Document MGwp1bQoNoy1o88D48rgvb379
Report Prepared by: Report Approved by:
NPDES Pretreatment Compliance Sampling Inspection Report
Corning Incorporated Integrated Die Manufacturing 905 Addison Road Painted Post, New York
NYR00E417
September 26-27, 2023
ROBERT
Digitally signed by ROBERT
MORRELL
_M_O__R_R_E__L_L________D_at_e:_20_23_.1_1._21_1_6:_04_:2_4 -_05_'0_0'
Robert Morrell, Geologist
Monitoring Operations Section
Date: ________________
PHILIP COCUZZA
Digitally signed by PHILIP COCUZZA Date: 2023.11.22 06:49:57 -05'00'
________________________________
Philip Cocuzza, Supervisor
Monitoring Operations Section
Date: ________________
Corning Incorporated Integrated Die Manufacturing
Inspection Date: September 26-27, 2023
Page 2 of 7
Corning Incorporated Integrated Die Manufacturing
Inspection Date: September 26-27, 2023
1.0 OBJECTIVE
On September 26-27, 2023, at the request of the Water Compliance Branch, the United States Environmental Protection Agency (USEPA) conducted a National Pollutant Discharge Elimination System (NPDES) Pretreatment Compliance Sampling Inspection (CSI) at the Corning Incorporated Integrated Die Manufacturing (IDM) facility in Painted Post, New York. The objective of the CSI was to gather information necessary to determine compliance with the requirements and limitations of 40 CFR Part 433 (Metal Finishing Point Source Category) and the industrial sewer use permit issued by the Town of Erwin Wastewater Treatment Plant (WWTP).
2.0 KEY PARTICIPANTS
Listed below are key inspection participants and contact information, grouped by organization.
U.S. Environmental Protection Agency Robert Morrell, Geologist, Lead Inspector Morrell.robert@epa.gov, 732-906-6804 Neal Johansen, Physical Scientist Johansen.neal@epa.gov, 732-321-6691
Corning Incorporated IDM Facility Richard Bills, Environmental Health and Safety Manager BillsRA@Corning.com, 607-974-0860 Frances Ciolino, Corporate Environmental Control CiolinoF@Corning.com, 607-438-0932
3.0 FACILITY DESCRIPTION
3.1 General Information
The Corning Incorporated IDM facility is located at 905 Addison Road in Painted Post, New York. The facility is a manufacturer of dies that are used in the production process for ceramic catalytic converters. The company is categorized as Standard Industrial Classification (SIC) Code 3559 (Special Industry Machinery, Not Elsewhere Classified). The plant operates 24 hours per day, 5 days per week, with three 8-hour shifts. The plant currently has approximately 150 employees.
3.2 Process Information
At the Machine Module, stainless steel comes into the facility in blocks. Using computer numeric controlled (CNC) machines, the blocks of stainless steel are sliced, planed, and leveled to create the desired shape. Additional machining processes include drilling, cutting,
Page 3 of 7
Corning Incorporated Integrated Die Manufacturing
Inspection Date: September 26-27, 2023
grinding, and electro discharge machining (EDM). The dies are coated using a chemical vapor deposition (CVD) process.
Process water for the facility is provided by the Town of Erwin. During the manufacturing process, high pressure tap water is used to clean the dies several times in the Die Wash Room. Most of the process wastewater is generated in this room. Other sources of wastewater include cooling water drains from the CVD process, filtered wire water from the EDM process, and sinks in the process areas. The process wastewater is collected in a holding tank prior to being discharged to the Town of Erwin WWTP.
3.3 Facility Self-Monitoring Information
Pretreatment wastewater samples are collected quarterly and analyzed by Adirondack Environmental Services in Albany, New York. In lieu of required monitoring for total toxic organics, Corning has submitted a Toxic Organic Management Plan and has been granted permission to submit a certification statement in its reports to EPA.
4.0 EPA SAMPLING/INSPECTION ACTIVITIES
4.1 Sampling Activities
On September 26, 2023, an automatic composite sampler was set up at the effluent monitoring location. The sampler was programmed to collect an aliquot of the effluent wastewater every 15 minutes for 24 hours. After 24 hours, the automatic composite sampler was disassembled, and the composite sample jug was mixed thoroughly before filling the sample containers. The 24-hour composite sample was analyzed for metals (cadmium, chromium, copper, lead, nickel, silver, zinc, barium, arsenic, mercury, and selenium), chloride, fluoride, 5-day biochemical oxygen demand (BOD5), chemical oxygen demand (COD), total suspended solids (TSS), total dissolved solids (TDS), total phosphorus, ammonia, total kjeldahl nitrogen (TKN), nitrate, and nitrite. During the 24-hour sampling survey, a grab composite sample was also collected by filling the sample containers with four aliquots over 24 hours. The grab composite sample was analyzed for total cyanide, TTO non-volatile organics, and total phenolics. During the 24-hour sampling survey, four grab samples were also collected at the effluent monitoring location for TTO volatile organics, and oil and grease. A fifth grab sample was collected on September 27, 2023, for hexavalent chromium. Grab samples for pH, temperature, and total residual chlorine were collected and analyzed in the field. The 24-hour flow was provided by the facility representative.
All sample containers, preservation techniques, and holding times were in accordance with U.S. EPA requirements specified in 40 CFR Part 136. All samples were placed in a cooler with wet ice and transported to the U.S. EPA Region 2 Laboratory in Edison, New Jersey.
Split samples were collected and given to the facility representative.
Page 4 of 7
Corning Incorporated Integrated Die Manufacturing
Inspection Date: September 26-27, 2023
5.0 ANALYTICAL RESULTS
Corning Incorporated IDM Facility Pretreatment CSI - Effluent to POTW
September 26-27, 2023
Parameter
Effluent to POTW Local Discharge EPA 433.17 -
Limit - Daily Daily Maximum
Maximum
pH (su)
8.11, 9.37, 8.25, 8.33 6.0 - 9.0 (range) 5.0 minimum
Flow (gpd)
28,592
100,000
--
Total Residual Chlorine (mg/l)
0.31
50.0
--
Cadmium (mg/l)
Not detected
0.39
0.11
Chromium (mg/l)
Not detected
3.0
2.77
Copper (mg/l)
0.0788
2.45
3.38
Lead (mg/l)
Not detected
0.21
0.69
Nickel (mg/l)
Not detected
3.98
3.98
Silver (mg/l)
Not detected
3.19
0.43
Zinc (mg/l
Not detected
3.0
2.61
Barium (mg/l)
0.142
2.34
--
Arsenic (mg/l)
Not detected
0.33
--
Mercury (mg/l)
Not detected
0.04
--
Selenium (mg/l)
Not detected
0.17
--
Cyanide (mg/l)
Not detected
0.25
1.20
TTO (mg/l)
Not detected
--
2.13
Chloride (mg/l)
38.6 (9.20 lbs/day)
25 lbs/day
--
Fluoride (mg/l)
0.550 (0.13 lbs/day)
1 lbs/day
--
Total Phenolics (mg/l)
0.0295
0.89
--
BOD5 (mg/l)
2.36
250
--
COD (mg/l)
35.4 L
350
--
TSS (mg/l)
Not detected
300
--
TDS (mg/l)
377
Monitor only
--
Hexavalent Chromium (mg/l)
Not detected
0.69
--
Oil and Grease (mg/l)
Not detected
100
--
Phosphorus (mg/l)
1.23
15
--
Ammonia (mg/l)
Not detected
30
--
TKN (mg/l)
0.568 K
50
--
Nitrate (mg/l)
4.20
Monitor only
--
Nitrite (mg/l)
0.0302
Monitor only
--
L - The reported value may be biased low.
K - The reported value may be biased high.
Page 5 of 7
Corning Incorporated Integrated Die Manufacturing
6.0 FINDINGS
Inspection Date: September 26-27, 2023
6.1 Sampling Result Findings
There were four grab samples collected for pH during the 24-hour sampling survey. The second pH sample, collected on the afternoon of September 26, was 9.37 standard units, which was outside of the pH range of 6.0 to 9.0 standard units listed in the industrial sewer use permit issued by the Town of Erwin WWTP.
Laboratory analytical results for the 24-hour sampling survey indicate that all other parameters did not exceed local discharge limitations in the industrial user permit, or the federal categorical limitations listed in 40 CFR Section 433.17.
The oil and grease sample containers provided by Adirondack Environmental Services are not the required containers listed in EPA Method 1664A or Standard Method 5520. The containers must be 1-liter wide mouth glass containers.
Hexavalent chromium is currently listed as a 24-hour composite sample in the industrial sewer use permit issued by the Town of Erwin WWTP. Because of the short holding time for hexavalent chromium (24 hours), this sample should be collected as a grab sample at the end of the sampling event.
The local limits in the industrial sewer use permit are less stringent than the federal categorical limits for the following pollutants: cadmium, chromium, silver, and zinc. Local limits should be at least as stringent as federal pretreatment standards (40 CFR Section 403.4).
7.0 ATTACHMENTS
Photograph #1 Laboratory Data Report Chain of Custody / Field Data Forms
Page 6 of 7
Corning Incorporated Integrated Die Manufacturing
Inspection Date: September 26-27, 2023
Photo #1: View of the pretreatment effluent location where samples were collected.
Page 7 of 7
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
2890 Woodbridge Avenue Edison , New Jersey 08837
732-906-6886 Phone 732-906-6165 Fax
October 17, 2023
Bob Morrell Monitoring & Assessment Branch LSASD/MAB Edison, NJ 08837
RE: Corning Inc - 2309043 Enclosed are the results of analyses for samples received by the laboratory on 09/27/2023. The signature below reflects the laboratory's approval of the reported results. If you have any questions concerning this report, please refer to Project Number 2309043 and contact the laboratory. Sincerely,
John R. Bourbon Chief, LSASD/LB
Project Narrative:
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
The National Environmental Laboratory Accreditation Conference Institute (TNI) is a voluntary environmental laboratory accreditation association of State and Federal agencies. TNI established and promoted a National Environmental Laboratory Accreditation Program (NELAP) that provides a uniform set of standards for the generation of environmental data that are of known and defensible quality. The EPA Region 2 Laboratory is NELAP accredited. The Laboratory tests that are accredited have met all the requirements established under the TNI Standards.
Condition Comments
None
Comment(s):
The "Sample Analysis Date and Time" is included in the results section for any analyte with a prescribed holding time of 72 hours or less.
SVOA analysis: Most analytes are qualified mainly due to poor surrogate recovery.
Data Qualifier(s):
U- The analyte was not detected at or above the Reporting Limit. J- The identification of the analyte is acceptable; the reported value is an estimate. K- The identification of the analyte is acceptable; the reported value may be biased high. L- The identification of the analyte is acceptable; the reported value may be biased low. NJ- There is presumptive evidence that the analyte is present; the analyte is reported as a tentative identification. The reported value is an estimate.
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 1 of 42
Reporting Limit(s):
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
The Laboratory was able to achieve the standard laboratory reporting limits, where applicable, for each analyte requested except for the following analyte(s):
NVOA GCMS
The reporting level of 5.00 ug/L was raised to 10 ug/L for the following analyte(s): 2-Nitrophenol, Pentachlorophenol for the following samples: 2309043-01 The reporting level of 5.00 ug/L was raised to 30 ug/L for the following analyte(s): 2,4-Dinitrophenol, 4,6-Dinitro-2-Methylphenol for the following samples: 2309043-01
SUMMARY REPORT FOR SAMPLES
Field ID
Laboratory ID
Effluent-Grab Composite
2309043-01
Trip Blank
2309043-02
Effluent-Grab#1
2309043-03
Effluent-Grab#2
2309043-04
Effluent-Grab#3
2309043-05
Effluent-Grab#4
2309043-06
Effluent-Grab#5
2309043-07
Effluent-24Hr-Comp.
2309043-08
Effluent-Lab Composite-Grab#1to Grab#4 2309043-09
Matrix Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous
Date Sampled 09/27/2023 09:12 09/26/2023 11:15 09/26/2023 11:30 09/26/2023 14:10 09/26/2023 18:03 09/27/2023 09:12 09/27/2023 10:01 09/27/2023 08:12 09/27/2023 00:00
Date Received 09/27/2023 16:30 09/27/2023 16:30 09/27/2023 16:30 09/27/2023 16:30 09/27/2023 16:30 09/27/2023 16:30 09/27/2023 16:30 09/27/2023 16:30 09/27/2023 16:30
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 2 of 42
Analysis 624.1 VOA EPA-NPDES 625.1 SVOA NPDES Ammonia [As N] Biochemical Oxygen Demand Chemical Oxygen Demand Chloride Chromium, Hexavalent Cyanide, Total Fluoride Mercury Metals ICP TAL NPDES/DW Nitrate [As N] Nitrite [As N] Nitrogen, Total Kjeldahl Oil & Grease Phenolics, Total Phosphorus Residue, Filterable Residue, Non-Filterable
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
SUMMARY REPORT FOR METHODS
Method
EPA 624.1 SOP C-89 Rev 3.7 EPA 625.1 SOP C-90 Rev 3.9 EPA 350.1 SOP C-80 Rev 2.8 SM 5210B SOP C-21 Rev 2.8 EPA 410.4 SOP C-53 Rev 2.8 EPA 300.0 SOP C-94 Rev 2.8 HACH 8023 SOP C-96 Rev 2.8 EPA 335.4 SOP C-28 Rev 2.8 EPA 300.0 SOP C-94 Rev 2.8 EPA 245.1 SOP C-110 Rev 2.8 EPA 200.7 SOP C-109 Rev 3.7 EPA 353.2 SOP C-79 Rev 3.7 EPA 353.2 SOP C-79 Rev 3.7 EPA 351.2 SOP C-40 Rev2.8 EPA 1664A SOP C-126 Rev 1.7 EPA 420.4 SOP C-29 Rev 2.8 EPA 365.1 SOP C-68 Rev 2.8 SM 2540C SOP C-37 Rev 2.8 SM 2540D SOP C-33 Rev 3.8
Certification
NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP NELAP
Matrix
Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 3 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
Analyte
Field ID: Effluent-Grab Composite NVOA GCMS Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2309043-01
Date and Time of Analysis*
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
2.20
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U J
33.0
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U J
11.0
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
33.0
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 4 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
Analyte
Field ID: Effluent-Grab Composite NVOA GCMS 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2309043-01
Date and Time of Analysis*
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
2.20
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
2.20
ug/L B310011
---
U L
5.49
ug/L B310011
---
U J
2.20
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
5.49
ug/L B310011
---
U L
11.0
ug/L B310011
---
U L
2.20
ug/L B310011
---
U
5.49
ug/L B310011
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 5 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
Analyte
Result
Qualifier
Reporting Limit
Units
Batch
Date and Time of Analysis*
Field ID: Effluent-Grab Composite Sanitary Cyanide, Total Phenolics, Total
Field ID: Trip Blank VOA GCMS Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene
Sample ID: 2309043-01
---
U L
10.0
ug/L B310010
29.5
20.0
ug/L B309138
Sample ID: 2309043-02
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 6 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
Analyte
Field ID: Trip Blank VOA GCMS Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Field ID: Effluent-Grab#1 GC Oil & Grease
Field ID: Effluent-Grab#2 GC Oil & Grease
Field ID: Effluent-Grab#3 GC Oil & Grease
Field ID: Effluent-Grab#4 GC Oil & Grease
Field ID: Effluent-Grab#5 Sanitary
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2309043-02
Date and Time of Analysis*
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
Sample ID: 2309043-03
---
U
6.76
mg/L B310062
Sample ID: 2309043-04
---
U
6.02
mg/L B310062
Sample ID: 2309043-05
---
U
6.67
mg/L B310062
Sample ID: 2309043-06
---
U
6.94
mg/L B310062
Sample ID: 2309043-07
Chromium, Hexavalent
Field ID: Effluent-24Hr-Comp. Metals ICP Arsenic Barium Cadmium
---
U
10.0
ug/L B309132 09/27/2023 17:09
Sample ID: 2309043-08
---
U
8.00
ug/L B309146
142
100
ug/L B309146
---
U
3.00
ug/L B309146
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 7 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
Analyte
Field ID: Effluent-24Hr-Comp. Metals ICP Chromium Copper Lead Nickel Selenium Silver Zinc Mercury CVAA Mercury Sanitary Ammonia [As N] Biochemical Oxygen Demand Chemical Oxygen Demand Chloride Fluoride Nitrate [As N] Nitrite [As N] Nitrogen, Total Kjeldahl Phosphorus Total Dissolved Solids Total Suspended Solids
Field ID: Effluent-Lab Composite-Grab#1to Grab#4 VOA GCMS Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2309043-08
Date and Time of Analysis*
---
U
5.00
ug/L B309146
78.8
10.0
ug/L B309146
---
U
8.00
ug/L B309146
---
U
20.0
ug/L B309146
---
U
20.0
ug/L B309146
---
U
5.00
ug/L B309146
---
U
20.0
ug/L B309146
---
U
0.050
ug/L B310050
---
U L
0.100
mg/L B310022
2.36
2.00
mg/L B309141 10/03/2023 10:10
35.4
L
20.0
mg/L B309140
38.6
1.00
mg/L B310004
0.550
0.0500
mg/L B310002
4.20
0.500
mg/L B309134 09/27/2023 16:48
0.0302
0.0250
mg/L B309134 09/27/2023 16:48
0.568
K
0.100
mg/L B310003
1.23
0.0500
mg/L B310048
377
10.0
mg/L B310013
---
U
10.0
mg/L B310014
Sample ID: 2309043-09
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U J
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 8 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
Analyte
Field ID: Effluent-Lab Composite-Grab#1to Grab#4 VOA GCMS Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2309043-09
Date and Time of Analysis*
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U J
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 9 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043
VOA GCMS - Quality Control
Analyte
Batch B309136
Blank (B309136-BLK1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
101
ug/L
100.0
105
ug/L
100.0
107
ug/L
100.0
101
60-140
105
60-140
107
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 10 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 VOA GCMS - Quality Control
Analyte
Batch B309136
LCS (B309136-BS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
51.2
5.00 ug/L
50.00
46.4
5.00 ug/L
50.00
45.7
5.00 ug/L
50.00
51.6
5.00 ug/L
50.00
52.8
5.00 ug/L
50.00
54.4
5.00 ug/L
50.00
55.4
5.00 ug/L
50.00
62.6
5.00 ug/L
50.00
57.6
5.00 ug/L
50.00
56.2
5.00 ug/L
50.00
55.7
5.00 ug/L
50.00
57.1
5.00 ug/L
50.00
55.5
5.00 ug/L
50.00
55.7
5.00 ug/L
50.00
56.7
5.00 ug/L
50.00
55.7
5.00 ug/L
50.00
57.1
5.00 ug/L
50.00
56.0
5.00 ug/L
50.00
56.5
5.00 ug/L
50.00
56.4
5.00 ug/L
50.00
59.8
5.00 ug/L
50.00
53.9
5.00 ug/L
50.00
52.6
5.00 ug/L
50.00
55.4
5.00 ug/L
50.00
54.4
5.00 ug/L
50.00
57.4
5.00 ug/L
50.00
55.1
5.00 ug/L
50.00
57.3
5.00 ug/L
50.00
53.6
5.00 ug/L
50.00
52.6
5.00 ug/L
50.00
53.2
5.00 ug/L
50.00
99.0
ug/L
100.0
106
ug/L
100.0
110
ug/L
100.0
102
19-205
92.8
5-195
91.5
15-185
103
40-160
106
50-150
109
50-150
111
60-140
125
60-140
115
70-130
112
70-130
111
70-135
114
70-130
111
70-130
111
70-130
113
65-135
111
65-135
114
35-165
112
65-135
113
25-175
113
70-130
120
50-150
108
70-130
105
70-130
111
70-135
109
65-135
115
60-140
110
70-130
115
60-140
107
70-130
105
65-135
106
65-135
99.0
60-140
106
60-140
110
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 11 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 VOA GCMS - Quality Control
Analyte
Batch B309136
LCS Dup (B309136-BSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
48.2
5.00 ug/L
50.00
43.0
5.00 ug/L
50.00
44.5
5.00 ug/L
50.00
49.0
5.00 ug/L
50.00
50.1
5.00 ug/L
50.00
51.6
5.00 ug/L
50.00
53.6
5.00 ug/L
50.00
62.0
5.00 ug/L
50.00
55.0
5.00 ug/L
50.00
53.5
5.00 ug/L
50.00
52.9
5.00 ug/L
50.00
53.7
5.00 ug/L
50.00
52.0
5.00 ug/L
50.00
54.7
5.00 ug/L
50.00
53.2
5.00 ug/L
50.00
53.0
5.00 ug/L
50.00
54.2
5.00 ug/L
50.00
53.5
5.00 ug/L
50.00
53.7
5.00 ug/L
50.00
52.4
5.00 ug/L
50.00
56.7
5.00 ug/L
50.00
52.8
5.00 ug/L
50.00
50.0
5.00 ug/L
50.00
53.6
5.00 ug/L
50.00
51.7
5.00 ug/L
50.00
54.5
5.00 ug/L
50.00
54.5
5.00 ug/L
50.00
55.1
5.00 ug/L
50.00
51.4
5.00 ug/L
50.00
50.9
5.00 ug/L
50.00
51.9
5.00 ug/L
50.00
97.8
ug/L
100.0
103
ug/L
100.0
109
ug/L
100.0
96.5
19-205
6.05
20
86.1
5-195
7.49
20
89.0
15-185
2.73
20
98.1
40-160
5.18
20
100
50-150
5.21
20
103
50-150
5.42
20
107
60-140
3.36
20
124
60-140
0.979
20
110
70-130
4.58
20
107
70-130
4.96
20
106
70-135
5.17
20
107
70-130
6.03
20
104
70-130
6.54
20
109
70-130
1.78
20
106
65-135
6.37
20
106
65-135
5.08
20
108
35-165
5.12
20
107
65-135
4.67
20
107
25-175
5.15
20
105
70-130
7.35
20
113
50-150
5.22
20
106
70-130
2.06
20
100
70-130
5.09
20
107
70-135
3.21
20
103
65-135
5.04
20
109
60-140
5.15
20
109
70-130
0.986
20
110
60-140
3.79
20
103
70-130
4.21
20
102
65-135
3.29
20
104
65-135
2.49
20
97.8
60-140
103
60-140
109
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 12 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 VOA GCMS - Quality Control
Analyte
Batch B309136
Matrix Spike (B309136-MS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309020-08
49.6
5.00 ug/L
49.7
5.00 ug/L
33.3
5.00 ug/L
55.2
5.00 ug/L
53.7
5.00 ug/L
52.8
5.00 ug/L
55.0
5.00 ug/L
57.9
5.00 ug/L
53.5
5.00 ug/L
55.6
5.00 ug/L
66.7
5.00 ug/L
54.9
5.00 ug/L
55.0
5.00 ug/L
54.0
5.00 ug/L
54.5
5.00 ug/L
54.1
5.00 ug/L
55.2
5.00 ug/L
55.2
5.00 ug/L
40.3
5.00 ug/L
53.5
5.00 ug/L
48.4
5.00 ug/L
52.8
5.00 ug/L
51.7
5.00 ug/L
53.1
5.00 ug/L
52.8
5.00 ug/L
54.8
5.00 ug/L
53.0
5.00 ug/L
56.2
5.00 ug/L
52.6
5.00 ug/L
52.1
5.00 ug/L
52.6
5.00 ug/L
98.2
ug/L
104
ug/L
110
ug/L
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
12.5
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
100.0 100.0 100.0
99.1
19-273
99.4
49-251
66.6
21-242
110
14-230
107
17-181
106
52-234
110
69-221
116
40-160
107
54-156
111
59-155
108
51-138
110
52-162
110
70-140
108
49-155
109
37-151
108
70-157
110
74-210
110
35-155
80.6
80-227
107
47-150
96.8
17-183
106
52-150
103
64-148
106
53-149
106
37-160
110
37-162
106
45-169
112
46-157
105
59-156
104
18-190
105
18-190
98.2
60-140
104
60-140
110
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 13 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 VOA GCMS - Quality Control
Analyte
Batch B309136
Matrix Spike (B309136-MS2) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309043-09
46.7
5.00 ug/L
49.3
5.00 ug/L
8.96
5.00 ug/L
53.4
5.00 ug/L
54.4
5.00 ug/L
53.3
5.00 ug/L
55.2
5.00 ug/L
58.8
5.00 ug/L
52.3
5.00 ug/L
55.3
5.00 ug/L
54.4
5.00 ug/L
54.6
5.00 ug/L
54.0
5.00 ug/L
53.4
5.00 ug/L
55.0
5.00 ug/L
54.7
5.00 ug/L
54.7
5.00 ug/L
54.6
5.00 ug/L
15.2
5.00 ug/L
54.2
5.00 ug/L
35.1
5.00 ug/L
53.0
5.00 ug/L
52.0
5.00 ug/L
54.5
5.00 ug/L
52.2
5.00 ug/L
54.5
5.00 ug/L
54.1
5.00 ug/L
55.5
5.00 ug/L
52.3
5.00 ug/L
52.4
5.00 ug/L
52.3
5.00 ug/L
99.3
ug/L
106
ug/L
111
ug/L
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
100.0 100.0 100.0
93.4
19-273
98.6
49-251
17.9
21-242
107
14-230
109
17-181
107
52-234
110
69-221
118
40-160
105
54-156
111
59-155
109
51-138
109
52-162
108
70-140
107
49-155
110
37-151
109
70-157
109
74-210
109
35-155
30.5
80-227
108
47-150
70.1
17-183
106
52-150
104
64-148
109
53-149
104
37-160
109
37-162
108
45-169
111
46-157
105
59-156
105
18-190
105
18-190
99.3
60-140
106
60-140
111
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 14 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 VOA GCMS - Quality Control
Analyte
Batch B309136
Matrix Spike Dup (B309136-MSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309020-08
45.2
5.00 ug/L
50.00
ND
90.4
19-273
9.18
28
44.6
5.00 ug/L
50.00
ND
89.1
49-251
10.9
28
26.6
5.00 ug/L
50.00
ND
53.1
21-242
22.6
28
49.6
5.00 ug/L
50.00
ND
99.3
14-230
10.5
28
48.7
5.00 ug/L
50.00
ND
97.4
17-181
9.75
28
47.8
5.00 ug/L
50.00
ND
95.7
52-234
9.76
28
50.4
5.00 ug/L
50.00
ND
101
69-221
8.69
28
55.4
5.00 ug/L
50.00
ND
111
40-160
4.34
28
49.5
5.00 ug/L
50.00
ND
99.0
54-156
7.84
28
50.6
5.00 ug/L
50.00
ND
101
59-155
9.51
28
60.7
5.00 ug/L
50.00
12.5
96.5
51-138
11.7
28
50.4
5.00 ug/L
50.00
ND
101
52-162
8.63
28
49.6
5.00 ug/L
50.00
ND
99.2
70-140
10.3
28
50.3
5.00 ug/L
50.00
ND
101
49-155
6.98
28
50.6
5.00 ug/L
50.00
ND
101
37-151
7.50
28
49.8
5.00 ug/L
50.00
ND
99.6
70-157
8.32
28
51.1
5.00 ug/L
50.00
ND
102
74-210
7.56
28
52.0
5.00 ug/L
50.00
ND
104
35-155
6.14
28
34.0
5.00 ug/L
50.00
ND
68.0
80-227
16.9
28
49.7
5.00 ug/L
50.00
ND
99.3
47-150
7.42
28
43.9
5.00 ug/L
50.00
ND
87.9
17-183
9.64
28
49.7
5.00 ug/L
50.00
ND
99.4
52-150
6.01
28
47.6
5.00 ug/L
50.00
ND
95.3
64-148
8.23
28
49.6
5.00 ug/L
50.00
ND
99.2
53-149
6.72
28
49.0
5.00 ug/L
50.00
ND
98.0
37-160
7.46
28
50.9
5.00 ug/L
50.00
ND
102
37-162
7.27
28
50.3
5.00 ug/L
50.00
ND
101
45-169
5.24
28
53.4
5.00 ug/L
50.00
ND
107
46-157
5.05
28
49.1
5.00 ug/L
50.00
ND
98.1
59-156
6.93
28
49.2
5.00 ug/L
50.00
ND
98.4
18-190
5.71
28
49.3
5.00 ug/L
50.00
ND
98.5
18-190
6.60
28
99.3
ug/L
100.0
99.3
60-140
104
ug/L
100.0
104
60-140
110
ug/L
100.0
110
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 15 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 VOA GCMS - Quality Control
Analyte
Batch B309136
Matrix Spike Dup (B309136-MSD2) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309043-09
45.3
5.00 ug/L
47.7
5.00 ug/L
6.04
5.00 ug/L
54.4
5.00 ug/L
53.5
5.00 ug/L
53.3
5.00 ug/L
53.9
5.00 ug/L
57.7
5.00 ug/L
52.5
5.00 ug/L
53.6
5.00 ug/L
53.5
5.00 ug/L
54.0
5.00 ug/L
53.5
5.00 ug/L
52.6
5.00 ug/L
54.6
5.00 ug/L
54.0
5.00 ug/L
54.4
5.00 ug/L
54.3
5.00 ug/L
9.68
5.00 ug/L
53.4
5.00 ug/L
29.9
5.00 ug/L
51.9
5.00 ug/L
51.1
5.00 ug/L
53.2
5.00 ug/L
52.0
5.00 ug/L
53.8
5.00 ug/L
53.1
5.00 ug/L
54.2
5.00 ug/L
52.0
5.00 ug/L
51.8
5.00 ug/L
52.2
5.00 ug/L
99.8
ug/L
105
ug/L
110
ug/L
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
100.0 100.0 100.0
90.6
19-273
3.02
28
95.5
49-251
3.19
28
12.1
21-242
38.9
28
109
14-230
1.87
28
107
17-181
1.69
28
107
52-234 0.0188
28
108
69-221
2.49
28
115
40-160
1.90
28
105
54-156
0.324
28
107
59-155
3.12
28
107
51-138
1.54
28
108
52-162
1.16
28
107
70-140
0.967
28
105
49-155
1.51
28
109
37-151
0.657
28
108
70-157
1.16
28
109
74-210
0.476
28
109
35-155
0.477
28
19.4
80-227
44.6
28
107
47-150
1.60
28
59.8
17-183
15.9
28
104
52-150
2.17
28
102
64-148
1.73
28
106
53-149
2.28
28
104
37-160
0.230
28
108
37-162
1.29
28
106
45-169
1.88
28
108
46-157
2.41
28
104
59-156
0.479
28
104
18-190
1.13
28
104
18-190
0.191
28
99.8
60-140
105
60-140
110
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 16 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
Blank (B310011-BLK1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
Page 17 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Batch B310011
Blank (B310011-BLK1) Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
LCS (B310011-BS1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
2.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
2.00 ug/L
--- U
5.00 ug/L
ND
ug/L
50.00
ND
ug/L
50.00
ND
ug/L
50.00
ND
ug/L
50.00
ND
ug/L
50.00
32.2
ug/L
50.00
32.6
ug/L
50.00
39.8
5.00 ug/L
50.00
37.6
5.00 ug/L
50.00
43.3
5.00 ug/L
50.00
45.2
5.00 ug/L
50.00
46.3
5.00 ug/L
50.00
47.3
5.00 ug/L
50.00
50.3
5.00 ug/L
50.00
47.4
5.00 ug/L
50.00
45.7
60-140
21.5
60-140
41.5
60-140
40.2
60-140
13.6
60-140
64.4
60-140
65.2
60-140
79.5
47-145
75.2
33-145
86.6
27-133
90.4
33-143
92.5
17-163
94.7
24-159
101
35-219
94.8
11-162
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 18 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
LCS (B310011-BS1) Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene
44.7
5.00 ug/L
50.00
47.8
5.00 ug/L
50.00
44.2
5.00 ug/L
50.00
42.1
5.00 ug/L
50.00
50.5
5.00 ug/L
50.00
36.3
5.00 ug/L
50.00
44.0
5.00 ug/L
50.00
33.1
5.00 ug/L
50.00
30.0
5.00 ug/L
50.00
35.3
5.00 ug/L
50.00
40.7
5.00 ug/L
50.00
46.9
5.00 ug/L
50.00
45.1
5.00 ug/L
50.00
4.37
5.00 ug/L
50.00
38.0
5.00 ug/L
50.00
35.1
5.00 ug/L
50.00
3.61
5.00 ug/L
50.00
50.8
5.00 ug/L
50.00
27.4
5.00 ug/L
50.00
43.6
5.00 ug/L
50.00
41.3
5.00 ug/L
50.00
41.9
5.00 ug/L
50.00
16.0
5.00 ug/L
50.00
38.5
5.00 ug/L
50.00
36.6
5.00 ug/L
50.00
35.1
5.00 ug/L
50.00
52.2
5.00 ug/L
50.00
44.9
5.00 ug/L
50.00
45.2
5.00 ug/L
50.00
44.3
5.00 ug/L
50.00
38.9
5.00 ug/L
50.00
47.2
5.00 ug/L
50.00
50.7
5.00 ug/L
50.00
43.0
5.00 ug/L
50.00
32.8
2.00 ug/L
50.00
89.4
17-168
95.6
33-227
88.4
26-137
84.3
59-121
101
39-171
72.7
21-133
88.0
54-120
66.1
44-142
59.9
37-144
70.6
39-135
81.4
32-120
93.8
39-139
90.2
50-158
8.74
21-191
76.0
60-120
70.1
23-134
7.22
29-182
102
38-262
54.8
17-181
87.2
53-127
82.7
22-147
83.8
25-158
32.1
9-132
77.1
33-184
73.2
12-158
70.2
36-166
104
8-158
89.8
38-152
90.5
60-115
88.6
31-114
77.7
28-120
94.5
1-120
101
4-146
86.0
35-152
65.5
24-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
Page 19 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Batch B310011
LCS (B310011-BS1) Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
LCS Dup (B310011-BSD1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
34.3
5.00 ug/L
50.00
31.2
5.00 ug/L
50.00
44.4
5.00 ug/L
50.00
40.5
5.00 ug/L
50.00
25.2
5.00 ug/L
50.00
40.5
5.00 ug/L
50.00
52.4
5.00 ug/L
50.00
--- U
5.00 ug/L
50.00
17.1
2.00 ug/L
50.00
43.3
5.00 ug/L
50.00
32.4
ug/L
50.00
14.9
ug/L
50.00
31.5
ug/L
50.00
30.9
ug/L
50.00
32.8
ug/L
50.00
40.3
ug/L
50.00
40.0
ug/L
50.00
39.3
5.00 ug/L
50.00
36.7
5.00 ug/L
50.00
45.5
5.00 ug/L
50.00
46.7
5.00 ug/L
50.00
47.2
5.00 ug/L
50.00
50.0
5.00 ug/L
50.00
50.9
5.00 ug/L
50.00
47.9
5.00 ug/L
50.00
45.6
5.00 ug/L
50.00
49.0
5.00 ug/L
50.00
44.7
5.00 ug/L
50.00
47.7
5.00 ug/L
50.00
52.3
5.00 ug/L
50.00
35.1
5.00 ug/L
50.00
46.6
5.00 ug/L
50.00
31.5
5.00 ug/L
50.00
68.6
15-76
62.5
40-120
88.8
21-196
81.0
35-180
50.5
17-127
81.0
43-230
105
79-139
14-176
34.2
5-120
86.6
52-120
64.7
60-140
29.8
60-140
62.9
60-140
61.9
60-140
65.6
60-140
80.6
60-140
79.9
60-140
78.6
47-145
1.16
30
73.4
33-145
2.34
30
91.0
27-133
4.91
30
93.3
33-143
3.22
30
94.4
17-163
1.97
30
100
24-159
5.47
30
102
35-219
1.23
30
95.8
11-162
1.05
30
91.1
17-168
1.91
30
97.9
33-227
2.46
30
89.3
26-137
1.08
30
95.4
59-121
12.4
30
105
39-171
3.44
30
70.3
21-133
3.36
30
93.2
54-120
5.74
30
63.0
44-142
4.86
30
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 20 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
LCS Dup (B310011-BSD1) 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol
31.0
5.00 ug/L
50.00
36.6
5.00 ug/L
50.00
36.7
5.00 ug/L
50.00
51.7
5.00 ug/L
50.00
43.6
5.00 ug/L
50.00
3.01
5.00 ug/L
50.00
36.9
5.00 ug/L
50.00
36.8
5.00 ug/L
50.00
6.52
5.00 ug/L
50.00
52.0
5.00 ug/L
50.00
25.2
5.00 ug/L
50.00
47.7
5.00 ug/L
50.00
42.1
5.00 ug/L
50.00
47.9
5.00 ug/L
50.00
13.1
5.00 ug/L
50.00
39.3
5.00 ug/L
50.00
37.8
5.00 ug/L
50.00
35.9
5.00 ug/L
50.00
53.8
5.00 ug/L
50.00
46.2
5.00 ug/L
50.00
49.4
5.00 ug/L
50.00
47.1
5.00 ug/L
50.00
34.2
5.00 ug/L
50.00
48.0
5.00 ug/L
50.00
52.1
5.00 ug/L
50.00
45.7
5.00 ug/L
50.00
30.2
2.00 ug/L
50.00
30.1
5.00 ug/L
50.00
29.8
5.00 ug/L
50.00
45.8
5.00 ug/L
50.00
39.8
5.00 ug/L
50.00
27.1
5.00 ug/L
50.00
41.3
5.00 ug/L
50.00
57.2
5.00 ug/L
50.00
--- U
5.00 ug/L
50.00
62.1
37-144
3.51
73.2
39-135
3.64
73.3
32-120
10.4
103
39-139
9.69
87.3
50-158
3.36
6.02
21-191
36.9
73.8
60-120
2.83
73.7
23-134
4.95
13.0
29-182
57.5
104
38-262
2.20
50.3
17-181
8.41
95.5
53-127
9.09
84.3
22-147
1.94
95.8
25-158
13.3
26.3
9-132
19.8
78.6
33-184
1.93
75.6
12-158
3.23
71.9
36-166
2.28
108
8-158
2.91
92.4
38-152
2.83
98.9
60-115
8.87
94.1
31-114
6.06
68.5
28-120
12.7
96.0
1-120
1.60
104
4-146
2.67
91.5
35-152
6.13
60.3
24-120
8.26
60.1
15-76
13.1
59.6
40-120
4.75
91.7
21-196
3.21
79.6
35-180
1.74
54.1
17-127
7.00
82.6
43-230
1.93
114
79-139
8.85
14-176
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30
Page 21 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Batch B310011
LCS Dup (B310011-BSD1) Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
Matrix Spike (B310011-MS1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
18.4
2.00 ug/L
50.00
44.2
5.00 ug/L
50.00
33.9
ug/L
50.00
16.1
ug/L
50.00
30.6
ug/L
50.00
30.2
ug/L
50.00
33.1
ug/L
50.00
42.1
ug/L
50.00
40.9
ug/L
50.00
36.8
5-120
7.26
30
88.4
52-120
2.10
30
67.9
60-140
32.2
60-140
61.1
60-140
60.5
60-140
66.3
60-140
84.2
60-140
81.7
60-140
Source: 2309020-02
33.3
5.05 ug/L
33.1
5.05 ug/L
35.5
5.05 ug/L
38.6
5.05 ug/L
38.0
5.05 ug/L
37.9
5.05 ug/L
35.2
5.05 ug/L
38.2
5.05 ug/L
38.5
5.05 ug/L
35.8
5.05 ug/L
35.6
5.05 ug/L
36.7
5.05 ug/L
36.7
5.05 ug/L
22.5
5.05 ug/L
36.3
5.05 ug/L
20.2
5.05 ug/L
27.2
5.05 ug/L
26.2
5.05 ug/L
24.2
5.05 ug/L
37.3
5.05 ug/L
35.0
5.05 ug/L
9.92
5.05 ug/L
29.6
5.05 ug/L
20.9
5.05 ug/L
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
66.0
47-145
65.5
33-145
70.2
27-133
76.5
33-143
75.3
17-163
75.0
24-159
69.7
35-219
75.7
11-162
76.3
17-168
70.8
33-227
70.5
26-137
72.6
59-121
72.8
39-171
44.6
21-133
71.8
54-120
40.1
44-142
53.9
37-144
51.9
39-135
48.0
32-120
73.9
39-139
69.3
50-158
19.6
21-191
58.6
60-120
41.4
23-134
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 22 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
Matrix Spike (B310011-MS1) 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10
Source: 2309020-02
--- U
5.05 ug/L
38.0
5.05 ug/L
24.2
5.05 ug/L
37.6
5.05 ug/L
34.8
5.05 ug/L
36.9
5.05 ug/L
13.4
5.05 ug/L
28.2
5.05 ug/L
22.7
5.05 ug/L
23.1
5.05 ug/L
43.9
5.05 ug/L
37.5
5.05 ug/L
39.1
5.05 ug/L
37.7
5.05 ug/L
34.3
5.05 ug/L
38.4
5.05 ug/L
42.3
5.05 ug/L
35.5
5.05 ug/L
18.8
2.02 ug/L
16.4
5.05 ug/L
15.9
5.05 ug/L
33.4
5.05 ug/L
26.5
5.05 ug/L
15.6
5.05 ug/L
30.3
5.05 ug/L
36.9
5.05 ug/L
9.28
5.05 ug/L
12.4
2.02 ug/L
35.1
5.05 ug/L
20.0
ug/L
10.8
ug/L
21.9
ug/L
21.3
ug/L
28.7
ug/L
33.0
ug/L
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51 50.51 50.51 50.51 50.51 50.51
29-182
75.3
38-262
47.9
17-181
74.4
53-127
69.0
22-147
73.0
25-158
26.5
9-132
55.8
33-184
44.9
12-158
45.8
36-166
87.0
8-158
74.2
38-152
77.3
61-106
74.6
31-114
68.0
28-120
76.1
1-120
83.7
4-146
70.3
35-152
37.2
24-120
32.4
15-76
31.4
40-120
66.0
21-196
52.4
35-180
30.9
17-127
59.9
43-230
73.0
79-139
18.4
14-176
24.5
5-120
69.5
52-120
39.6
60-140
21.3
60-140
43.3
60-140
42.1
60-140
56.7
60-140
65.4
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
Page 23 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Batch B310011
Matrix Spike (B310011-MS1) Surrogate: Chrysene-D12
Matrix Spike (B310011-MS2) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Source: 2309020-02
34.0
ug/L
Source: 2309043-01
38.3
5.56 ug/L
37.9
5.56 ug/L
45.4
5.56 ug/L
45.6
5.56 ug/L
49.3
5.56 ug/L
47.3
5.56 ug/L
51.2
5.56 ug/L
49.0
5.56 ug/L
45.6
5.56 ug/L
50.9
5.56 ug/L
44.9
5.56 ug/L
46.0
5.56 ug/L
54.1
5.56 ug/L
28.7
5.56 ug/L
47.0
5.56 ug/L
26.2
5.56 ug/L
38.1
5.56 ug/L
34.2
5.56 ug/L
32.1
5.56 ug/L
50.8
5.56 ug/L
41.4
5.56 ug/L
22.2
5.56 ug/L
34.9
5.56 ug/L
28.4
5.56 ug/L
7.80
5.56 ug/L
41.2
5.56 ug/L
40.9
5.56 ug/L
47.6
5.56 ug/L
41.7
5.56 ug/L
45.7
5.56 ug/L
20.5
5.56 ug/L
34.4
5.56 ug/L
50.51
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
67.4
60-140
68.9
47-145
68.2
33-145
81.8
27-133
82.0
33-143
88.7
17-163
85.1
24-159
92.2
35-219
88.2
11-162
82.0
17-168
91.7
33-227
80.8
26-137
82.8
59-121
97.3
39-171
51.7
21-133
84.6
54-120
47.2
44-142
68.6
37-144
61.5
39-135
57.8
32-120
91.4
39-139
74.6
50-158
39.9
21-191
62.8
60-120
51.1
23-134
14.0
29-182
74.1
38-262
73.6
17-181
85.6
53-127
75.1
22-147
82.3
25-158
36.8
9-132
61.9
33-184
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
Page 24 of 42
Analyte
Batch B310011
Matrix Spike (B310011-MS2) Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309043-01
30.6
5.56 ug/L
31.6
5.56 ug/L
54.1
5.56 ug/L
48.1
5.56 ug/L
48.5
5.56 ug/L
46.7
5.56 ug/L
33.3
5.56 ug/L
50.0
5.56 ug/L
54.6
5.56 ug/L
47.3
5.56 ug/L
25.2
2.22 ug/L
21.8
5.56 ug/L
21.1
5.56 ug/L
39.8
5.56 ug/L
33.2
5.56 ug/L
20.5
5.56 ug/L
36.9
5.56 ug/L
48.1
5.56 ug/L
23.0
5.56 ug/L
15.5
2.22 ug/L
44.2
5.56 ug/L
25.9
ug/L
13.5
ug/L
27.5
ug/L
27.3
ug/L
34.6
ug/L
42.9
ug/L
40.4
ug/L
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56 55.56 55.56 55.56 55.56 55.56 55.56
55.0
12-158
57.0
36-166
97.4
8-158
86.6
38-152
87.3
61-106
84.1
31-114
60.0
28-120
90.0
1-120
98.3
4-146
85.1
35-152
45.4
24-120
39.2
15-76
38.0
40-120
71.6
21-196
59.7
35-180
36.9
17-127
66.4
43-230
86.7
79-139
41.5
14-176
27.9
5-120
79.6
52-120
46.7
60-140
24.3
60-140
49.6
60-140
49.2
60-140
62.4
60-140
77.2
60-140
72.8
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 25 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
Matrix Spike Dup (B310011-MSD1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate
Source: 2309020-02
41.6
5.05 ug/L
42.0
5.05 ug/L
48.2
5.05 ug/L
50.6
5.05 ug/L
51.5
5.05 ug/L
50.8
5.05 ug/L
49.4
5.05 ug/L
51.8
5.05 ug/L
50.1
5.05 ug/L
50.0
5.05 ug/L
48.4
5.05 ug/L
51.2
5.05 ug/L
52.8
5.05 ug/L
33.5
5.05 ug/L
50.2
5.05 ug/L
28.7
5.05 ug/L
39.4
5.05 ug/L
38.7
5.05 ug/L
28.7
5.05 ug/L
55.8
5.05 ug/L
45.4
5.05 ug/L
18.0
5.05 ug/L
39.3
5.05 ug/L
28.3
5.05 ug/L
10.6
5.05 ug/L
45.2
5.05 ug/L
39.0
5.05 ug/L
50.9
5.05 ug/L
45.1
5.05 ug/L
50.4
5.05 ug/L
18.2
5.05 ug/L
42.5
5.05 ug/L
32.3
5.05 ug/L
35.1
5.05 ug/L
57.8
5.05 ug/L
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
82.3
47-145
22.0
83.1
33-145
23.7
95.4
27-133
30.4
100
33-143
26.7
102
17-163
30.1
101
24-159
29.2
97.9
35-219
33.7
102
11-162
30.0
99.2
17-168
26.2
99.0
33-227
33.1
95.7
26-137
30.4
101
59-121
33.0
105
39-171
35.8
66.2
21-133
39.0
99.4
54-120
32.2
56.9
44-142
34.8
78.0
37-144
36.5
76.7
39-135
38.5
56.8
32-120
16.8
111
39-139
39.8
89.9
50-158
25.9
35.6
21-191
57.8
77.8
60-120
28.2
55.9
23-134
29.9
21.0
29-182
89.5
38-262
17.2
77.2
17-181
46.8
101
53-127
30.0
89.3
22-147
25.7
99.8
25-158
31.0
36.0
9-132
30.4
84.1
33-184
40.5
64.0
12-158
35.0
69.4
36-166
41.1
114
8-158
27.3
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24
Page 26 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Batch B310011
Matrix Spike Dup (B310011-MSD1) Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
Matrix Spike Dup (B310011-MSD2) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309020-02
50.8
5.05 ug/L
50.51
ND
101
38-152
30.2
24
53.5
5.05 ug/L
50.51
ND
106
61-106
31.2
24
52.0
5.05 ug/L
50.51
ND
103
31-114
32.0
24
41.6
5.05 ug/L
50.51
ND
82.4
28-120
19.2
24
51.8
5.05 ug/L
50.51
ND
103
1-120
29.6
24
57.1
5.05 ug/L
50.51
ND
113
4-146
29.8
24
49.3
5.05 ug/L
50.51
ND
97.5
35-152
32.4
24
25.9
2.02 ug/L
50.51
ND
51.3
24-120
31.9
24
24.5
5.05 ug/L
50.51
ND
48.5
15-76
39.8
24
17.0
5.05 ug/L
50.51
ND
33.7
40-120
6.88
24
46.9
5.05 ug/L
50.51
ND
92.9
21-196
33.8
24
39.9
5.05 ug/L
50.51
ND
79.0
35-180
40.4
24
17.0
5.05 ug/L
50.51
ND
33.6
17-127
8.43
24
45.1
5.05 ug/L
50.51
ND
89.2
43-230
39.3
24
51.1
5.05 ug/L
50.51
ND
101
79-139
32.4
24
19.2
5.05 ug/L
50.51
ND
37.9
14-176
69.5
24
17.4
2.02 ug/L
50.51
ND
34.5
5-120
33.6
24
47.5
5.05 ug/L
50.51
ND
94.0
52-120
29.9
24
25.8
ug/L
50.51
51.1
60-140
15.1
ug/L
50.51
29.8
60-140
32.4
ug/L
50.51
64.1
60-140
31.3
ug/L
50.51
62.0
60-140
37.5
ug/L
50.51
74.3
60-140
46.4
ug/L
50.51
92.0
60-140
45.8
ug/L
50.51
90.7
60-140
Source: 2309043-01
36.5
5.62 ug/L
56.18
ND
65.0
47-145
4.83
24
36.3
5.62 ug/L
56.18
ND
64.7
33-145
4.09
24
48.1
5.62 ug/L
56.18
ND
85.7
27-133
5.77
24
49.1
5.62 ug/L
56.18
ND
87.4
33-143
7.44
24
49.8
5.62 ug/L
56.18
ND
88.6
17-163
1.05
24
49.6
5.62 ug/L
56.18
ND
88.3
24-159
4.74
24
49.1
5.62 ug/L
56.18
ND
87.4
35-219
4.27
24
50.6
5.62 ug/L
56.18
ND
90.1
11-162
3.34
24
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 27 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike Level
Source Result
%REC
%REC Limits
Batch B310011
Matrix Spike Dup (B310011-MSD2) Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene
Source: 2309043-01
49.3
5.62 ug/L
49.2
5.62 ug/L
46.1
5.62 ug/L
50.3
5.62 ug/L
50.2
5.62 ug/L
25.6
5.62 ug/L
50.1
5.62 ug/L
22.6
5.62 ug/L
37.8
5.62 ug/L
33.1
5.62 ug/L
25.7
5.62 ug/L
56.6
5.62 ug/L
42.1
5.62 ug/L
22.3
5.62 ug/L
32.6
5.62 ug/L
24.0
5.62 ug/L
8.39
5.62 ug/L
41.1
5.62 ug/L
44.0
5.62 ug/L
51.7
5.62 ug/L
41.6
5.62 ug/L
50.2
5.62 ug/L
20.4
5.62 ug/L
33.1
5.62 ug/L
25.2
5.62 ug/L
27.6
5.62 ug/L
59.2
5.62 ug/L
47.6
5.62 ug/L
52.4
5.62 ug/L
51.2
5.62 ug/L
31.7
5.62 ug/L
51.7
5.62 ug/L
59.8
5.62 ug/L
50.5
5.62 ug/L
21.0
2.25 ug/L
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
87.8
17-168
87.5
33-227
82.0
26-137
89.6
59-121
89.3
39-171
45.6
21-133
89.3
54-120
40.3
44-142
67.2
37-144
58.9
39-135
45.8
32-120
101
39-139
74.9
50-158
39.6
21-191
58.0
60-120
42.7
23-134
14.9
29-182
73.2
38-262
78.2
17-181
92.1
53-127
74.0
22-147
89.3
25-158
36.4
9-132
59.0
33-184
44.9
12-158
49.2
36-166
105
8-158
84.7
38-152
93.2
61-106
91.2
31-114
56.5
28-120
92.1
1-120
106
4-146
89.8
35-152
37.3
24-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD
7.90 3.50 2.59 8.91 7.43 11.4 6.52 14.7 0.915 3.24 22.2 10.8 1.57 0.363 6.96 16.7 7.33 0.159 7.28 8.36 0.331 9.37 0.0299 3.68 19.1 13.6 8.97 1.05 7.65 9.20 4.93 3.38 9.01 6.56 18.3
RPD Limit
24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24
Page 28 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 NVOA GCMS - Quality Control
Analyte
Batch B310011
Matrix Spike Dup (B310011-MSD2) Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309043-01
17.7
5.62 ug/L
56.18
ND
31.6
15-76
20.5
24
15.6
5.62 ug/L
56.18
ND
27.8
40-120
29.9
24
39.0
5.62 ug/L
56.18
ND
69.4
21-196
1.95
24
29.4
5.62 ug/L
56.18
ND
52.4
35-180
11.9
24
16.4
5.62 ug/L
56.18
ND
29.2
17-127
22.1
24
35.7
5.62 ug/L
56.18
ND
63.5
43-230
3.35
24
52.3
5.62 ug/L
56.18
ND
93.0
79-139
8.22
24
25.2
5.62 ug/L
56.18
ND
44.9
14-176
9.12
24
14.7
2.25 ug/L
56.18
ND
26.1
5-120
5.69
24
45.2
5.62 ug/L
56.18
ND
80.5
52-120
2.29
24
21.0
ug/L
56.18
37.4
60-140
13.0
ug/L
56.18
23.2
60-140
24.9
ug/L
56.18
44.3
60-140
24.4
ug/L
56.18
43.4
60-140
34.2
ug/L
56.18
60.9
60-140
45.3
ug/L
56.18
80.6
60-140
43.9
ug/L
56.18
78.1
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 29 of 42
Analyte
Batch B310062 Blank (B310062-BLK1)
Oil & Grease
LCS (B310062-BS1) Oil & Grease
LCS Dup (B310062-BSD1) Oil & Grease
Matrix Spike (B310062-MS1) Oil & Grease
Matrix Spike (B310062-MS2) Oil & Grease
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 GC - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 mg/L
37.1
5.00 mg/L
40.00
92.8
78-114
35.4
5.00 mg/L
40.00
88.5
78-114
4.69
20
Source: 2309020-03
47.0
6.17 mg/L
49.38
ND
95.2
78-114
Source: 2309043-03
44.0
5.81 mg/L
46.51
3.20
87.7
78-114
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 30 of 42
Analyte
Batch B309146
Blank (B309146-BLK1) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
LCS (B309146-BS1) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
LCS Dup (B309146-BSD1) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Metals ICP - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
8.00 ug/L
--- U
100 ug/L
--- U
3.00 ug/L
--- U
5.00 ug/L
--- U
10.0 ug/L
--- U
8.00 ug/L
--- U
20.0 ug/L
--- U
20.0 ug/L
--- U
5.00 ug/L
--- U
20.0 ug/L
199
8.00 ug/L
200.0
202
100 ug/L
200.0
198
3.00 ug/L
200.0
199
5.00 ug/L
200.0
197
10.0 ug/L
200.0
201
8.00 ug/L
200.0
200
20.0 ug/L
200.0
199
20.0 ug/L
200.0
200
5.00 ug/L
200.0
204
20.0 ug/L
200.0
198
8.00 ug/L
200.0
202
100 ug/L
200.0
198
3.00 ug/L
200.0
199
5.00 ug/L
200.0
196
10.0 ug/L
200.0
201
8.00 ug/L
200.0
200
20.0 ug/L
200.0
199
20.0 ug/L
200.0
200
5.00 ug/L
200.0
204
20.0 ug/L
200.0
99.7
85-115
101
85-115
99.2
85-115
99.7
85-115
98.3
85-115
100
85-115
99.9
85-115
99.4
85-115
99.8
85-115
102
85-115
99.2
85-115
0.503
20
101
85-115 0.0397
20
99.2
85-115 0.0151
20
99.6
85-115 0.0903
20
98.2
85-115 0.0763
20
101
85-115
0.214
20
100
85-115 0.0550
20
99.4
85-115 0.0855
20
99.9
85-115 0.0952
20
102
85-115 0.0734
20
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 31 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Metals ICP - Quality Control
Analyte
Batch B309146
Matrix Spike (B309146-MS1) Cadmium Chromium Lead Zinc
Matrix Spike (B309146-MS2) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
Matrix Spike Dup (B309146-MSD1) Cadmium Chromium Lead Zinc
Matrix Spike Dup (B309146-MSD2) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309020-01
201
3.00 ug/L
200
5.00 ug/L
295
8.00 ug/L
302
20.0 ug/L
Source: 2309043-08
205
8.00 ug/L
340
100 ug/L
195
3.00 ug/L
201
5.00 ug/L
277
10.0 ug/L
198
8.00 ug/L
194
20.0 ug/L
201
20.0 ug/L
200
5.00 ug/L
219
20.0 ug/L
Source: 2309020-01
201
15.0 ug/L
195
25.0 ug/L
294
40.0 ug/L
299
100 ug/L
Source: 2309043-08
204
40.0 ug/L
337
500 ug/L
197
15.0 ug/L
199
25.0 ug/L
271
50.0 ug/L
198
40.0 ug/L
196
100 ug/L
205
100 ug/L
197
25.0 ug/L
220
100 ug/L
200.0 200.0 200.0 200.0
0.750 ND 92.6 90.3
100
80-120
100
80-120
101
80-120
106
80-120
200.0
ND
200.0
142
200.0
ND
200.0
2.34
200.0
78.8
200.0
ND
200.0
2.83
200.0
ND
200.0
ND
200.0
19.7
103
80-120
98.9
80-120
97.5
80-120
99.2
80-120
99.2
80-120
98.8
80-120
95.8
80-120
101
80-120
100
80-120
99.7
80-120
200.0
ND
100
80-120 0.0796
10
200.0
ND
97.6
80-120
2.44
10
200.0
92.6
101
80-120
0.258
10
200.0
90.3
104
80-120
1.15
10
200.0
ND
102
80-120
0.773
10
200.0
142
97.6
80-120
0.753
10
200.0
ND
98.4
80-120
1.01
10
200.0
ND
99.6
80-120
0.740
10
200.0
78.8
96.2
80-120
2.21
10
200.0
ND
98.9
80-120 0.0708
10
200.0
ND
98.0
80-120
0.856
10
200.0
ND
103
80-120
2.05
10
200.0
ND
98.5
80-120
1.72
10
200.0
19.7
100
80-120
0.442
10
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 32 of 42
Analyte
Batch B310050 Blank (B310050-BLK1)
Mercury
LCS (B310050-BS1) Mercury
LCS Dup (B310050-BSD1) Mercury
Matrix Spike (B310050-MS1) Mercury
Matrix Spike (B310050-MS2) Mercury
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Mercury CVAA - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
0.050 ug/L
0.965
0.050 ug/L
1.000
96.5
85-115
0.962
0.050 ug/L
1.000
96.2
85-115
0.311
20
Source: 2309020-01
0.980
0.050 ug/L
1.000
ND
98.0
80-120
Source: 2309043-08
0.978
0.050 ug/L
1.000
ND
97.8
80-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 33 of 42
Analyte
Batch B309132 Blank (B309132-BLK1)
Chromium, Hexavalent
Blank (B309132-BLK2) Chromium, Hexavalent
LCS (B309132-BS1) Chromium, Hexavalent
LCS (B309132-BS2) Chromium, Hexavalent
LCS Dup (B309132-BSD1) Chromium, Hexavalent
LCS Dup (B309132-BSD2) Chromium, Hexavalent
Matrix Spike (B309132-MS1) Chromium, Hexavalent
Batch B309134 Blank (B309134-BLK1)
Nitrate [As N] Nitrite [As N]
Blank (B309134-BLK2) Nitrate [As N] Nitrite [As N]
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
10.0 ug/L
--- U
10.0 ug/L
597
10.0 ug/L
585.0
102
85-115
617
10.0 ug/L
585.0
105
85-115
616
10.0 ug/L
585.0
105
85-115
3
20
600
10.0 ug/L
585.0
103
85-115
3
20
Source: 2309043-07
209
10.0 ug/L
200.0
5.03
102
80-120
--- U
0.0500 mg/L
--- U
0.0250 mg/L
--- U
0.0500 mg/L
--- U
0.0250 mg/L
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 34 of 42
Analyte
Batch B309134 LCS (B309134-BS1)
Nitrite [As N] Nitrate [As N]
LCS Dup (B309134-BSD1) Nitrite [As N] Nitrate [As N]
Matrix Spike (B309134-MS1) Nitrate [As N] Nitrite [As N]
Batch B309138 Blank (B309138-BLK1)
Phenolics, Total
Blank (B309138-BLK2) Phenolics, Total
LCS (B309138-BS1) Phenolics, Total
LCS (B309138-BS2) Phenolics, Total
LCS Dup (B309138-BSD1) Phenolics, Total
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
0.461 17.1
0.0250 0.500
mg/L mg/L
0.4560 16.50
101
90-110
104
90-110
0.461 17.2
0.0250 0.500
mg/L mg/L
0.4560 16.50
101
90-110
0
20
104
90-110
0.6
20
Source: 2309043-08
4.36
0.500 mg/L
0.2000
4.20
80
90-110
0.226
0.0250 mg/L
0.2000 0.0302
98
90-110
--- U
20.0 ug/L
--- U
20.0 ug/L
743
20.0 ug/L
784.0
743
20.0 ug/L
784.0
726
20.0 ug/L
784.0
95
90-110
95
90-110
93
90-110
2
20
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 35 of 42
Analyte
Batch B309138 LCS Dup (B309138-BSD2)
Phenolics, Total
Matrix Spike (B309138-MS1) Phenolics, Total
Batch B309140 Blank (B309140-BLK1)
Chemical Oxygen Demand
Blank (B309140-BLK2) Chemical Oxygen Demand
LCS (B309140-BS1) Chemical Oxygen Demand
LCS Dup (B309140-BSD1) Chemical Oxygen Demand
Matrix Spike (B309140-MS1) Chemical Oxygen Demand
Batch B309141 Blank (B309141-BLK1)
Biochemical Oxygen Demand
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
775
20.0 ug/L
784.0
99
90-110
4
20
Source: 2309043-01
482
20.0 ug/L
500.0
29.5
90
90-110
--- U
20.0 mg/L
--- U
20.0 mg/L
140
20.0 mg/L
155.2
90
90-110
143
20.0 mg/L
155.2
92
90-110
2
20
Source: 2309043-08
124
40.0 mg/L
100.0
35.4
88
90-110
--- U
2.00 mg/L
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 36 of 42
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Sanitary - Quality Control
Analyte
Batch B309141 LCS (B309141-BS1)
Biochemical Oxygen Demand
LCS (B309141-BS2) Biochemical Oxygen Demand
LCS (B309141-BS3) Biochemical Oxygen Demand
Duplicate (B309141-DUP1) Biochemical Oxygen Demand
Matrix Spike (B309141-MS1) Biochemical Oxygen Demand
Matrix Spike Dup (B309141-MSD1) Biochemical Oxygen Demand
Batch B310002 Blank (B310002-BLK1)
Fluoride
Blank (B310002-BLK2) Fluoride
LCS (B310002-BS1) Fluoride
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
193
2.00 mg/L
198.0
97.5 84.6-115.4
190
2.00 mg/L
198.0
96.0 84.6-115.4
198
2.00 mg/L
198.0
100 84.6-115.4
Source: 2309043-08
1.52
2.00 mg/L
2.36
43.3
25
Source: 2309043-08
35.3
2.00 mg/L
31.68
2.36
104
75-125
Source: 2309043-08
27.6
2.00 mg/L
23.76
2.36
106
75-125
24.5
200
--- U
0.0500 mg/L
--- U
0.0500 mg/L
4.46
0.0500 mg/L
4.860
92
90-110
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 37 of 42
Analyte
Batch B310002 LCS Dup (B310002-BSD1)
Fluoride
Matrix Spike (B310002-MS1) Fluoride
Matrix Spike (B310002-MS2) Fluoride
Batch B310003 Blank (B310003-BLK1)
Nitrogen, Total Kjeldahl
Blank (B310003-BLK2) Nitrogen, Total Kjeldahl
LCS (B310003-BS1) Nitrogen, Total Kjeldahl
LCS Dup (B310003-BSD1) Nitrogen, Total Kjeldahl
Matrix Spike (B310003-MS1) Nitrogen, Total Kjeldahl
Batch B310004 Blank (B310004-BLK1)
Chloride
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
4.50
0.0500 mg/L
4.860
93
90-110
0.9
20
Source: 2309020-01
40.5
0.500 mg/L
2.000
40.0
25
90-110
Source: 2309043-08
2.38
0.0500 mg/L
2.000
0.550
92
90-110
--- U
0.100 mg/L
--- U
0.100 mg/L
12.7
0.200 mg/L
12.40
102
90-110
12.8
0.200 mg/L
12.40
103
90-110
0.8
20
Source: 2309043-08
5.12
0.100 mg/L
4.000
0.568
114
90-110
--- U
1.00 mg/L
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 38 of 42
Analyte
Batch B310004 Blank (B310004-BLK2)
Chloride
LCS (B310004-BS1) Chloride
LCS Dup (B310004-BSD1) Chloride
Matrix Spike (B310004-MS1) Chloride
Batch B310010 Blank (B310010-BLK1)
Cyanide, Total
Blank (B310010-BLK2) Cyanide, Total
LCS (B310010-BS1) Cyanide, Total
LCS Dup (B310010-BSD1) Cyanide, Total
Matrix Spike (B310010-MS1) Cyanide, Total
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
1.00 mg/L
96.3
5.00 mg/L
91.20
106
90-110
97.6
5.00 mg/L
91.20
107
90-110
1
20
Source: 2309043-08
53.1
10.0 mg/L
20.00
38.6
72
90-110
--- U
10.0 ug/L
--- U
10.0 ug/L
721
10.0 ug/L
726.0
99
90-110
698
10.0 ug/L
726.0
96
90-110
3
20
Source: 2309043-01
361
10.0 ug/L
500.0
8.39
71
90-110
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 39 of 42
Analyte
Batch B310013 Blank (B310013-BLK1)
Residue, Filterable
Blank (B310013-BLK2) Residue, Filterable
LCS (B310013-BS1) Residue, Filterable
LCS Dup (B310013-BSD1) Residue, Filterable
Duplicate (B310013-DUP1) Residue, Filterable
Batch B310014 Blank (B310014-BLK1)
Residue, Non-Filterable
Blank (B310014-BLK2) Residue, Non-Filterable
LCS (B310014-BS1) Residue, Non-Filterable
LCS Dup (B310014-BSD1) Residue, Non-Filterable
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
10.0 mg/L
--- U
10.0 mg/L
255
mg/L
279.0
91.4
85-115
257
mg/L
279.0
92.1
85-115
0.781
20
Source: 2309043-08
380
10.0 mg/L
377
0.793
20
--- U
10.0 mg/L
--- U
10.0 mg/L
87.0
mg/L
96.70
96.0
mg/L
96.70
90.0
85-115
99.3
85-115
9.84
20
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 40 of 42
Analyte
Batch B310014 Duplicate (B310014-DUP1)
Residue, Non-Filterable
Batch B310022 Blank (B310022-BLK1)
Ammonia [As N]
Blank (B310022-BLK2) Ammonia [As N]
LCS (B310022-BS1) Ammonia [As N]
LCS Dup (B310022-BSD1) Ammonia [As N]
Matrix Spike (B310022-MS1) Ammonia [As N]
Batch B310048 Blank (B310048-BLK1)
Phosphorus
Blank (B310048-BLK2) Phosphorus
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309043-08
3.00
10.0 mg/L
ND
20
--- U
0.100 mg/L
--- U
0.100 mg/L
7.52
0.100 mg/L
8.340
90
90-110
7.82
0.100 mg/L
8.340
94
90-110
4
20
Source: 2309043-08
2.48
0.100 mg/L
5.000
0.0434
49
90-110
--- U
0.0500 mg/L
--- U
0.0500 mg/L
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 41 of 42
Analyte
Batch B310048 LCS (B310048-BS1)
Phosphorus
LCS Dup (B310048-BSD1) Phosphorus
Matrix Spike (B310048-MS1) Phosphorus
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Corning Inc - 2309043
Project Number: 2309043 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
8.75
0.250 mg/L
8.450
104
90-110
8.75
0.250 mg/L
8.450
104
90-110
0
20
Source: 2309043-08
2.91
0.500 mg/L
1.000
1.23
168
90-110
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 42 of 42
Decision Unit Code
~_ _ ~~_--==::- _._-~_' c
US EPA REGION 2 LABORATORY
CHAIN OF CUSTODYI FIELD DATA FORM
_
_
~ ._ "'- _.=-=-
Page __ of ~ pages
.... ~
RCRA D
oo
z
;ri '*"
;tI 0
RCRA ENF D
D307
NPDES D
8304
SDWA D
C215
s: DESCRIPTION & INSTRUCTIONS CHECK IF ESTIMATED CONCENTRATIONS,
~ SPLIT
~ SAMrLE
LIMITS, ~------------------------------------~
AM D
8224
CM D
A305
INCLUDING LOCATION, SPECIAL REPORTING
-
PROJECT LEADER ,-,
PROGRAM RESULTS CODE
TSCA D
L306
OD D
8253
FIFRA
I I Preservative I +(circle)
vtd'"e;11
_
D
CRIMINAL ENF D
Collection Time (24hr clock)
11111111111111 Begin I End
I
Collection Date -
mm/dd/yy
g~_.:_::.:: ::..-:.:.:-J . : ~........... ~_...
+
r
A=aqueous 8=aqueous C=soil D=sediment ,t::=sludge
,
alnx:
(chlorinated)
F=multiphasic G=solvent H=biota I=oil J=other
_
Y l:] N D
Relinquis~d By: Relinquished By: Relinquished By:
j7~
( . II b
"'1\
Person Assuming Responsibi!ity for Sample(s):
Received By:
Preservative Added & Checked
O=ice
7=FAS
1=H2S04 pH<2
8=ZnAc
2=HN03 pH<2
9=NaOH pH>12
3=HCI pH<2
10=NH4CI
4=Na2S203
5=NaOH pH>9
6=Ascorbic Acid
It, :1/0
1\MSftd 10/25/2004
U~ I::PA KI::GIUN 2 LABORATORY
CHAIN OF CUSTODYI FIELD DATA FORM
Page __ of _ pages
SURVEY NAME & LOCALITY - _. , \
.r ~
. _
PROGRAM: SF 0
Decision Unit Code
RCRA 0
SIITE 10
RCRA ENF 0~DES
D307
B304
d
_
v,
I
OPERABLE UNIT
_
SDWA 0
C215
AM 0
B224
CM 0
A305
DESCRIPTION & INSTRUCTIONS
~ CHECK IF ESTIMATED CONCENTRATIONS,
-t SPLIT
LIMITS
~ SAMPLE ~----'----------------------------------~
INCLUDING LOCATION, SPECIAL REPORTING
PROJECT LEADER!
,~ . _
PROGRAM RESULTS CODE
_
TSCA 0
L306
OD 0
B253
FIFRA 0
CRIMINAL ENF 0
I I r=--::-;--,
Preservative
I
(circle)
Collection Time
(24hr clock)
11/1/1/11/1/1/
Begin:
End
Collection Date
mm/dd/yy
A=aqueous B=aqueous C=soil D=sediment ,E=sludge
alnx:
(chlorinated)
F=multiphasic G=solvent H=biota I=oil J=other
>
YON
0
Relinquisbed By: Relinquished By: Relinquished By:
s
Person 1ssumtg Responsibility for Sample(s): Re Received By:
Preservative Added & Checked
O=ice
7=FAS
1=H2S04 pH<2
8=ZnAc
2=HN03 pH<2
9=NaOH pH>12
3=HCI pH<2
10=NH4CI
4=Na2S203
5=NaOH pH>9
6=Ascorbic Acid
revised 10/25/2004
