y ` TLV ----%-----!---(-U-n-i-t-s-l - i ---- 1j---------- i 1 TLV (Units) ;7 j48 ,2 0 mppcf SECTION III - PHYSICAL DATA boiling point (f.) VAPOR PRESSURE (mm Hg.) VAPOR DENSITY (AIR-1) SOLUBILITY IN WATER SPECIFIC GRAVITY (H20=1) PERCENT, VOLATILE BY VOLUME (%) EVAPORATION RATE ( =D appearance and odor Off-white solid block - no odor SECTION IV - FIRE AND EXPLOSION HAZARD DATA FLASH POINT (Method used) FLAMMABLE LIMITS EXTINGUISHING MEDIA Non-flammable special fire fighting procedures Lei UNUSUAL FIRE AND EXPLOSION HAZARDS 0.2 PAGE (1) (Continued on reve, <e side) Form OSHA-20 Rev. Mey 72 CRMC-Thermo&Cement-000039 SECTION V - HEALTH HAZARD DATA i I iwi S> ii.)| () UMI I VAt.WI See Section II I I I I i, I S ()l OVI HI XPOSURf. Overexposure to excessive concentrations. of_airborne-. ssbos.tos. dustmay cause pulmonary disease. t Ml.RGLNCY ANI) FIRST AID PROCEDURES ...Avoid .creating excessive dust._______ ______ ___ __________ _______ ________ SECTION VI - REACTIVITY DATA STABll.n v UNSTABLE CONDITIONS TO AVOID STABLE X INCOMPAT ABILITY (Materials lo avoidj HAZARDOUS DECOMPOSITION PRODUCTS None None HAZARDOUS POLVMf. R 12 AT ION MAY OCCUR WILL NOT OCCUR CONDI 1 IONS TO AVOID X SECTION VII - SPILL OR LEAK PROCEDURES STPS TO BE TAKEN 'N CASE MATERIAL IS RELEASED OR SPILLED ' .vacuum clean dust and chips from fabricating operations. WASTF DISPOSAL METHOD .Comply with, all applicable, .local, state-and -te^eral-r-egurla-t-ions- I----------------------- SECTION VIII - SPECIAL PROTECTION INFORMATION RESPIRATORY PROTECTION /SpaitV tvpcl See attached . VENT ILATiON < local exhaust Mechanical Ventilatio svstems should be installed on faj 1 X special ricating mechanical (General) OTHER eqtii "* PROTECTIVE GLOVES eye protection OTHER PROTECTIVE EQUIPMENT _... SECTION IX - SPECIAL PRECAUTIONS PRECAUTIONS TO BE TAKEN IN HANDLING AND STORING Maintain good housekeeping practices, dust or chips created by fabricating operations. OTHER PRECAUTIONS See caution label on shipping carton, While the information and recommendations set forth herein gpr if*) 54oare believed to be accurate as of the date hereof, S7^A20 '9 M JOHNS-MANVILLE CORPORATION MAKES NO WARRANTY WITH RESPECT** THERETO AND DISCLAIMS ALL LIABILITY FROM RELIANCE THEREON. CRMC-Thermo&Cement-000040 r' ;> /. *J Johns-Manville n* ^ I k v/CJ^1' f*'S*1, rr-'^ .0*'% ' U U Wi 'mr \i ii W W TO: SEE BELOW * Date: JANUARY 4, 1974 From: F. D. AFFLERBACH Copies- B. W. YERRY Subject: MANUFACTURING SPECIFICATIONS The following Manufacturing Specifications are being cancelled. Please remove and destroy these specifications from your active file. SPEC. NO. 11-4324-10 11-4324-10.1 II-4324-11.1 11-4324-12 / 11-4324-13 11-4324-17 TITLE . Thermobestos Block and Pipe Covering Thermobestos Finishing Operation Scored Thermobestos Block Extended Leg - Thermobestos 'P/I Sodium Silicated Thermobestos Blk. and P/I Thermobestos Molded Elbows * R. E. KIZIS ' V. P. SORICE D. E. GUY R. L. LEWIS P. G. KAIN G. HINDUS LIBRARIAN D. B. WINGERTER - DEN 4S E. J. WARWICK - DEN R CRMC-Thermo&Cement-000041 1 Johns-Manville MANUFACTURING SPECIFICATION PRODUCT: ` SODIUM SILICATED THERMOBESTOS BLOCK AND P/I PUNT & DIV. SPEC NO. Mvl. IID 4324-13 PAGE NO. 1 L.... ... i V. I. FORMULA: A. Manufacturing Specification 4324-10. B. The following ingredients are added to the slurry at the metering tank. 1. Dry granular sodium silicate at a concentration of 0.150 lbs./bd. ft The silicate is produced by Philadelphia Quartz Company to meet Tylar Screen requirements of the applicable purchase specification. xi 2. Aquablak #51 diluted to one part aquablak/18 parts water at a concentration of 35 cc/bd. ft. This is done to distinguish sodium silicated Thermobestos from regular Thermobestos. ,, II. BATCH PREPARATION: A. Manufacturing Specification 4324-10. III. MOLDING: A. Manufacturing Specification 4324-10. 1. Minimum and maximum probe settings are unchanged. X2 2. Green hardness 65-75 on Dietert green hardness tester. Same procedure as in Manufacturing Specification 4324-10. B. Addition of granular sodium silicate and aquablak as follows: 1. After metering tank fills with slurry to prescribed probe level, short out probe and activate lightnin mixer. 2. Add granular sodium silicate at a concentration of 0.15 lbs/bd. ft. and aquablak at a concentration of 35 cc/bd. ft. 3. Allow lightnin mixer to run until metering tank empties. 4. Stop lightnin mixer and open probe circuit. 5. Repeat process starting with Step 1. NOTE: The addition of granular sodium silicate and aquablak as outlined above in Step 1 thru Step 5 refers to a manual operation. An exact sequence of operation shall apply when performed by automatic dispersing equipment. --1/1 r PLEASE RETURN TO <(31i J-M RESEARCH => I LIBRARY (MM) V X-- INDICATES CHANGE --1REASON: X2 X.1 - To To correct Green Hardness to 65-75 delete rej*^rence of aquablak in regular Thermobestos cy nr(4o1l AUTHORITY FOR CHANGE D. B. Wingerter^s^/f ^atec* 1-28-70 51 SUPERSEDES: Same spec, page*! < a. 0-27- 67. DIR. Q.C. MGR. Q.C. SUPR. Q.C. PROD. SUPT. PL NT. R FIN. * U Ind. Engr. DATE ISSUED 4-8-70 CRMC-Thermo&Cement-000042 Johns-Manvjjle MANUFACTURING SPECIFICATION PRODUCT: Sodium Sllicated Thermobestos Block and P/I " PLANT & DIV. SPEC NO. PAGE NO. Mvl. IID. 4324-13 1 I. FOBMULA: A. Manufacturing Specification 4324-10. B. The following ingredients are added to the slurry at the metering tank. 1. Dry granular sodium silicate at a concentration of 0.150 lbs./bd.ft. The silicate is produced by Philadelphia Quartz Co. to meet Tyler Screen requirements of the applicable purchase specification. y 2. Aquablak #51 diluted to one part equablak/18 parts L water added in a proportional quantity to give three times the normal amount contained in regular Thermobestoj This is done to distinguish sodium siliceted Therntobestos from regular Thermobestos. II, BATCH FBEPABATION: A. Manufacturing Specification 4324-10. III MOLDING: A. Manufacturing Specification 4324-10. 1. Minimum and maximum probe settings are unchanged. 2. Green hardness 70-80 on Dietert green hardness'tester. Same procedure as in Manufacturing Specification 4324-10. B. Addition of granular sodium silicate snd aquablak ss follows: 1. After metering tank fills with slurry to prescribed probe level, short out probe snd activate llghtnin mixer. 2. Add granular sodium silicate at e concentration of 0.15 lbs./bd.ft. and aquablak at a concentration of 35 cc/bd.ft. _ 3. Allow llghtnin mixer to run until metering tank empties. 4. Stop llghtnin jmixer and open probe circuit. 5. Repeat process starting with step 1. NOTE: ,x The addition of granular sodium silicate and Iaquablak)as ffV-^ outlined above in step 1 thru step 5 refers to a manual operation. An exact sequence of operation shall apply when performed by automatic dispersing equipment. INDICATES change AUTHORITY FOR CHANGE reason. B. W. Honnlg Specification SUPERSEDES: DIR. Q.C. MGR. Q.C. Same spec - pages 1-2-3 dated 1/31/66 SUPR. "Q.C.. PROD. SUPT. PLEASE F;EOI TO J-M ESEAI'Cr! iion.ir?;/ r'm DATE issued 2/27/67 CRMC-Thermo&Cement-000043 :r MANUFACTURING . SPECIFICATION * PRODUCT: ` PLANT & DIV. r> Sodium Siliceted Thermobesto* SPEC NO. Block and P/l ..... -wi-iMvl. TT . fb : PAGE NO. Iff'- r ;I: ^ I. FORMULA A* Manufacturing Specification 4324-10 B.` The following ingredients are added to the slurry at, * ;; the Meeting tank. "' i '1. Dry granular sodium silicate at a concentration of 0.l0 Lbs/bd. ft. The silicate is nroduced by Philadelphia Quartz Co. to meet Tyler Screer Requirements of the applicable nurchase specification. :/ 2. Aauablak-diluted to one part Aquable/24 parts ./ Water added in a proportional quantity to'give ? three times the normal amount contained in regular Thermobestos. This is donelto distinquish s Sodium silicated thermobestos from regular thermobestos. lr* BATSH PREPARATION : Vm. s. 4324-10 III.v MOLDING ,.' ; f v 4 " A. M. S. 4324-10 : .. 1. Minimum and maximum probe settings are unchanged. 2. Green hardness 60-70 on Dietert green hardness tester. Same procedure as in M. S. 4324-10. ^ B. Addition of granular sodium silicate and aquablak .as follows: ' ... 1. After metePing tank fills with slurry to prescribed probe level, short out probe and activate lightning mixer. : v . .' .1 2. Add granular sodium silicate at a concentration of O.lS lbs/bd.ft. and" aquablak at a concentration of 3oc/bd.ft. . 32. Allow Lightnin miker to run until metering tank ' empties. .v v INDICATES X CHANGE ~REAS0N- To add reaulred concentration of acuablak AUTHORITY forchangfr. w. Honnlg's letter to K. H. Slater date<| 1/2P/66 SUPERSE ES DIR. MGR Q.C Q.C. SUPR QC. PROD. SUPT mrPENT. WfsV Ind. FIN. Engr. ISSUED 3/31/66 CRMC-Thermo&Cement-000044 V Johns-Manvllle MANUFACTURING PRODUCT: PUNT & DIV. Sed-iws Silic8ted Thermobest.os Mvl. II SPECIFICATION Block (Tentative) SPEC NO. 4324-13 PAGE NO. 1 I. Formula* A. Manufacturing Specification 4324-10 flJLO B. The following ingredients are added to the slurry at the;^:. metering tank. *4-` 1. Dry granular sodium sll/lcat-e at a concentration of 0.15 lbs/bd.ft. The^iilcate is produced by Philadelphia ( Quartz Co. to the following Tylea,screen requirement -12 Mesh +35 Mesh 100# 100# 2. Aqua black - diluted to one pskrt Aquablack/24 pa^ts^^.^.,; -siuwy-added in a proportional quantity to give two , times the normal amounyplecz II. Batch Preparation: M.S. 4324-10 III. Molding Block: A. M.S. 4324-10 1. Minimum and maximum probe settings are unchanged. 2, Green hardness 60-70 on Dietert green hardness tester. Same1procedure as in M.S. 4324-10. : B. Addition of granular sodium silicate and aqua blsck as follows: 1. After metering tank fills with slurry to prescribed probe level, short out probe and activate <L>ightnln mixer. s K 2. Add granular sodium silicate at a concentration of 0.15 lbs/bd.ft. and required'smount of aqua black.* 3. Allow t-ightnin mixer to run until metering tank empties. 4. Stop tightnin mixer and open probe circuit. 5* Repeat process starting with step 1. PLEASE RETURN TO J-M RESEARCH ---------------------------------mm-4 v INDICATES pr.criM x change reason. New Specification AUTHORITY ._ forchangf E.C. Lindstrom's letter to K. H. Slater dated 1/28/66. SUPERSE ES None DIR. MGR SUPR PROD. PLNT. RES. iwd.-- Q.C Q.C. QC. SUPT FIN. Engr. DATE ISSUED 2n//8a/j6,s6 CRMC-Thermo&Cement-000045 tesly! Johns-Manville Internal Correspondence To. SEE BELOW * Date: JANUARY 4, 1974 From: F. D. AFFLERBACH Copies- B- W* YERRY Subject: MANUFACTURING SPECIFICATIONS The following Manufacturing Specifications are being cancelled. Please remove and destroy these specifications from your active file. ' SPEC. NO. /11-4324-10 11-4324-10.1 11-4324-11.1 11-4324-12 11-4324-13 11-4324-17 TITLE Thermobestos Block and Pipe Covering Thermobestos Finishing Operation Scored Thermobestos Block Extended Leg - Thermobestos P/I Sodium Silicated Thermobestos Blk. and P/I Thermobestos Molded Elbows * R. E. KIZIS . ~ x V. P. SORICE D. E. GUY R. L. LEWIS P. G. KAIN G. MINDOS LIBRARIAN D. B.. WINGERTER - DEN 4S E. J. WARWICK - DEN R Note for record: First Proposed Manufacturing Specifications for THERMOBESTOS See Research Report No. 432-60 CRMC-Thermo&Cement-000046 Johns-Manvillc MANUFACTURING SPECIFICATION \ I. Formula: PRODUCT: THERMOBESTOS BLOCK AND P/C (Lime Silica) PLANT & DIV. SPEC NO. PAGE NO. Mvl. IID 4324-10 1 Spec. No. Material Std. Formula lbs. % Std. Formula Homogenized Fiber lbs. % F.P.S. 44.19 F.P.S. 41.14 P.S. 11-1830 J.M. Fiber Celite 256 Celite 392 Hydrated Lime ^ 4K30 Fiber Water 650 650 1300 300 * 22.4 22.4 44.8 10.4 650 700 1350 200 k 22 A 24.1 46.6 6.9 -v Total 2900 100.0 2900 100.0 Notes: Above is 14.5 to 1.0 water solids ratio by weight. Batch made up to a total of 5,032 gallons . *For each batch of Thermobestos, 2900 lbs. of raw materials are made up to a final volume of 5,032 gallons with hot lime silica tailing water and service water. 1. Incoming shipments of 256 Celite marked L, M and H are grouped by Lompoc to the following gel times: L - 25-30 minutes M - 35-55 minutes H - 60-plus minutes 2. Each incoming shipment of Celite 256 L, M or H and Celite 392 shall be tested in the Quality Control Laboratory to determine the actual Gel Comparator time. Based on this gel time, each batch of Thermobestos slurry shall be treated by adding the following quantity of Aluminum Sulphate to the-batch just prior to the additon of the Celite to the pre-mixer: Gel Time (Minutes) Celite 256 (Lbs. Alum/batch) Celite 392 ' (Lbs. Alum/batch) 20 25 - 30 35 40 45 *50 - 55 60 plus . 8 7 5-1/2 4 .... ' 3 2 8 7 5-1/2 4 3 2 Note: Both Celites, 256 L, M or H and 392 require the above quantity of Alum. For example: .. If the gel time of Celite 256 M = 35 minutes: add 5-1/2 lbs. of alum. If the gel time of Celite 392 = 40 minutes: add 4 lbs. of alum. Total amount added to batch 9-1/2 lbs. - INDICATES CHANGE -REASON: Correct Celite 329 to Celite 392 AUTHORITY FOR CHANGE Correction o SUPERSEDES: Page 1, Same spec id 1/19/70 PLEASE RETURN TO J-M RESEARCH LIBRARY DIR. Q.C. MCR. Q.C. cun?. Q.C. PROD. SUPT. PINT. TIN. Ind. Engr. _ i DATE ISSUED 6/8/71 CRMC-Thermo&Cement-000047 Johns-Manville MANUFACTURING SPECIFICATION PRODUCT: THERMOBESTOS BLOCK AND P/C (Lime Silica) PUNT & DIV. SPEC NO. PAGE NO. Mvl. IID 4324-10 1 I. Formula: CANCELLED Spec. No. Material Std. Formula lb's. % Std. Formula Homogenized Fiber lbs. % F.P.S. 44.19 F.P.S. 41.14 P.S. 11-1830 J.M. Fiber Celite 256 Celite 392 Hydrated Lime 4K30 Fiber Water 650 650 1300 300 * 22.4 - 22t4 44.8 10.4 650 700 1350 200 * 22.4 24.1 46.6 6.9 '. v Notes: Total 2900 100.0 ^* Above is 14.5 to 1.0 water solids ratio Batch made up to a total of 5,032 gallons 2900 100.0 . *For each batch of Thermobestos, 2900 lbs. of raw materials are made up to a final volume of 5,032 gallons with hot lime silica tailing water and service water. 1. Incoming shipments of 256 Celite marked L, M and H are grouped by Lompoc to the following gel times: L - 25-30 minutes M - 35-55 minutes - V H - 60-plus minutes 2. Each incoming shipment of Celite 256 L, M or K and celite 329 shall be tested in the Quality Control Laboratory to determine the actual Gel Comparator time. Based on this gel time, each batch of Thermobestos slurry shall be treated by adding the following quantity of Aluminum ,y-K Sulphate to the batch just prior to the addition of the Celite to the v- l-t' pre-mixer: nd. in U.S.A. Gel Time (Minutes) Celite 256 (Lbs. Alum/batc'n) Celite 392 (Lbs. Alum/batch 20 25 - 30 ' 35 40 . 45 50-55 60 plus 8 7 5 1/2-----------4 3 2 0 8 7 5 1/2 ... 4 3 2 0 Note: Both Celites, 256 L, M or K and 392 require the above quantity of Alum. For example: - If the gel time of Celite 256 M = 35 minutes: add 5 1/2 lbs. of alum. If the gel time of Celite 392 = 40 minutes: add 4 lbs, of alum. Total amount added to batch 9 1/2 lbs. X-- chan^*^S --REASON: To delete use of 4D28 Fiber and show use of 11P0Q0%% _44KK3300_FFibibeerr.. AUTHORITY PLEASE RETUnN TO FOR CHANGE D. B. Wingerter/R. Nebel's letter dated 9-18-69 JM RESEARCH SUPERSEDES: Page 1, Same spec dated 10-28-68 MDIR. MGR. SUPR. PROD. PLNT. Q.C. Q.C. Q.C. SUPT. FIN. n\ Ind. Enr:r. 1 LiPfWir 1MMJ---------------- ISSUED 1-19-70 CRMC-Thermo&Cement-000048 Form 33.: Johns-Manville MANUFACTURING specification f PRODUCT; Thermobestos Block and P/C (Lime Silica) PLANT & DIV. SPEC NO. PAGE NO. y-d -r Mvl. IID. 4324-10 ' 1 I. Formula: Spec. No. F.P.S. 44.19 F.P.S. 41.14 P.S. 11-1830 J.M. Fiber Material Celite 256 Celite 392 Hydrated Lime '4D28 Fiber Water Total Std. Formula 650 lbs. 650 lbs. 1300 lbs. 300 lbs. * 2900 lbs. Percent 22.4 22.4 44.8' 10.4 100.0 lb Notes: Above is 14.5 to 1.0 water solids ratio Batch made up to a total of 5,032 gallons C *For each batch of Thermobestos, 2900 lbs. of raw materials are made up to a final volume of 5,032 gallons with hot lime silica tailing water and service water. l ... 1. Incoming shipments of 256 Celite marked L, M and H are grouped by >'V'S/ Lompoc to the following gel times: PLEASE RETURN JQ L - 25 - 30 minutes M - 35 - 55 minutes , ,, J-M RESEARCH H - 60 - plus minutes LIBRARY (MM) - : 2. Each incoming shipment of Celite 256 L, M or H and Celite 392 shall be tested in the Quality Control Laboratory to determine the actual Gel Comparator time. Based on this gel time, each batch of Thermobestos slurry shall be treated by adding the following quantity of Aluminum : Sulphate to the batch just prior to the addition of the Celite to the pre-mixer: Gel Time (Minutes) * Celite 256 (Lbs. Alum/batch) Celite 392 (Lbs. Alum/batch) 20 * 8 8 25 - 30 7 7 ,- c 35 5 1/2 5 1/2 > F 40 - ------ 4 - . 4 45 50 - 55 3 3 | 2 60 plus 0 8 Note: Both Celites, 256 L, M or H and 392 require the above quantity of 1 Alum. For example: ' * If the gel time of Celite 256 M 35 minute^: add 5 1/2 lbs. of alun| If the gel time-of Celite 392 40 minutes:- add 4 lbs. of alum % Total amount added to batch . 9 l/2 lbs. , v INDICATES General revision and to reduce the quantity of 4D28 fibers \ X CHANGE REASON. to 300 lbs. ' ft N FOR^change D# B* Wingerter's letter to T. M. Brickley .dated 10-23-?68 Tts V."i SUPERSEDES: Same page of same spec dated 11-24-67 4 hi).DIR. Q.C. MGR. | SUPR. Q.C. | Q.C. PROD. SUPT. PLNT. FIN, Axlnd* Engr. DATE issued 10-28-68 t IT :u b CRMC-Thermo&Cement-000049 ;'J&hfiS'Manville ; MANUFACTURING ^SPECIFICATION PRODUCT: Tharmobestos Block and F/C (Lime Silica) ' PLANT & DIV. SPEC NO. Mvl. IID. 4324-10sy/f^ PAGE NO. IL,. `'i: C .V, ':' X .( I- lISlii&L Spec Ho. Material Std. Formula Percent F.P.S. 44.19 P.P.S. 41.14 t.8; 11-1830 J.M. Fiber Celite 256 .*** Celite 392 Hydrated Lime 4D28 Fiber , Water . 650 lba. v 650 lba. 1300 lba. 325 lba. * 2ZiZ ^", 22.2\"`= ^ 44*4- 11.2 Notes: Above is 14.3 to 1.0 water eolids. ratio -vv.. Batch made up to a total of >5*032 gallona 1 *For each batch of Thermobeatos, 2,925 lba. of raw materials are made tip to fe final volume oi 5,032 gallons with hot lime silica tailing water and - service water. . - .* ' . ' . ***Batch88 containing 256 Celite marked L, M, and H will be treated by. adding the following quantities of Aitmimm Sulphate to the batch just prior , to the addition of the Celite to pre-mixer: ' 1 't L - (25 - 30 minutes) M - (35 - 55 minutes) H - (60 plus minutes) Add 8 pounds per batch Add 5pounds per batch Ho additive 1. Production should be scheduled to conform to .the following gel times:. a. Minimum - 1-3/4 hours b. Maximum - 3-1/2 hours c. Optimum - 2 hours and 10 minutes* , ! ,j ! ` -f *Hotes Predicated'on 27 molder operation/ ' ! 2. Weight checks, pre made on the bagged Celltes and Lime at least once per , shift as follows: . . !_ ; A. Weigh up six 50 lb. bags of lime and record. - i B. Weigh up six 50 lb. bags of Celite 256 and record* C. Weigh up six 50 lb. bags of Celite 392 and record. !^ . v PLEASE RtTURN TO J-M RESEARCH ' '. rtCohM CO '' E v indicates PF..n, X CHANGE ~REAS0N- To remove aqua black from formula LIBRARY AUTHORITY .' . FOR Change D, B. Wingerter*s letter to A. W; Jung dated 5/16/67 (MM1. supersedes: DIR. MGR. Q.C. Q.C. game page of same spec dated 10/22/65 -- ----U, .SUPR. PROD. PLNT. RES. ind. S'. ' Q.C. SUPT. PIN. LAB. Engr. DATE ' ' " issued 11-24-67 '' ........... --~............. . r " ` ; 1 i\A '. 1 ' CRMC-Thermo&Cement-000050 Johns-Manvtlld MANUFACTURING . SPECIFICATION PRODUCT: Thermobestos Block & P/C (Lime Silica) PLANT & DIV. SPEC NO. PAGE NO. Mvl. II 4324-10 1 Formula s Spec. No. Material Std. Formula Percent X F.P.S. 44.19 Celite 256-C*** 650 lbs. X F.P.S. 41.14 Celite 392 650 lbs. X Hydrated Lime 1300 lbs. X J.M. Fiber 4D28 Fiber ' 325 lbs. 22.2 22.2 v 44; 4 11.2 P.S. 11-3299 Aqua Black 2 qts. MOTES: ____ _ S&t?' ** 7 /><&'<>*' ft FCu 7/2*?/# S' Above is(l4.l)to 1.0 Water Solids Ratio Batch made up to a total of 5032 gallons. . For each batch of Thermobestos, 2,925 pounds of raw materials are made up to a final volume of 5,032 gallons with hot lime : silica tailing water and service water. .................................... ** Batches containing 256C Celite marked L, M. and H, will be treated by adding the following quantities of Aluminum Sulphate to the batch just prior to the addition of the Celite to pre-mixer: .. L - (25-30 minutes) M - (35-^5 minutes) H - (60 plus minutes) Add 8 pounds per bstch Add 5 pounds per batch No additive. O Production should be scheduled to conform to the following gel tiroes: * ==? V 1a11ir u3-j Ii - 1 n i j S. NOTE: 1 a. Minimum - 1-3/4 hours b. Maximum - 3-1/2 hours - c. Optimum - 2 hours and 10 minutes* Predicated on 27 molder operation. K- 2. Weight checks are made on the bagged Celltes and Lime once per shift as follows: i' I-Vfy- a. Weigh up nine 50 lb. bags of Lime and record. b. Weigh up six 60 lb. bags of Celite 256 and record. c. Weigh up six 50 lb., bags of Celite 392 and record. x_ INDICATES oricnN* CHANGE ~REASON: To show current operating procedure. authority A.B. Girardl's letter to K.H. Slater aatftd 2/5/^5 releasing for change summary to product proposal 432-64--SI._________ _________________ SUPERSE ES DIR. Q.C. MGR Q.C. Same page of same spec, dated 9/17/65 SUPR QC. PROD. SUPT PLNT. FIN. RES. ~TncT7---LAB Engr. DATE ISSUED IO/22/65 CRMC-Thermo&Cement-000051 , ;-ii irWiW Johns-Maiwllle . JFACTURING 'ECIFICATION Formula* PRODUCT: __ rtO'r'7- ! v*: PLANT & DIV. Thermobestos Block and P/C (Lime. Silica) ....~y ..---nr-i . -..- SPEC NO. PAGE NO. <t-5' ' Mvl. II J 4324-10 1 " Material x: Std. Formula 'Percent F. P. S. 44.19 f.:p. S. . 41.14 : 3t~/2 V7 J.M. Fiber P.S. 11-3299 Cellte 25,6fC*#* Cellte 392,- Hydrated Lame 4D28 Fiber5 * . Aqua Black Water 650 lbs. 650 lbs. 1300 lbs. 325 lbs. 2 qts. 22.3 2442..63.. 10.? NOTES* . Above is 14.3 to 1.0 Water Solids Ratio h Batch made up to a total of 5,032 gallons. . ':*A' T^WKmy. For each batch of Thermobestos . 2.800 poundsiof raw materials are made up to a final volume oT 5,032 gallons, with hot lime silica tailing water end service water. I" * Milled fiber used in formula. Three hundred founds of erude fiber weighed at the mill (Sprout Waldron plus'Vertical Willow). No allowance made for loss due to drops and lljne loss. 1 * Batches containing 256-C Cellte Marked L, M, and H, wfill be treated by adding the following quantities of!Aluminum Sulphate to the batch just prior to the addition of th<&, Cellte to pre-mixer* r' L - (25-30 Minutes) Add 8 pounds per batch. M - (35-55 Minutes) Add 5 pounds per batch. H - (60 plus minutes) No additive. 1. Production should be scheduled to conform to the following gel times t NOTE* 8. Minimum - 1-3/4-hours b. Maximum - 3-1/2 hours c. Optimum - 2 hours and 10 minutes*- Predicated on 27 molder operation. I'M /?/>, :tjru 2. Weight checks are made on the bagged Celltes and Lime once per shift as follows* a. Weigh up nine 50 lb..bags of Lime and record. b. Weigh up six 60 lb. bags of Cellte 256'and record. 0, Weigh up six 50 It* b8gs of Cellte 392 and record. F r 333-2 PM. o U.S.A. x__ INDICATES * CHANGE REAS0N Correction AUTHORITY _A. _B._ O_ irardi's letter to K.H. Slater, dated 2/5/65 releasing FOR change ssuummmmaarryy to product proposal 432-64-SI. SUPERSE ES Page 1 same spec, dated 6/30/65 DIR. HGR SUPR PROD. PLNT. RES. Ind. Q.C. q.c. QC. SUPT FIN. LAB DATE ISSUED , 9/17/65 CRMC-Thermo&Cement-000052 'i . ' ^ M'yf- X lr X 333-2 Ptd. n U.S.A. Johns-Manvilte MANUFACTURING SPECIFICATION Formula: Soec. No. PRODUCT: PUNT & DIV. Thermobestos Block and P/C (Lime Silica) ------ ------------ i v <t SPEC NO. PAGE NO. Mvl II 4324-10 1 Material Std. Formula Percent F.P.S. 44.19 F.P.S. *41.14 ---------J.M. Fiber P.S. 11-3299 -- Celite 256-C*** * Celite 392 Hydrated Lime 4D28 Fiber Aqua Black Water 600 lbs. 650 lbs. 1250 lbs. 300 lbs. 2 qts. * 21.5 : 23*2t 44.6 NOTES: Above is 15*0 to 1.0 Water Solids Ratio Batch made up to a total of 5*032 gallons. * For each batch of Thermobestos* 2,800 pounds of raw material's are made up to a final volume of 5*032 gallons with hot lime silica tailing water and service water. v^ . ** Milled fiber used in formula. Three hundred pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops and line loss. *** Batches containing 256-C Celite Marked L, M, and H, will be:, treated by adding the following quantities of Aluminum Sulphate tc ` the batchxjust prior to the addition of the Celite to pre-mixer: L - (25-30 minutes) Add 8 pounds per batch. vV.' M - (35-55 minutes) Add 5 pounds per batch. ; j H - (60 plus minutes) No additive. .. Production should be scheduled to conform to the following gel times: ' - a. Minimum - 1-3/4 hours b. Maximum - 3-1/2 hours c. Optimum - 2 hours and 10 minutes * *N0TE: Predicated on 27 molder operation. 2. Weight checks are made on the bagged Celites and Lime once per shift as follows: ` r-- *7--' **g a. Weigh up nine 50 lbP bags of Lime and record. S2 21 Fri b. Weigh up six 50 lb. bags of Celite 256 and record. c. Weigh up six 50 lb. bags of Celite 392 and record. ^ t3r-o0n rr! c= I-30: Y * INDICATES CHANGE -REASON:: Revised as per Product proposal 432-64-51 AUTHORITY A. R. Girardi's letter to K. H. Slater, dated 2/5/65 releasing FOR change summary to product proposal 432-64-SI.__________________ ______~ SUPERSE ES DIR. Q.C MGR Q.C. Page 1 Same spec, issued 2/27/64 SUPR QC. PROD. SUPT PLNT. FIN. RES. Ind. T. G. LAB .Engr. Fuller DATE ISSUED 5 CRMC-Thermo&Cement-000053 PHOUUC i : ui v iiun. "IP" afiiWD&EFORMULA: Standard Furnish; Spec. Ho. Theraobestos Blocks & P/C (lima Silica) i Batch Weight Celite 256-C Celite 392 Mississippi Lime Crude Fiber Blend _ 60C# 300 900 for Thermdbestos Prod.** 275 2075# 28.9# 14.5 42^4 I3V2 100.0$ p.s. 63299 Aquablak Water 2 qts< .* r Notes; * - Hot Lime-Silica tailing water and service water is used to make a ratio of 25 gallons of water to 1 pound of solids, Water must be kept free from magnesia contamination. ** - Crude Fiber Blend consists of following: W-3 Amosite D-3 Amosite - 1. Minimum Gel time shall be 1.5 hours. 2. Full hag quantities are not weighed - part bag quantities shall be weighed. , i 3. When Crude Fiber Blend is not available due to Attrition Mill failure "T" Blend or "I" Blend (until current inventory of "I" 31andx4s exhausted) from "C" Building may be used as alternates oh a pound for pound basis. ' 4. .'ill incoming lime and celite will be identified and stencilled With lot numbers assigned by Control Laboratory. Ho lime dr celite is to be used until it is released by Control Laboratory. Stocks should be arranged so that oldest material is used first. M. *s o c5 32 o --4 3S o o Y_A. INDICATES CHANGE . -REASON: General Revision. 'V ) AUTHORITY -- FOR CHANGE Memo of P.D. Cannon dated 5/27/54. / FILE-HOLDERS SUPERSEDES: Form 50132 10 PRINTED IN U.S.A. CONTROL IffibuSmR:-P. & SI- WAUKEGAN __ _______ COSQNUUTAPRL*O.. L PURPOTD.. FOPINFUAFNNICCTEE res/arch \JA. CODNNUOTARRL.O. L COQDNUITRA DATE 18SUEI See Reverse Side. J>UhL 6 195 CRMC-Thermo&Cement-000054 I Johns-Manvllle MANUFACTURING SPECIFICATION Formula: Soec. No. PRODUCT: `* Thermobdstoa Block and P/C (Lime Silica) PLANT & DIV. SPEC NO. PAGE NO. . Material Std. Formula Mvl II 4324-10 1 Percent " ' ' ^ F.P.S. 44.19 F.P.S. *.41.14 ------ J.M. Fiber p.s. 11-3299 ------- Celite 256-C*** CelitO 392 Hydrated Lime 4D28 Fiber Aqua Black Water 600 lbs. 650 lbs. 1250 lbs. 300 lbS. jf-fr 2 qts. * 21.5 23/2 ,, 44.6 ' 10 NOTES: Above is 15*0 to 1.0 Water Solids Ratio < Batch made up to a total of 5*032 gallons. .* For each batch of Thermobestos, 2,800 pounds of raw materials are made up to a final volume of 5*032 gallons with hot lime silica tailing water and service water. ** Milled fiber used in formula. Three hundred pounds of- crude fiber weighed at the mill (Sprout Waldron plua Vertical Willow). No allowance made for loss due to drops and line loss. , *** Batches containing 256-C Celite Marked L, M, and R, will be treated by adding the following quantities of Aluminum Sulphate t< " the batch just prior to the addition of the Celite to pre-mixer: X L - (25-30 minutes) Add 8 pounds per batch. .... M - (35-55 minutes) Add 5 pounds per batch, H - (60 plus minutes) No additive. ' 1. Production should be scheduled to conform to the following gel times: - a. Minimum - 1-3/4 hours b. Maximum - 3-1/2 hours c. Optimum - 2 hours and 10 minutes * *N0TB: Predicated on 27 molder operation. 2. Weight checks are made on the bagged Celites and Lime once per shift as follows: a. Weigh up nine 50 lb. bags of Lime and record. b. Weigh up six 50 lb. bags of Celite 256 and record, c. Weigh up six 50 lb. bags of Celite 392 and record, DO fT 20 '$ rri. SET rn r3-?v F r . 333-2 Ptd. n U.S.A. _ INDICATES_DrAC.nw. ,, change______so ` Revised as per Product Proposal 432-64-SI _________ ^ AUTHORITY A. R. Girardi's letter to K. h! Slater, dated 2/5/65 releasing FORCHANGF summary to product proposal 432-64-SI.__________________ ' SUPERSE es DIR. Q.C. MGR Q.C. page x Same spec, issued 2/27/64 SUPR Q C. PROD. SUPT PLNT. FIN. RES. Ind. T. G. UB Engr. Fuller DATE ISSUED JUN 2 4 IQRCp CRMC-Thermo&Cement-000055 ! < 7 ' ; *i Johns-Marwlllo MANUFACTURING SPECIFICATION Formula: PRODUCT: Thermobestos Block and P/C (Lime Silica) T PUNT & DIV. SPEC NO. PAGE NO. Mvl IL;: ?V /4324-101 Standard Furnish Spec, No. Material ALTERNATE Std. Formula Formula Percent F.P.S. 44.1? F.P.S. 41.14 P.S. 11-1827 J.M. Fiber Celite 256-C**** Celite 392 . Hydrated Lime W-3 Amoslte Fiber *** 4D28 Fiber 600 lbs. 700 lbs. 450 lbs. 35^ lbs. .1050 lbs. 1050 lbs. LlQ lbs.** -25Q:J]*s^ ' lOOlbS. ... 53B6"TEi7 2350 lbs. : 2$' .6'!-v 19..1 44.7 6.4 4.2 ' P.S. 11-3299 Aqua Black Water # 2 qts. * 2 qts. (M an alternate the Plant can use 100$ W-3 for orders involving IgLlitary Spec. MII-I-278ID and MH-I-2819D. This m$y be done to ^ciiltate manufacture and to-meet the density and thermal conductivity requirements of the specifications if it is deemed advisable.) NOTES: Above is 17.5 to 1.0 Water Solids Ratio. Batch made up to a total of p,032 gallons. * For eaoh batch of Thermobestos, 2,350 pounds of raw materials are made up to a final volume of 5>032 gallons with hot lime silloa tailing water and service water. ** Milled fiber used in formula. One hundred and fifty pounds of erude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops and line loss, *** Fiber is processed in pre-mixer with hot H2O for 15 minutes. > This fiber is not processed in attrition mill. **** Batches containing 256-C Celite Marked L, M, and H, will be treated % by adding the following quantities of Aluminum Sulphate to the / batch just prior to the addition of the Celite to pre-mixer: Lv~- (25-30 minutes) Add 12 pounds per batoh. M - (35-55 minutes) Add 8 pounds per batch. H - (60 plus minutes) No additive, 1. Production should be scheduled to conform to the following gel a. Minimum.- 1-3/4 hours b. Maximum - 3-1/2 hours , c. Optimum - 2 hours and 10 minutes * NOTE: Predicated on 27 molder operation. J-fyj % -'cnSes-*eas* lSS.&ggvWFmW:ti4 approved by AUTHORITY FOR CHANGF D. B. Wingerter's letter of 2/3/64 SUPERSE ES DIR. MGR Y~Q.C V Q.C. Page 1 Same spec, issued 4/18/63 SUPR QC. PROD. SUPT PLNT. FIN. RES. LAB _EInngdr.. Fuller! DATE ISSUED FEB 27 1964 !/]//> 17 CRMC-Thermo&Cement-000056 >. T( Cl Johns-Manville MANUFACTURING SPECIFICATION FOHMtTLAi PROOUCT: Thermobostes Bloek and P/C (Lima Slliaa) 4T>J PLANT & DIV. 4. SPEC NO. PAGE NO. Mamrills II 4524-10 1 Standard Furnish Saaa. Bo, PoESo 44,,19 PoP.So 4lol4 PoSo 11-1827 ( PoSo 11-5299 Material Calita 256-C**** Calita 592 Hydrated Lima W-3 Amoaita Fiber*** *<3' Aquablak Water Batah 700# 550 1050 250** 2350# ytsmli 29o8 14*9 440 7 104 IOO0O5C 2 quarta * C Botest Abere ia 175 to 1 Water Solids Ratio. Batah made up to a total of 5032 gallenso * * For aaeh batch of Thermobestoa, 2,350 panada of raw materials ara made up ta a final reluma of 5032 gallons with hot lima si lisa tailiag water and aerriee watero ** Milled fiber used ia formula. Two hundred and fifty pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow)o Be allowance made for less due to drops and lima lasso *** Fifty (30) pounds of AX-4, 3095 or A628 Fiber, wham arailable, nay replace 50# of the V-5,, **** Batohaa cant aiming 256-C Calito Marked L, M and H will be treated by adding the following quantitiee of Aluminum Sulphate to the batah just prior ta the addition of the Cellte to pre-mixert L - (25-50 minutes) M - (35-55 minutes) H - (60 pins minutes) Add 12 pounds par batah. Add 8 pounds par batehc Be additire. Production should be scheduled to conform to the following gal timest So Minimum - 1-3/4 hours b. Maximum - 3~l/2 hours So Optimum - 2 hours and 10 minutes* Soto* Predicated on 27 solder operation,. RETURN TO J-M RESEARCH X-'Sf-EASON: p, + ^ * FILt KOOM change Chance to maw numbering arstam ( AUTHORITY ? for change Verbal agreement between Rasaarah, HamTille Plant add DHQ SUPERSEDES: < Pane 1 DIR. MGR. SUPR. Q.C. Q.C. Q.C. name PROD. SUPT. anealfleat-i an ianuid 5/25/62 . PENT. RES. Imdo T 0 Go FIN. LAB. Fuller (Old Bo TH-l'J DATE " ISSUED 4-18-63 ' CRMC-Thermo&Cement-000057 r V w \lohns-Manvllle MANUFACTURING SPECIFICATION FORMULA: PRODUCT: Thermobestos Block and P/C (L;Ljne Silica) PLANT .4 D'V. PAGE NO. Manville II TH<t -to 1 Standard Furnish Spec. No.______ _ Material F.P.S. 44.1 F.P.S. 41.1 P.S. 11-1827 '(*7837 Celite 256-C**** Celite 392 Hydrated Lime W-3 Amosite Fiber*** Batch Weight Percent 700# 350 1050 250** " 291.1.8 14.'9 44.7 10.6 2350# 100.0# P.S. n-3299 Aquablak Water 2 quarts * Notes: Above is 17.5 to 1 Water Solids Rfctio. Batch made up to a total of 5*032 gallons. ...... * For each batch of Thermobestos, 2,350 pounds of raw materials are made up to a final volume of 5*032 gallons with hot lime silica tailing water and service water. ** Milled fiber used in formula. Two hundred and fifty pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertioal Willow). No allowance made for loss due to drops and line loss. *** Fifty (50) pounds of AX-4, 3093 or A628 Fiber, when available,! may replace 50# of the W-3. **** Batches containing 256-C Celite Marked L, M and H will be treated by adding the following quantities of Aluminum Sulphate to the batch Just prior to the addition of the Celite to pre-mixer: L - (25-30 minutes, M - (35-55 minutes, H - (60 plus minutes) Add 12 pounds per batch. Add 8 pounds per batch. No adltive. 1. Production should be scheduled to conform to the following gel times a. Minimum - 1-3/4 hours b. Maximum - 3-1/2 hours c. Optimum - 2 hours and 10 minutes `Note Predicated on 27 molder operation. RETURN TO J-M RESEARCH !ND:CAT EX CHANGE AUTHORITY For chano _,,FIUE RL7 Remove reference to Mississippi and Warner Limes. E.C.Lindstrom*s letter to R.W.Honnig dated 5/1/62. SUrt.'CEDE DIR. ~| M C f?. Page 1 same spec, issued 4/25/62. Ind. Eng. i DATE n.U L'L =/2c/62 CRMC-Thermo&Cement-000058 Johns-Manvllle MANUFACTURING ' SPECIFICATION r FORMULA: PRODUCT: Thermobestos Block and P/C (Lime Silica) Standard Furnish Spec. No. F.P.S. 44.19 F.P.S. 41.14 p.s. 61827 -- Material Celite 256-C**** Celite 392 Mississippi Lime W-3 Amosite Fiber*** PLANT & DIV. SPEC NO. PAGE NO. Manville II TH-dr 1 A Rsfcrth . Weight Percent 700# 350 1050 250** 29.8 44.7;.jjauL. 2350# 100.0# p.s. n-3299 -- Aquablak Water 2 quart s * Notes: Above Is 17.5 to 1 Water Solids Ratio. c . Batch wade uo to a total of 5*032 gallons Warner Co. Hydrated Lime is an acceptable alternate lime. * For fcaSTTbatch of Thermobestos, 2,350 pounds or raw materials are made up to a final volume of 5*032 gallons with hot lime silica tailing water and service water. ** Milled fiber used in formula. Two hundred and fifty pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops and line loss. *** Fifty (50) pounds of AX-4, 3093 or A628 Fiber, when available, may replace 50# of the W-3. *##* . Batches containing 256-C Celite marked L, M and H will be treated by adding the following quantities of Aluminum Sulphate to the batch Just prior to the addition of the Celite to pre mixer: L - (25-30 minutes) M - (35-55 minutes) H - (60 plus minutes) Add 12 pounds per batch. Add 8 pounds per batch. No additive V. 1. Production should be scheduled'to conform to the following gel times: ,, a. Minimum.- 1-3A hours b. : Maximum,- 3-1/2 hours c. Optimum - 2 hours and 10 minutes* Note: Predicated on 27 molder operation. INDICATES * " CHANGE reason Addition of Warner Lime as alternate. Return to G AUTHORITY FOR CHANGE E.C.Lindstrom, J-M RESEARCH SUPERSEDES; Page No. 1 same spec, issued 3/14/62 TTIFR0OM SMDIR. MGR. SL'^R. o.c. ^ j DATE 1 ISSUED APR 2 5 1962 CRMC-Thermo&Cement-000059 r C / \ c JohnsMarollte MANUFACTURING SPECIFICATION PRODUCT: Thermobestos Block and P/C (Lime Silica) FORMULA: Standard Furnish Spec. No. F.P.S. 44.19 F.P.S. 41.14 P.S. 61827 Material Celite 256-C**** Celite 392 Mississippi Lime W-3 Amosite Fiber*** PUNT & DIV. SPEC NO. Manville II TH-1 PAGE NO. j1 Batch Weight Percent TOO# 350 1050 250** 2350# 29.8 1-4.9 4140..76. 100.0# P.S. 11-3299 Aquablak Water 2 quarts * Notes: Above is 17.5 to 1 Water Solids Ratio. Batch made up to a total of 5>032 gallons For each batch of Thermobestos, 2,350 pounds of raw materials are made up to a final volume of 5>032 gallons with hot lime silica tailing water and service water. ** Milled fiber used in formula. Two hundred and fifty pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops and line^-- loss. ---------- *** Fifty 50) pounds of AX-4, 3093 or A628 Fiber, when available, may replace 50# of the W-3. **** Batches containing 256-C Celite marked L, M and H will be treated by adding the following quantities of Aluminum Sulphate to the batch just prior to the addition of the Celite to pre- ' mixer: L - (25-30 minutes) M - (35-55 minutes) H - (60 plus minutes) Add 12 pounds per batch. Add 8 pounds per batch. No additive 1. Production should be scheduled to conform to the following gel t/ iin6 3 a. Minimum,- 1-3/4 hours b. Maximum - 3-1/2 hours c. Optimum - 2 hours and 10 minutes* ... Note: . Predicated on 27 molder operation. RETURN TO J-M RESEARCH FILE-ROOM-- INDICATED CHANGE reason: To incorporate 17.5 to 1 Water Ratio shown in --------------De Y---#5.v.t______________________________________;_______ AUTHORITY . ,, ,- forchange Letter E.C.Lindstrom to R.W.Honnig dated 1/22/52. SUPERSEDE; Page 1 of same specification issued 5/18/61. DIR. Q C. MGR. Q.C. SU PR. C C. PROD. SUPT. PLNT. FIN. RES. UB. "Ik ISSUED MAR 1 4 1962 CRMC-Thermo&Cement-000060 Johns-Manville MANUFACTURING SPECIFICATION PRODUCT: Thermobestos Block and P/C (Lime Silica) PUNT & DIV. SPEC NO. PAGE NO. Manville II TH-1 FORMULA: Standard Furnish Spe o. No. F.P.S. 44.19 F.P.S. 41.14 P.S. 61827 r p.s. 11-3299 Material Cellte 256-C**** Cellte 392 Mississippi Lime W-3 Amosite Fiber*** Aquablak Water Batch WeightPer Cent 600# 300 900 250** 2,050# 29.27 14.. 63 43/90 12.20 100.00# 2 quarts * Notes: * For each batch of Thermobestos, 2,050 pounds of raw materials are made up to a final volume of 5*032 gallons with hot lime silica tailing water and service water. ** Milled fiber used in formula. Two hundred and fifty pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops and line loss. / V. *** Fifty (50) pounds of AX-4, 3093 or A628 Fiber, when _ available, may replace 50# of the W-3. **** Batches containing 256-C Celite marked L, M and H will be treated by adding the following quantities of Aluminum Sulphate to the batch just prior to the addition of the Celite to pre-mixer: L - (25-30 minutes) Add 10 pounds per batch. M - (35-55 minutes) Add 6 pounds per batch. H - (60 plus minutes) No Additive r 1. Production should be scheduled-to conform to the following gel times: a. Minimum - 1-3/4 hours b. Maximum - 3-1/2 hours c. Optimum - 2 hours and 10 minutes* *Note: Predicated on 27 molder operation. RETURN to J-M RESEARCH' INDICATES To- rewrt"tD_250"lbs. W-3 "Aftosite Fiber". RLE ROOM* CHANGE -REAS0N' G AUTHORITY FOR CHANGE E. C. Lindstromvs letter of 5/5/61 to R.W.Honnig. SUPERSEDES: DIR. Q.C. MGR. Q.C. SUPR. Q.C. Page #1 of same specification issued 4/6/61. PROD. SUPT. PLNT. FIN. RES. LAB. IND. ENG. date 1 MY 1 8 1961 ISSUED .* CRMC-Thermo&Cement-000061 Johns-Manville MANUFACTURING SPECIFICATION r \ PRODUCT: y o s-- Thermobestos Block and P/C (Lime Silica) PLANT & DIV. SPEC NO. PAGE NO. Manville II TH-1 FORMULA: Standard Furnish Spec. No. Material F.P.S. 44.19' Celite 256-0 **** F.P.S. 41.14 Celite 392 P.S. 61827-1 Mississippi Lime W-3 Amosite Fiber *** ( Batch Weight Per Cent 600# 300 900 225 * 2,025# 2LQ.6 m* .4^4 11'.2 100.0# P.S. 11-3299 Aquablak 2 quarts Water c Notes: For each batch of Thermobestos, 2,025 pounds of raw materials are made up to a final volume of 5,032 gallons with hot lime silica tailing-water and service water. Milled fiber used in formula. Two hundred and twenty-ive pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops and line loss. *** Fifty (50) pounds of AX-4, 3093 or A628 Fiber, when available, may replace 50# of the W-3. Batches containing 256-C Celite marked L, M and H will be treated by adding the following quantities of Aluminum Sulphate to the batch just prior to the addition of the Celite to pre-mixer: 25-30 minutes, 35-55 minutes. 60 plus minutes) Add 10 pounds per batch. Add 6 pounds per batch. No Additive Production should be scheduled to conform to the following gel times: _ a. Minimum - 1-3/4 hours b. Maximum - 3-1/2 hours c. Optimum - 2 hours and 10 minutes* RETURN TO*Note: Predicated on 27 molder operation. J-M RESEARCH _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ FILE ROOM INDICATES CHANGE -REASON: To incorporate Deviation #27 dated 8/10/60 into Spec. AUTHORITY FOR CHANGE E. C. Lindstrom. SUPERSEDES: Page #1 of DIR. Q.C. MGR. Q.C. SUPR. Q.C. PROD. S'jpr. same PLNT. FIN. specification issued 8/1/60 stAB. IND. ENGR. DATE ISSU ED APR 6 19611 CRMC-Thermo&Cement-000062 Johns-Manville PRODUCT: MANUFACTURING SPECIFICATION r Thermobestos Block and P/c (Lime Silioa) PLANT & DIV. SPEC NO. PAGE NO. Manville II TH-1 1' FORMULA: Standard Furnish Spec, No. Material Batch freight Per Pent* F.P.S. 44.19 F.P.S. 41.14 P.S. 61827 Celite 256-C**** Cellte 392 Mississippi Lime W-3 Amosite Fiber*** 600# 300 900 250** 29:27 14.63 43.90s 12.20 C 2,050# 100.00# P.S. 11-3299 Aquablak Water 2 quarts # c Notes: * For each batch of Thermobestos, 2,050 pounds of raw materials are made up to a final volume of 5,032 gallons with hot lime silica tailing water and service water. ** Milled fiber used in formula. Two hundred and fifty pounds . of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops r and line loss. *** Fifty (50) pounds of AX-4, 3093 or A628 Fiber, when available, may replace 50# of the W-3. **** Batches containing 256-c celite marked L, M and H will be treated by adding the following quantities of Aluminum Sulphate to the batch Just prior to the addition of the Celite to pre-mixer: L - (25-30 minutes) M - (35-55 minutes) H - (60 plus minutes) Add 10 pounds per batch. Add 6 pounds per batoh. No Additive 1. Production should be scheduled to conform to the following gel times: RETURN lu J-M RESEARCI FILE ROOM *Note: a. Minimum - 1-3/4 hours b. Maximum - 3-1/2 hfeurs 0. Optimum - 2 hours and 10 minutes* Predicated on 27 raolder operation. C* INDICATES CHANGE -- REASON: TO show new gel time limit for M & H Celite. AUTHORITY FOR CHANGE E. C. Lindstrom. SUPERSEDES: Page #1 of same specification issued 12/10/59. DIR. MrQ.C. MGR. Q.C. SUPR. Q.C. PROD. SUPT. PL NT. FIN. 8$. date AUG 1 I960 ISSUED CRMC-Thermo&Cement-000063 CRMC-Thermo&Cement-000064 Johns-Manville MANUFACTURING SPECIFICATION PRODUCT: Thermobestos Blocks and P/C (Lime Silica) &PLANT DIV. T~ -------jManville II SPEC NO. PAGE NO. : TH-1 |1 of 19 FORMULA: Standard Furnish Spec. No. F.P.S. 44.19 P.P.S-..41.14 p.s. 61827 P.S. 63299 Material Celite 256-C**** Celite 392 Mississippi Lime W-3 Amosite Fiber*** Aquablak Water Batch Weight Per Cent' 600# 29.27 300 14.63/ 900 43.90 250** 12.20 2o5o# 166.06$ 2 quarts * Notes: * For each batch of Therraobestos, 2,050 pounds of raw materials are made, up to a final volume of 5>032 gallons with hot lime silica tailing water and servioe water. ** Milled fiber used in formula. Two hundred and fifty pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops and line loss. c *** Fifty (50) pounds of AX-4, 3093 or A628 Fiber, when available, may replace 50# of the W-3. **** Batches containing 256-C Celite marked L, M and II will be treated by adding the following quantities of Aluminum Sulphate to the batch just prior to the addition of the Celite to pre-mxer: LMH- '25-30 minutes) Add 10 pounds per batch. ,35-50 minutes) Add 6 pounds per bateh. (50 plus minutes) No additive. Production should be scheduled to conform to the following gel times: _ RETURN TO J-'.l RESEARCH t<o i. G| FILE ROOM a. Minimum - 1-3/4 hours b. Maximum - 3-1/2 hours c. Optimum - 2 hours and 10 minutes* *Note: Predicated on 27 molder operation. 0 INDiCATE CHANGE "Supply of AX-4, 3090 ana A628 Fiber~Ts depleted. To RLA3o0NN show addition of Aluminum Sulphate when using L,M&H Cfllijt s? i Fo^ctHANr-c Lindstrom and Produot Proposal 432-41. E I Page #1 of same "specif ication "issued 11/14/58 and Notice of UPERSoEtLD/S Deviations #20 issued 4/14/59 and #69 issued 11/18/59. DIR. MGR O.C. r,n; 1cyvSn imd. r.N. NGR. DATE ISSUED DEC 1 0 1959 " Yvm77*r- CRMC-Thermo&Cement-000065 Johns-Manville MANUFACTURING <r SPECIFICATION PRODUCT: 2^ Thermobestos Blocks and P/C (Lime Silica) " PLANT & DIV. SPEC NO. PAGE NO. Manville II TH-1 1 of 19 FORMULAS Standard Furnish Spec. No. P.P.S. 44.19 Material Celite 256-C Batch Weight------- Per Cent '<et ` 600# 29.27* F.P.S. 41.14 Celite 392 300 14.63 P.S. 61827 Mississippi Lime 900 43.90 W-3 Amosite Fiber 200** 9.75 r AX-4 or 3090 or A628 50** 2.45 2050# 100.00* p.s. 63299 Aquablak 2 qts. Water * G Notest * For eaeh batoh of Thermobestos, 2,050 pounds of raw materials are made up to a final volume of 5,032 gallons with hot lime silioa tailing water and service water. ** Milled fiber used in formula. Two hundred and fifty pounds of orude fiber weighed at the mill (sprout Waldron plus Vertloal Willow). No allowance made for loss due to drops and line loss. 1. Production should be scheduled to conform to the following gel timess G a. Minimum - 1-3/4 hours -- b. Maximum - 3-1/2 hours o, Optimum - 2 hours and 10 minutes* Note: Predicated on 27 molder operation. RETURN TO J-M RESEARCH FILE ROOM G y _INDICATES DrAcn,. To show change in relative amounts of W-3 and AX-4 and X-- ^uAMor --REASON: change addition of alternate fibers. ____________^ ^ authority e.c. Lindstrom per Agreements Manville Celite Meeting 11/6/56. FOR CHANGE SUPERSEDE; Page #1 of same specification issued 7/11/58. DIR. Q.C. MGR. Q.C. SUPR. i p.-OC. j ILM. J IC.C. SUIM. i P.T ! IND. ENQR. 1GLH0V 1 i '95* i ISSUED CRMC-Thermo&Cement-000066 Manufacturing Specifications Manvills Theriftobestoa -PLANT -DEPT. FORMULAt Standard Furnish. Theraobestos Blocks and P/C (Lisa Silica) </-3 v -5H-4- Spec. No, Material Wiser per cent F.P.S. 44,19 cent 256-c 600# 29.27$ F.P.S. 4l.l4 Celite 392 300 14,63 _.r FPS, 61827 Mississippi Lime 900 43.90 3 Amos its Fiber 170** 8.20 AX4 80** 4.00 2050# 100.00$ p.s. 63299 Aquabl&k Water 2 qts. notesi * For each batch of Theraobestos, 2,050 pounds of raw materials are wade up to a final volume of 5*032 gallons with hot line silica tailing water and service water, . Milled fiber used In formula. Two hundred and fifty pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops and line loss. Production should be scheduled to conform to the following gel times: a, Mitiisam - 1-3/4 hours b, Maxisam - 3-1/2 hours e. Optimum - 2 hours and 10 minutes * ' , *Note< Predicated on 2?' molder operation, return to j-M RESEARCH file room FORM 90132*10 PRINTED IN U.8.A. X-,chanIes_REA80N! To elioer use of fiber blend and to reflect automatic ----------------------------- .--------------- -------------------------- ;-aqsiipaento FORCHANGE E.C, Lindstro. FILE-HOLDERS SUPERSEDES: page IND. EN8R a CONTROL LAB.j 8UPR. QUAL. CONTROL PROS. SUPT. 1 of sqm specification issued 5/24/57 DATE ISSUED W JUL 11 19 CRMC-Thermo&Cement-000067 manufacturing specifications Many1 lie -PLANT Magnesia. -DEPT. FORMULA; PRODUCT! DIVISION Thermobestos Blocks and P/C (Lime Silica) SPEC. NO. TH-1 PASE NO. 1 Standard Furnish: ry /" Spec. No. F.P.S. 44.19 Material Celite 256-c Weight 600# Ter 'Cent 29.27^ F.P.S.- 4.1.14 Celite 392 300 14.63 F.P.S. .61827 Mississippi Lime 900 43.90 -3 Amoslte Fiber 250** 2050# 12.20 100.00# P.S. 63299 Aquablak '" . ' . ' ` Water 2 qts ' Notes: * For each batch of Thermobestos, 2,050 pounds of raw materials are made up to a final volume of 5*032 gallons with hot lime silica tailing water and service water. . ** Milled fiber used in formula. Two hundred and fifty pounds of crude fiber weighed at the mill (Sprout Waldron plus Vertical Willow). No allowance made for loss due to drops and line loss 1.Production should be scheduled to conform to the following gel times: (a} Minimum - 1-3/4 hours fb) Maximum (s) Optimum - 2-3/4 hours , 2.All bag quantities shall be weighed and the total weight adjusted to formula requirements. 3.All incoming Lira and Celite will be identified and stencilled with lot numbers assigned by Control Laboratory. No Lime or Celite is to be used until it is released by Control Laboratory. Stocks should be arranged so that oldest material is used first. FORM 80132-10 X.INDICATES CHANGE "REASON: To reflect latest approved practice AUTHORITY _ FOR CHANGE FILE-HOLDERS j .Result of Meetings --n---- Watson Ind. Cdntro 1 -4-------- Engr. Lab. on Thermobestos Quality problems SUPR. QUAL. CONTROL PROD. SUPT ( PLANT FINANCE OFFICE RESEARCH Mgr. I dir. QUAL. QUAl CONTROL CONTR Page 1 of same specification issued 9/20/56. M'ra CRMC-Thermo&Cement-000068 Manville Massesla PLANT DEFT. FORMULA: Standard Furnish: ThtfoDoctoo motto M p/5 Jiam iiu) /i V Spec. No. F.P.S. 44.19 F.P.S. 4l.l4 P.S. 61827 p.s. 6329s Material Cellte 256-C Celite 392 Mississippi Lime W-3 Amosite Fiber Aquab iak Water Batch WeigKt- Per cent 600# 300 29.27# uf 1 14.63 900 43.90 250 .** 050$ 12.20 150700# 2 qts. * j. Notes: * - Hot Lime Silica tailing water and service water is used to make a ratio of 2.5 gallons of water to 1 pound of solids. Water must be kept free from Magnesia contamination. ** - Use 250# of Milled Fiber. (Sprout-Waldron plus Vertical Willow). 1. Minimum gel time shall be 1-5 hours, Optimum gel time is 2.0 - 2.5 hours and should be scheduled. 2. Full bag quantities are not weighed - part bag quantities shall be weighed. 3- All incoming Litae and Celite will be identified and stencilled with lot numbers assigned by Control Laboratory. No Lime or Celite is to be used until it is released by Control Laboratory. Stocks ahould . be arranged so that oldest material is used first. ww aoiaa-fo *,NTKD m U.O. X-'^NTM "MASON: Corrections AUTHORITY - FOR CHANGE Letter of A.B. Cummins dated 3/13/56 and production conourranc FILE-HOLDER* WATSON Ind.ENGR. CONTROL WKQJ LAB. COtQuNUTrARtL..OL HOD. POR1PNIATAINCNTSCI RRLSAIANR.CH COONNUOTARRL.O. L COODNIIIARTII supersedes: page #1 0f same specification issued 1/27/56. DATE ISSUEt APR 10 19 CRMC-Thermo&Cement-000069 Marvilie Mag nesia -PLANT FORMULAi Stands r.4 Furniah s PRODUCT: Dl Thermohe stos Electee and p/c (Lime Silica) PAGE NO. X\ Spec* Mo, Material .batch WeigHt Per Cent F.P-S. 44,19 F.F.S. 41.14 Celite g5<5-c Celite 393 600# 3C0 . 29*27/:'' -i 14,63 F.P.S. 61827 Mississippi Lime - 900 43 * 90 11-3 Araosite Fiber? 250** mm 12,20 mr?m ?*s. 63299 Aquablak Water 2 qts, ' Motes % * For each batch of. Thearaobestos, 2,050 pounds of raw materials are made up to a final volume of . 5a03S gallons with hot lira silica tailing water and service water, `4 * ** Milled fibre used in formula* Two hundred said fifty pounds of crude fibre weighed at the mill (Sprout Waldron plus Vertical Willow), Mo ' allowance made fcv loss due to &i?ot>b and ii^e loss 1*7? 1 .Minimum gsl>iae shall re JUr^ hours, Optimum gel time is * J^fLturars and should be sehoclulcd., 2, All bag Quantities shall be weighed and the total weight adjusted to formula requirements, ' . 3, All incoming Lime and Celite will be identified and stencilled. with lot numbers assigned l:j Control Laboratory, Mo Lime or Celite is to 'be iv:**d until it is released by Control Laboratory., Stocks- suouiijr fee arranged so that oldest material is'used first. Return to J-M RESEARCH file room X--'^anoe8-rea8N! corrections-To reflect, present Manufacturing . pyg.e 1: s , Ml 9008-10 \NTBD IN U.8.A* MeetingAUTHORITY -- FOR CHANGE of .Research Production & Quality Control of .9/12/56* FILE-HOLDERS Watson Ind Engr. Control Lair ,, SUPR. QUAL. CONTROL PROD. SORT, PUNT PINANCK OPPICI RESEARCH UR. NCR. QUAL. CONTROL DIR. QUAL. CONTRC SUPERSEDES: jPsge #1 of s<vffi;i epeclfie&tiori issued 4/10/56 DATE ISSUED 0 1958 CRMC-Thermo&Cement-000070 RETURNTO J-M RESEARCH FILE ROOM X--1 change8 ~REASON! General Revision. CRMC-Thermo&Cement-000071 Manufacturing Specifications MAHVILLE MAGNESIA ' -DEPT. -PLANT PRODUCT: IP DIVISION. Thermobestos Blocks and Pipe Covering (Lima Silica) m~X6 PAGE NO X INi'UUU biWiFIOATiON -y' X FOaMULA? SpaCo Nc, 11 idriwii---- Material Batch* M.S, PC-226il P,S, 6182$ Celite #256~C Fiber Blend for Thenaobestos Products I^drated Lie 202" Solution Lime Silica Plastic Hot Water , $203# 10 0 Hotsei *Siza of batch may b varied to allowed limit of gel tankso **!Jp to 10% of Lima Silica Plastic may be added to each batcho **-inough to make a total gallonage of 5500 gallons, This figure is'based upon an addition of 10$ Plastic and 2=5 to 1 solid ratio,, BfriNUFACTBRING IMSBHJCTXCMSb ..... . No tot &m iifa^iirlng~Sp<?cification MG<=-0il for Flow Chert of Operation, XX A, Mining Oparation; ' '' 1= ""Run'Tint"TLsa silica tailing water from storage tanks into paddle mixer up to shaft* Desired temperature of water 175 - 185F Note? Above temperature is not essential* . 2,, Add Celite and mix three minutes, 3= Add fiber, ko Add Lime Silica Plastic if desired, not to exceed 10$ of total batch weight,, 5o Add Hydrated Lime and mix ten minutes, 6, Add water to a level If* from the top of tank and mix for five minutes, 7, Add approximately 3/?4 gallon 202 as'water runs in, - 8, ffith mixer running* start pump and pump into gel tank, . 9o Flush out mixing tank with approximately two hundred gallons of hot water, , .......... . . RETURN TO J-M RESEARCH To &rm larger Batch siae, ' / X--'ch'ange8 " RE^Nfc To show temperatiare of water Additional information? see letter of JJt, Robson to E,C AUTHORITY FOR CHANGE f dated PILE-HOLDERS ' I iD.ENQ. WTOo Page L ox-------------------------- #] gas Spec, issued 3/3/53, RUPR. QUAL. CONTROL PROD. SUPT. PUNT FINANCE OPP1CI RESEARCH LAB, H6R. QUAL. CONTROL DIR QUA OONT DATE ISSUJ^j CRMC-Thermo&Cement-000072 Manufacturing Specifications MANVILLE MAGNESIA -PLANT IP D1VI8ION- Thermobestos Blocks and Pipe Covering (Liras Silica) */3 tiPLC. NU. MO-16 PAGE NO. Formula; Batch*' <o F Specc No, Material In eight Per Cent M,S, PC-226;1 CglTCfe"ff256^r~"---------Fibre Blend for Thermobestos 750F TiTub$" Producte 212 12.7 P,S. 61825 Hydrated Lime 710 ...... kZ& - "202" Solution t;sw 3/k Gal, * - Lima Silica Plastic 167 10,0$** Hot Water *** c Notes; *Siae of batch may be varied to allowed limit of gel tanks, **Up to 10$ of Lime ^jllica Plastic may be added to each batch* ***Enough to make a total gallonaga of h600 gallons6 This figure is based upon an addition of 10$ Plastic and 2c5 to 1 solid ratio. Manufacturing Instructions; Note: See Manui'acturing- Specification MG*"0;1 for Flow Chart of Operation, Ao Mixing Operation: Tl Sun hot iiine""silica tailing water from storage tanks into paddle mixer up to shaft, 2, Add Celite and mix three minutes, 3, Add fibre,' ho Add Lime Silica Plastic if desired, not to exceed 10$ of total batch weight, ' Add Hydrated Liras and mix ten minuteBo 6, Add water to a level h from the top of tank and mix for five minuted, ?, Add approximately 3/i* gallon "202? as water runs in, 8, With mixer running, start pump and pump into gel tank, 23 55 50 Ss3 g O m 52 O '- 33* ^ g=a. 0: 0-HI FORM 80132-10 9o Flush out mixing tank with approximately two hundred gallons of hot water, B Gel Tank Operation: XI Before receiving batch, close outlet valve at bottom of gel mixer, * *1 ' r'*''--i ' '--i ;'n rTTr*,'j|***j^_ . Start agitator and run batch into gel tank, fi " -' -'l-j/f/T ' __'NDICATES -- REASON: CHANGE Correction AUTHORITY FOR CHANGE FILE-HOLDERS SUPERSEDES: Current Practice IND.ENG.I WKO, page i?i oi ,, saae1 sps c, issued pAia ft- _& 11H1__U -- v.. . m vdf ' R. Williams SUPR. QUAL. . CONTROL PROD. 8UPT. PLANT FINANCE OFFICE RESEARCH LAB. MGR. QUAL. CONTROL DIR. QUAL. CONTR( , Ait Til CRMC-Thermo&Cement-000073 Manufacturing Specifications MAGNESIA MANVILLE -DEPT. .IP.DIVISION. fhermobestos Blocks and Pipe Covering (Line Silica) *f3 v' MO-16 PAGE NO. #1 Formula: Spec. No, Material JK" qglgHS*" Per dent m M.S. PC-226:1 P.S. 61825 Ceiite #256-0 Fibre Blend for Thermobestos Products Hydrated Lime*** "202" Solution Lime Silica Plastic Hot Water 750# 44.8# 212 710 17573T 12.7 4i 3/4 Gal. - 167 10.0#** Enough to make total gallongage of 5*010 gallons . Notest * Size of batch may be varied to allowed limit of gel tank) ** Up to 10# of Lime Silica Plastic may be added to each batch. *** Mississippi or Warner Lime may be used. RETURNJO J-M RESEARCH FILE ROOM Manufacturing Instructions s Note: See Manufacturing Specification MG-0:1 for Flow Chart of Operation. A. Mixing Operation: 1. Run hot lime silica tailing water from storage tanks into paddle mixer up to shaft. 2. Add Celite and mix three minutes. 3. Add fibre. 4. Add Lime Silica Plastic if desired, not to exceed 10# of total batch weight. 5. Add Hydrated Lime and mix ten minutes. 6. Add water to a level 4" from the top of tank and mix for five minutes. 7. Add approximately 3/4 gallon "202n as water runs in, 8. With mixer running, start pump and pump into gel tank. 9. Flush out mixing tank with approximately two hundred gallons of hot water. B. Gel Tank Operation: 1. Before receiving batch, close outlet valve a gel mixer. Start agitator and run batch into 2. Bring level of batch up to 4*6" from top of ------- water or hot lime silica-tailing water.-------- x-`changI8 -"o*<Eo show alternate lime, _ Letter of E.G. Carlson to R. Jacobs, dated 4/6/52. AUTHORITY FOR CHANGE FILE-HOLDERS Ind.Engjr. Wkg. page #1 of same specification SUPERSEDES: FORM SOISS'IO PRINTED IN U.S.A. SUPS. QUAL. CONTROL PROD. SUPT. PLANT . FINANCE 1 "E"` Issued 3/15/52 MAY DIR. QUAL CONTR \ DATE ISSUED 9 1952 CRMC-Thermo&Cement-000074 MAMVILLR MAGNESIA -DEPT. rnjuui.1; Thermobestos Olocke cad Pips Covering (Lise Silica) 10-16 RAGE NO. v^< 1 Z formula: Material Batch j, , Weight* J0 Per pent Celite #256~c Amosite Fibre Blend Mississippi Hydrated Line *202" Solution Line Silica Plastic Hot Water 750# Ul*08 212 12,7** 710 h2,$ 1672# 100.# 3A Gl 167 10.0#*** Enough to sake total gallonage of 5010 gallons, Hoteet * Size of batch may be varied to allowed limit of gel tanks, ** Fibre Blend nay be varied as follows: (1) 50# D-3 & 50# W-3 (2) U056D-3 & 60jg W-3 (3) 60* D-3 & m W-3 *** Up to 10# of Line Silica. Plastic nay ba added to each batch. I anufacturing Instructional ' | ote> .^ee afinufacturlng Specification MB-Q*X for Flow chart of Operation, A. Mixing Operation! ' ' 1, Run hot 11m silica tailing water from storage tanks into paddle mixer up to shaft, return to J-M RESEARCH RLE ROOM 2. Add oelite and mix three minutes, 3 o Add fibre. ho Add lime silica plastic if desired, not to exceed 10# of total batch weight, 5 Add Mississippi Hydrated Lime and mix ten minutes, 60 Add water to & level fc" from the top of tank and mix for five minuteso 7. Add approximately 3/k gallon "202" as water runs in, 8, With mixer running, start pump and pump into gel tmk, 9e . Flush out mixing tenk with approximately two hundred gallons of hot water, B. Qel Tank operation: . 1, Before receiving batch, close outlet valve at bottom of gel mixer, start agitator and run batch into gel tank, '' " , ; rp fTn 20 Bring level of batch up to hi6u from top of tank With hotwatetforiiiu : lime silica tailing water. I 17 1852 XA -,NC"HJAN^GES "- REASON:.General Revision ) i f ;! L.. ! ; ; ------------------------------------------------------------------------------------------------------ -------------------------------------------------------------------------------------------------------J---------- - . :*, .- X# W authority -Product proposal #U32-pp-3, Supp. #2, dated 1/23/52 and letter L;j mfcssS-r-\ ------------- m C. LaGatt FOR CHANGE A * FILE-HOLDERS Znd. En|g. Wkg. SUPR. QUAL. CONTROL PROD. 8UPT. DIR QUA CONTI SUPERSEDES: Page #1 of Specification entitled "Thermobestos Blocks (Lime I DATE ISSUED FORM 80132-10 PRINTED IN U.8.A. Silica)" issued 13/3/51* MAH 1$ m i CRMC-Thermo&Cement-000075 ummiE Thermohestos Blocks -L1 PAOE NO. % -P Formula: Spec* No, Materialm Willowed Amoelte Fiber (HX) Celite #379 ^Hydrated lime _ Batch MSWHWWWPiii!rr-- Lbs. =**SfWS 94# 300 jT 1h Bnc ( V "" ,rc " S UgL" - ; o , :..,! O p;,OS3L?U *3?ote:. Warner or similar low magnesia, z* equivalent quick-' lime, .-. " '. Mannfac torlag Instructions ;1 1 1wa^roi << ^Kiiij m<ri > < mmi iFfTC -rrr-runrnirr'rr i> . faffnffnwwn A Mixing Operationj. / 1. Run approximately 200 Elions of water into the paddle mixer. Use; either, fresh water or water from the hot 11se-silica tailing water storage tank, 2. Add willowed fibre and mix three minut 3. Add Celite #379 And mix three minutes. 4. Add Hydrated Lime and mix fifteen minutes. 5* Add water to a level 4* from the top of tank and mi; minutes. 6. With mixer running, start pump and pump to gel tan out and run down* 7. Repeat- section A as necessary, being sure next batch goes to a different gel tank. Bo' 0X Tank'axsres <* 'rwci'sacuv&:oi Operations 80 Close outlet valve at bottom of gel tank, run anchor to bottom, of tank and run approximately 1,000 gallons of hat lime-silica tailing or plain eater from storage tank into gel tank.1;: _, 9. Fill discharge pip by-'opening and closing plug cock;start direct steam' into gel tank and notify mixer-man that ta is ready to receive slurry. ,cangIS"REASON!l: lie* Specification.. L*** d fkx^U' ** w fo^ghTnge - FILE-HOLDERS SUPERSEDES* FORM 80132*10 PRINTED IN U.8.A. ' Srflfcu-wcvt Pa aroposal 44y32i*-wP* P* -'V3 auweiiPitiiiiunM|gii; iiwjitfe'iumVC1 / (2 a v/vo/r^. ,,.XJ) I C/ ipd.Sngc1 SUM. Wkg 0QUUAAL. CONTROL MSPPURR2OPn5DTD-.. PUNT rfs FINANCE "2 >* Bone. Enter in JZeMX*. p DATE ISSUE and file in numerical order. ' /- FEB 13 185C CRMC-Thermo&Cement-000076 Manville Magnesia FORMULA: -PLANT -DEPT. PRODUCT: DIVISION-- Thermobestos Blocks and P/C (Lime Silica) TH-1 PAGE NO 1 \J- ( Standard Furnish: Spe c. No. Material hi Batch weignt Per cent .- Celite 256-C Celite 392 600# 300 ' 29.27# ' 14.63 P.S. 61827 Mississippi Lime 900 43.90 V - W-3 Amoslte Fiber 250 ** 12.20 2050# 100.00# P.S. 63299 Aquablak 2 qts. Water # Notes s * - Hot Lime Silica tailing water and service water is used to make a ratio of 2,5 gallons of water to 1 pound of solids. Water must be kept free from Magnesia contamination. . ** - Use 250# of Milled Fiber. 1. Minimum gel time shall be 1.5 hours. 2. Full bag quantities are not weighed - part bag quantities shall be weighed. 3. All incoming Lime and Celite will be identified and stencilled 'with lot numbers assigned by Control Laboratory. No Lime or Celite is to be used until It is released by Control Laboratory. Stocks should be arranged so that oldest material is used first. FORM 80131-10 PRINTED IN U.8.A. X--'NDICATES -- REASON: CHANGE To change w-3 Ataesite from 275#' Lo-SDO#. _ AUTHORITY FOR CHANGE FILE-HOLDERS supersedes: Letter.of E.C. Lindstrom to J.B. McCarty d&t6d CONTROL. WATSON IND.ENOR. WKG, LAB. SUPR. I IOVAL. CONTROL r*00' -page #1 -of'..same1-specification lapsed o/p/S N0ice of Deviation ND-886 issued 12/6/55. PLANT FINANCE OFFICE . and i/13/56. RESEARCH LAI. OR. QUAL, CONTROL DIR. DUAL. CONTRO CRMC-Thermo&Cement-000077 MANVILLE mmsw FORMULA: Standard Famish: Spec* go. P.S. 61827 P.S. 63299 -PLANT PRODUCT: Thermobestos Blocks & P/C (Lias Silica) if3>< m PAGE NC 1 7*7, Material Celite 256-C Celite 392 Mississippi Lime ^W3 Amosite Fiber Aquablak Water '//m;-r Batch Weight Per cent 600# 28.956 300 *14.5 900 43.4 275 2075# 13.2 IOO.O56 2 qts. * rt O! Botes: Silica tailing water and service water is a ratio of 2.5 gallons of water to 1 pound of solids. Water must he kept free from Magnesia contamination. X ** - Use 275# of Billowed Fiber. X 3-* Minimum gel time shall he 1. 5 hours.) 2s. Full hag quantities are not weighed - part hag quantities shall he weighed. 3. All incoming Tfime and Cellte will he identified and stencilled with lot numbers assigned by Control Laboratory. No Lime or Celite is to he used instil it is released by Control Laboratory. Stocks should be arranged so that oldest material is used first. RETURN TO J-M RESEARCH Fill ROOM x-*SIKm2* General Revision. AUTHORITY -- FOR CHANGE FILE-HOLDERS pom 00132-10 PRINTED IN U.8.A. SUPERSEDES: Memorandum of New Process Insulation Meeting Held 7/lV WATSON IND. CONTROL SUPR. AN LAS. QUAL. CONTROL PROD. UPT. PLANT FINANCE OFFICE MOR. QUAL. CONTROL DIR. QUAL. CONTRG Page #1 of same specification issued 3/18/55* DATE ISSUED A,'UG 5 1955 CRMC-Thermo&Cement-000078 tVlMhwi'Mwi MHYILLE waghesia FORMULA: i -PLANT DIVISION- Thenaobastos Blocks & P/C (Lime Silica) 2E&L- P^GE NO. *:i Standard Furnish: Spec. No. Material # /* ,; Batch, 1 >; Weight Pea* cent v. X Cellte 256-C Celite 392 i Mississippi Lime. grade W-3 Amosite Fiber PJUtJLJU+*jl 600$ 300 900 279MK. 2075# 28*9$. sis P.S. 63299 Aquablalc 2 q,tB* Water * -?* *- 1 ' ' Motes: Hot Lime-Silica tailing water and service water is used to*4maKi a ratio of 2.5 gallons of v/ater to 1 pound of solids. Watgr in^st be kept free from Magnesia contamination. fl-S - Hecessary amount of crude fiber to yield 275# of clean, fiber shall be used. * Aa * ' ` VI 1. Minimum gel time shall be 1,5 hours. . ' ;>?. 2. Full bag quantities are not weighed part bag quantities Shall fbe weighed. f. All incoming Lime and Celite will be identified and stencilled tfitp lot numbers assigned by Control Laboratory. Ho Lime or Cei^fip.'^s to be used until it is released by Control Laboratory. Stocks should be arranged so that oldest material is used first. - y* . t ; ;> '*v A 1 .*8* > a fZtfiJ'kt-k XA--'^CLHu'AFNmGJEI8 -- REASON: *5* ,,iL--' r. v A\ y>- To show approval of 100$ w~3 Fiber as replacement for Crude Ifiber. FORM 00132-10 PRINTED IN U.0.A. AUTHORITY -- FOR CHANGE FILE-HOLDERS SUPERSEDES: Letter of C. LsGattuta to H.J. O'Brien dated 3/7/55* 1 CONTROL 8UPR. INDoENOR , WAUKEGAfI LAB. QUAL. CONTROL PROD. SUPT. PLANT FINANCE OFFICE RESEARCH US. NOR. QUAL. CONTROL DIR. QUAL, 00NTR4 Page #1 of same specification issued 7/6/5^. DATE I8SUED MAiR 18 1955 CRMC-Thermo&Cement-000079 WMtsmA MAHVmB FORMULA: pi-awt ___ Thensobeeto Blocks & Pipe Covering (Lime-Silica) A3V^ PAGE NO. #1 xhtsbim sHscmcAiEiQg c/A4w^ea,, ^//c/sz - . ^7 Ca >,itu rdAZte., -~y 3pee. Mo. m m M.B. CP-145 p.s. 61825 Material Cellte @0. 392 Cellte Bo. 256-C Asbestos Fiber Bleed for Tbemobestos Prod. Hydrated Line Batch -/V** Wiits. mBmm 3Z CANCELLED '7fd/s4 14.9$ 600 28.9 375 13.2 900 2075# . $100 0 Aqua Black "202" Soap Solution Water 1/2 0*1. 1/2 Gel, #gote: Hot Lime-Silica tallies water and series water is used to mke a ratio of 2*5 gallons of S.tsr to 1 pound of solids. Water East be kept free from mgasia coatairation. MAmwAomim jmmwnoss) See Manufactraring Specification JSJ-Gil for Floy Chart of Operation. A. Pel, Tank Preparation: 1. Fill "5000 Gallon" Pel Tank to shaft with hot Lime Silica tailing water. 2 Sura os steals and agitator in Gel Sank. *\\ 3 Start to raise temperature of water ia. Gsl Tank. Pre-Mixing Operstiom 1. Run hot Lime-Silica tailing crater from storage tanks into the c. Pre-Miser up to shaft. (The Pre-Mixer is the paddle mixer with horizontal shaft on the second floor of "g" Building atat room). 2. Add the Asbestos Fiber to the water ia the Pre-Mixer, start agitator of Pre-Mixer, mix one minute, sad stop agitator. 3. Add Cellte and the "208" solution to the water and fiber la the Pre-Miser, and add water to 4" tram the top of tbs Pra-Mixer, start agitator of Pre-Mixer end mix for approximately 5 minutes. y INDICATES tA"" change - reason To ^ addition of Agas. Black, AUTHORITY -- FOR CHANGE FILE-HOLDERS FORM 80132.10 PRINTED IN U. 8. SUPERSEDES: Letter of C. LaGattuta to H.J. O'Brien dated 12/15/53- IKD.EK, 8UPR. IccaasoL QUAU P1aLgAeB#1 of Psa.a& Ssp. ecification wismsu.ed 8/7/521. notice oi CONTROL PROD. 8UPT. 1 PLANT FINANCE I OFFICE Re6eAJ|h MOR. jkHB. QUAU CONTROL DIR. QUAL CONTRi DATE ISSUEC 28 $53 L0/01/53X. /v&-/? & MZl.cC c/r/s:i. CRMC-Thermo&Cement-000080 ( X ( 0(f-3c^ Manufacturing Specifications PRODUCT: DIVISION. Magnesia Manvill Thsraobeetos Blocks and Pipe Covering (Lime-Silica) -PLANT ___________________ INTfRIM specification cANcatiu 4* FORMULA: UO-16- PASE NO. 1 Spec. No. - H.S. CT-litp / P.S. 61825 Material Celite No. 392 Celite No. 256-0 Asbestos Fiber Blend for Thermobostos Products Hydrated Lime Batch Wgts 300# 6oo 275 1U.5 28.9 13.2 900 U3.U 2075# 1WM "202" Soap Solution Water 1/2 gal, # -aitotes: Hot Line-Silica tailing water and service water is used to make a ratio of 2.5 gallons of water to 1 pound of solids. Water must be kept free from magnesia contamination. MANUFACTURING INSTRUCTIONS: See Manufacturing Specification MG-Q;1 for Flow Chart of Operation. A. Gel Tank Preparation 1, Fill "5000 Gallon" Gel Tank to shaft with hot Lime-Silica tailing water, 2o Turn on steam and agitator in Gel Tank, 3, Start to raise temperature of water in Gel Tank, Bo Pre-Mixing Operation 1. Run hot Lime-Silica tailing water from storage^tanks into the Pre-Mixer up to shaft. (The Pre-Mixer is th'e paddle mixer with horizontal shaft on the second floor of t!E" Building mix room). 2. Add the Asbestos Fiber to the water in the Pre-Mixer, start agitator of Pre-Mixer, mix one minute, and stop agitator. 3. Add Gelite and the "202" solution to the water and fiber in the Pre-Mixer, and add water to it" ft*ora the top of the Pre-Mixer, start agitator of Pre-Mixer and mix for approximately 5 minutes. X--'ch'ange8 ~REASON: To show change of Celite number from 379 to 392. FORM BOI3X-IO PRINTED IN U.8.A. authority- Letter of 5, Collier to L, C. Lindstrom dated 7/21/53* FOR CHANGE 9* FILE-HOLDERS CONTROL LAB. P,, St S. INB.liNuft . WKB. 8UPR. QUAL. CONTROL PROD. SUPT. PLANT FINANCE OFFICE SUPERSEDES: Page #1 of same Specification issued 6/15/53 f NOR. uvRESEARCH/ QUAL. CpNTROL DIR. QUAL. C0MTR1 DATE ISSUED MK 1 CRMC-Thermo&Cement-000081 Manufacturing specifications MAN TILLS MAGNBSXA DEPT. ' -PLANT IP PRODUCT: DdIiVvIiSsIiOoNn. Thermobestoe Blocks and ip Covering (Lime-Silica) IHT&tDK SPECIFICATION arcu. NO. tfc-16 PAGE NO. 1 X FORMULA; Speco NOo Batch m*' it *//, r BR aa MoSo CT-U5 PpSd 61825 <* Celita No0 379 Celite No0 256-0 Asbestos Fibre Blend for Thermobestoa Products Hydrated Lime 202** Soap Solution Water = . 3m 600 28c9 275 13*2 900 U3Jl 2075F X80TQ& 1/2 gal. #' Notes: XV * Hot lime-silica tailing water and service water is used to sake a ratio of 2o5 gallons of water to 1 pound of solids.. Water must be kept free from magnesia contamination;; MANUFACTURING INSTRUCTIONS; See Manufacturing Specification MG- 'Hi for Flow Chart of Operationc A = Pel Tank Prepam&lon lo Fill -'*5000 Gallon" Gel Tank to shaft with hot lime-silica tailing water ,, ^ 2, Turn on steam and agitator in Gel Tanko 3o Start to raise temperature of water in Gel Tanko Bo FTe-Mixlng Operation lo Run hot lime-silica tailing water from storage tanks into the Pre-Mixer up to shaft . (The Pre-Mixer is the paddle mixer with horizontal shaft on the second floor of nEn Building mix room) 2o Add the asbestos fiber to the water in the Pre-Mixer, start agitator of Pre-Mixer, mix one minute, and stop agitators 3d Add celite and the `'202" solution to the water and fiber in the Pre-Mixer, and add water to from the top of the Pre-Mixer,......... start agitator of Pre-Mixer and mix for approximately 5 minute8 RETURNTO M RESEARC FILE ROOM FORM 80191-10 Geii6ilal ravision to show current practice 0 X-,SanS"REASON! --------------- Joint meeting between Ity Control, Research, Production authority--Control Laboratory on 5/28/53 FOR CHANGE ' LDE%ge IndoEngo Wkgc SUPR. DUAL. of same 8Peclfid&tion is sued 5/5/shf^CifONTROL PROD. SUPT. SUPERSEDES: . DATE ISSUE! JltN 15 195,; CRMC-Thermo&Cement-000082 iviMhurnwi ukiimu wn;winuHi iwimo makvillk MAQNKSIA _DEPT. PRODUCT: DIVISION-IP-- Thermobestos Blocks (Line Silica) JM.6-. PACK N< #1 Formulat Material Celite #256~C Arooeite Fibre 13*3 * W~3 Mississippi Hydrated Lima a202B Solution Hot Water Lime Silica Plastic Batch Weight * Per Cen^ 525# 75 75 5oo 1&.5* 6o5# 6*5## !ESd0jC... 1/2 Gel. Enough to 120# 3,525 k total gallonage 10.0$#** -n S ^ =s m ' m cI -ri 1 J ^3 w S3 |&So o--H 3C NOTES; * Size of batch may be varied to allowed limit of gel tanks. Fibre blend may be varied from 75# D-3 and 75^ T-3 to either 60# D3 and 90# W-3 or 90# D-3 and 60# W-3 *#* Up to 10^5 (120#/batch) of lime silica plastic may be added with hot water. Manufacturing Instructions; ?^ing Operation: 1. Run hot lime silica tailing water from storage tanka into paddle mixer up to shaft. ...... 2. Add Celite and nix three minutes. 3'. Add fibre. 1ao Add lime silica plastic if desired, not to exceed 120 pounds. 5. Add Mississippi Hydrated Lima and mix ten minutes. 6. Add water to a level UM from the top of tank and mix for five minutes. ?. Add approx, ono-half gallon !,2Q2!* as water'runs in. 8. With mixer running, start pump and pump into gel tank. 9. Flush out mixing tank with approximately two hundred gallons of hot water. Gel Tank Operation; X. Before receiving batch, dost; outlet valve at bottom of gel mixer. Start agitator and run batch into gel tank. 2. Bring level of batch up to 1a 8 6" from top of tank with hot water or hot lime silica tailing water. ' 3. Turn steam on. Within 20 minutes reach a temperature of 195 - 200F with glass thermometer.or 175 with recorder. Turn off ateera and run agitator for five minuteSo f^Vj 1 FORM 80138-10 PRINTED IN U.8.A. X_ INDICATES _ | CHANGE General Revision recommended, by Research and W&m TuE AUTHORITY -- FOR CHANGE Current Manufacturing Procedure. FILE-HOLDERS supersedes: Ind Engr. Vfkgo SUPR. QUAL. CONTROL PROD. 8UPT. Page #1 of same spec. issued 8/28/51 and Notice of Deviation INiP^n^dated Ip/ij/51. DIR QUAI CONTI |Ufjw *TE issuei 6 1351 CRMC-Thermo&Cement-000083 -mnrmne maqhgsia Formula* Thermobostos Blocks (Line Silica^ _______________________ J m.16 PAGE NO. #1 Batch Material Weight Per Cent - 1S\ ( Amosite Fibre RX or i)-3 Hydrated Lime* 50# 825 2.h% 39.3 "it 5* 09 Cellte #379 Cent #2$6-C ISO 750 7.2 35.6 5 A> / Fibre Blend for Magnesia & TV yL As Superex 325 2,ix)6# 15.5 lo6lb% [pr >'P u ( Sote; Warner or similar loir Magnesia, or equivalent quick lime may be usedo ' Manufacturing Instructions; X A Mixing Operations 1 Run appreKimateljc-^OO cnTlche-ef water into paddle mixer (up to shaft). aaaju nn firmrt'n rnlri water t wfter from the hot lime silica tailing water O sft.onrraagme *tanny,ktr^- f e**eJAM 'tag/*. ii UM"" t 3 2. Add fibre >-t ^ ^ p3L#jDb-~ y*--Add water until' xnm foot above, shaft tft3tj>g*'mnutes ^ & Add Celite and mix three minutes. 5, Add Hydrated Lime and mix fifteen minutes. 3D tf> 30 oo ! 30 --l Cin* O 6, Add .water to a level h'[ from the top of tank and mix for five minutes* 6 'V- wa*#*'* 7. With mixer running, start pump and pump into gel tank*8 8. Flush out mixing tank with^aae-hundrsd gallons of said water6 Bo Gal Tank Operation i 1 Before receiving batch, close outlet valve at bottom of gel mixera Start agitator and run batch into gel tanka 2, Bring level of batch up to h*6* from top of tank with hot water or hot lime silica tailing water. (Total gallons of batch 3120 calo) Turn steam on until a temperature of 195 - 200^ steam and run agitator for -ten minutes. { ---------- -------- :------ i INDICATES -- . CHANGE General Revisions ' r5ura : - ' 1*7 S *UG 29 1951 AUTHORITY FOR CHANGE FILE-HOLDERS SUPERSEDES: FORM MltMO PRINTED IN U.8.A. Current Manufacturing Procedure, Ind.Enga V/kg, "Saras spec. Pages-#!, SUPR. QUAL CONTROL . F>. W=n21i .VH-jaPROD. SUPT. PLANT FINANCE OFFICE MGR. QUAL. CONTROL DIR QUA! CONTR TssuaT^TW^O^ DATE ISSUE! AUG 28 1! CRMC-Thermo&Cement-000084 KAftVJtLLg PIPE COVERING Iliencobestos 9$ rC.-3 2 PAGE NO. 1 JUi Nc, Amosite K4 Fibre J&l. 870 35 Of Ufe ST 63202 61880 Aluminum Stearate IP Grade Sale * 4 Total Sateh 1000# 10Gt Motet Building Superintendent or bis delegated authority m.y proportionately increase or decrease batch* size to meet requirements . Manufacturing Instructions: 1. 6elgh out Stearate Talc Mixture in nixing drum (1/2 batch at a time) stearate first end, mix 5 o 10 minutes. 2* Hun laosite through crusher once and spread on floor approx, 2 ft. deep. Sift Stearate Talc Mixture over crushed Asosite and turn twice with shovel. Use 1-1/2 screen in the crusher. 3. Bun fetch through fan of crusher once. U Heat treat material in bags is k Brier for 24 hours at 130 200F. 5* Bo not store on drier until sample of each production run sub mitted to Inspection & Control laboratory Is approved. For packaging see Packaging Schedule - Dry Cements. * -- REASON: To delete packaging instructions. AUTHORITY FOR CHANGE" FILE-HOLDERS ,RTM 10-49 RINTED IN U. S. A. SUPERSEDES: J^nd. SELg| WB ukegan I. St c. pC. iSSUS 7/13^2. ' BLOG. JUFT. LOCIL COST DEPT. R^H GEN. 1. ft C. DEPT. GEN. COST LOCAL DEPT. 1. ft C. DEPT DATE ISSUED f 21 CRMC-Thermo&Cement-000085 Johns-Manville MANUFACTURING SPECIFICATION PRODUCT; THERMOBESTOS BLOCKS AND PIPE COVERING \* PLANT & DIV. SPEC NO. l! , ,, , , , !1l----L--o--n--q----B---e--a--c--h----1---1 --- 4324-10 PAGE NO. co't M O I . GENERAL DESCRIPTION: This specification covers the molding, autoclaving, drying, and finishing of Thermobestos Blocks and Pipe Covering. I I. STANDARD FORMULA: '. 1 XL A. STANDARD FURNISH: SPECIFICATION MATERIAL # I (STANDARD) HOMOGENIZED WEIGHT % #2 (ALTERNATE) NON-HOMOGEN I ZED WEIGHT % FPS 44.19 FPS 41.19 JM 4K30 FIBRE PS I 1-1827 CELITE #256 600 Lbs. 26.0 CELITE #392 500 Lbs. 21.7 ASBESTOS FIBRE 150 Lbs. 6.5 QUICKLIME (800 Lbs.) -- HYDRATED LIME EQUIV.1057 Lbs. 45.8 TOTALS (DRY WEIGHT) WATER TO A FINAL VOLUME OF: GEL TANK LEVEL (DOWN FROM TOP) WATER TO SOLIDS RATIO (LBS.) 2307 Lbs. 100.0 5032 Gal. ' 20.5 In. 18.0 to I 600 Lbs. 500 Lbs. 225 Lbs. (800 Lbs.) 1057 Lbs. 25.2 21.0 9.4 44.4 2382 Lbs. 00.0 5131 Gal. 19.0 In. 18.0 to I #1 STANDARD BATCH is to be used unless the homogenizer is not operational. Asbestos fibre is to be processed through the homogenizer. $2. ALTERNATE BATCH is to be used when the homogenizer is not operational, fibre is to be added through the feed hopper and blower, B. Noteis: I. The listed quantity of raw materials is to be made up to a final volume as listed above using hot lime-silica tailing water, service water, and steam. This is accomplishedi by adding the "final water" to the listed levels (measured down from the top of the gel tank.) Tailing water is preferred and should be used. The remaining re quired "make up" water should be obtained from the high pressure cc d c=_r>r - cc sprays, water used for cleaning molders and floors, and the water from the vacuum pump discharge; all of which should be diverted into 2X 0&0 ;oo OC cc the process water system in a regular flow during moldj.n.q...ope.ratlons., jn order to keep the water storage system in balance. Hydraulic,leaks "'should be repa Fred 'as'-sbon,`as`possible' tb~mih'imize contaminat ion_ of_ __ oc S cn process water*.-" Form 333-2-,. Ptd. In U.S.A. INDICATES IX Revised homogenized fibre formula, delete small batch except X CHANGE ~REASON: on deviation basis -- General Revision.__ 2X Clarify .ilYd.rau,l..ic. AUTHORITY FOR CHANGE D . B. Wingerter 9-10-71 d i scnarge. SUPERSEDES: MGR. MGR. G.Q.C. Q.C. p9. 1 of same -- speck 515^tion, dated 2-9-70. SUPR. PROD. PLNT, V'j } Mv i. Q.C. SUPT. JuLLmffl'.A Q-c supr. DATE ISSUED ' - CAT mow. wrp PROTFOTOR SWRFT RFFORF TTPTNC - 9-10-71 CRMC-Thermo&Cement-000086 X K Johns-Manviiie 'Manufacturing SPECIFICATION rnuuuuii THERMOSESTOS BLOCKS AND PIPE COVERING ' GENERAL DESCRIPT ION: PLAN I & UIV. || Long Beach |, SPEC NO. PAGE NO. 4324-10 . Page 1 of 18 mm This specification covers the molding and finishing.of Thermobestos Blocks and Pipe Covering. ., ' STANDARD FORMULA:' . T. \' ' 1. Standard furnish.- ;. Spec. No. Material - #1 Weiqht . % FPS 44.19 FPS 41.19 PS 11-1827 JM Fibre Celite #256 500# Celi te #392 450# Quicklime,Granula r 700# 4K30 Fibre 200# 27.0 24.4 37.8 10.8 . Total y . 1850# 100.0 Water to a Final Volume of .. ; yy .. . 4465 Gal. ;y.: . #2'-'-'f Weiqht 0//o 600# 500# 800# 225# 28.2 ' 23.6* 37.6 10.6 2125# 100.0 5131 Gal'. Water to Sol ids Ratio 18.0/1 y 18.0/1 Gel Tank Level (Down From Top) ' 29 Inches - 19 1nches 2. Notes: *The Foreman' wi11 determine which of the above formulas are . . appropriate based on expected slurry usagje as controlled by the molding schedule, mechanical breakdowns, number of molder Operators available, etc. Good judgement must be used to prevent old slurry or slurry waits. . ` -"-'Most commonly used batch (standard). - \, ; j (a) For each, batch of Therrmobestos the listed quantity of raw materials are made up to a final volume as specified above with hot lime silica tailing water, service water, and steam. This *is determined by adding the "final water" to the gel tank to the levels listed in the formulas. Form 333-2-A PUI. In U.S.A. y_INDICATES pp&cnM. X New formulas due to fibre reduction. CHANGE -REASON... Correct rat;QSj_________________ AUTHORITY FOR CHANGE D. B. Wingerter's wire 2-9-70. SUPERSEDES; Pg. 1 of same Specification, dated 3-14-69 MGR; G.Q.C. MGR* ac. SUPR. Q.C. PROD. SUPT. PLNT. cmFIN. PLEASE PETPPH TO j ' i ' i I iuJI i wI 1 LIBRARY (MM) DATE ISSUED 2-9-70 CRMC-Thermo&Cement-000087 Johns-Manville MANUFACTURING SPECIFICATION PRODUCT: THERMOBESTOS BLOCKS AND PIPE COVERING PLANT & DtV. SPEC NO. PAGE NO. Long Beach I I 4324-10 Page 1 of 18 IX General Description: ' .' This specification covers the molding and finishing of Thermobestos blocks and pipe covering. , . /. j Standard Formula: '. . *-"r- 1. Standard Furnish* . #1 % , , #2** #3 Spec. No. Material , Weight % Weight % We i'qht % : . FPS 44.19 Cel i.te #256 f^ps 41.19 Cqlite #392 PS 11-1827. Quicklime 500#. 26.7 600#. 27.9 '450#,: ; 700# ' 24' i,0 ' 37-3 : 500# 800# ' 23.2 37 2 650#. 27.7 550# 23.4 . 875# 37-2 " JM Fibre ' 4028 Fibre 225# 12.0 250# 11,7 275# 11.7' Total 1875# looio 2150# 100.0 2350# 100.0 . Water, to a j Final Volume of 4506 Gal.V. 5200 Gal 5870 Gal. - \ Water to . I . ' : 2X Solids Rati of, 17.5/1 .; . ; 17-5/1 17-5/1 ` .. II .Gel Tarik Level (Down From'Top) \ 28 Inches ' . f - __________ 18 1nches fl 7 Inches - 3X ^ cn DCTIink! -riy * The Foreman will determine which of the above formulas I'LEA RETURN TOjl : are appropriate based on expected slurry usage as controlled v nrt, V J-jT hllwilAiiUll " | (MM) : by the' molding-schedule, mechanical breakdowns, number of ` moldet.operators avai table-, etc, . Good judgement must be A:'used to prevent slurry becoming old or having slurry waits. . ' -irii: Most commonly used batchA ; 2. Notes: . =5 c 6 V < ccrooo (a) For each batch of Thermobestos the listed quantity of raw materials are made up to a final v.olume as specified above, with hot lime silica tailing water, service water, and steam. This is determined by adding the "final water" to the gel tank to the levels listed in the formulas. y INDICATES ------------- IX IncTtWe general description, 3X Discontinue use of 100^ W-3 CHANGE -REASON:2X Include water to'sol ids ratio. fibre. General Revision : AUTHORITY FOR CHANGE D. B . Wingerter per visit 1-27-69 SUPERSEDES: Pg. 1 of same Specification dated 11-9-67. MGR. G.Q.C. MGR. Q.C. SUPR. Q.C. PROD. SUPT. PUNT. mRN. DATE - issued 3-14-69 CRMC-Thermo&Cement-000088 % +r~ ;/ . .'ik;' ' SPEC* : lOAHOE |V,V>5 . sLn-; :i,m; Pip;' Co.-. b:JV ^ . ... .. PAGE NO. ton k;:T;`-K' I of 14 ........ - Standard Formula Standard Furnish* Sfiec,JJo^ Material Weight % WeSqhfc % Weiqh t % rra *i, 19 Cel 1te #256 Cel!te #392 Qu 1 ck 1 i me 4D28 Fibre** 500# 26,7 600# 27.9 650# 27.7 ' 450# 24,0 500# 23,2 550# 23.4 700# 225# 37,3 12,0 800# 250# 37.2 875# 37.2 Lu. . 275# Jihl 1875# 100,0 2150# 100.0 2350# 100.0 Water co a final - volume of 4506 Gal, 5200 Gal ,, 5370 Gal, Gel Tank Lave'* (Down from top) 28 inches 18 i'i&flfcjS 7 inches 1. As an alternate,formulas containing 100% W-3 Amoslte may be used when a situation warrants such action. Particularly for orders Involving ccmpliance to specific military and/or other specifieations< ^>rmulas containing 300% W-3 may be necessary to meet the dens 1ty .and/or thermal conductivity requirements, *The Foreman will determine which of the above formulas are appropriate based on the expected slurry usage as controlled by the molding schedule,, mechanical break downs s number of molder operators available etc. Good judgement should fee used to prevent slurry becoming old or having slurry waits, (a) For each batch of Thennobestos the listed quantity of raw materials are made up to a final volume as specified above with hot lime silica tailing water* service water and steam. This is determined by adding the "final water" to the gel tank to the levels listed in the formulas. Tailing water is preferred and should be used. The remaining required ifiake-up water should be obtained from the high pressure sprays^'TOie Water used for cleaning the moiders and the floor* and the water from the vacuum pump discharge should be diverted Into the process water system In a regular flow during molding to keep the process water storage in balance. Water contaminated with oil such as the hydraulic, water discharge must not be used, **Fibre to.be processed with plates in full open position. v INDICATES X-- CHANGE --REASON: 0tscontinueo use oi Aquablack AUTHOR!^. FOR CHANGE D. 8. Wingerter's Wire of 11-0-67 PLEASE RETURN TO. J-M RESEARCH SUPERSEDES: & MGR. G.Q.C. MGR. Q.C- SUPR. w.c. Same specification dated 4-17-67 Page 1 PROD. SUPT. nm. FIN. RES. U\<3. LIBRARY (MM1. DATE ISSUED 11-9-67 CRMC-Thermo&Cement-000089 ,H :! tR'i . # SPECIFICATION Standard Formula fiv-'rmcbosto-" 0 iocR and Pipa Covering spec no. PAGE NO, 432*1-10 i i of 14 Standard Furnish^ No., FPS 44.13 rr& 4i,,!3 Materia 1 Cellte #256 Cel i te i/332 Q.u f ckl ims 4D28 Fibre** ` PS 3293 ' Aquablack Water to a final volume of Wei qfit 0/ We ight JL Weigh t 500# 450# 700if 225# 18 75// sa 26.7 2.4.0 37.3 12.0 100.0 600# 500# 800# -Jig# 2150# 57/ 27 3 23,2 37,2 JLL..Z 100,0 550# 8/5# J-W 2350# 6# 2.7.1 23.4 37.2 - 11.7 1 00.0 4906 Gal, 5200 Gal n 58/0 Gal Gel Tank Level (Down from top) 28 incSies 18 inches 7 inches 1. As an alternate formulas containing )0fl% V/-3 Amos 1te may be used when a situation warrants such action. Particularly for orders involving compliance to specific mi 1 itary and/or other specifications;, formulas containing 100% V?-3 may be necessary to meet the density and/or thermal conductivity requirements. . . *The Foreman will determine which of the above formulas are appropriate based on the expected slurry usage as controlled by the molding schedule- mechanics! break downs, number of molder operators available etc. Good judgement should be us-.d to prevent slurry becoming old or having slurry wafts. ' (a) For each batch of Tbermobestos the 1isted tqunt!ty of raw materials ore made up to a final volume as specified above with hot lime silica tailing wafcer,, service water and steam. This is determined by adding the "final water" to the gel tank to the levels listed in the formulas,, m ^Tai ling water is preferred and should be used. The remaining racuArec! 1 make-up water should be obtained from the high pressure spraysr the water used for cleaning the molders and the floor, and the water fro:;! the vacuum pump discharge should be diverted into the process 'water system in a regular flow during molding to' keep the process water storage in balance. Viater contaminated with oil such as the hydraulic water discharge must not be used,, **Fibre to be processed with plates in full open position. PLEASE UPTURN TO CHANGE^--REAS0M: Discontinued use of W-3 Amosite Fibre. ] M RESEARCH (MM)...... AUTHORITY FOR CHANGE E,, C. Lindsitrom's Letter of 12-20-66 SUPERSEDES: MGR. G.Q.C. KGR. Q.C. S'! PR. Q.C. Same specification dated 5-25-65 Page 1 PROD. 5UPT. PENT. " Pin. tea. fp'R j msivo 4-17-67 CRMC-Thermo&Cement-000090 Johns-Manvillo MANUFACTURING SPECIFICATION PRODUCT:. V. Theraobestos Blocks and Pipe Covering PLANT & DiV. Long Beach II SPEC NO. 4324-10 PAGE NO. ' 1 of 14 Standard Formula Standard Furnish* Spec* Ko. Material JLWeight JL Weight Weight % / FPS 44.19 FPS 41.19 PS 3299 Celite #256 Celite #392 Quicklime W-3 Amosite Fibre 4D23 Fibre Aquablack ' Water to a final volume of 500# 450# 700# 100# 125# 1875# 5# 26,7 24.0 37.3 5.3 6*7 100*0 4506 Gal0 600# 500# 800# 100# 150# 2150# 5# 27*9 23.2 37.2 4.7 7.0 100*0 5200 Galn 650# 550# 875# 125# 150# 2350# 5# 27.7 23.4 37.2 5.3 6*4 100*0 5870 Gal* X Gel Tank Level ' (Down from top) 30 Inches 21 Inches 11 Inches 1* As an alternate formulas containing 100/ W-3 Amosite may be used when a situation warrants such action* Particularly for orders involving compliance to specific military and/or other specifications, formulas containing 100/ W-3 may be necessary to meet the density and/or thermal conductivity requirements,, , *The Foreman will determine which of the above formulas are appropriate based on the expected slurry usage as controlled by the molding schedulep mechanical brea] downs, number of molder operators available etc* Good judgement should be used to prevent slurry becoming old or having slurry waits0 (a) For each batch of Theraobestos the listed quantity of raw materials are made up to a final volume as specified above with hot lime silica tailing water, service water and steam* This is determined by adding if? the 'final water" to the gel tank to the levels listed in the formulas* Tailing water is preferred and should be used* The remaining required make-up water should be obtained from the high pressure sprays, the water used for cleaning the molders and the floor, and the water from the vacuum pump discharge should be diverted into the process water' system in a regular flow during molding to keep the process water storage in balance,. Water contaminated with oil such as the hydraulic water discharge must not be used* Form 333-2-A Ptd. In U.S.A. Y INDICATES CHANGE --REASON: AUTHORITY FOR CHANGE V SUPERSEDES: Correction E. C* Lindstrom's Wire of 5-18-65 Same specificut ion dated 8-4-64 Page 1 -PLEASE--RETURN--TO PW-fiE5EARGH--- UMRY-4MM)----- MGR. G.Q.C. MGR. 1 SIIPR. Q.C. | Q.C. PROD. SUFT. purr, 1 RES, FIM. j LAP. --.rr\ '5 " f"?--.------rv 1 DATE | ISSUED 5-25-65 * JJJ CRMC-Thermo&Cement-000091 MAN U FACTUFt i MQ SPECIFICATION rKG'' Thermohestos Blocks and H.pe Covering SPEC NO. PAGE NO. V Long Beach HE 4324-10 1 of 14 fe.V/O "Wu/ SsSLtJk* FPS 44*19 FPS 41*3,9 Iterisi Weight JL JfL Weight JL. Gelite #256 5 GO# 26*7 Cellto #392 450# 24*0 Quicklime 70c# W3 Amsite fibre 10c# 4D28 Fibre 125# 37*3 5*3 6*7WMWHHWM 1875# 100*0 Aquablaclc Water to a final 5# volume of 4506 Gal 600/1 500# 80C# 100# 15C#wl'aiiiin 215C# 5# 27*9 23,2 37*2 4*7 7.0 100*0 5200 Gal, 65C#/ 550# 875# 125# 15C# 2350# 5# 27.7 23.4 37*2 5.3 6*4 100*"o 5870 Gal, Gel Tank Level 28 Inch3 18 Inches 7 Inches 1. As an alternate formulas containing lfX$ W-3 Amosite may be used when a situation warrants such action. Particularly for orders involving compliance to specific military and/or other specifications, formulas containing 100$ W-3 nay be necessary to meet the density and/or thermal conductivity requirements* : HThe Foreman will detond.m which of the above formulas are appropriate based on the expected slurry usage as controlled by the molding schedule, mechanical breakdowns, number of siolder operators available etc* Good judgement should be used to prevent slurry becoming o3.d or having slurry waits* (a) For each batch of Themobestos the listed quantity f raw materials are made up to a. final volume as specified above with hot lime silica tailing water, service water and steam* This is determined by adding the flfinal water" to the gel tank to the levels listed in the ^ formulas* . Tailing water is preferred and should be used* The remaining required make-up water should foe obtained from the high pressure sprays, the water used for cleaning the solders and the floor, and the water from the vacuum pump discharge should be diverted into the process water system in a regular flow during molding to keep the process water storage in balance* Water contaminated with oil such as the hydraulic i water discharge must not be used* ' ' r * ' '. 7r~v INDICATES CHANGE --reason: Show use of 60% 4JD28 Fibre AUTHORITY FOR CHANGE v E, C* Lindstrom s letter of 7*-2164 `ij SUPERSEDES: | MGR. G.f, C. | Q.C. SfJPR. | C.C. 1 Same specification dated 1--7~63 Page 1 A ,PROD, i PLNT. j R1T3. I , ! .! SUrT. 1 vtv, 1 LAS. \jffijy !SL 8-4-64 CRMC-Thermo&Cement-000092 jehn:, ;*innvi!io MANUFACTURING SPECIFICATION PfiOO: 'Gi; ' Th<sg*3fcsgi*>, Blocks Pip GQ'?crtlg FLAW ' A .... SPEC NO. PAGE NO. 1 of 14 # Altsrnativs >w AltrmtiTO Foxsmla iiool Ponaula Bo* IE ~~' Es^mML 1 Mstslil , FP3 44,19 Celite #256 FPS 41*19 Oelite $392 CM . 32.0S ?DC# 32*# 350# '32,$S 35C# 18.7,S 400? 18*6# 2001 18.& 3^ Quicklime 'tom 37.3ES 80($ 372$ 40C# 374$ W3 Arnosit Fiber 12, Qg 25C# 11,6$ 125# 11.6# iillf 100*0# Sfcf 100*0# iqtJ ibd.ci; Aouablack - 5# ' 5# 2o9# Water 1 4506 Cfe'.lo 5200 Gal* '2600 Gsl. * Alternate formula Eb,l to b used at PIx.daatin Superintended9a diserrki-; for large? sIjcsq when Up or Block .pisses pessait. Alternate forssula .EboII to be used at Prediction Superintendent* 9 discretion for. mailer ,,aai:oa deposing upon Pip .ort Block slats'being soldedL'' , a) For 'each batch 'of Therteobeatosj, 1875 lbs, (or 2150 lbs. for alternate 1 ` formula llot.1 ad 1075 lb* for 'alternate forospla ftb*2X) of raw materials are mad up to a final volume of .4506 gals* (or 5200 gale, for for/mla Mool and 2*500 gals, for FioJI Alternate Forsaala) Kith hot 1mm silica : tailing water* eervlc water ami stsaa* This'is detemirasd by aiding '. the "final water" to the g@l tank t-o a I@*el which is 2firt - (or IB'* for ' ;; fomila IfoI and 53" for Alternate Formula Bo*21) below the inside disaster of the gel tank at the top eat point. Tailing water 1 preferred and should be used* The ma&ining reqrtlred mak*=>up water Should- fee tibtdssd fresa the high pressor sprays* tho water used for cleaning the Holders &?:xi the floorp and the water frem ^the y&cum psrap discharge should fo* dieorted into the process water /system in. a regular flow-during .3aoldij\g to keep the Procters water ' storage in balance* feafeer ecft&iralnatttd with oil such an the hydraulic .water discharge aaiai not bo used* Both full and part bag qaanfciti@3j must b weighed d adjusted to th{ specified .net weight* - The combination of bags of Celtt 256 and Cellte 392 may fee weighed a a gross mii and adjusted to 930 lbs* net for standard foiraula (llGO IK* for formal Bo* I and 550 lbs* foj. foxmla IoH) by restoring or adding to as bag of Cslit 2360 ,,'v iCnHdAicNaGtEes -REAoON: Geasr.&l Beulsdoa : AUTHOR??? " FOR CHANGE E Go Xindotma* Letter of lOd.G-42 RETURN TO J-M RESEARCH. FILE ROOM SUPERSEDES: Sasio specification dated 12~2gs<&l DIR, CM*/}2vrH>(t - SUPR. PROD, PLMT. RES. Q.0, <J.C. Q.a SUPT. FI PI. LAB. Page 1 (old tm&wr I%l) DATE . ISSUED l-~7-"63 CRMC-Thermo&Cement-000093 (0: Johns-Manvilie MANUFACTURING SPECIFICATION PROOUOr; Thermsbesfcoa Blocks and Pipe Covering rjL/\in & i'lv. SPEC NO. PAGE NO. Beach Iw Standard Fomul& Standard Furnish; SpSCa Np G&X FS5 44*19 a, FPS 41*19 Celite #256 Celite #392 Powdered Nelson Quick laics XI W-3 Amosite Fiber X2 Aquablack -K-Papemakers Alum Water X3 -^Alternative #** Alternative Formula No*I . , Formula No* MM * Weight / % 600# 32<# 700# 35C# 18*752 400# 32*6% 35C# 18*655 20c# 32*6% IB 06% 70C# 37*352 aM i2a 1875# 100,$ 5# 6# 4506 Gal* (a) 800# 37*2$ 40c# 37*252 22S& mi Ha&f. 215# 100*$ 1075# 100,$ 5# 2.9# 6# 3 # 5200 Gal. 2600 Gal (a) (a) *May be used with 256 Celite Gel classification "M" only* To be added in pre mixer with Celite* .V r., 3 -^Alternata forawla No* I to be used at Production Superintendentf s discression .. for larger mixes when Pipe or Block sizes permit* , fc^Alternate formula No* II to be used at Production Superintendent's discression for smaller mixes depending upon Pips or Block sizes being molded* X5 (a) For each batch of Therroobsstosj 1875 lbs. (or 2150 lbs* for alternate , formula No* I and 1075 lbs* for alternate formula No* II) of raw materials X6 are made up to a final volume of 4506 gals* (or 5200 gals* for formula No. and 2600 gals* for No* II Alternate Formula)with hot lime silica tailing v tor, service water and steam* This is determined by adding the"final wate X7 to the gel tank to a level which is 3** ( or IS" for formula No* I and 53" for Alternate Formula No* II) below the inside diameter of the gel tank at the top most point* vTailing water is preferred and should be used* The remaining required JRN TO 1 make-up water should be obtained from the high pressure sprays, the water 1 _f,y used for cleaning the molders and the floor, and the water from the vacuum fw'pump discharge should be diverted into the process water system in a regu- - onnM ^,ovr <^ig molding to keep the process water storage in balance* - RUvW' Water contaminated with oil such as the hydraulic water discharge must not be used* (b) Both full and part bag quantities must b weighed, and adjusted to the spec fled net weight* indicates p n Xl Ghga~to~S25 lbs. Fiber. X3 Alt* formula large batch. CHANGE ~KtAS0N: X2 w 1875 Raw Matl. X4 Alt. small batch. AUTHORITY FOR change C* Lindstrom's letter of Dec* 14, 1961, E* C Lindstrom's wire SUPERSEDES: Pg* one* same spec* >d .5/13/60a Dev, Niot . T2 dated 155,*" " & M0.19P DIR. MGR. SD PR, PROD. PENT. m 3. Q.C. Q.C. Q.C. surr. FIN. LAB. Eng, Manv. DATE ISSUED- 12/28/61 X Indicates Changes; X5 Chg. to 1875(& to show alt* hatches ).X6 Chg, to A506(& to sh CRMC-Thermo&Cement-000094 Johns-iVianviiiG MANUFACTURING SPECIFICATION l-KODU^t l Themoboetos Blocks and Kip Covering PLAN f o; D1V. SPEC NO. 'S PAGE NO. Long Eeaeh IIi- Mg*l 1:0 The combination of bags of Celit 256 and Oolite 392 may be weighed as a IB gross unit and adjusted to 950 lbs* net for standard formula (1100 lbefor formula No* I and 550 lbs* for formula No* XX) by removing or adding to one bag of Celiie 256* (e) lime must be weighed and adjusted to the required net weight* Ibe lime bags 19 may be weighed as a gross unit and adjusted to 700 lbs* for standard formula (309 lbs* for femila No* X and 400 lbs* for formula No* XX) Hilled fiber is used in the fomula* The crude fiber must be weighed at the feeder to the mill with no allowance made for losses due to drops and line loss* The preferred grade of fiber is W-3* Use of other grade* must bo handled through deviation procedure* ( CRMC-Thermo&Cement-000095 MANUFACTURING SPECIFICATION Thersobeatos Blocks and P/C ----R*-. SPEC NO. PAGE NO. Hi W&fceon II!) Formula Standa^Furnij&x Spec*..JpA Weight Percent FES 44.19 XX. FK5 41*19 X2 Celite #256 600// Celit #392 , Powdered Kelson 35C# Quick Lima 70C# W-3 Amosite Fiber 2M 1900# Aquablack 5# K-Pfepermaker Alusa Water (A) &i*6$ 1S*4# 36*$$ 13_*2| iooM * Key ba used with. 256 Celite Gel classification *W* onlya To be added in premiassr with Colit* X3 (a) ' . . For each batch of Tharmbbestoa# 1900 lbs* of raw materials are made up to a final volume of 5120 gallons with hot lime silica tailing water* service water and steam* . This ia determined by adding the "final water" to the gel tank to a level which is 17-1/2 inches i below the inside dia- ? meter of the gel tank at the top most point* T; RETUii, J-M RESEARCH RLE RCOM Tailing water is preferred and should be used* The remaining required make-up water should b obtained from the high pressure uprqys* the water used for cleaning the maLdera and the floor* and the water from the vacuum pimp discharge should be diverted into, the process water system in a regular flow during molding to keep the process water storage in balance* Water amisminated with oil such as the hydraulic water discharge mat not be used* n (to) Both full and part bag quantities must be weighed and adjusted to the opacified net weight* . ,r The combination f bags of Celite 256 and Oolite 392 may be weighed m a gross unit and adjusted to 950 lbs* net by removing or adding to one . bag of Celite 256* (c) lime must be weighed and adjusted to the r-equired net weight* The lime bags may be weighed as a gross unit and adjusted to 700 lbs* weight* (d) Killed fiber is used in the formula* The crude fiber must be weighed at the feeder to the mill with no allowance made for losses due to drops ?d ling loss* TIi preferred grade of fiber is W-3* Use of other grade) must be handled through deviation procedure* :#F X--change'8 ~REAS0N: -- Change to 350 lbs* #392 Celite X3 Change to 1900 lbs* of rai _X2_Clmrig_tp_ powderedJ^em.Quick-iima. mat F0exchange C* Xindstrom* letter of March 2P I960 SUPERSEDES: t^sge one same specification, dated 7/28/59andDeviation #8, dated 10/26/5' DIR. Q.C. MGR. Q.C. SUPR. Q.C. PROD. SUPT. PLNT. FIN. RES. LAB. W$- 5/L3/60 CRMC-Thermo&Cement-000096  \ ' # Johns-Manvilie MANUFACTURING SPECIFICATION PRODUCT: Thermobestoa Blocks and P/C PUNT & DIV. SPEC NO. PAGE NO. Watson IID Kg-^ FORMULAS' Standard Furnish: 4$^ Spec. m>* FPS 44.19 FPS 41*19 P.S.61827-1 XL Material *() Celite' #256 Cellte #392 Miss Line W-3 Amosite Fiber Aquablak Water ! Msk Weight 600#Tb) 300# (b) 900# (c) _2M (d) 2Q5C# , 5# (a) Par ^nt 29.3 14.6 43.9 12.2 100.0 (a) For each batch of Therjnobestos, 2050 lbs. of raw materials are made up to a final volume of 5120 gallons with hot lime silica tailing water, service water and steam. This is determined by adding the "final water" to the Gel X2 Tank to a level which is 17-1/2 inches below the inside diameter of the Gel " Tank at the top moat point. , ,, Tailing water is preferred and should be used. The remaining required make up water should be obtained from the high pressure water sprays, the water used for cleaning the molders and the floor, and the water from the vacuum pump dis charge. Sufficient water from the vacuum pump discharge should be diverted in to the process water system in a rsgular flow during molding to keep the process water storage in balance. Water contaminated with oil such as the hydraulic water discharge must not be used. (b) Both full and paid.bag quantities must be weighed and adjusted to the specified net weight. k. The combination of bags of Celite 256 and Celite 392 may be weighed as a gross unit and adjusted to 900 lbs net by removing or adding to nne bag of Celite " ' 256. ,,' '` (c) Lime must be weighed and adjusted to the required net weight. The lime bags may be weighed as a gross unit and adjusted to 900 lbs net weight. (d) Milled fiber is used in the formula. The crude fiber must be weighed at the feeder to the mill with no allowance made for losses due to drops and line loss. The preferred grad of fiber is W3 Use of other grades must be handled through deviation procedure. cR., return to J-M RESEARCH INDICATES CI^NGE " -REASON: HEE ROOM 'XTC&arigQ~to^0'lbs of'W-3.Mosite-------12 Change measurement of water and corrections AUTHORITY FOR CHANGE E. C. Lindstrom's letter of 7-23-59 supersedes: Rag 1 same specification dated 10-23-57 & Deviation #5 dated 4-13-59 DIR. MGR. SUPR. PROD. PLNT. RES. I Ind. Q.C. Q.C. Q.C. SUPT. FIN. Jlab. Manv. J&3&__ DATE ISSUED 7/28/59 CRMC-Thermo&Cement-000097 MANUFACTURING SPECIFICATIONS -PLANT -v . PRODUCT: Vmsz$s^m Mmkm .tet f/Q - -. DIVISION. ^ fi i/vQn ,0 wmkkoW wm 4ioi4 wMim1 . , V4 m&t m$$> cfeait $m mm Urn fed feto&fe ^sr 11 & Wm ai<) ... W# w lkh k3*$ 1^.1 ldo %RMslt ' . . : ' .' Mates* ^ l) (m) F@s? emh f 3.ejriteb8fey2077 lbs sw strils ar ad ._ . lias BHiea teiltssg @iaia This 1 dtsii@d by adding fete. "fiaal water* t fete si Ta&k t@ 1@^I whih is 21 ijsstes teta? fete XasMa $Xasfer f fete 0@i Tank at fete t@p ssosfe psissfe - Tailing is preferred ai etemld to ej40 Its maa&alisg raqs&red ate=p water femM to btedaed fr fete high pressor water epyasr , fete water used f elwssiisg fete a@XIr@ and ill fie?,0/. e;mS fete water : fete ^astsass pump 4issehargs Swffleieiife tstfr frsa th-vssinsa p*ap 1seterg tetaM b diwrfeM iafe fete t3r8 water asystoas in a regular flaw during @MXssg fe k@p fete pr$9gjs water ter&g is balM80 Wa.te? : ates&mtei with XI @u@h sa fete hydraulic water di^eterge atst afe be (h) Bth fall ansi p$rt <^iafeifei@a smsfe to wigh4 ; spaslfte! mt t$@i@hfe adjusted .Tte easbisaaiiaa @ bags @ CJ@Xife 256 alite SfS agr to weighed as s@r08 unit B& adjusted fe 900 lbs sfe sy missis r acidic t a big f Cslite aS-So anst to weighed 'm& adjusted fe th re^!ri mt wight fit 3J togs my to wlgte$ && & gross wsaife s?f adjusted i fOS lbs mt wiflat Ct) Milled fiber is ud i fete feraa&a Sh rI@ fitos* Mssfe to at fell s4@r t fete seIII with aSlass@ jgs&d! far l@sss 4a fe drops sffii line l@so $h preferred grad f fltor & b3 Us @ fetes* grades last fe handled fehms^ dl.tXa preG^dws8, I- -- REASON: CHANCE AUTHORITY -- FOR CHANGE 6a Qe FILE-HOLDERS FORM 80131-10 PRINTED IN U.S.A. SUPERSEDES: $Sg tetter Wsgc return to J-M RESEARCH THFRDOM SUPR. QUAL. CONTROL yi-Ju^Y" PROD. SUPT. PLANT FINANCE OFFICE RESEARCH LAB. NOR. QUAL. CONTROL CRMC-Thermo&Cement-000098 Manufacturing Specifications rV' Ilmmsfeestes -PLANT. _DEPT. PRODUCT: &M p/c DIVISION- i/~3 ^>4 PAGE I 1 mmut x PPS 44.19 FPS 41ol4 Po S,6182? x MsM ceiiM 256 - c Oolite 392 MssAsslppl Li W-3' Aasit Fibs1 CNBBIB K?|5S Wtoiebt 600# 3m 925 21 J^Cgst 2Sof 14.3 44.0 13 o2 XCOoGjI P So 63299 Aquablaek Water 5# B&tess * - Bet 1dm Sill a tailing water md mrwle wat@r is used t msk & rati f 25 galleys f water t 1 pound f solidSo Water asset b kept free fnm Magnesia eesxtaadnatioiia ** - Oe 277# of Milled Fibre. (SprovMfeltean Plus ' ' ''; ' ' .' ' Herismtal Willow)e ; lo MAssta gel tisi shall b 1 hoar fO sdsso Msstami gel tte shall be 2 hoars $0 simtes* 2* Full bag quantities ay net weighed - pari bag quantities shall be weighed. 3 K Li r Celito is t b used until it is released by Cntrl Laboratory. Steeks strold .be arranged that eldest material is used first* return to J-Nl RESEARCH Flit ROOM X___'^DICATES -- REASON: Change to 10(05 W~3 Assslt AUTHORITY -- FOR CHANGE FILE-HOLDERS E* C* LAndstra9e wire 9-l@-57 Mass?. Wkg. lad* Em FORM 80I3R-10 PRINTED IN U.S.A. SUPERSEDES: Page 1 ease specification dated 1-2S-57 SUPR. QUAL. PROD. PLANT FINANCE RESEARCH MGR. QUAL. m CRMC-Thermo&Cement-000099 CRMC-Thermo&Cement-000100 Thennobostei? -PLANT PRODUCT: , - x :v, o arni J.;/0 2s: 4 iv- KOiW/LM [ Standard FiEfnitshi- . A'V fs7 1*C s da;,f)rial ^ ''r*/asvjcirg`mshsatri- .wwn*nu.4-.u *naja.ii- FPS lliiol? Ae 255 - c sow ' 28.5 FPS 2 s11 to 3S2 3C)Qf 1U.3 P* 2 * 62 S7 'Fr,;:.syijpi liras w Ur.O H D Amosita Fibre 6.8 c ii T.A2C Gs-~i&di&n Fibre h t. or hi = 28 2102# 2Q0*C$ ' i' t- S * 2$$> V:lui ttUcfc E .tit!' ' is# a Tioimm * * Hot idm Silica telling water and sersrice mates' is used to ma& a ratio of 2*5 gallons of r>ter to : i pijund ut i* /ii ViSi r<Ulji& V Dei .V^: i **vOsiii. 314 corrtafticlnation ? ,i * Us 27?# of billed Fib re* (Sorouti5f5ldrt3`: & ,0B Horissontal *ir, L;j f)c - 1 v, Liin:L Z-M g;.l t:jwb shall to 1 hour $0 ain. litoiSirasa gel y*j. m eoa'il h 2 hoxirs 50 hq.b>iia, - x A-^J ^ : Full bag x\iahii.tie are not waighed * part Fag que ntities ehail be 'xeighffidU X, hj-, |/U$a or Qal J to its to be u3od uni*] 1 -*Y.A6? i? ?!.? ad h;T Z<`U%:to 1 i^boratorj. Stocks shoiuid b ari ,513. -so tli4t it ira*Uor:Ul in' used first* " - r: / jR:/ )':J Ji -;p:'-; ""QTr j -li ji5i' EiPjIL ROOM vA"INCDHIACNACTEES -- KRtEAABSUOWN:' !'.;q oiu:> j- % i'ibi'0.. Add 25 lbs . lime & FS6 Hoe* FAOURTCHHOARNITGYE-- I?'t FILE-HOLDERS FORM 90131-10 PRINTED IN U.E.A. SUPERSEDES: 'OS ij, G, .. IMf tre? sated September l ?s> l?56 ii Hovo 30f 1956 ; laav Ind>2'C{ f/ ! fj :.i: A 7 *w*":r.TT!. j. .. ^ a.i ____ . SUM. QUAL. CONTROL MOD. PLANT FINANCE OFFICI RESEARCH CEV. NOR. QUAL. CONTROL DIR. QUAL. CONTR< DMMM CRMC-Thermo&Cement-000101 Manufacturing Specifications fi'iltfUK1 -----------------------------------------------------------------PLANT Magnesia _DEPT. ' jPRODUCT: , v5r .iiji r/Q DIVISION. . PAGE 1 IsfeS y yyyLyvk y ykkk-yy ' ;c" ' fV;'. y FOKkUIAs X Standard f umlEte* Spec. No. Material P. S. 61827 Gslita 256 - G Celit 392 . Mississippi Lis M D Araoaite fibre li TAX Canadian Fibre , Batcfc Weight Per Cent. 600? 300? 900# ieg?* -jgfe* 2orm 28.9 lit. 5 U3*3 8,9 U.U 100. c# . ^. .#;:; ' yyy;kk. (P yy ;:?. ;V-' yClV - ;o;{y:y - ' , .. ` r. , - , "*C , . mp: r. s. 63299 Aquablaek Water * Not* * * 1. 2. ..Hot Lima Silica telling water* and aerwie water is used : to mak a ratio of 2.5 gallon of water to 1 pound of solid., Water raust bo kept Svm fro Magnesia contamination. Use 277# of Milled fibre. (Sprout-Waldrcm Five Horizontal Willow). Minimum gel time shall be .1 hour 50 lain fc&admua gel time shall ba 2 hour 50 minute. Full bag quantities are not weighed pert bag quantities shall be weighed. No Idas or Gelite is to ba used until it is released- by Control Laboratory. Stock should bo arranged so that oldest material i used first. Wky TTZTZZ to change % Fibre. li FORM BOI9MO PNINTKO IN U.S.A. authority- FOR CHANGE FILE-HOLDERS supersedes: Latter of b. c. JLindetyom - dated September 17. 1956 \ Manv. ffkg* Ind.Etig SUPR. QUAl. CONTROL PaL 1 earn specification dated 6-2b5> PROO. ' SUPT. * PLANT FINANCE OPPICK RESEARCH LAB. NOR. QUAL. CONTROL i Q CO ,DA5^S!fi CRMC-Thermo&Cement-000102 :(\C^ t)5.1 Manufacturing specifications -PLANT -DEPT. PRODUCT! i/C BX^ates DIVISION- Llrl PAGE ' II FORMOSA* tbmrfe'aca.'swTttdffi.* ,, ^. J J Pwr&inhssxiawsawjrkura*s*b)p.-*s u rn-jLctt'tw trui 'Vzsa SSffOJjfe. Po S, 63.82? F, So 65299 \ u* ;*? InterMl e.ixt ;t *$(>*c . : eXXt# 35# ' : KiffXe3J.|^i LSffi M D Awaits 'Fibre " U TAX Citna&Ua Flb;ws Aqm&Utffc fm&h ' InrIVU<| f**tiv-rfi;.KOMIMIW'F Per Gssat wrum.: ftwi. iom !!, 3oe# .. 2U3 . 9QW k2n 200# ** 9$ 200$ ** I: luB UHhwffitv* . . *,\?<m:iini3r"aKi,.nant J10C# XQQ*C$ Kobo? & , ; - Hat .Lime Si.3ii.ea telling watm* aad sendee water in 'tv.mi . t snake . ratio. of .2* galXona of mter to X pound of " ' " acUta Wster"ust".l:io kajft,fP8U.;frcm. Mat^sXR ywi'twsiiUtiJ.osa, #* tfs 3Q0# :of aii3X.ed Fibre* jSp^^-WttXdroo : Hoclmtal Rlilcni}* ' :- Xo EiialKOM gX tSasffl afoaXX tie X hmn? #2 fl&n* Ksodasrum gal tiara shall be 2 .hours, $0 minute;Sc \ .full bag qwiMititiss an* not wlgtod - p*xt ba& c^atitlea shall ibs weighed. . 3. Ko Mae or C^iit In to he 'laed watAX it by (teatrol Lsiwata^v StecJra Nton&i-Ui arrange! e tbafc eldest mterl&l i uiod firsto I : RETUW v INDICATES --reason. a change Correction and add iusaTi.rau;s 4;sl tinie. J-M HI --flLTF-Uum AUTHORITY -- FOR CHANGE Letter of If* i* M1 C* t* * w till x&Jstrcsft datsd June ip9 1^.56\ FILE-HOLDERS roHH BOI3X- to PRINTED IN U.S.A. SUPERSEDES: Mav Wfeigo XifKioi'Jnf;;.. Page .1 s#obo specification dated SUPR. QUAL. CONTROL PROD. SOFT. PLANT FINANCE OFFICE RESEARCH LAB. ?/*76 NOR. QUAL. CONTROL D Ql COR DATE I88U 6/25/56 CRMC-Thermo&Cement-000103 .mxu? # #; m Manufacturing Specifications f U'i.utir'O'Si'. -PLANT ^ -DEPT. PRODUCT: t['ii3:^Xicb<@,'?t43S Block wad P/C ; `. DIVISION- PAGE % ' . . FOSMUXAs - : ; ' Standard Fmraiaht Spac.Nc* : .. Material %6 '^[n , Batata StM~ Per dSSE P. S. 61827 ---\ Callto 256-C , Qolite 392 *7 Mississippi him : M D Amosdte Fibre JU TAX Canadian Fibre ^ : : :-.. 6m 3Q<W . . 9?M 20G# 100$ * ; 2&M !Uo3 1*2.8 . 9.5 U.9 mm 1GG.C# P. So 6^99 . : Aquablaek Water sr ' # . Skates* # - Hot lime Silica tailing water and service water is sd to make a ratio of 2*? gallons of water to 1 pound if i ; eolido. Water must be kept ism from Ktogrosia conteadnatioQ. m Ca 300# of Milled. Fibre gSprout^Jaldroa Pliaa ; . ..... : .<, Vortical Willow). ` : 1. . Mnimrs gel time shall b 1 hour 50 mine , X. 2,, Full bag quantities &r not weighed part bag quantities .shall be weighed. ., . m 3. Wo Mb or Glite is to foe laced until it is released by Control Laboratory. S teste should b arranged so that oldest material is used first* . ft.. > .. . FORM 90131.10 PitINTRO IN U.9.A. v INDICATES A CHANGE -reasons General Roviffsion AUTHORITY -- FOR CHANGE Letter of i!i. C. lindstrom to P V. lybdal dated January 25$ 19$6 FILE-HOLDERS ' SUPERSEDES: j&terv. Wkg. |lnd.i^g SUPR. 0UAL. CONTROL All of same Specification dated 3/18/517 PROD. SUPT. PLANT FINANCE OFFICE RESEARCH LAS. HSR. OVAL. CONTROL 0 C0I DATE issu % 5/6 CRMC-Thermo&Cement-000104 Manufacturing Specifications ' *v ' i/atsor. .PLANT Kagnesia -DEPT. PRODUCTl Th?iniiobaL-to3 EXockw & Pip Covering X.P. spec, rs Mgl' paJse h t !'. Predicta .rA ?: t 'i;; :i';v; ' *.' V *"* MKk - *' {`rv'-W ' Thers^bsetos - Bleaks Tharuobsstos - Pipe Coveriiig See Fisdehad Product Specification II* Formi!*;. ~ Standard gtonlch Purclu . 8pgc No. ^ 61827-1 , 63299 ' ' '' Material wWNMNdiMW4n Batch . -JL-' Cellto Ho* 256 r C Oolite No 392 ISl.saiesippt Kycliatsd Lime I'O or EE* Amooit Fibre Tharmobs&tas Piastio ss addition Aquv'vblack as addition - 600 3C0 900 300 2100 ICO 10 28*5 14.3 42*9 2kX1<X).0 }S %(<,ry -'-f-i'V1 ' i,,- . Noto-tis :y Ilot lime BiXica tailing vaster and service vratsr is used to make a ratio f . - 2*4 gallons of vciitor to 1 pound of aolida. Kop gel tai^sratttro from 195 - 200P* \ .The sdniimsa gol time will bo. HO minutes . '. . - ' The jaitstemsn autoclaving tima at pressure will bo 180 Ednutsa* XXX* Ifenufacturltvr XnoSafuotiona - ' A. Raw Me.te'rf.ale . v ' . ' .: lw Celite and Ida will be purchased to a Purchase Specification and | ,vendors <M2jyais mast bo rsquented* :. ' 2* Only lilssissippi Hydrated 13.xse esj;i be need at this time* 3* Uco or V?~3 Aiaosita Fibre* , . 4* Thoraobeutos P3.4-.stic is obtained -from YheMsobeetos crushed trim* ; 5* Dss only fresh or Themobestos Eio3.dev filtrate. r ' a. Sfcgnaaia water cannot ba used* ' `V ^ 6* All incoiaiag ohipsenta of eslit lime anti asbestos fibre will be v identified with numbers assigned by the laboratory, a* Bo not us the above materials until released by the laboratory* , b* Arrango stocks so the oldest shipiaents ara used first* . 7* . Flbra Praoarati<m*. . . . ' '. ' '<' ...........a* .:foad 3<X> lbe of cruda'M or W-3" fibre into Psvctor and / ^ Scha.v'ts feodar* . : 1 "'. X--^change-reason! To establish Specificatlon 1 oftM 00131-10 forhchange~ 'Product Proposal CIJQ 107 dated 2/13/55 FILE-HOLDERS SUPERSEDES! SUPft. OUAL. CONTROL PROD. 8UPT. PLANT MGR. D FINANCE RESEARCH QUAL. OU OFFICE LAB. CONTROL CON DATE ISSU 3A&/55 CRMC-Thermo&Cement-000105