Document M456eEOyv1aEYr8YYo11D5mg7
Report Prepared by: Report Approved by:
NPDES Pretreatment Compliance Sampling Inspection Report
Thomas Electronics 208 Davis Parkway Clyde, New York 14433 NPDES Permit: NYP080230 Inspection Date: September 26, 2023
THUAN TRAN Digitally signed by THUAN TRAN
_________________Da_te_: 2_0_23_.1_2.1_2_16_:3_0:_08_-_05_'00_' Thuan Tran, Physical Scientist
Digitally signed by PHILIP
PHILIP COCUZZA COCUZZA _________________Da_te_: 2_0_23_.1_2.1_3_14_:1_4:_59_-0_5_'00_' Phil Cocuzza, Chief Monitoring Operations Section
Thomas Electronics, Clyde, NY 14433 NPDES Permit: NYP080230
1.0 OBJECTIVE
Inspection Date: September 26, 2023
On September 26, 2023, the United States Environmental Protection Agency (USEPA) conducted a Pretreatment Compliance Sampling Inspection (CSI) at Thomas Electronics in Clyde, New York (NY). The objective of the Pretreatment CSI was to gather information necessary to determine if the pretreated effluent from Thomas Electronics is in compliance with the requirements and limitations set forth in the Federal Categorical Electrical and Electronic Components Point Source Category Subpart C - Cathode Ray Tube Subcategory under 40 CFR Part 469.34, the Federal General Pretreatment Standards for Existing and New Sources of Pollution under 40 CFR Part 403, and their Industrial User Permit; ISUP-001. The Industrial User Permit, issued by the Village of Clyde, was effective on December 01, 2022, and expired on November 30, 2023.
2.0 KEY PARTICIPANTS
Listed below are key inspection participants and contact information, grouped by organization.
U.S. Environmental Protection Agency Thuan Tran, Lead Inspector 732-321-4455, email: tran.thuan@epa.gov Molly Hillenbrand, Life Scientist
Thomas Electronics Corey Hall, Facility Manager 315-286-5541 (mobile), email: corey.hall@thomaselectronics.com Abe Hurtic, Process Engineer
3.0 FACILITY DESCRIPTION
3.1 General Information
Thomas Electronics is located on 208 Davis Parkway in Clyde, New York. The facility is a manufacturer of cathode ray tubes, which are used in the monochromatic displays for the defense, aerospace, and medical industries. There are three buildings on the property. Manufacturing operations began in 1975 in Building #1 and continue to the present day. Building #2 is used for wiring and assembly operations. Building #3 is a warehouse which has been used for storage since 2001. There are 90 employees that work one 9-hour shift (7:00 am to 4:30 pm), Monday to Friday, with every other Friday off. Thomas Electronics is categorized under Standard Industrial Classification (SIC) 3671- Electron Tubes and the North American Industry Classification System (NAICS) 334419 - Other Electronic Manufacturing.
3.2 Process Information
Thomas Electronics uses city water. Sanitary water usage is drained to the City of Clyde Sewer Collection System. For manufacturing operation, the city water is treated through a Reverse Osmosis (RO) System, followed by a Ultraviolet (UV) Sterilization Unit, followed by Ion Exchange System to produce deionized water at the Point-of-Use (POU).
Page 2 of 7
Thomas Electronics, Clyde, NY 14433 NPDES Permit: NYP080230
Inspection Date: September 26, 2023
The Cathode Ray Tube (CRT) glass bulbs come into the receiving area and are conveyed to the dirty washing station. The bulbs are washed with a 3% hydrofluoric acid solution, rinsed with city water, and then rinsed with deionized water. Some bulbs undergo an ultrasonic vibration cleaning to remove stubborn residuals. The glass bulbs move to the grinding/buffering/polishing station before the face and base are attached. The CRT bulb with base is cleaned and rinsed with DI water. A phosphors coating is applied onto the inside surface of the bulb, then moved into the oven to be baked to lock the phosphors onto the surface. A lacquer film is applied on the backside of the bulb after the bulbs come out of the oven. After drying, a graphite-based coating is applied to the bulb. The bulb is placed into a vacuum, where aluminum is vaporized onto the lacquer film. The bulb is moved into a furnace and baked to harden binders and remove organics. A sparker is used to check for defect in the phosphors the following day.
An electron gun is inserted by fusing the base of the bulb to the face plate using frit tape. At the exhaust station, a turbomolecular pump is used to create a vacuum. A "getter flash" is used to maintain the vacuum inside the CRT. After sparking and degaussing, the cathode is activated by aging.
The finished CRTs are sent as a kit to be wire and assemble in Building #2. The assembled product is tested for alignment. The product is then sent to the Clean Room for final lamination with silicone. The finished product is tested to simulate variations in temperature and altitude. After final inspection, the CRT is transferred to the packaging area for shipment.
Process wastewater is generated from dirty, ultrasonic, grinding, buffering, and polishing wash stations, as well as cleaning wash with RO rinse, coating wash, lacquer water, and welding wash.
Process wastewater is directed into the floor drain then flows into the Collection Pit. A pH probe is positioned in the Collection Pit to monitor the pH of the incoming wastewater. Depending on the pH, the pH probe communicates with the dosimeter to either add muriatic acid or sodium hydroxide. A high-low level sensor monitors the level of wastewater in the Collection Pit. As the pit fills up, the high-level sensor is triggered to pump the wastewater to Settling Tank #1 until the low-level sensor is triggered to shut-off the pump. The effluent from Settling Tank #1 is pumped to Settling Tank #2 for additional retention time. The effluent from Settling Tank #2 passes through a sequence of cartridge filters from 50-micron down to 5-micron. The effluent is further treated through two (2) sets of 2 Cylindrical Ion Exchange Tanks. The effluent emerges from the ion exchange tanks is filtered through a 1micron cartridge filter. The pretreated effluent discharges into the monitoring location (Sample Box), where it comingles with the RO reject water. A pH probe monitors the pH of the pretreated effluent in the Sample Box before continuing to the sewer collection system.
The settling solids from Settling Tanks #1 and #2 are removed and collected in a 55-gallon drum twice a year. The liquid is allowed to evaporate from the drum. The
Page 3 of 7
Thomas Electronics, Clyde, NY 14433 NPDES Permit: NYP080230
Inspection Date: September 26, 2023
concentrated solids are disposed of as hazardous waste.
3.3 Facility Self-Monitoring Information
Thomas Electronics contracts Pace Analytical Services, LLC to collect and analyze the parameters in 40 CFR Part 469.34 and their Industrial User Permit. The parameters are Metals (Cadmium, Chromium, Lead, Mercury & Zinc), Fluoride, pH, Temperature, Oil & Grease, and Total Toxic Organics (TTO). TTO consists of Volatile Organic Compounds (VOCs) and Semi-Volatile Organic Compounds (SVOCs). Pace Analytical Services, LLC. is located on 575 Broad Hollow Road, Millville, New York.
4.0 EPA SAMPLING/INSPECTION ACTIVITIES
4.1 Sampling Activities
An ISCO automatic composite sampler was programmed to take 32 sample aliquots during the 8-hour sampling event from the monitoring location. The 8-hour composite sample was collected and analyzed for Metals (Cd, Cr, Pb, Zn & Hg) and Fluoride. Grab-Composite samples were collected for Semi-Volatile Organic Compounds (SVOCs). Grab samples were collected for Volatile Organic Compounds (VOCs) and Total Petroleum Hydrocarbons (TPH). The four (4) sets of VOCs grab samples were composited in the laboratory.
In addition, on-site grab samples were collected and analyzed for pH, Temperature, and Total Residual Chlorine (TRC)
All sample containers, preservation techniques and holding times were in accordance with USEPA requirements specified in 40 CFR Part 136. Signed and dated custody seals were placed across the lids and along the sides of the sample containers. The custody sealed sample containers were placed inside plastic sample bags and sealed. All samples were transported on ice to the USEPA Laboratory in Edison, New Jersey for analysis.
Flow monitoring data were provided by the facility representative.
Split samples were collected and given to the facility representative.
4.2 Inspection Activities
A Pretreatment CSI at Thomas Electronics was conducted on September 26, 2023. The inspectors met with Cory Hall; Facility Manager, and Abe Hurtic; Process Engineer. Inspector's credentials were presented, and business cards were provided during the opening conference. The facility representatives were explained that the purpose of the inspection with supporting on-site activities was to determine if the facility is in compliance with the Federal Electrical and Electronic Components Point Source Category Subpart C - Cathode Ray Tube Subcategory under 40 CFR Part 469.34, the Federal General Pretreatment Regulations for Existing and New Sources of Pollution under 40 CFR Part 403, and their Industrial User Permit.
Page 4 of 7
Thomas Electronics, Clyde, NY 14433 NPDES Permit: NYP080230
Inspection Date: September 26, 2023
The on-site supporting activities consist of collecting samples of the pretreated discharge from the On-Site Industrial WWTP, observing and evaluating the monitoring location, observing and evaluating the On-Site Industrial WWTP, observing and evaluating the flow monitoring devices, taking a tour of the CRT Manufacturing Operation, observing where process wastewater is generated within the CRT Manufacturing Process, and interviewing the facility's representatives.
During the closing conference, the facility representatives were briefed on the inspection activities. On-site sample results and concerns observed during the inspection were communicated to the facility representatives.
4.3 Deviations and/or Environmental Conditions
Compliance samples were collected from the monitoring location. The discharged effluent from the On-Site Industrial WWTP into the monitoring location was intermittent throughout the workday. Furthermore, the RO reject water was observed discharging continuously into the monitoring location.
5.0 ANALYTICAL RESULTS
Thomas Electronics - Pretreated Discharge to the Village of Clyde WWTP
Inspection Date: September 26, 2023
Pollutants Units
40CFR469.34
SIU Permit
EPA Results
Maximum for Mo. avg. shall Daily Maximum
any 1 day
not exceed
Fluoride
mg/L 35.0
18.0
35 (18-Mo. avg.) 40
Cadmium, T mg/L 0.06
0.03
0.06 (0.001 lbs/d) U
Chromium, T mg/L 0.65
0.30
0.65 (0.017 lbs/d) U
Lead, T
mg/L 1.12
0.41
1.12 (0.07 lbs/d) 0.093
Zinc, T
mg/L 1.38
0.56
1.38 (0.09 lbs/d) 0.090
Mercury
mg/L ----
----
700
(0.70 ug/l) U
TTO:
mg/L 1.58
----
----
U
VOAs ----
----
----
U
NVOAs ----
----
----
UJ
pH
SU >/= 5.0
5.0 - 10
8.15
TPH
mg/L shall not be in amount to cause
</=100
U
interference or pass through.
Temperature C
</= 40C
</= 65 (150F)
19
Flow
GPD
----
Metered
2,514
TRC
mg/L Per Sample Collection
----
0.15
Notes: U- The analyte was not detected at or above the Reporting Limit.
J- The identification of the analyte is acceptable; the reported value is an estimate.
Page 5 of 7
Thomas Electronics, Clyde, NY 14433 NPDES Permit: NYP080230
6.0 FINDINGS
Inspection Date: September 26, 2023
6.1 Sampling Result Findings
The EPA analytical results obtained during this inspection show the following parameter(s) as being outside of the acceptable limits:
6.1.1 According to 40 CFR Part 469.34 and the Industrial User Permit, the daily maximum for any 1 day/daily maximum for fluoride is 35 milligrams per liter (mg/L). The analytical result for fluoride was determined to be 40 mg/L.
6.2 Inspection Findings
In addition to the analytical data, an inspection of the facility operation was conducted as discussed in Section 4.2 above. During the inspection, the following observations were noted which may contravene the requirements of the permit or the applicable regulations:
6.2.1 RO reject water was continuously discharging into the monitoring location while the On-Site Industrial WWPT discharged effluent was intermittent. As a result, compliance samples collected at the monitoring location was not representative of the On-Site Industrial WWTP discharge. According to the Industrial User Permit, Part 1 B., it states, "Effluent from this outfall consist of wastewater from the following operations (Glass fritting, Defritting, Bulb washing/rewashing, Bulb screening & Bulb lacquering)." In 40 CFR Part 403.7(b)(2)(i) - Representative data; quality and quantity, it states, "The data shall be representative of the yearly and seasonal conditions to which the POTW is subjected for each pollutant for which a discharge limit revision is proposed." Furthermore, 40 CFR Part 403.12(b)(5)(ii) states, ".... The sample shall be representative of daily operations."
7.0 ATTACHMENTS
Attachment #1. An overview site plan shows Thomas Electronics facilities and property.
Attachment #2. CRT Manufacturing Operation is performed in Building #1.
Attachment #3. Process flow of CRT production is between Building #1 and Building #2.
Attachment #5. Process wastewater is pretreated by the On-Site Pretreatment System.
Attachment #5. Samples were submitted to the USEPA-R2 Laboratory on 09/27/23.
Attachment #6. USEPA Analytical Data Package was received on 10/17/23.
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Thomas Electronics, Clyde, NY 14433 NPDES Permit: NYP080230
8.0 PHOTOGRAPHS
Inspection Date: September 26, 2023
Photo #1. Compliance samples were collected from the monitoring location (Sample Box).
Photo #2. RO backwash was discharging continuously into the Sample Box.
Photo #3. A close-up photo shows no discharge from the Pretreatment System (grey pipe) .
Page 7 of 7
Thomas Electronics, Clyde (V), NY 07860 NPDES Permit: NYP080230
Inspection Date: September 26, 2023
7.0 Attachments
Attachment #1. An overview site layout shows Thomas Electronics facilities and property.
Attachment #2. CRT Manufacturing Operation is performed in Building #1.
Attachment #3. CRT Process is performed in Building #1. Wiring & Assembly are performed in Building #2.
Attachment #4. Process wastewater is directed to the On-Site Pretreatment System.
Attachment #5. Samples were submitted to the EPA Laboratory on 9/27/23.
Attachment #6. USEPA Analytical Data Package was received on 10/17/23.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
2890 Woodbridge Avenue Edison , New Jersey 08837
732-906-6886 Phone 732-906-6165 Fax
October 17, 2023 Thuan Tran Monitoring & Assessment Branch LSASD/MAB Edison, NJ 08837
RE: Thomas Electronics - 2309020 Enclosed are the results of analyses for samples received by the laboratory on 09/27/2023. The signature below reflects the laboratory's approval of the reported results. If you have any questions concerning this report, please refer to Project Number 2309020 and contact the laboratory. Sincerely,
John R. Bourbon Chief, LSASD/LB
Project Narrative:
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020
The National Environmental Laboratory Accreditation Conference Institute (TNI) is a voluntary environmental laboratory accreditation association of State and Federal agencies. TNI established and promoted a National Environmental Laboratory Accreditation Program (NELAP) that provides a uniform set of standards for the generation of environmental data that are of known and defensible quality. The EPA Region 2 Laboratory is NELAP accredited. The Laboratory tests that are accredited have met all the requirements established under the TNI Standards.
Condition Comments
None
Comment(s):
The "Sample Analysis Date and Time" is included in the results section for any analyte with a prescribed holding time of 72 hours or less.
SVOA analysis: All of the compounds are qualified mostly due to poor surrogate recovery or the MS MSD pair not meeting the %RSD criteria.
Data Qualifier(s):
U- The analyte was not detected at or above the Reporting Limit. J- The identification of the analyte is acceptable; the reported value is an estimate. K- The identification of the analyte is acceptable; the reported value may be biased high. L- The identification of the analyte is acceptable; the reported value may be biased low. NJ- There is presumptive evidence that the analyte is present; the analyte is reported as a tentative identification. The reported value is an estimate.
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 1 of 33
Reporting Limit(s):
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020
The Laboratory was able to achieve the standard laboratory reporting limits, where applicable, for each analyte requested except for the following analyte(s):
NVOA GCMS
The reporting level of 5.00 ug/L was raised to 10 ug/L for the following analyte(s): 2-Nitrophenol, Pentachlorophenol for the following samples: 2309020-02 The reporting level of 5.00 ug/L was raised to 30 ug/L for the following analyte(s): 2,4-Dinitrophenol, 4,6-Dinitro-2-Methylphenol for the following samples: 2309020-02
SUMMARY REPORT FOR SAMPLES
Field ID
Laboratory ID
Outfall 003 - Comp
2309020-01
Outfall 003 - Grab-Comp
2309020-02
Outfall 003
2309020-03
Outfall 003 -Lab Comosite - Grab#1 to #4 2309020-08
TRIP BLANK
2309020-09
Matrix Aqueous Aqueous Aqueous Aqueous Aqueous
Date Sampled 09/26/2023 16:12 09/26/2023 15:50 09/26/2023 15:50 09/27/2023 00:00 09/25/2023 09:45
Date Received 09/27/2023 14:36 09/27/2023 14:36 09/27/2023 14:36 09/27/2023 14:36 09/27/2023 14:36
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 2 of 33
Analysis 624.1 VOA EPA-NPDES 625.1 SVOA NPDES Fluoride Mercury Metals ICP TAL NPDES/DW Petroleum Hydrocarbons, Tot.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020
SUMMARY REPORT FOR METHODS
Method EPA 624.1 SOP C-89 Rev 3.7 EPA 625.1 SOP C-90 Rev 3.9 EPA 300.0 SOP C-94 Rev 2.8 EPA 245.1 SOP C-110 Rev 2.8 EPA 200.7 SOP C-109 Rev 3.7 EPA 1664A SOP C-126 Rev 1.7
Certification
NELAP NELAP NELAP NELAP NELAP NELAP
Matrix
Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 3 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020
Analyte
Field ID: Outfall 003 - Comp Metals ICP Cadmium Chromium Lead Zinc Mercury CVAA Mercury Sanitary Fluoride
Field ID: Outfall 003 - Grab-Comp NVOA GCMS Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2309020-01
Date and Time of Analysis*
---
U
3.00
ug/L B309146
---
U
5.00
ug/L B309146
92.6
8.00
ug/L B309146
90.3
20.0
ug/L B309146
---
U
0.050
ug/L B310050
40.0
0.500
mg/L B310002
Sample ID: 2309020-02
---
U L
5.15
ug/L B310011
---
U L
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
2.06
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U L
5.15
ug/L B310011
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 4 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020
Analyte
Field ID: Outfall 003 - Grab-Comp NVOA GCMS 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2309020-02
Date and Time of Analysis*
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
30.9
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
10.3
ug/L B310011
---
U L
5.15
ug/L B310011
---
U J
30.9
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U L
2.06
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
2.06
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
2.06
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U L
5.15
ug/L B310011
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 5 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020
Analyte
Field ID: Outfall 003 - Grab-Comp NVOA GCMS N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Field ID: Outfall 003 GC Petroleum Hydrocarbons, Tot.
Field ID: Outfall 003 -Lab Comosite - Grab#1 to #4 VOA GCMS Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2309020-02
Date and Time of Analysis*
---
U J
5.15
ug/L B310011
---
U J
5.15
ug/L B310011
---
U J
10.3
ug/L B310011
---
U J
2.06
ug/L B310011
---
U J
5.15
ug/L B310011
Sample ID: 2309020-03
---
U
6.33
mg/L B310062
Sample ID: 2309020-08
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
12.5
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 6 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020
Analyte
Result
Qualifier
Reporting Limit
Units
Batch
Date and Time of Analysis*
Field ID: Outfall 003 -Lab Comosite - Grab#1 to #4 VOA GCMS cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Field ID: TRIP BLANK VOA GCMS Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane
Sample ID: 2309020-08
---
U L
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
Sample ID: 2309020-09
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 7 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020
Analyte
Field ID: TRIP BLANK VOA GCMS Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Result
Qualifier
Reporting Limit
Units Batch
Sample ID: 2309020-09
Date and Time of Analysis*
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
---
U
5.00
ug/L B309136
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 8 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020
VOA GCMS - Quality Control
Analyte
Batch B309136
Blank (B309136-BLK1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
101
ug/L
100.0
105
ug/L
100.0
107
ug/L
100.0
101
60-140
105
60-140
107
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 9 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 VOA GCMS - Quality Control
Analyte
Batch B309136
LCS (B309136-BS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
51.2
5.00 ug/L
50.00
46.4
5.00 ug/L
50.00
45.7
5.00 ug/L
50.00
51.6
5.00 ug/L
50.00
52.8
5.00 ug/L
50.00
54.4
5.00 ug/L
50.00
55.4
5.00 ug/L
50.00
62.6
5.00 ug/L
50.00
57.6
5.00 ug/L
50.00
56.2
5.00 ug/L
50.00
55.7
5.00 ug/L
50.00
57.1
5.00 ug/L
50.00
55.5
5.00 ug/L
50.00
55.7
5.00 ug/L
50.00
56.7
5.00 ug/L
50.00
55.7
5.00 ug/L
50.00
57.1
5.00 ug/L
50.00
56.0
5.00 ug/L
50.00
56.5
5.00 ug/L
50.00
56.4
5.00 ug/L
50.00
59.8
5.00 ug/L
50.00
53.9
5.00 ug/L
50.00
52.6
5.00 ug/L
50.00
55.4
5.00 ug/L
50.00
54.4
5.00 ug/L
50.00
57.4
5.00 ug/L
50.00
55.1
5.00 ug/L
50.00
57.3
5.00 ug/L
50.00
53.6
5.00 ug/L
50.00
52.6
5.00 ug/L
50.00
53.2
5.00 ug/L
50.00
99.0
ug/L
100.0
106
ug/L
100.0
110
ug/L
100.0
102
19-205
92.8
5-195
91.5
15-185
103
40-160
106
50-150
109
50-150
111
60-140
125
60-140
115
70-130
112
70-130
111
70-135
114
70-130
111
70-130
111
70-130
113
65-135
111
65-135
114
35-165
112
65-135
113
25-175
113
70-130
120
50-150
108
70-130
105
70-130
111
70-135
109
65-135
115
60-140
110
70-130
115
60-140
107
70-130
105
65-135
106
65-135
99.0
60-140
106
60-140
110
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 10 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 VOA GCMS - Quality Control
Analyte
Batch B309136
LCS Dup (B309136-BSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
48.2
5.00 ug/L
50.00
43.0
5.00 ug/L
50.00
44.5
5.00 ug/L
50.00
49.0
5.00 ug/L
50.00
50.1
5.00 ug/L
50.00
51.6
5.00 ug/L
50.00
53.6
5.00 ug/L
50.00
62.0
5.00 ug/L
50.00
55.0
5.00 ug/L
50.00
53.5
5.00 ug/L
50.00
52.9
5.00 ug/L
50.00
53.7
5.00 ug/L
50.00
52.0
5.00 ug/L
50.00
54.7
5.00 ug/L
50.00
53.2
5.00 ug/L
50.00
53.0
5.00 ug/L
50.00
54.2
5.00 ug/L
50.00
53.5
5.00 ug/L
50.00
53.7
5.00 ug/L
50.00
52.4
5.00 ug/L
50.00
56.7
5.00 ug/L
50.00
52.8
5.00 ug/L
50.00
50.0
5.00 ug/L
50.00
53.6
5.00 ug/L
50.00
51.7
5.00 ug/L
50.00
54.5
5.00 ug/L
50.00
54.5
5.00 ug/L
50.00
55.1
5.00 ug/L
50.00
51.4
5.00 ug/L
50.00
50.9
5.00 ug/L
50.00
51.9
5.00 ug/L
50.00
97.8
ug/L
100.0
103
ug/L
100.0
109
ug/L
100.0
96.5
19-205
6.05
20
86.1
5-195
7.49
20
89.0
15-185
2.73
20
98.1
40-160
5.18
20
100
50-150
5.21
20
103
50-150
5.42
20
107
60-140
3.36
20
124
60-140
0.979
20
110
70-130
4.58
20
107
70-130
4.96
20
106
70-135
5.17
20
107
70-130
6.03
20
104
70-130
6.54
20
109
70-130
1.78
20
106
65-135
6.37
20
106
65-135
5.08
20
108
35-165
5.12
20
107
65-135
4.67
20
107
25-175
5.15
20
105
70-130
7.35
20
113
50-150
5.22
20
106
70-130
2.06
20
100
70-130
5.09
20
107
70-135
3.21
20
103
65-135
5.04
20
109
60-140
5.15
20
109
70-130
0.986
20
110
60-140
3.79
20
103
70-130
4.21
20
102
65-135
3.29
20
104
65-135
2.49
20
97.8
60-140
103
60-140
109
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 11 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 VOA GCMS - Quality Control
Analyte
Batch B309136
Matrix Spike (B309136-MS1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309020-08
49.6
5.00 ug/L
49.7
5.00 ug/L
33.3
5.00 ug/L
55.2
5.00 ug/L
53.7
5.00 ug/L
52.8
5.00 ug/L
55.0
5.00 ug/L
57.9
5.00 ug/L
53.5
5.00 ug/L
55.6
5.00 ug/L
66.7
5.00 ug/L
54.9
5.00 ug/L
55.0
5.00 ug/L
54.0
5.00 ug/L
54.5
5.00 ug/L
54.1
5.00 ug/L
55.2
5.00 ug/L
55.2
5.00 ug/L
40.3
5.00 ug/L
53.5
5.00 ug/L
48.4
5.00 ug/L
52.8
5.00 ug/L
51.7
5.00 ug/L
53.1
5.00 ug/L
52.8
5.00 ug/L
54.8
5.00 ug/L
53.0
5.00 ug/L
56.2
5.00 ug/L
52.6
5.00 ug/L
52.1
5.00 ug/L
52.6
5.00 ug/L
98.2
ug/L
104
ug/L
110
ug/L
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
12.5
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
100.0 100.0 100.0
99.1
19-273
99.4
49-251
66.6
21-242
110
14-230
107
17-181
106
52-234
110
69-221
116
40-160
107
54-156
111
59-155
108
51-138
110
52-162
110
70-140
108
49-155
109
37-151
108
70-157
110
74-210
110
35-155
80.6
80-227
107
47-150
96.8
17-183
106
52-150
103
64-148
106
53-149
106
37-160
110
37-162
106
45-169
112
46-157
105
59-156
104
18-190
105
18-190
98.2
60-140
104
60-140
110
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 12 of 33
Analyte
Batch B309136
Matrix Spike (B309136-MS2) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 VOA GCMS - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309043-09
46.7
5.00 ug/L
49.3
5.00 ug/L
8.96
5.00 ug/L
53.4
5.00 ug/L
54.4
5.00 ug/L
53.3
5.00 ug/L
55.2
5.00 ug/L
58.8
5.00 ug/L
52.3
5.00 ug/L
55.3
5.00 ug/L
54.4
5.00 ug/L
54.6
5.00 ug/L
54.0
5.00 ug/L
53.4
5.00 ug/L
55.0
5.00 ug/L
54.7
5.00 ug/L
54.7
5.00 ug/L
54.6
5.00 ug/L
15.2
5.00 ug/L
54.2
5.00 ug/L
35.1
5.00 ug/L
53.0
5.00 ug/L
52.0
5.00 ug/L
54.5
5.00 ug/L
52.2
5.00 ug/L
54.5
5.00 ug/L
54.1
5.00 ug/L
55.5
5.00 ug/L
52.3
5.00 ug/L
52.4
5.00 ug/L
52.3
5.00 ug/L
99.3
ug/L
106
ug/L
111
ug/L
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
100.0 100.0 100.0
93.4
19-273
98.6
49-251
17.9
21-242
107
14-230
109
17-181
107
52-234
110
69-221
118
40-160
105
54-156
111
59-155
109
51-138
109
52-162
108
70-140
107
49-155
110
37-151
109
70-157
109
74-210
109
35-155
30.5
80-227
108
47-150
70.1
17-183
106
52-150
104
64-148
109
53-149
104
37-160
109
37-162
108
45-169
111
46-157
105
59-156
105
18-190
105
18-190
99.3
60-140
106
60-140
111
60-140
Page 13 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 VOA GCMS - Quality Control
Analyte
Batch B309136
Matrix Spike Dup (B309136-MSD1) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309020-08
45.2
5.00 ug/L
50.00
ND
90.4
19-273
9.18
28
44.6
5.00 ug/L
50.00
ND
89.1
49-251
10.9
28
26.6
5.00 ug/L
50.00
ND
53.1
21-242
22.6
28
49.6
5.00 ug/L
50.00
ND
99.3
14-230
10.5
28
48.7
5.00 ug/L
50.00
ND
97.4
17-181
9.75
28
47.8
5.00 ug/L
50.00
ND
95.7
52-234
9.76
28
50.4
5.00 ug/L
50.00
ND
101
69-221
8.69
28
55.4
5.00 ug/L
50.00
ND
111
40-160
4.34
28
49.5
5.00 ug/L
50.00
ND
99.0
54-156
7.84
28
50.6
5.00 ug/L
50.00
ND
101
59-155
9.51
28
60.7
5.00 ug/L
50.00
12.5
96.5
51-138
11.7
28
50.4
5.00 ug/L
50.00
ND
101
52-162
8.63
28
49.6
5.00 ug/L
50.00
ND
99.2
70-140
10.3
28
50.3
5.00 ug/L
50.00
ND
101
49-155
6.98
28
50.6
5.00 ug/L
50.00
ND
101
37-151
7.50
28
49.8
5.00 ug/L
50.00
ND
99.6
70-157
8.32
28
51.1
5.00 ug/L
50.00
ND
102
74-210
7.56
28
52.0
5.00 ug/L
50.00
ND
104
35-155
6.14
28
34.0
5.00 ug/L
50.00
ND
68.0
80-227
16.9
28
49.7
5.00 ug/L
50.00
ND
99.3
47-150
7.42
28
43.9
5.00 ug/L
50.00
ND
87.9
17-183
9.64
28
49.7
5.00 ug/L
50.00
ND
99.4
52-150
6.01
28
47.6
5.00 ug/L
50.00
ND
95.3
64-148
8.23
28
49.6
5.00 ug/L
50.00
ND
99.2
53-149
6.72
28
49.0
5.00 ug/L
50.00
ND
98.0
37-160
7.46
28
50.9
5.00 ug/L
50.00
ND
102
37-162
7.27
28
50.3
5.00 ug/L
50.00
ND
101
45-169
5.24
28
53.4
5.00 ug/L
50.00
ND
107
46-157
5.05
28
49.1
5.00 ug/L
50.00
ND
98.1
59-156
6.93
28
49.2
5.00 ug/L
50.00
ND
98.4
18-190
5.71
28
49.3
5.00 ug/L
50.00
ND
98.5
18-190
6.60
28
99.3
ug/L
100.0
99.3
60-140
104
ug/L
100.0
104
60-140
110
ug/L
100.0
110
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 14 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 VOA GCMS - Quality Control
Analyte
Batch B309136
Matrix Spike Dup (B309136-MSD2) Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
Surrogate: 1,4-Difluorobenzene Surrogate: 2-Bromo-1-Chloropropane Surrogate: 1,4-Dichlorobutane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309043-09
45.3
5.00 ug/L
47.7
5.00 ug/L
6.04
5.00 ug/L
54.4
5.00 ug/L
53.5
5.00 ug/L
53.3
5.00 ug/L
53.9
5.00 ug/L
57.7
5.00 ug/L
52.5
5.00 ug/L
53.6
5.00 ug/L
53.5
5.00 ug/L
54.0
5.00 ug/L
53.5
5.00 ug/L
52.6
5.00 ug/L
54.6
5.00 ug/L
54.0
5.00 ug/L
54.4
5.00 ug/L
54.3
5.00 ug/L
9.68
5.00 ug/L
53.4
5.00 ug/L
29.9
5.00 ug/L
51.9
5.00 ug/L
51.1
5.00 ug/L
53.2
5.00 ug/L
52.0
5.00 ug/L
53.8
5.00 ug/L
53.1
5.00 ug/L
54.2
5.00 ug/L
52.0
5.00 ug/L
51.8
5.00 ug/L
52.2
5.00 ug/L
99.8
ug/L
105
ug/L
110
ug/L
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
50.00
ND
100.0 100.0 100.0
90.6
19-273
3.02
28
95.5
49-251
3.19
28
12.1
21-242
38.9
28
109
14-230
1.87
28
107
17-181
1.69
28
107
52-234 0.0188
28
108
69-221
2.49
28
115
40-160
1.90
28
105
54-156
0.324
28
107
59-155
3.12
28
107
51-138
1.54
28
108
52-162
1.16
28
107
70-140
0.967
28
105
49-155
1.51
28
109
37-151
0.657
28
108
70-157
1.16
28
109
74-210
0.476
28
109
35-155
0.477
28
19.4
80-227
44.6
28
107
47-150
1.60
28
59.8
17-183
15.9
28
104
52-150
2.17
28
102
64-148
1.73
28
106
53-149
2.28
28
104
37-160
0.230
28
108
37-162
1.29
28
106
45-169
1.88
28
108
46-157
2.41
28
104
59-156
0.479
28
104
18-190
1.13
28
104
18-190
0.191
28
99.8
60-140
105
60-140
110
60-140
Page 15 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
Blank (B310011-BLK1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
Page 16 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Batch B310011
Blank (B310011-BLK1) Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
LCS (B310011-BS1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
2.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
5.00 ug/L
--- U
2.00 ug/L
--- U
5.00 ug/L
ND
ug/L
50.00
ND
ug/L
50.00
ND
ug/L
50.00
ND
ug/L
50.00
ND
ug/L
50.00
32.2
ug/L
50.00
32.6
ug/L
50.00
39.8
5.00 ug/L
50.00
37.6
5.00 ug/L
50.00
43.3
5.00 ug/L
50.00
45.2
5.00 ug/L
50.00
46.3
5.00 ug/L
50.00
47.3
5.00 ug/L
50.00
50.3
5.00 ug/L
50.00
47.4
5.00 ug/L
50.00
45.7
60-140
21.5
60-140
41.5
60-140
40.2
60-140
13.6
60-140
64.4
60-140
65.2
60-140
79.5
47-145
75.2
33-145
86.6
27-133
90.4
33-143
92.5
17-163
94.7
24-159
101
35-219
94.8
11-162
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 17 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
LCS (B310011-BS1) Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene
44.7
5.00 ug/L
50.00
47.8
5.00 ug/L
50.00
44.2
5.00 ug/L
50.00
42.1
5.00 ug/L
50.00
50.5
5.00 ug/L
50.00
36.3
5.00 ug/L
50.00
44.0
5.00 ug/L
50.00
33.1
5.00 ug/L
50.00
30.0
5.00 ug/L
50.00
35.3
5.00 ug/L
50.00
40.7
5.00 ug/L
50.00
46.9
5.00 ug/L
50.00
45.1
5.00 ug/L
50.00
4.37
5.00 ug/L
50.00
38.0
5.00 ug/L
50.00
35.1
5.00 ug/L
50.00
3.61
5.00 ug/L
50.00
50.8
5.00 ug/L
50.00
27.4
5.00 ug/L
50.00
43.6
5.00 ug/L
50.00
41.3
5.00 ug/L
50.00
41.9
5.00 ug/L
50.00
16.0
5.00 ug/L
50.00
38.5
5.00 ug/L
50.00
36.6
5.00 ug/L
50.00
35.1
5.00 ug/L
50.00
52.2
5.00 ug/L
50.00
44.9
5.00 ug/L
50.00
45.2
5.00 ug/L
50.00
44.3
5.00 ug/L
50.00
38.9
5.00 ug/L
50.00
47.2
5.00 ug/L
50.00
50.7
5.00 ug/L
50.00
43.0
5.00 ug/L
50.00
32.8
2.00 ug/L
50.00
89.4
17-168
95.6
33-227
88.4
26-137
84.3
59-121
101
39-171
72.7
21-133
88.0
54-120
66.1
44-142
59.9
37-144
70.6
39-135
81.4
32-120
93.8
39-139
90.2
50-158
8.74
21-191
76.0
60-120
70.1
23-134
7.22
29-182
102
38-262
54.8
17-181
87.2
53-127
82.7
22-147
83.8
25-158
32.1
9-132
77.1
33-184
73.2
12-158
70.2
36-166
104
8-158
89.8
38-152
90.5
60-115
88.6
31-114
77.7
28-120
94.5
1-120
101
4-146
86.0
35-152
65.5
24-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
Page 18 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Batch B310011
LCS (B310011-BS1) Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
LCS Dup (B310011-BSD1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
34.3
5.00 ug/L
50.00
31.2
5.00 ug/L
50.00
44.4
5.00 ug/L
50.00
40.5
5.00 ug/L
50.00
25.2
5.00 ug/L
50.00
40.5
5.00 ug/L
50.00
52.4
5.00 ug/L
50.00
--- U
5.00 ug/L
50.00
17.1
2.00 ug/L
50.00
43.3
5.00 ug/L
50.00
32.4
ug/L
50.00
14.9
ug/L
50.00
31.5
ug/L
50.00
30.9
ug/L
50.00
32.8
ug/L
50.00
40.3
ug/L
50.00
40.0
ug/L
50.00
39.3
5.00 ug/L
50.00
36.7
5.00 ug/L
50.00
45.5
5.00 ug/L
50.00
46.7
5.00 ug/L
50.00
47.2
5.00 ug/L
50.00
50.0
5.00 ug/L
50.00
50.9
5.00 ug/L
50.00
47.9
5.00 ug/L
50.00
45.6
5.00 ug/L
50.00
49.0
5.00 ug/L
50.00
44.7
5.00 ug/L
50.00
47.7
5.00 ug/L
50.00
52.3
5.00 ug/L
50.00
35.1
5.00 ug/L
50.00
46.6
5.00 ug/L
50.00
31.5
5.00 ug/L
50.00
68.6
15-76
62.5
40-120
88.8
21-196
81.0
35-180
50.5
17-127
81.0
43-230
105
79-139
14-176
34.2
5-120
86.6
52-120
64.7
60-140
29.8
60-140
62.9
60-140
61.9
60-140
65.6
60-140
80.6
60-140
79.9
60-140
78.6
47-145
1.16
30
73.4
33-145
2.34
30
91.0
27-133
4.91
30
93.3
33-143
3.22
30
94.4
17-163
1.97
30
100
24-159
5.47
30
102
35-219
1.23
30
95.8
11-162
1.05
30
91.1
17-168
1.91
30
97.9
33-227
2.46
30
89.3
26-137
1.08
30
95.4
59-121
12.4
30
105
39-171
3.44
30
70.3
21-133
3.36
30
93.2
54-120
5.74
30
63.0
44-142
4.86
30
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 19 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
LCS Dup (B310011-BSD1) 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol
31.0
5.00 ug/L
50.00
36.6
5.00 ug/L
50.00
36.7
5.00 ug/L
50.00
51.7
5.00 ug/L
50.00
43.6
5.00 ug/L
50.00
3.01
5.00 ug/L
50.00
36.9
5.00 ug/L
50.00
36.8
5.00 ug/L
50.00
6.52
5.00 ug/L
50.00
52.0
5.00 ug/L
50.00
25.2
5.00 ug/L
50.00
47.7
5.00 ug/L
50.00
42.1
5.00 ug/L
50.00
47.9
5.00 ug/L
50.00
13.1
5.00 ug/L
50.00
39.3
5.00 ug/L
50.00
37.8
5.00 ug/L
50.00
35.9
5.00 ug/L
50.00
53.8
5.00 ug/L
50.00
46.2
5.00 ug/L
50.00
49.4
5.00 ug/L
50.00
47.1
5.00 ug/L
50.00
34.2
5.00 ug/L
50.00
48.0
5.00 ug/L
50.00
52.1
5.00 ug/L
50.00
45.7
5.00 ug/L
50.00
30.2
2.00 ug/L
50.00
30.1
5.00 ug/L
50.00
29.8
5.00 ug/L
50.00
45.8
5.00 ug/L
50.00
39.8
5.00 ug/L
50.00
27.1
5.00 ug/L
50.00
41.3
5.00 ug/L
50.00
57.2
5.00 ug/L
50.00
--- U
5.00 ug/L
50.00
62.1
37-144
3.51
73.2
39-135
3.64
73.3
32-120
10.4
103
39-139
9.69
87.3
50-158
3.36
6.02
21-191
36.9
73.8
60-120
2.83
73.7
23-134
4.95
13.0
29-182
57.5
104
38-262
2.20
50.3
17-181
8.41
95.5
53-127
9.09
84.3
22-147
1.94
95.8
25-158
13.3
26.3
9-132
19.8
78.6
33-184
1.93
75.6
12-158
3.23
71.9
36-166
2.28
108
8-158
2.91
92.4
38-152
2.83
98.9
60-115
8.87
94.1
31-114
6.06
68.5
28-120
12.7
96.0
1-120
1.60
104
4-146
2.67
91.5
35-152
6.13
60.3
24-120
8.26
60.1
15-76
13.1
59.6
40-120
4.75
91.7
21-196
3.21
79.6
35-180
1.74
54.1
17-127
7.00
82.6
43-230
1.93
114
79-139
8.85
14-176
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30
Page 20 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Batch B310011
LCS Dup (B310011-BSD1) Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
Matrix Spike (B310011-MS1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
18.4
2.00 ug/L
50.00
44.2
5.00 ug/L
50.00
33.9
ug/L
50.00
16.1
ug/L
50.00
30.6
ug/L
50.00
30.2
ug/L
50.00
33.1
ug/L
50.00
42.1
ug/L
50.00
40.9
ug/L
50.00
36.8
5-120
7.26
30
88.4
52-120
2.10
30
67.9
60-140
32.2
60-140
61.1
60-140
60.5
60-140
66.3
60-140
84.2
60-140
81.7
60-140
Source: 2309020-02
33.3
5.05 ug/L
33.1
5.05 ug/L
35.5
5.05 ug/L
38.6
5.05 ug/L
38.0
5.05 ug/L
37.9
5.05 ug/L
35.2
5.05 ug/L
38.2
5.05 ug/L
38.5
5.05 ug/L
35.8
5.05 ug/L
35.6
5.05 ug/L
36.7
5.05 ug/L
36.7
5.05 ug/L
22.5
5.05 ug/L
36.3
5.05 ug/L
20.2
5.05 ug/L
27.2
5.05 ug/L
26.2
5.05 ug/L
24.2
5.05 ug/L
37.3
5.05 ug/L
35.0
5.05 ug/L
9.92
5.05 ug/L
29.6
5.05 ug/L
20.9
5.05 ug/L
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
66.0
47-145
65.5
33-145
70.2
27-133
76.5
33-143
75.3
17-163
75.0
24-159
69.7
35-219
75.7
11-162
76.3
17-168
70.8
33-227
70.5
26-137
72.6
59-121
72.8
39-171
44.6
21-133
71.8
54-120
40.1
44-142
53.9
37-144
51.9
39-135
48.0
32-120
73.9
39-139
69.3
50-158
19.6
21-191
58.6
60-120
41.4
23-134
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 21 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
Matrix Spike (B310011-MS1) 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10
Source: 2309020-02
--- U
5.05 ug/L
38.0
5.05 ug/L
24.2
5.05 ug/L
37.6
5.05 ug/L
34.8
5.05 ug/L
36.9
5.05 ug/L
13.4
5.05 ug/L
28.2
5.05 ug/L
22.7
5.05 ug/L
23.1
5.05 ug/L
43.9
5.05 ug/L
37.5
5.05 ug/L
39.1
5.05 ug/L
37.7
5.05 ug/L
34.3
5.05 ug/L
38.4
5.05 ug/L
42.3
5.05 ug/L
35.5
5.05 ug/L
18.8
2.02 ug/L
16.4
5.05 ug/L
15.9
5.05 ug/L
33.4
5.05 ug/L
26.5
5.05 ug/L
15.6
5.05 ug/L
30.3
5.05 ug/L
36.9
5.05 ug/L
9.28
5.05 ug/L
12.4
2.02 ug/L
35.1
5.05 ug/L
20.0
ug/L
10.8
ug/L
21.9
ug/L
21.3
ug/L
28.7
ug/L
33.0
ug/L
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51 50.51 50.51 50.51 50.51 50.51
29-182
75.3
38-262
47.9
17-181
74.4
53-127
69.0
22-147
73.0
25-158
26.5
9-132
55.8
33-184
44.9
12-158
45.8
36-166
87.0
8-158
74.2
38-152
77.3
61-106
74.6
31-114
68.0
28-120
76.1
1-120
83.7
4-146
70.3
35-152
37.2
24-120
32.4
15-76
31.4
40-120
66.0
21-196
52.4
35-180
30.9
17-127
59.9
43-230
73.0
79-139
18.4
14-176
24.5
5-120
69.5
52-120
39.6
60-140
21.3
60-140
43.3
60-140
42.1
60-140
56.7
60-140
65.4
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
Page 22 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Batch B310011
Matrix Spike (B310011-MS1) Surrogate: Chrysene-D12
Matrix Spike (B310011-MS2) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Source: 2309020-02
34.0
ug/L
Source: 2309043-01
38.3
5.56 ug/L
37.9
5.56 ug/L
45.4
5.56 ug/L
45.6
5.56 ug/L
49.3
5.56 ug/L
47.3
5.56 ug/L
51.2
5.56 ug/L
49.0
5.56 ug/L
45.6
5.56 ug/L
50.9
5.56 ug/L
44.9
5.56 ug/L
46.0
5.56 ug/L
54.1
5.56 ug/L
28.7
5.56 ug/L
47.0
5.56 ug/L
26.2
5.56 ug/L
38.1
5.56 ug/L
34.2
5.56 ug/L
32.1
5.56 ug/L
50.8
5.56 ug/L
41.4
5.56 ug/L
22.2
5.56 ug/L
34.9
5.56 ug/L
28.4
5.56 ug/L
7.80
5.56 ug/L
41.2
5.56 ug/L
40.9
5.56 ug/L
47.6
5.56 ug/L
41.7
5.56 ug/L
45.7
5.56 ug/L
20.5
5.56 ug/L
34.4
5.56 ug/L
50.51
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
67.4
60-140
68.9
47-145
68.2
33-145
81.8
27-133
82.0
33-143
88.7
17-163
85.1
24-159
92.2
35-219
88.2
11-162
82.0
17-168
91.7
33-227
80.8
26-137
82.8
59-121
97.3
39-171
51.7
21-133
84.6
54-120
47.2
44-142
68.6
37-144
61.5
39-135
57.8
32-120
91.4
39-139
74.6
50-158
39.9
21-191
62.8
60-120
51.1
23-134
14.0
29-182
74.1
38-262
73.6
17-181
85.6
53-127
75.1
22-147
82.3
25-158
36.8
9-132
61.9
33-184
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
Page 23 of 33
Analyte
Batch B310011
Matrix Spike (B310011-MS2) Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309043-01
30.6
5.56 ug/L
31.6
5.56 ug/L
54.1
5.56 ug/L
48.1
5.56 ug/L
48.5
5.56 ug/L
46.7
5.56 ug/L
33.3
5.56 ug/L
50.0
5.56 ug/L
54.6
5.56 ug/L
47.3
5.56 ug/L
25.2
2.22 ug/L
21.8
5.56 ug/L
21.1
5.56 ug/L
39.8
5.56 ug/L
33.2
5.56 ug/L
20.5
5.56 ug/L
36.9
5.56 ug/L
48.1
5.56 ug/L
23.0
5.56 ug/L
15.5
2.22 ug/L
44.2
5.56 ug/L
25.9
ug/L
13.5
ug/L
27.5
ug/L
27.3
ug/L
34.6
ug/L
42.9
ug/L
40.4
ug/L
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56
ND
55.56 55.56 55.56 55.56 55.56 55.56 55.56
55.0
12-158
57.0
36-166
97.4
8-158
86.6
38-152
87.3
61-106
84.1
31-114
60.0
28-120
90.0
1-120
98.3
4-146
85.1
35-152
45.4
24-120
39.2
15-76
38.0
40-120
71.6
21-196
59.7
35-180
36.9
17-127
66.4
43-230
86.7
79-139
41.5
14-176
27.9
5-120
79.6
52-120
46.7
60-140
24.3
60-140
49.6
60-140
49.2
60-140
62.4
60-140
77.2
60-140
72.8
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 24 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
Batch B310011
Matrix Spike Dup (B310011-MSD1) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate
Source: 2309020-02
41.6
5.05 ug/L
42.0
5.05 ug/L
48.2
5.05 ug/L
50.6
5.05 ug/L
51.5
5.05 ug/L
50.8
5.05 ug/L
49.4
5.05 ug/L
51.8
5.05 ug/L
50.1
5.05 ug/L
50.0
5.05 ug/L
48.4
5.05 ug/L
51.2
5.05 ug/L
52.8
5.05 ug/L
33.5
5.05 ug/L
50.2
5.05 ug/L
28.7
5.05 ug/L
39.4
5.05 ug/L
38.7
5.05 ug/L
28.7
5.05 ug/L
55.8
5.05 ug/L
45.4
5.05 ug/L
18.0
5.05 ug/L
39.3
5.05 ug/L
28.3
5.05 ug/L
10.6
5.05 ug/L
45.2
5.05 ug/L
39.0
5.05 ug/L
50.9
5.05 ug/L
45.1
5.05 ug/L
50.4
5.05 ug/L
18.2
5.05 ug/L
42.5
5.05 ug/L
32.3
5.05 ug/L
35.1
5.05 ug/L
57.8
5.05 ug/L
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
50.51
ND
82.3
47-145
22.0
83.1
33-145
23.7
95.4
27-133
30.4
100
33-143
26.7
102
17-163
30.1
101
24-159
29.2
97.9
35-219
33.7
102
11-162
30.0
99.2
17-168
26.2
99.0
33-227
33.1
95.7
26-137
30.4
101
59-121
33.0
105
39-171
35.8
66.2
21-133
39.0
99.4
54-120
32.2
56.9
44-142
34.8
78.0
37-144
36.5
76.7
39-135
38.5
56.8
32-120
16.8
111
39-139
39.8
89.9
50-158
25.9
35.6
21-191
57.8
77.8
60-120
28.2
55.9
23-134
29.9
21.0
29-182
89.5
38-262
17.2
77.2
17-181
46.8
101
53-127
30.0
89.3
22-147
25.7
99.8
25-158
31.0
36.0
9-132
30.4
84.1
33-184
40.5
64.0
12-158
35.0
69.4
36-166
41.1
114
8-158
27.3
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD Limit
24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24
Page 25 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Batch B310011
Matrix Spike Dup (B310011-MSD1) Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
Matrix Spike Dup (B310011-MSD2) Acenaphthene Acenaphthylene Anthracene Benzo(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(G,H,I)Perylene Benzo(K)Fluoranthene
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309020-02
50.8
5.05 ug/L
50.51
ND
101
38-152
30.2
24
53.5
5.05 ug/L
50.51
ND
106
61-106
31.2
24
52.0
5.05 ug/L
50.51
ND
103
31-114
32.0
24
41.6
5.05 ug/L
50.51
ND
82.4
28-120
19.2
24
51.8
5.05 ug/L
50.51
ND
103
1-120
29.6
24
57.1
5.05 ug/L
50.51
ND
113
4-146
29.8
24
49.3
5.05 ug/L
50.51
ND
97.5
35-152
32.4
24
25.9
2.02 ug/L
50.51
ND
51.3
24-120
31.9
24
24.5
5.05 ug/L
50.51
ND
48.5
15-76
39.8
24
17.0
5.05 ug/L
50.51
ND
33.7
40-120
6.88
24
46.9
5.05 ug/L
50.51
ND
92.9
21-196
33.8
24
39.9
5.05 ug/L
50.51
ND
79.0
35-180
40.4
24
17.0
5.05 ug/L
50.51
ND
33.6
17-127
8.43
24
45.1
5.05 ug/L
50.51
ND
89.2
43-230
39.3
24
51.1
5.05 ug/L
50.51
ND
101
79-139
32.4
24
19.2
5.05 ug/L
50.51
ND
37.9
14-176
69.5
24
17.4
2.02 ug/L
50.51
ND
34.5
5-120
33.6
24
47.5
5.05 ug/L
50.51
ND
94.0
52-120
29.9
24
25.8
ug/L
50.51
51.1
60-140
15.1
ug/L
50.51
29.8
60-140
32.4
ug/L
50.51
64.1
60-140
31.3
ug/L
50.51
62.0
60-140
37.5
ug/L
50.51
74.3
60-140
46.4
ug/L
50.51
92.0
60-140
45.8
ug/L
50.51
90.7
60-140
Source: 2309043-01
36.5
5.62 ug/L
56.18
ND
65.0
47-145
4.83
24
36.3
5.62 ug/L
56.18
ND
64.7
33-145
4.09
24
48.1
5.62 ug/L
56.18
ND
85.7
27-133
5.77
24
49.1
5.62 ug/L
56.18
ND
87.4
33-143
7.44
24
49.8
5.62 ug/L
56.18
ND
88.6
17-163
1.05
24
49.6
5.62 ug/L
56.18
ND
88.3
24-159
4.74
24
49.1
5.62 ug/L
56.18
ND
87.4
35-219
4.27
24
50.6
5.62 ug/L
56.18
ND
90.1
11-162
3.34
24
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 26 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Result
Reporting Limit
Units
Spike Level
Source Result
%REC
%REC Limits
Batch B310011
Matrix Spike Dup (B310011-MSD2) Chrysene Dibenzo(A,H)Anthracene Fluoranthene Fluorene Indeno(1,2,3-Cd)Pyrene Naphthalene Phenanthrene 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2,4-Dinitrophenol 2-Chloronaphthalene 2-Chlorophenol 2-Nitrophenol 3,3'- Dichlorobenzidine 4,6-Dinitro-2-Methylphenol 4-Bromophenyl-Phenylether 4-Chloro-3-Methylphenol 4-Chlorophenyl-Phenylether 4-Nitrophenol Bis(-2-Chloroethoxy)Methane Bis(2-Chloroethyl)Ether Bis(2-Chloroisopropyl)Ether Bis(2-Ethylhexyl)Phthalate Butylbenzylphthalate Azobenzene Diethylphthalate Dimethyl Phthalate Di-N-Butyl Phthalate Di-N-Octyl Phthalate Hexachlorobenzene Hexachlorobutadiene
Source: 2309043-01
49.3
5.62 ug/L
49.2
5.62 ug/L
46.1
5.62 ug/L
50.3
5.62 ug/L
50.2
5.62 ug/L
25.6
5.62 ug/L
50.1
5.62 ug/L
22.6
5.62 ug/L
37.8
5.62 ug/L
33.1
5.62 ug/L
25.7
5.62 ug/L
56.6
5.62 ug/L
42.1
5.62 ug/L
22.3
5.62 ug/L
32.6
5.62 ug/L
24.0
5.62 ug/L
8.39
5.62 ug/L
41.1
5.62 ug/L
44.0
5.62 ug/L
51.7
5.62 ug/L
41.6
5.62 ug/L
50.2
5.62 ug/L
20.4
5.62 ug/L
33.1
5.62 ug/L
25.2
5.62 ug/L
27.6
5.62 ug/L
59.2
5.62 ug/L
47.6
5.62 ug/L
52.4
5.62 ug/L
51.2
5.62 ug/L
31.7
5.62 ug/L
51.7
5.62 ug/L
59.8
5.62 ug/L
50.5
5.62 ug/L
21.0
2.25 ug/L
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
56.18
ND
87.8
17-168
87.5
33-227
82.0
26-137
89.6
59-121
89.3
39-171
45.6
21-133
89.3
54-120
40.3
44-142
67.2
37-144
58.9
39-135
45.8
32-120
101
39-139
74.9
50-158
39.6
21-191
58.0
60-120
42.7
23-134
14.9
29-182
73.2
38-262
78.2
17-181
92.1
53-127
74.0
22-147
89.3
25-158
36.4
9-132
59.0
33-184
44.9
12-158
49.2
36-166
105
8-158
84.7
38-152
93.2
61-106
91.2
31-114
56.5
28-120
92.1
1-120
106
4-146
89.8
35-152
37.3
24-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
RPD
7.90 3.50 2.59 8.91 7.43 11.4 6.52 14.7 0.915 3.24 22.2 10.8 1.57 0.363 6.96 16.7 7.33 0.159 7.28 8.36 0.331 9.37 0.0299 3.68 19.1 13.6 8.97 1.05 7.65 9.20 4.93 3.38 9.01 6.56 18.3
RPD Limit
24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24 24
Page 27 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 NVOA GCMS - Quality Control
Analyte
Batch B310011
Matrix Spike Dup (B310011-MSD2) Hexachlorocyclopentadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodimethylamine N-Nitroso-Di-N-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyrene
Surrogate: 2-Fluoroaniline Surrogate: Phenol-D6 Surrogate: Naphthalene-D8 Surrogate: 1-Fluoronaphthalene Surrogate: 2,4-Dibromophenol Surrogate: Anthracene-D10 Surrogate: Chrysene-D12
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309043-01
17.7
5.62 ug/L
56.18
ND
31.6
15-76
20.5
24
15.6
5.62 ug/L
56.18
ND
27.8
40-120
29.9
24
39.0
5.62 ug/L
56.18
ND
69.4
21-196
1.95
24
29.4
5.62 ug/L
56.18
ND
52.4
35-180
11.9
24
16.4
5.62 ug/L
56.18
ND
29.2
17-127
22.1
24
35.7
5.62 ug/L
56.18
ND
63.5
43-230
3.35
24
52.3
5.62 ug/L
56.18
ND
93.0
79-139
8.22
24
25.2
5.62 ug/L
56.18
ND
44.9
14-176
9.12
24
14.7
2.25 ug/L
56.18
ND
26.1
5-120
5.69
24
45.2
5.62 ug/L
56.18
ND
80.5
52-120
2.29
24
21.0
ug/L
56.18
37.4
60-140
13.0
ug/L
56.18
23.2
60-140
24.9
ug/L
56.18
44.3
60-140
24.4
ug/L
56.18
43.4
60-140
34.2
ug/L
56.18
60.9
60-140
45.3
ug/L
56.18
80.6
60-140
43.9
ug/L
56.18
78.1
60-140
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 28 of 33
Analyte
Batch B310062 Blank (B310062-BLK1)
Petroleum Hydrocarbons, Tot.
LCS (B310062-BS1) Petroleum Hydrocarbons, Tot.
LCS Dup (B310062-BSD1) Petroleum Hydrocarbons, Tot.
Matrix Spike (B310062-MS1) Petroleum Hydrocarbons, Tot.
Matrix Spike (B310062-MS2) Petroleum Hydrocarbons, Tot.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 GC - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
5.00 mg/L
37.1
5.00 mg/L
40.00
93
64-132
35.4
5.00 mg/L
40.00
88
64-132
5
20
Source: 2309020-03
58.0
6.17 mg/L
49.38
0.506
116
64-132
Source: 2309043-03
51.2
5.81 mg/L
46.51
4.32
101
64-132
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 29 of 33
Analyte
Batch B309146
Blank (B309146-BLK1) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
LCS (B309146-BS1) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
LCS Dup (B309146-BSD1) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 Metals ICP - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
8.00 ug/L
--- U
100 ug/L
--- U
3.00 ug/L
--- U
5.00 ug/L
--- U
10.0 ug/L
--- U
8.00 ug/L
--- U
20.0 ug/L
--- U
20.0 ug/L
--- U
5.00 ug/L
--- U
20.0 ug/L
199
8.00 ug/L
200.0
202
100 ug/L
200.0
198
3.00 ug/L
200.0
199
5.00 ug/L
200.0
197
10.0 ug/L
200.0
201
8.00 ug/L
200.0
200
20.0 ug/L
200.0
199
20.0 ug/L
200.0
200
5.00 ug/L
200.0
204
20.0 ug/L
200.0
198
8.00 ug/L
200.0
202
100 ug/L
200.0
198
3.00 ug/L
200.0
199
5.00 ug/L
200.0
196
10.0 ug/L
200.0
201
8.00 ug/L
200.0
200
20.0 ug/L
200.0
199
20.0 ug/L
200.0
200
5.00 ug/L
200.0
204
20.0 ug/L
200.0
99.7
85-115
101
85-115
99.2
85-115
99.7
85-115
98.3
85-115
100
85-115
99.9
85-115
99.4
85-115
99.8
85-115
102
85-115
99.2
85-115
0.503
20
101
85-115 0.0397
20
99.2
85-115 0.0151
20
99.6
85-115 0.0903
20
98.2
85-115 0.0763
20
101
85-115
0.214
20
100
85-115 0.0550
20
99.4
85-115 0.0855
20
99.9
85-115 0.0952
20
102
85-115 0.0734
20
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 30 of 33
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 Metals ICP - Quality Control
Analyte
Batch B309146
Matrix Spike (B309146-MS1) Cadmium Chromium Lead Zinc
Matrix Spike (B309146-MS2) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
Matrix Spike Dup (B309146-MSD1) Cadmium Chromium Lead Zinc
Matrix Spike Dup (B309146-MSD2) Arsenic Barium Cadmium Chromium Copper Lead Nickel Selenium Silver Zinc
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
Source: 2309020-01
201
3.00 ug/L
200
5.00 ug/L
295
8.00 ug/L
302
20.0 ug/L
Source: 2309043-08
205
8.00 ug/L
340
100 ug/L
195
3.00 ug/L
201
5.00 ug/L
277
10.0 ug/L
198
8.00 ug/L
194
20.0 ug/L
201
20.0 ug/L
200
5.00 ug/L
219
20.0 ug/L
Source: 2309020-01
201
15.0 ug/L
195
25.0 ug/L
294
40.0 ug/L
299
100 ug/L
Source: 2309043-08
204
40.0 ug/L
337
500 ug/L
197
15.0 ug/L
199
25.0 ug/L
271
50.0 ug/L
198
40.0 ug/L
196
100 ug/L
205
100 ug/L
197
25.0 ug/L
220
100 ug/L
200.0 200.0 200.0 200.0
0.750 ND 92.6 90.3
100
80-120
100
80-120
101
80-120
106
80-120
200.0
ND
200.0
142
200.0
ND
200.0
2.34
200.0
78.8
200.0
ND
200.0
2.83
200.0
ND
200.0
ND
200.0
19.7
103
80-120
98.9
80-120
97.5
80-120
99.2
80-120
99.2
80-120
98.8
80-120
95.8
80-120
101
80-120
100
80-120
99.7
80-120
200.0
ND
100
80-120 0.0796
10
200.0
ND
97.6
80-120
2.44
10
200.0
92.6
101
80-120
0.258
10
200.0
90.3
104
80-120
1.15
10
200.0
ND
102
80-120
0.773
10
200.0
142
97.6
80-120
0.753
10
200.0
ND
98.4
80-120
1.01
10
200.0
ND
99.6
80-120
0.740
10
200.0
78.8
96.2
80-120
2.21
10
200.0
ND
98.9
80-120 0.0708
10
200.0
ND
98.0
80-120
0.856
10
200.0
ND
103
80-120
2.05
10
200.0
ND
98.5
80-120
1.72
10
200.0
19.7
100
80-120
0.442
10
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 31 of 33
Analyte
Batch B310050 Blank (B310050-BLK1)
Mercury
LCS (B310050-BS1) Mercury
LCS Dup (B310050-BSD1) Mercury
Matrix Spike (B310050-MS1) Mercury
Matrix Spike (B310050-MS2) Mercury
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 Mercury CVAA - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
0.050 ug/L
0.965
0.050 ug/L
1.000
96.5
85-115
0.962
0.050 ug/L
1.000
96.2
85-115
0.311
20
Source: 2309020-01
0.980
0.050 ug/L
1.000
ND
98.0
80-120
Source: 2309043-08
0.978
0.050 ug/L
1.000
ND
97.8
80-120
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 32 of 33
Analyte
Batch B310002 Blank (B310002-BLK1)
Fluoride
Blank (B310002-BLK2) Fluoride
LCS (B310002-BS1) Fluoride
LCS Dup (B310002-BSD1) Fluoride
Matrix Spike (B310002-MS1) Fluoride
Matrix Spike (B310002-MS2) Fluoride
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 2 Laboratory
Final Report Project: Thomas Electronics - 2309020
Project Number: 2309020 Sanitary - Quality Control
Result
Reporting Limit
Units
Spike
Source
%REC
Level
Result %REC Limits
RPD
RPD Limit
--- U
0.0500 mg/L
--- U
0.0500 mg/L
4.46
0.0500 mg/L
4.860
92
90-110
4.50
0.0500 mg/L
4.860
93
90-110
0.9
20
Source: 2309020-01
40.5
0.500 mg/L
2.000
40.0
25
90-110
Source: 2309043-08
2.38
0.0500 mg/L
2.000
0.550
92
90-110
U.S.E.P.A Region 2 Laboratory
NOTE: The results recorded in this report relate only to the samples as received on the date and at the time noted Reported: 10/17/2023
Page 33 of 33
Thomas Electronics, Clyde (V), NY 07860 NPDES Permit: NYP080230
Inspection Date: September 26, 2023
8.0 Photographs
Thomas Electronics, Clyde (V), NY 07860 NPDES Permit: NYP080230
Inspection Date: September 26, 2023
Photo #1. Compliance samples were collected from the monitoring location (Sample Box).
Photo #2. RO backwash was discharging continuously into the Sample Box.
Thomas Electronics, Clyde (V), NY 07860 NPDES Permit: NYP080230
Inspection Date: September 26, 2023
Photo #3. Discharge of pretreated effluent was intermittent into the Sample Box (grey pipe).
