Document MBmV73ZKY9MQ6pYzXQX8kxxj

PRELIMINARY SCOPE REPORT CEA 2518 AROCLOR DISTILLATION NEWPORT PLANT - SOUTH WALES Prepared by: A. J. Heinze ' Date: July 15, 1971 osw 147915 STLCOPCB4039525 TABLE OF CONTENTS I. PROJECT SCOPE SUMMARY A. Title B. Objectives C. Tone D. Design Capacity E. Project Status F. Description ofFacilities II. PROCESS TECHNOLOGY A. Process Description B. Status of process C. Raw Materials D. Products and By-Products E. Yields and Usages F. Manning Requirements G. Waste Streams H. personnel. Property& Public Hazards III. BATTERY LIMITS FACILITIES A. Design Capacity B. Flexibility Requirements C. Future Expansion D. Physical Appearance E. Storage and Shipping Requirements F. Description of Facilities. IV. EX-BATTERY LIMITS FACILITIES A. Utilities Summary B. Description of Facilities V. EXPENSE ITEMS VI. FIELD CONDITIONS APPENDICES A. Intermediate & Product Specifications B. Equipment Information summary sheets C. Utility Summary & Requirement sheets D. Process Flow Diagrams and Material Balance E. Instrument List F. Plot Plan and Preliminary Equipment Layout G. Scope of Work Page 1 1 1 1 1 1 2 3 3 4 5 .5 5 6 6 7 8 8 12 12 12 12 13 14 14 14 DSW 147916 STLCOPCB4039526 I * PROJECT SCOPE SUMMARY A. Title Project title: Product name: Division: Plant: CEA Number: Expected Cost: Expected completion: Aroclors Distillation - Newport Aroclor 1016; MCS-1109 Organic Chemicals Newport, Mon. Great Britian 2518 December, 1972 B. Objectives Recent pollution problems associated with polychlorinated biphenyls (PCBs) have created an urgent need for PCBs with minimum amounts of the more slowly degradable homo logs. The primary objective of this project is to pro vide the necessary manufacturing facilities to produce such an improved biodegradable product (Aroclor-1016) at a volume consistent with current and foreseeable sales requirements, A secondary objective is to provide sufficient capacity in the new column system to manufacture monochlorobiphenyl (MCS-1109) on a blocked out basis. C. Tone Due to the ecological nature of this project, time is of the essence in completing the work and starting opera tion as soon as reasonably possible. Although no over time engineering or construction work is planned, the overall design and construction schedules will be tight and will be carefully followed and expedited as required to meet the expected completion date. D. Design Capacity The design capacity of the new column system at approxi mately 90% O.S.T. is as follows: Aroclor 1016 MCS-1109 Total Products M Lb/Year 15.0 0.8 15.8 E. Project Status All pertinent research and design information are avail able for Aroclor 1016 design work. Initial research work has been done on the distillation of Aroclor 1115 for the production of MCS-1109. Certain process variables relating to the manufacture of 1109 still need to be explored. DSW 147917 STLCOPCB4039527 E. Project Status (cont'd) Based on the research work done to date on both Aroclor 1016 and MCS-1109, process risks appear to be minimal. Also, the same manufacturing process currently used at the Newport plant will be employed to produce the Aroclor 1142 feedstock for Aroclor 1016. F, Description of Facilities The project provides for the installation of facilities to produce Aroclor 1016 and MCS-1109 on a blocked basis. These new facilities include a 30 tray distillation column and auxiliaries and a new crude Aroclor inter mediate storage tank. Existing raw material and finished goods tankage will be utilized. The new column and auxiliaries will be located west of existing Aroclor building 35 at the Newport plant. A new small control panel for the column panel-mounted instruments will be installed in the existing Aroclors department control room. New starters for motors will be incorporated into the existing Aroclors motor control center. The project utility requirements will be supplied from existing Newport plant utilities facilities. DSW 147918 STLCOPCB4039528 II. PROCESS TECHNOLOGY A. Process Description X. Aroclor 1016 Aroclor 1142 (column feed) will be produced via the existing manufacturing process in the three (3) existing batch chlorinators and batch blow (aeration) tanks. Recovered HCl from the chlorination opera tion is sent to the muriatic acid department, as presently done, The air-blown crude Aroclor 1142 is dropped into a new 15,000 imp. gallon storage tank. The new column system, which will be operated semicontinuously, will be fed from the new crude Aroclors storage tank. An initial 1142 charge, including lime, will be pumped into the column still pot. Vapors are then generated by pumping the still pot liquid through the oil-fired reboiler and the column is put on total reflux. After temperatures have lined out, distillate product is cut forward and pumped through the existing Porocel column to storage. As distillate product is withdrawn, an equal volume of crude Aroclor 1142 enters the still pot on level control. At the end of a column run, the still pot contents are "boiled down" to an end point tempera ture of about 300C and the pot residue is trans ferred to the residue surge tank. Residue from the residue surge tank is pumped to the existing still (1207) where "high boilers" are taken overhead and Montar is removed. This distillate high boiler stream is then batch chlorinated to Aroclor 1154 in the existing chlorinators. The Aroclor 1154 is then distilled in the existing 1207 still, refined in the existing earth treatment facilities and then pumped to storage. 2, Monochlorobiphenyl (MCS-1109) Aroclor 1115 (column feed) will be produced in the existing three (3) batch chlorinators. The crude 1115 is then Nj-blown in the chlorinator vessels to remove the majority of dissolved HCl. The recovered HCl from this chlorination operation is passed through an Aroclor 1242 (or 1016) scrubber to recover biphenyl (and the lower PCBs) prior to transfer to the muriatic department. The blown Aroclor 1115 is then pumped into the new 15,000 imp. gallon crude storage tank. DSW 147919 STLCOPCB4039529 2. Monochlorobiphenyl (MCS-1109) (cont'd) The new column system, which is operated batchwise on this product, will be charged from this new crude Aroclor storage tank. An initial Aroclor 1115 charge, including lime, is pumped into the column still pot. Column vapors are then generated by pump ing the still pot liquid through the oil-fired re boiler and the column is put on total reflux. After temperatures have lined out, a biphenyl-rich forecut is taken and directed back to the biphenyl storage tank. After the forecut fraction has been removed, the product is cut forward to storage. A column batch run will consist of approximately 4,000 imp. gallons of MCS-1109 product. At the end of a column run, the still pot contents are transferred to the residue surge tank. The residue from this operation is further processed into Aroclor 1254 as described above under Aroclor 1016. The following references give the process details for the Aroclor 1016 and MCS-1109 products: a. "Tentative Process on MCS-1016", Report No. P-1579 dated 7 October 1970 by J. E. Silver. b. "Tentative process on MCS-1109". (Report number and date to be transmitted later.) B. Status of Process 1. Aroclor 1016 The design of the new distillation column facilities proposed for the Newport plant is essentially identi cal to the WGK Aroclors column system. The only difference between the two locations is the method of crude Aroclor 1142 production. Aroclor 1142 is produced continuously (both chlorination and air blowing) at WGK vs. batchwise 1142 production at Newport. 2. MCS-1109 The process to be used at Newport for MCS-1109 pro duction differs from that at WGK in the chlorinated level of the column feedstock. MCS-1109 is produced from a 5% chlorinated biphenyl at WGK using a semicontinuou s/batch column operation. At Newport, MCS-1109 will be produced from a 15% chlorinated biphenyl using a batch column operation. This feed stock change from Aroclor 1105 to 1115 was made for Newport due to the impractical nature of making 1105 batchwise on a plant production scale. 4. DSW 147920 STLCOPCB4039530 Q. Raw Materials The basic raw materials (biphenyl, chlorine and ferric chloride) used to produce Aroclor 1142 and 1115 will be the same as currently used. The Aroclor 1142 currently produced in the batch chlorinators will be used as feedstock for Aroclor 1016. Aroclor 1115 is used as feedstock for MCS1109 production. Specifications for Aroclor 1115 are included in Appendix A of this report. Aroclor 1142 and 1115 will be stored in a new 15,000 imp. gallon storage tank which will serve as surge volume between the chlorinators and column system. D, products and By-Products On completion of this project, the Newport Aroclor department will be producing four Aroclor products. These are (1) Aroclor 1016, (2) Aroclor 1242 for transformer blends, (3) Aroclor 1254 and (4) MCS1109. Aroclor 1248 and 1260 are forecasted to phase out of the market at the end of 1973 and 1971, respectively. The Aroclor 1016 and MCS-1109 product specifications are included in Appendix A. The product specifica tions for Aroclor 1242 and 1254 will remain the same as currently used. Shipping of all the Aroclor products, along with MCS-1109, will be via road tanker as per current practice. E. Yields and Usages Crude Aroclor and lime usages for Aroclor 1016 and MCS-1109 production are as follows: Material Usage Lbs/100 Lbs Aroclor 1016 MCS-1109 Aroclor 1115 Aroclor 1142 Lime 122.0 0.13 220.0 0.35 5. DSW 147921 STLCOPCB4039531 E. Yields and Usages (cont'd) For Aroclor 10X6, the remaining 22 lbs of Aroclor 1142 feed is the still pot residue. This residue is further distilled in the existing Aroclors department still where about 98% of the residue is recovered. The recovered residue distillate is further chlorinated to Aroclor 1254 product. For MCS-1109, of the remaining 120 lbs of Aroclor 1115 feed, 47.8 lbs represents recycle biphenyl column forecut and 72.2 lbs are the still pot residue. This residue is also further distilled in the existing S.T.O. still where about 98% of the residue is recovered. This recovered residue distillate is further chlorinated to the Aroclor 1254 product. F. Manning Requirements There will be no change in the Aroclors department manning requirements as a result of this project. The new column system will be designed such that the process can be monitored from the control room and many of the operations can be executed remotely from the control painel. Operator attention in the department will be required mainly for making up lime slurry for each column run. G. Waste Streams The major potential waste stream which would require disposal (incineration) is excess residue or high boilers from the column operation. One of the basic economic premises of this project is that all the column high boilers (from both the Aroclor 1016 and MCS-1109 operations) will be further chlorinated to Aroclor 1254. With the current Aroclor 1016 sales forecast and a modest MCS-1109 sales requirement (0.5 to 0.8H lbs/yr), all the high boilers would be consumed in making the forecasted volume of Aroclor 1254. However, a product requirement imbalance could occur such that the high boilers1 production would exceed the Aroclor 1254 requirements. Should this situation materialize, the excess high boilers would be sent to Purle Bros, for incineration. The Montar (1207 still bottoms) waste volume should be the same as present. We anticipate no change in the disposal of this waste as a result of this pro ject. 6. DSW 147922 STLCOPCB4039532 G. Waste Streams (cont'd) The Aroclor atmospheric emission from the new column jet ejectors Bhould be in the order of less than 1 lb/day. H. Personnel, property & Public Hazards The project will not create any new hazards in the Newport Aroclors department compared to the present manufacturing process. The only potential hazard associated with this project is personnel safety in processing and transporting (pumping) Aroclor at high temperatures. This type of operation is currently done in the present Aroclors department. 7. DSW 147923 STLCOPCB4039533 XII. BATTERY LIMITS FACILITIES A. Design Capacity 1. New Column system The design capacity of the new column system at approximately 90% O.S.T. (7,900 operating hours/year) is as follows: Aroclor 1016 . MCS-1109 ; Total Products M Lbs/Year 15.0 0.8 15.8 For Aroclor 1016, the anticipated column cycle time (EX chlorinator hold-up time) is 72.5 hours/run, broken down as follows: Hours/Run a. Start charging Aroclor 1142 to the still pot 0. b. Start the still pot circulating pump 0.25 c. Heat still pot contents to the initial boiling point 0.85 d. Establish trays liquid inventory .e Line out column temperature 0.40 0.6 f. Distill @ 3:1 reflux ratio 27.8 g* Distill 5:1 reflux ratio (including boil down) 41.6 h. Cut burner and continue circu lating .i Pump out residue and turnaround 0.25 0.75 Total Aroclor 1016 time 72.5 The actual total column cycle time will be approx imately 100 hours/run which includes about 30 hours for crude Aroclor 1142 volume accumulation from the chlorinators. To minimize the Aroclor time-at-temperature in the still pot/column system, approximately 7,500 imp. gallons of Aroclor 1142 will be accumulated in the crude storage tank prior to a column run. . DSW 147924 8 STLCOPCB4039534 1. New column System (cont'd) I For MCS-1109, the anticipated column cycle time (EX chlorinator hold-up time) is 22.5 hours/batch, broken down as follows: a. Start charging Aroclor 1115 to the still pot Hours/Batch 0. b. Start the still pot circu lating pump 0.25 c. Heat the still pot content to the initial boiling point d. Establish trays liquid inven tory 2.0 0.4 e. Line out column temperature 0.6 f. Take off forecut @ 4:1 reflux ratio g. Take off product @ 8:1 reflux ratio h. Cut burner and continue circu lating 2.55 15.7 0.25 i. Pump out residue 0,75 Total MCS-1109 time 22.5 The actual total column cycle time will be approx imately 37 hours/batch which includes about 14.5 hours for Aroclor 1115 volume accumulation from the chlorinator. 2. Crude Aroclor Production The nominal capacity of the existing three batch chlorinators (and blow tanks) is 20H lbs/yr. This crude production capacity is adequate through 1975 based on current sales forecasts for all Aroclor products. Chlorinator occupancy calculations based on current sales forecasts are shown on Table 1. chlorinator capacities when producing Aroclors 1115, 1142 and 1154 are given in Table 2. 9. DSW 147925 STLCOPCB4039535 AROCLOR PRODUCT MCS-1109 1016 1242 1254A(1) 1254B(Z> AROCLOR CRUDE 1115 1142 1142 ll$4A(l> 11548(2) 4 CRUDE 4 PRODUCT 2.2 1.22 1.03 1.03 1.03 CRUDE RATS 1.87 1.85 1.85 4.12 2.10 PR0DlCTf4> PROD. SALES. H# MCS-1109 1016 1242 1254A<1) 1254B(2) 0.5 (3) 7.6 1.4 3.3 0.2 Totals * 13.0 Available Turnaround Time 1973 REQUIRED CSVBE. 5 1.1 9.27 1.44 3.40 0.21 15.42 CHIORINAIDR MONTHS 0.6 5.0 0.8 0.8 oa 7.3 4.7 TABLE 1 BgWBM_CT[LORPWrTO OCCUPANCY PROD. SALES. 0.65 <3) 9.7 1.5 2.9 0.2 14.95 1974 REQUIRED CRUDE. 1.43 11.33 1.55 3.00 0.21 18.02 CKLORINAm MONTHS 0.8 6.4 0.8 0.7 0*1 8.8 3.2 PROD. SALES. 0.8 (3) 10.1 1.6 3.2 .-0^ 15.9 1975 REQUIRED CRUDE. R* 1.76 12.32 1.65 3.30 0-2t 19.24 CHLORtNATOR MONTHS L.O 6.7 0.9 0.80.1 9.5 2.5 Notes: (1) Aroclor 1154 Bade by chlorination of Aroclor 1016 residue. , (2) Aroclor 1154 nad by chlorination of MCS-1109.residue. (3) Estimated MCS-1109 sales voluaes. ' 10. DSW 1 4 7 9 2 6 STLCOPCB4039536 o 1 DSW 1 4 7 9 2 7 TABLE 2 NEWPORT CHLORINATORS' CAPACITY Cycle Time, Hrs- Charge Biphenyl (Residue) Chlorinate " ~ Circulate and Sample Nitrogen Blow Pump Out and Turnaround Total Cycle Time 1115 1142 1154(1) 1154(2) 0.30 0.25 0.5 0.35 4.4 0.30 6.75 0.25 0.35 7.65 (0.40) 3.25 ` 0.25 0.4 4.3 (0.40) 7.35 0.25 0.4 8.4 Batch Weight Per Chlorinator, Lbs. 4,200 7,200 9,000 9,000 Total Crude Aroclor Rate, M Lbs/Month 1.87 1.85 4.12 2.10 Notes: 1 2 Made from Aroclor 1016 residue. Made from MCS-1109 residue. 11. STLCOPCB4039537 B. Flexibility Requirements The new column system will be designed to process the entire capacity of the existing three batch chlorinators. Prom current sales forecasts, the 1975 column requirements are about 70% of the column design capacity. The proposed column design capacity will allow for future growth of Aroclor 1016 and MCS-1109 type products. C. Future Expansion Due to the expected limited sales life of the Aroclor 1016 product, no specific provisions for future expansion are included in this project. D. Physical Appearance Paragraph (F) of this section adequately describes the general type of construction to be employed for the new column system. One special consideration inherent in this project is adequate provision to minimize the possibility of allowing Aroclor materials (PCB's) of significant quantity to enter the environment, such as through spills, equipment leakage, etc. This objective will be achieved through the use of concrete slabs under and curbs around all new equipment installed on this project which contains or handles PCB's. E. Storage and Shipping Requirements Existing facilities will be used to load tank trailers and to produce the required Pyroclor blends. No extensions are to be made to the existing loading/un loading facilities. The finished goods from the Aroclors department will be stored in existing aluminum storage tanks as follows: Product Existing Tank Item No. Volume Imp. Gal Aroclor 1016 1307 20,000 Aroclor 1016 1308 20,000 MCS-1109 1286 12,500 Compartmented Tank Aroclor 1242 1305 12,500 Compartraented Tank Aroclor 1254 1312 20,000 12. DSM 147928 STLCOPCB4039538 E. storage and Shipping Requirements (cont'd) The product specification sheets for Aroclor 1016 and MCS-1109 are included in Appendix A of this report. The specifications for the Aroclor 1242 and 1254 products will remain as currently docu mented. F. Description of Facilities The following information is included in the Appen dix of this report: a. Equipment summary Sheets - Appendix B b. Process Flow Diagrams - Appendix D c. Instrument List - Appendix E d. Plot Plan and Equipment Layout - Appendix F e. Scope of Work - Appendix G The major equipment items to be installed for the production of the Aroclor 1016 and MCS-1109 products are as follows: 1. Distillation Column - A 30 sieve-tray, carbon steel, insulated, self-supported column. 2. Column Condenser - A 500 sq ft Monel (tubes) she11-and-tube unit supported above the top of the column for gravity reflux return back to the column top tray. 3. Column Reboiler Furnace - A vertical, oil-fired tubular heater rated for 4.OH BTU/hr absorbed. 4. Column Still pot - A 12,000 imp. gallon, hori zontal, steel, insulated, saddle supported vessel. 5. Residue Surge Tank - A 7,500 imp. gallon, hori zontal, steel, insulated, saddle supported vessel. 6. crude Aroclor storage Tank - A 15,000 imp. gallon, vertical insulated storage vessel. 13. DSW 147929 STLCOPCB4039539 IV. EX-BATTERY LIMITS FACILITIES The utility requirements along with the various utility sources are discussed below. A. Utilities Summary The utilities summary and requirements sheets for the new column system and auxiliaries installed as part of this project are attached as Appendix C of this report. B. Description of Facilities The required utilities for the new column system will be supplied as extensions of the existing Newport plant utilities. Sources of these utilities are as follows: 1. 175 PSIG Saturated Steam - The design requirement for 175# steam is 770 lbs/hr. Connection will be made to the existing 6" steam header. 2. cooling Tower Water - The design requirement for cooling water is 100 IGPM. Connection will be made to the existing 12" water supply and return (underground) headers. 3. Fuel Oil - The reboiler furnace will be fired with gas oil with the following typical properties: Ash, wt.% Gross Htg. Value, BTU/Lb Flash point Closed Cup, F Neutralization No. Sediment, wt.% Specific Gravity 60F Sulfur, wt.% Viscosity @ 100F, Redwood No. 1 Sec. Moisture Content, Vol.% pour point. Upper, F Acidity, mg. KOH/gm Carbon Residue (10% Bms), wt.% Final Boiling Point, c 0.02 18,000 180 Nil 0.01 0.92 1.4 200 0.2 <0 0.1 0.9 360 The source of this oil for the new reboiler fur nace will be the existing 3940 fuel oil tank. The design fuel oil usage rate is 37 IGPH. 4. 100 PSIG Plant Air - Design requirements are 3,500 ACFH. This air will be supplied from the exist ing 4" supply header. 14. DSW 147930 STLCOPCB4039540 B. Description of Facilities (cont'd) 5. Electrical - Design requirements for 415 v power is 66.5 connected HP. The power supply source will be existing substation "C" (to be verified). 6. 130 PSIG Nitrogen - The design requirement for nitrogen is 2,475 SCPH (instantaneous usage). 15. DSW 147931 STLCOPCB4039541 Appendix A-l AROCLOR 1016 TENTATIVE SPECIFICATIONS Unrestricted Information (R) Color (APHA) (R) Condition (R) Sp. Gr. at 25/15.5 C. (R) Acidity (mg. KOH/g.) (R) Moisture (R) Refractive Index at 25C. (R) Inorganic (Free) Chlorides (R) Pour Point (R) Dielectric Constant (60 Hz at 100 C) (R) Resistivity _ (500 VDC at 100VC, 0.1" Gap) (R) Hydrolysis Stability Test (As chlorides) (R) Monsanto Stability Test (As chlorides) (R) Distillation Range (ASTM D-20 corrected) 10% Distilled by Wt. 90% Distilled by Wt. (R) Penta and Hexachloro Biphenyls* Sulfates Dielectric strength > 25C. KV Flash Point, F. . Fire Point Corrosion Test (6 hrs @ 210C with bright Al foil) Change in wt. of Al % A.C. Color (APHA) A.C. Condition A.C. Acidity (mg. KOH/G) A.C. Inorganic (Free) Chlorides Vise. 100 F (SUS) 40, max. Clear 1.362 - 1.372 0.010 max. 35 ppm, max. 1.6215-1.6235 0.05 ppm., max -14C. or lowej 4.70- 4.90 500, min. 0.5 ppm, max. 0.4 ppm, max. _ 323 C.min. 356C. max. 0.4% max. None 35 min. 338 min. None to B.P. 0.0 60, max. Clear 0.010, max. 0.05 ppm, max. 71-81 General information Specific Heat 25C. Coefficient of Expansion (25-65 C) CC/CC C Fixed Chlorine Power Factor @ 100C. Typical Values 60 Hz 1,000 Hz 0.30 0.00068 41.3 + .5% 5 (R) Routine Analysis: all others by request only. *By Physical Chemistry Method 71-11, Job No. 1348522. Disc integrator is standard. Electronic integrators may be used after proper standardization against a disc integrator. ^C 6 l*rX MS0 STLCOPCB4039542 Appendix A-2 AROCLOR 1115 PRELIMINARY SPECIFICATIONS Biphenyl, % o-chlorobiphenyl, % m-Chlorobiphenyl, % p-Chlorobiphenyl, % Polychlorobiphenyl, % Acid Number, meq/100 gms Temperature, C Specific Gravity 30 max. 35 min. 0-3 19 min. 13.2 max. 6.5 max. 110-115 1.080-1.085 @ 85C CSW 147933 STLCOPCB4039543 APPENDIX A-3 MCS-1109 SUGGESTED TENTATIVE SPECIFICATIONS Condition Color, APHA Acidity, mg KQH/gm Crystallizing Point Range, c Clear 100 Max. 0.014 Max. 10-16 Concentration Ranges, Wt.% Biphenyl o-Chlorobiphenyl m-Chlorobipheny1 p-Chlorobiphenyl Dichlorobiphenyl 18-22 50-70 0-5 12-23 1 DSW 147934 STLCOPCB4039544 ! Monsanto Ap P A/DIX 3-J CENTRAL ENGINEERING DEPARTMENT I EQUIPMENT INFORMATION SUMMARY PROJECT NAME f\ __ *. _ MRO^LORS . T\ . 0lSTLLATfOM - /v/eiw Port NUMBER l-l 01-000 1 BlPHEHYL STOSAEE TANK SIZE. RATING, MODEL. ETC. 4ooq imp. Sal. l-IOfc-OOO 1 |-| 03-000 \ l-104-ooo 1 l-l 05-000 1 l-l o4-ooo 1 1-107-000 1 QlPHErtYLCHflR.EE PUMP filPHNyL HEAD TANK. blSTli-L ETO Residue Receive*. bliT. RES iDug TftANS. Pum p SCRu B 6&Z. PumP TANK. Scrub bep. C t R t. PumP CENTRIFUGAL IMP, SAL. I0,4oo ,Mpr GAL. ZEpJTRiFU&AL 25*0 /Mfi GAL. x 4'-3 H 30 XGPm <g> rr'-ro k (-107-001 l l-l 08-000 1 PumP moToE. 5C.Ru 88*. TemP. vJAte* PumP 3 MP f S'oo pp*\ 7J*I5PM > 4o' TO/4 1-109-000 1 |- no-ooo 1 l- 1II- 000 1 SCRU &BeR Cooler. HC$ Sc RUBBER. W"l GHL0R1MAT0R Fb 50. FT U-TuBE x 4'-o" i" 6S.KL 5flOOi.es /Ooo /*A SAL. /6'- PREPARED BY A.J. He(N'*.' CCA NO. ZS/% AREA 1 PACE 1 or 4 APPROVEO BY EQUIPMENT DESCRIPTION ' MATERIAL OF CONSTRUC TION Steel INITIAL ISSUE 1-15-71 REV. NO. REV. ISSUED REMARKS Jc,,* ue E ESTIMATED PRICE (SI EHofctCONTAL .... EXIST, iT. 3905-1 (Rod 5Ttl A steel/ AL. 5PRAYED VERTICAL exist, it. n01 CoMpARTMSNTS EXIST, IT. IZZ5 E /Rod STEEL Ductile /od E VERTICAL 100 C, 30 AS I ZnT. MECR. J*L A/ A/ '-- Dutr/Lf /iPod All Steel STEEL STEEL TIE Ft. e-CNr, Pa cat/a/s g'Tuees VI*'* SHEUL S/&RT.LUC, sopp. 200C ZOfiSI, WEWncWL exijt: /r 1202/1 AJ Kl 14 a/ 1- lt-ooo 1 WCZ CH LORfWAtoR. SAME AS |T. |-1M EXIST, it. 1202/z /- II3-000 l 1- 114-000 1 l-l 15-000 l N-3 CHLORiNAToR. OFF-GAS Cooler. dATCH TAW< SAME A5 IT. 1 --M1 12.0 SO. FT. SHELL flw TUBE 74o imp. Gal. Fio" 4 x G'-O" 1- life-000 1 TRANSFER PumP DSW l- los-ool ce>224 -7d 147935 1 PumP Motor S HP /S'OO PPM JOURC El H NEW COEXISTING R - TO 0C RELOCATED STEEL STEEL -- EXIST. IT. I2&2 EXIST, it. 1X94 exist, rr. 127s* C5VTR//SUGAL TEFL A/ STLCOPCB4039545 Monsanto ApPMPly. 6-2 CENTRAL ENGINEERING DEPARTMENT I EQUIPMENT INFORMATION SUMMARY PREPARED BY A.O. HetutE CEA NO. 25V AREA t PACE z o'4 t,<JJECT NAME . *. f\ AR.OC.LOR5 UlSJlLLATloM - NEWPORT APPROVED BY NUMBER SIZE. RATING. MODEL. ETC. EQUIPMENT DESCRIPTION MATERIAL OP CONSTRUCTION i-in-ooc 1 bl2-1 Blow TAUK. (200 /mA GAL. STEEL 1-118-000 l U2I CRUDE ZOOo IMP GAL. AROCCOR STORAGE STEEL- 1- 114-000 1 Ate./ CPU Of ARoCLoR.5 PuMP 4o gpm ff as' rDM QA ST 1R0H 1- 12,0-000 1 MSZ CRUDE ARoCLOR STORAGE /5t OOO /-*p. GAL. 1% '-o'' R X ia'-o" STEfL STORAGE TAa>K, 1- I2jO-00\ Z HEATING PANEL Deaa/ 6/?oi. EMBoSitO PflVEUS STEEL 1- 12.1-000 1 MS 2 CRUDE STORAGE PUMP ISO' XGPM <> 90 TOM C/1ST IROaI 1-12.1-00 \ 1 PumP motor. /0 //F tffoo PPM INITIAL ISSUE REV. NO. REV. ISSUED 7-/5-7/ REMARKS S=u " u"=c ESTIMATED PRICE U> VERTICAL exist, rz.04.// Ho,Ra. EXl&T. I5U.4. CaitRiFuGAL. EXiLT. (2,61 & VERT. Flat &m. 2Sb*C Atm. AJ (& "wiOf Rolled to /3 '4 ZE^TRIPUGA L MECH. SEAL TFFC R/ 1- 1X2-000 1 Lime slur Ry tank. 4-oo 1 Mp. (Sal. 4--0* X 5 3 i .Steel VERTICAL. ZtSC. 30 PJW a; 1- 12Z-OOI 1 tau< A&itator. AxiAL Fcotfl TuRBidE 45 Pitch STEEL /< " //*. /So RPf a/ l-tZZ-002 1 Agitator moto/e. 3 HP tooo RPm - TEPQ. A/ 1-123-000 1 lime slurry PUM P l-IZS-OOl 1 POMP MOTOft. 1- (24-005 1 I-1X5-000 ! Lime Hois r Distil, latiom Co LUM M 1-125-6o| 30 |- 124-000 1 1-127-000 1 Iolumu Trays CoLumU STILL. POT Still CiRC. PumP ^ X 7 1- 127-001 1 l-\x.S-ooo l PUMP MOTOR. "* ZOLUM K> LJ iawDEwieR, O' zo XGPM <? st>' rz>/* Z HP j"oo Ppm I ooo LBS. CA FJY PUTOP TYPE 6-0" D'P. no'-o* high si e ve Type 3/il" 4 holes 12,000 ImP. SAL, lo'-o" x ZS-On 3SO Z<rPM <s> 9s ' ro H ZC HP ,, IOOO HPm poo &<s>. PT. FXT5 C A S T (RoP -- steel Steel steel cusr STEEL -- MODEL TU Bi steel Shell CE/UTRlFUGAL MEZM. ZEAL. w tef<l ptJEuMA Te AO Pr/mtP. SELF-SUPPORT. 350*C F.V. N tJ Si 18" SPRc/dS Hoftiz. F.V. CEDTRlKUGAL M CW. L sf A) M 7-fFc J'LOWG 5/C" Tttf Z4oC FV A/ C *22* IRE \ . P76l JOU*CCi N NEW r, ~ RVISTIMfi f - TO B r D oCTtn STLCOPCB4039546 Monsanto APpEVDtx B~3 CENTRAL ENGINEERING DEPARTMENT L EQUIPMENT tNFORMATION SUMMARY PROJECT NAUC . ^ AROCLORS DlSTl LLATIOn! - NimPo%t EQUIPMENT NUMBER 1-121-000 1 l- 130-000 1 1- 131-000 1 M31-oo| 1 |- IJS-ooo 1 1- l33-ooo I |- 133-oof 1 1- \34-ool \ 1- 135-000 1 l-135-oof 1 Column VElOT (LoNDEAliER, Column! Elector, Q.0HT>EH3ER. TEMP. VM ATEtZ. PumP PwmP motoA. REJIDU RECEIVE R. Residue Pomp Pump motur. Re Boiler Furmale Gas oil. Pump Pump motor. SIZE. RATfNC, MOD El-- ETC. 4-0 s<s.FT. FXT5 30t.es/MZ. fj/Cm C 2 0 MM Wf 3S"o XSPNA <s> 1 So' TOR (O H-P ASoo fcP 7Soo /mP. Gfli, `I'-G* <t> x IL'-O1* I S' X PM Ao* TDM *1 Yv HT t5oo RPm 4 m &tu/h/z. Absorb. 4-n sen. 4o ooil 4o ISPM <? loo PSiG Dsc. 1 HP \000 RPNA PREPAREO BY A.O. Hein-ze APPROVED BY EQUIPMENT DESCRIPTION MATERIAL OP CONSTRUCTION Mon) El TUSE^ Steel Shell MoOEt M8l*tC c.x. Eooy Qfi&T t/ca*) CEA NO. AREA PACE 1 3 OF 4 INITIAL. ISSUE Rev. no. REV. ISSUED n-is~-n REMARKS 'ft. * e estimated PR<$IC E VERTICAL a/ /as^c. F.V. ruo stage AJ0W- CON)&, a/ Cea'T'Rjfusal. PACKi/JG A/ -- STEEL. CAST STEEL. TEFO. Han 12. 3SD*C. ZOPS! CeMTRiFUiSrtiMECH. seal Ai N/ Ai -- Steel tube C40T IRotJ TEFC. Nj VERTICAL. on. Fntet> w/fcoVTRw. fi Rotary seaa ___________ FALKiPE Pi -- repc A) M3(*-ooo l 1-131-000 1 1- 138-000 l l- 131-000 1 1- V4o-ooo 1 <SAS> Oil StG.TanK. o/ltillate ___ PROD. RECEIVE*. PoRoCEL Column! feed Pump po fi.oC.Ei. CflLUM N/ Aroolor Still ISoo imp. Sal. lo fT <3P1 (? &T ' TO jut 3-o"4> * I?1 tf-io'V x /*-*" STEEL. ZlUC.- SPRAY60 steel CAST* STEEL. Alumimum o GO 3TEEL EXIST. 3340 EiO\T. IL8 l EXIST. I2E2. EXIST. 13 0 1 VERTICAL EXIST. IZOT E t e I- 141-000 1 l- l+Z-000 1 1- 143-000 1 i-144-ooo 1 still Receiver. earth treatment TAM K. -|LTR PREO-S Pu AP rILTCATE RECEIVER. REO /ft GAL. //00 l*P, G>9L. IS SAM (S> ^*o A>47G D'SCW, ?5"0 /AfR SrtL. sJ U> -u MOW. Zj Aic- sprayed Steel 8Row2 ZIVC- spraye StESL EXIST IZI5/1 AS IT ATE* EXl IT. IZIfi rxisr. iazi/f EXIST. \Z%3 STLCOPCB4039547 Monsanto APPEa/Dix B-4 CENTRAL ENGINEERING DEPARTMENT 1 E'Ql//PMENT' INFORMATION SUMMARY PREPAW CO BY A.O, He/nie PROJECT NAME 1 .^ .. AfcoCAoRs 0 i$t/ llat ioa> - New port APPROVED BY EQUIPMENT NUMBER OTY. EQUIPMENT NAME SIZE. RATING. MOOCL. ETC. EQUIPMENT DESCRIPTION MATERIAL OF CONSTRUCTION 1-145-600 \ 1-144-000 1 1--147-660 \ i- 148-000 1 l-144-ooo 1 1-150-060 1 -- 1-151-000 1 AROQLOR 1254 storage tamk AROCLOR. iZA-Z. STORAGE TAmK A- 1242 STORAGE Pump m2 1 AROCloR \G\U Storage tank. mSE AROCLOR 1014 Storage taok M 2 1 A- liGO STORAGE PumP NiZ A-IXG6 storage Pump 12,470 1mP. Gal. Z0,ooc> XMftGAt. ZO, 060 IMP. S/1L. - 2,0,000 IMP. SflU Aluminum Alum /mum ALom )M a Auumi/uM 1-152-000 t 1-153-6 00 \ M0S-iio4 STORAGE TAWK MCS-UOl STORAGE PumP u;4to x^P. gal. Aluminum i CA HO. AREA PACE ZS/8 1 4 or 4 INITIAL ISSUE REV. NO. REV. ISSUED 7->5"7/ . REMARKS *c * U"c E ESTIMATED PR(SIC) E Exist?.I365H2 Exsrrv*^3i2 CEMT/pfFWGAt VERT. EXIST. 1307 VERT. EX 1-XT. 1308 dEUTfllFUMt. CEAJT^jFoMt e Ho/tri. exist. i234-i.g 4^T/?I*I/GAL rj n <s> SE Vi -- sc Li 1---- 00 _____________________ -> STLCOPCB4039548 UTILITIES SUMMARY CENTRAL ENGINEERING DEPARTMENT CAPPgA/QI* -1 ; OBOJECT N amE ! Aroolord UTILITY ' SERVICE Distillatioai - Hewpcnr INITIAL issue UNITS D`TE T-IS-TI AVERAGE DESIGN PRtOAISO y A-0. DATE He/A/-*i= REV. 1 APPROVED BY DATE REV. 2 CEA NO- zs/s AREA i >AGE f or REV. 3 DATE 2. AVERAGE DESIGN AVERAGE DESIGN AVERAGE DESIGN LBVfa. 175 Psi& Steam | Cooliams iTowgA Water, X$PN\ IpbEL Oil. i `ELecrRic.Au. rsPH Coma;. HP Process Air, ACPH 6o ZS -- 3 ooo 7 70 too 37 64.5* 35*00 M itrocca/ Proc. Water i iNsr Air i *. SCFH XSPM ACFM Zoo S' to Z4 7S ~ ts o . ^ i * 1 *o 1 0 ' U) i > Blank Space Indicates This Utility Requirement Has Not Been Checked Since Last Revision. Reoeated Number indicates This Utititv Reouirement Has Been Cheeked Sinre The l *t Revision. and Remain* The *me STLCOPCB4039549 central engineering department UTILITIES REQUIREUENTS FoA NEW Column System, ompmcnt ietNT*r:ATii* MUR* CD /Iroclor.3 DfST><-i-ATioAi - NewpoR-r 175 PSI 5TMM COO'LVf/ALUTC6RTdMjER Fu^L. Oil* ttCNcqu'MitNt L6 */* RVtRMC MAXIMUM AVCftAQC MAXIMUM IGPM AVTRUt MAXIMUM 1-107 I-IQ& l-IO<? HI I I- (20 i-iai aS/CARcu.BBpEv*f.\F SCRUBBED. TE*P. NUTK PI/MP SCCOiQSuN6tA6fiA Kl-I CHlORlMtltm Mix fliWEi Ag&ctoa. STtf. D? Z. ERODE era. PkmO 4o 4>o 1-122 1-123 lime Su/RRr Tk, LI**A suuRRy PvmP 1-124 lime Hoist STJi-L For 1-127 SCtoilllumPnuriP 1-128 CQMOjfoiafa; WgsArATf/IfeT&^'~cuwPuy 50 ?5 (-127 'JetJT C.OND. 1-13 0' 1-13 I 1-132 CEOJELUCMTONR Cot>SH W ATgR Pl/MP EfCgii/gK- Soo 54-0 J ^Wf' I- >3 3 REEeSaIDoUEn.Pfiump 1-134- FuRPAag 40 /oo 25 37 1-135' FugL Oil PumP Stm. TrAciaic 50 70 lcctrcac Coww. H P 10 2? 10 T/Z Appeudix g-2 A-J. HE/NziC 2^/$ 2-2 pooc.es* Am AcfH AVERAGE MAXIMUM AI ITROSEA! SCFH AVXRA6C MAXIMUM 7-rs-7f Process Wawta IPM AVD1MK MOOMM IOO b7S (total Fog 3 c 410X1*1/ TKs) loo /goo 5 3ooo 3Soo Paw+J re/M>ecy kO (/) s: TotalS 450 770 60 /oo 25 37 4 C.S 3 ooo 35Q0 2oo 2475 sC I- 4* O STLCOPCB4039550 DSW 1 4 7 9 4 1 STLCOPCB4039551 DSW 1 4 7 9 4 2 STLCOPCB4039552 *f 6 t * > l MSO STLCOPCB4039553 HSQ STLCOPCB4039554 $ * r6 L * tl MSO STLCOPCB4039555 q*rbL*r1 C3 V> s. ear STLCOPCB4039556 DSW 1 4 7 9 A 7 STLCOPCB4039557 Material- Balance Appehdix D-S .Stream Al iImMA CO 1 2 3 45 47 8 9 /O // /* /3 IS Stream name AfioOcP:E-oRfAt TIiOoNio. ACSF.rTIr?oooocROmlAEoCrE SUluMrrfy OTSnOptrbTirlrAslLE PFeeoewdtEt RSebonrtleerR VATP&ORS G6Looi7lqTuum/idJf. Av. C%Coo4wjvolou*m*tfpS*a6J^ CERoXEUTPLfLW*U**AX)L Aye. Aye. Co*.U*W PfOOvcT Avr. CouvmM Fopetvr CCoeVwnBoTOeMrf^TsXeT*r C/oCcrjitfoc>5TwA#!/. COLUM*/ Restore AKOCLOR |OtW Hi&H BoILERS L| ' 242+ <27*5) (222,eec& SIC (lst) (4S,73o) -- (3oo) (Soo) <> ; able[Comp saiTiod 10,500 7,300 3200 -- ' ---- ------ -- -- -- -- -- --_ -- (+a,75o) -- < )300 Total 1.83/tut 7200 W -- 252,600 XS'Z,ooo 14,000 12,700 io,5oo 1,300 J,ZOO -- -( -- -- Total. lAs/RoN ZL?,I90 Temp. *C ICO Preswa, wiq Q0 0 3?40 27/,/30 -- -- -- -- -- ICO ICO 140 300 MMWNU- 175 315 M.rf, wax. 240 300 NWAi#X.. 300 WAM/*r. S5 *+0 mmaiRx., O 0 C4o) (l4o) 0+o) 040) .(+> -- 222,073 US US (40) 0 -- -- -- L 2 4A,0SO l 45 70 *0O O (xsj O MoCpSe-IrIOat<io? n ,, (V 61 phenyl 20,020 mcs- iioq 4l,1oo Hish Boilers Lim 30,730 _ 92,7ooTotal <-S:/gArUf TemT. *C 1+0 PRevruRE, ftlS (w) o 600 20,020 (2+0 43,140 420 3l, 430 ISO /So 2^+30 2,4*02700 9S,t,o0 199,Sbo 194,Sbe 29,000 >,I90 1 1 IS 0 135 0 3JAJS5 M**r<W. (4Lo7 j1i<P MMXMX,, C440) *23.^05 MMAltXf.. C+to) *30 */*. MAX* (440) 225 i*. 2(43f0cow)ax. ?0 (Ka) -- 43,140 -- -- 43,140 70' 0 20,4/7 -- 20,4/7 SO 0 -- -- -- -- -- -- -3__ -- -- -- 3 30 (745? 3/, 4?0 /so 31, (40 X?S 0 'Jarss : I. set Proc.es:. Flow ThagpAm Sheets 3 Ant> 4. 2. Avr. H4-2 Peeo Pate 5u4/4 chaw peeo Phase op ftua. 3. PRELIMINARY MATERIAL. BAlAjucE. DSW 147948 STLCOPCB4039558 Central Enoinczkino 0*RARTMKNT I stRumemt...List PHOJ/D*P.T - _ plant n'&ujport MMMPII jWIWn I MO,. Appmo'k xi_ CEA NO J__AREA NO. V jjL oatT2I :,15,~-?,/....HgET. . OR. Inst, ws DESCRIPTION ............ TYPE TORI- l-iio-l 1-125-1 H25-2 l-J5-3 1-125-4 H2A-I 1-IS6-I I-I2V' l-l?2-l 1-134-1 Multipoint Temp, Pr 1 Scrubber $4s outlet 2 Column Bottom TRAy 3 Column T*/iy Ali /5 4 Column ToP TftAy 5 Column Reflux. 4 Still Pot Liquid 7 Condenser ai/c cases 8 M/c $4SA To Of T3 A Residue Receiver. Liquid id ReBO/LETjC outlet* ti spare 12 SPARE RecoRb Lot. Panel .i Auto \JAlVG Sl?F MAT% --! TIC lovi FI U 1 - 1 FX H2- l fr n3-i LX 17.0-1 PCV 17.0-Z PCV 12.0-3 LI (22-1 PIC 12.5-5 PDX 125-4. LRC IZ4.-2 PCV 124.-3 P5E 17.4-4 FQ Fit FX KCV XCV I2B-2 128-2 IZft-3 128-4 J28-5 Cooler TEaaP. Water Cowr. J ajdic Ate Local W2 1 Chlor. fJz, FlouJ A722. - - AJ- ? <- - " /KJDICA7E W Die ATE indicate Local LoCA L Local R-Z Crude Storage Level. 1*1 LEr AiZ Regulator. Vent outlet F$ulA indicate -- Lime ^uuRRy tank Level. in Die ATE Pa nEl local Local i Local Column PpEcsuR* Control. tutucfire PAaJEL Column PflEst. Differ ifmeal ia/ Dilate PfiAtE L Still PoT Liquid Lcvel 5t/ll pr A/* Regulator. Stm-l For puprufif Disc. Record ".-- PAaIEL Local Local D/5T/LLATE Totalizer. Dot, Floin Controller ReFLox Flow OiiTiLL, Remote Block Valvmt FoRecut Remote - ^ indicate INDICATE Indicate Plur Plug, Panel Panel Local ~ *' r STEEL ---- ---- --- . /" C.T, i" c.z. ---- r Steel -.. -- / i*1 -- r -- vk" z" STEEL c.x. 0CONf C -- 3K. s.s. (3IL5.S.. Alum. Steel DSW 147949 STLCOPCB4039559 Central fNOlNBMIHO OtPARTMINT .1N STR.U.MEMT...11 4T- PPLKAONJT/DjEPL471SMA !1_OIVI*(On!IS5332I2Z Imst. k/s t>E SCRlPTlOA/ TYPE . Appenoix 25/&_ceX ho. AREA HO. . _J_ or A.O. HEtA/zE____ DATE 7-<5-*7/ imkt .T OP- I Loc, Avto. Valve MAT 'L Pcv 130-1 Xcv l$0'Z Jets 5tam Regulator ---- Suctiov Line /?motc Valve Plug -- /" $TL 4" STEEL TIC 1 31- 1 FI 1 31- Z LX 13 2-2 PSf 133-3 Pro /34-2 PC'/ 12.4-3 FT 134-4 TX 134-5 BE \ZA-L Temp. MateiS. Gov-rc>LL.Elt, tempered Water. Flow Residue Receiver Level.. Receiver Rupture Z>i*e Reo|LA Fuel. CONTROLLER Steam Press. Chut, ValvE Proc. outlet Flow # Stack. temper atuRE # PlAme Failure * IWDICLATE Local INDICATE Local 1NOtC/tTE Panel - mmmm iajdicate -- INDICATE iWD ICATE Panel -- PAfJEL Lee, Pavel l/t* -- -- *3/4' -- Steel -- JrfEt STEEL -- * ReBoileA interlock SAFIEguard system. THE Poulowim^ Uwe-Mouwra) instruments ARe Also tucuji>0 3 - ftouROow-Type Pressure a<se*. 4 - Chemical SCTU-TyPE P/?f*Su/? GAGES. 4 - Aesocurf READ/MS MANOMETER, TYPE VACUUM GASES. 6 - 8r~A1tTALLfC T>I/)L THERMOMETERS. <o - M I 3 C. IWSTRUMeUT Alft, /STEAM ReSUL fiTORi (V4'1 i>*e) DSW 147950 STLCOPCB4039560 G-l APPENDIX G SCOPE OF WORK 01 - Equipment Items . Refer to the Equipment Information Summary Sheets, Appen dix B (4 sheets). 02 - Instrument Items A new 2-foot control panel is required for the electronic panel-mounted instrumentation. This new panel will be installed in the Existing Aroclors department control room. Refer to the preliminary Instrument index. Appendix E. 03 - Setting and Testing Equipment No unusual difficulties are anticipated. It should be noted that the new fractionator and auxiliary equipment will be erected inside the existing Aroclors department battery limits and that "tight" conditions may exist as far as the mobility of construction equipment is con cerned . 04 - Setting and Testing Instruments No unusual circumstances are anticipated. Normal instru ment setting and testing factors may be used. 05 - Piling The following equipment will be supported by 50-foot long concrete shell piles: Item No. Description_________ No. of Piles 1-120 1-125 1-126 1-132 1-134 No. 2 Crude Aroclor Stg. Distillation Column Column Still Pot Residue Receiver Reboiler Furnace Total number of piles required DSW 147951 STLCOPCB4039561 G-2 06 - Excavation The following excavation and backfill volumes will be required; Item No. _________Description Cu Yds Excavation Backfill 1-106 Scrubber Pump Tank 1-120 No. 2 crude Aroclor 1-125 Distillation Column 1-126 Column Still Pot 1-132 Residue Receiver 1-134 Reboiler Furnace Misc. Pumps, Etc. Totals Allowance should be made for the costs involved in removal of unforeseen underground obstructions. 07 - Foundations The following volume of concrete is required; Item No. _________Description__________ Cu Yds 1-106 Scrubber Pump Tank 1-120 No. 2 Crude Aroclor Stg. 1-122 Lime Slurry Tank 1-125 Distillation Column 1-126 Still pot 1-132 Residue Receiver 1-134 Reboiler Furnace Misc. Pipe Supports Misc. Paving and Curbing Pump Foundations @ 1 Cu Yd Ea 8.0 Total Concrete 08 - Supports, Platforms & Structures Steel requirements are as follows; a) Saddles for items 1-126 &. 1-132 b) Access Platform Above Column c) Ladders & Stairways d) Handrail & Toeplate . e) Pipe Supports & Brackets f) Access Platform for Lime Slurry Tank Tons Total Steel 0SW 147952 STLCOPCB4039562 G-3 09 - Other Building Items None required. 10 - Sprinklers and Fire Protection No automatic sprinkler protection is required. The exist ing fire hydrant protection around Building 35 is considered adequate. 11 - Piping A preliminary indication of the amount of process and utility piping required can be obtained from the seven process flow diagrams and the overall plot plan. Process piping will be 150# flanged or screwed pipe and will include considerable parallel steam-traced pipelines. Process pipe handling crude Aroclors upstream from the new column will be steel. Spec. lD-M-E (Spec. 3E-E-F for the reboiler furnace process piping). Process pipe handling Aroclors (distillate) downstream from the new column will be steel. Spec. 1J2-C2-H. The utility piping to be used is as follows: Utility Pipe Material Sizes Range Piping Spec. 175# Steam Cooling Tower Water Fuel Oil Instrument Air Nitrogen process Air Steel Steel Steel Gal. Steel Steel Steel V-3" l"-6" V-l" V'-l" V'-iV' j"-i" lC-M-D lB-B-B 1C-D-C 1A-L-B 1B-A-B 1B-A-B Liberal allowance should be made for steam tracing tubing as the majority of the process pipe will be traced. A liberal number of steam trap assemblies should also be included. 12 - Ductwork None required. 13 - Electrical The electrical classification to which the electrical systems apply is water-tight. No flame-proof areas are involved. DSW 147953 STLCOPCB4039563 G-4 13 - Electrical (cont'd) New Allen West DOL type starters are required for motors as follows: Item No. Description Remote Inter- HP P.B. lock 1-107-001 1-108-001 1-121-001 1-122-002 1-123-001 1-127-001 1-131-001 1-133-001 1-135-001 Scrubber Pump Motor Scrubber Water Pump Motor No. 2 Crude Stg. Pump Motor Lime slurry Agitator Motor Lime Slurry Pump Motor Still pot Pump Motor Condenser Water Pump Motor Residue Pump Motor Gas Oil Pump Motor 3 5 10 3 2 25 10 7^5 1 No NO Yes No No Yes NO No Yes No Yes Yes No No Yes Yes No Yes Allowance should be made for new lighting requirements around the column system and new tankage. A new 15-point annunciator panel is included. Local start/stop push button stations are required for each new motor. 14 - site Preparation None required. 15 - Sewerb, Drains and Plumbing (Requirements for a trench sewer for the new equipment tied into the existing Aroclors interception pit should be determined.) 16 - Underground Mains Allowance should be made for at least one cooling tower water return tie-in from the new process area to the existing underground water return main. 17 - Yards. Roads and Fencing (If the new No. 2 crude Aroclor storage tank is to be set in an existing tank farm, requirements for concrete, excavation and backfill for curbing and pad need to be determined.) Also, the need for a paved accessway for fork truck loads of lime bags to the lime slurry tank area is required. 18 - Railroads None DSW 147954 STLCOPCB4039564 G-5 19 - insulation The thermal insulation for elevated temperature use on pipelines and equipment will be calcium silicate. Spec. K1032-100. weather barriers used will be galvanized sheet (K1032-164) for vessels and Hard Setting Composition (K1032-143) for process pipelines. Approximately 80% of the steel and aluminum process pipe lines indicated under Code 11 will be insulated. The, new equipment will be insulated as follows: Item No. Insulation Spec. Surface Sq Ft 1-106 1-107 1-108 1-110 1-120 1-121 1-122 1-123 1-125 1-126 1-127 1-128 1-131 1-132 1-133 Scrubber Pump Tank Scrubber Circulating Pump Temp. Water Pump HCl Scrubber No. 2 Crude Aroclor Stg. No. 2 crude Stg. Pump Lime Slurry Tank Lime Slurry Pump Distillation Column Column Still Pot Still Circulating Pump Condenser - Heads Only Condenser Water Pump Residue Receiver Residue pump 1"100-164 1"105-145 1"105-145 1"100-164 2"100-164 1"105-145 1"100-164 1"105-145 3"100-164 3"100-164 2"105-145 1"100-164 1"105-145 3"100-164 2-105-145 75 5 5 30 735 5 100 5 1,350 975 5 30 5 660 5f Allowance should be made for instrument metering applica tions and for insulation required on steam and condensate lines of steam trap assemblies. 20 - Painting The main painting requirements will be much of the steel platforms, pipe supports, etc., listed under Code 08. Painting in accordance with the current Newport plant practice for the Aroclors department. 21 - Walls, Masonry, Roofs and Roofing None required. 22 - Spares None required. DSM 147955 STLCOPCB4039565 *90 - Dismantling *92 - Repairs Expense *93 - Relocation and Modification Expense G-6 *To be determined by CED-Europe based on actual Newport plant conditions as related to the preliminary plot plan and equip ment arrangement layout. DSW 147956 STLCOPCB4039566