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TABULATION OF RESPONSES pg 1 of 7 Company OaeiQnation Set Pressure Con*ideretions Reactor Six* (US6) Vessel Rating tpslg) RO Sit* In Series with $V ? <in. ) RO Burst P 0 72F (psig) Design Burst T (F) Burst P 1 Burst T (psig) Manufacturing Range-over/under(X ) Special manufacturing range 7 Burst tolerance (1) Special burst tolerance 7 SV capacity red*n due to RO (X) SV setting (psig) c0 Manufacturing and Installation SO Typa Manufacturer Nunber of disc* per location Oise Material Disc orientation device Torque requirenents used 7 Discs not recommended-type -reason teal detection device Vent method for space above RO Vent destination Press monitoring fraq for space Frequency of RD leaks Frequency of RO pin-holes RO fouling prevention nethod RO inspection freq (react cycles) Type of inspec tion RO replacenent freq (no.s) Genera 1 Present concerns Number of failures in 1964 Fat lure causes-t. -2. -3. Overpressure ever occurred 7 Overpressure amount (psig) Last overpressure Overpressure causes- 1 . -2. Other comments A B C0 3709 209 4 yes 200 135 194 10/5 no 5 no 0 IBS 17000 170 8 yes 160 130 1S6 10/5 no 5 no 0 155 4-8 yea 90-95X of VPR 0/0 yes 5 no <1X 90-100X of VPR 34000 130 6 end 8 yes 178-195 168-177 175-190 0/0 no 2 no none sene as RO 3600 265 2*6 no 260 212 235 0/0 S no pr^tcor^d and bulgad Fike Poly SO t nickel 10 tag no complete discs premature failure pressure gauge RO manual valva atmosphere rarely rarely routine inspect ion 1-3 visual 6 prase * bulged 8S&8/6FN 16 nickel none no vac supp/knife , leaks/no good for hydrostats red ball ind j rad balKSpsig) atn >6mos never water spray 3-5days visual 6 rev. knife gate Continental KBA/ZAP nickel/teflon ZAP holder no Rev. buckling Marston Palmer 1 SS Spigot on carrier yes pressure gauge manual block atn 3X/day none none clean hdr every no 600 pressure test 24 close to reac replace 3 10 preasure test physical damage no 0-5 fatIgue no 0-5 nishandl mg reactor hydrostat Jprenature failures :screwt loosening 6 unknoun no no Recommend sol id nickel discs 1 1 i :do not use ! knife discs 1:do not use VS discs ^preventive disc changes :water spray on discs :Keep RO close to reac tor :Use ZAP holder to prevent faulty installation :Tram mtee people RD technology is continuing to advance EF G 10S00 330 12 no 291 160 273 0/0 yes S yes 100 m3 23 berg 16 no 2S.3 barg 157 24.1 ba^g 5/5 no 5 no 6600 2 IS 4 yes 230 7 205 0/5 no 5 no 20 2 IS Conv. domed Marston Palmer ii Aluminum Carrier spigot no Vacuum supported Obstruction of blest pipe 1 visual 225 cycles Reverse buck 1 mg scored,tension 1 oade 85&B S-90 as&e GFN 1ncone1 Pins yes SS 316 J bolts no press.switch auto back to reactor never never 2nd RO at low P 6-12 mo's V|1U*1 46 press, md. manual valve b1Ower sue 11on 3 hr s once/year very rare l y coat with inhibitor 4 visual 12 Creep failure of A1 0 0 none no no no tCurrent disc :6ood experience reliable but has with BS&8'a. a short life. Reverse buckling RO may be bet ter :Auxi1iary system relieves at 601 of mam System for small overpressures. CTL0199S6 Company Designation Set Pressure Constderations Peector Size (U5G> Vessel Rating (psig) RO Size <in. ) In Series with SV 7 s0 Burst P 72F (ps ig ) Design Burst T <F > Burst P $ Burst T (psig) Manufacturing Range-over/under<X > Special nanufacturing range 7 Burst tolerance Special burst tolerance 7 SV capacity red'n due to RO (X) SV setting (psig) RC flanufacturing and Installation PO Typa Manufacturer Number of discs per location Oise Material Oise orientation device Torque requirements used 7 Discs not reconnended~type -reason Leak detection device Vent method for space above RO Vent dest mat ion rress monitoring freq for space Frequency of RO leaks Frequency of RO pin-holes RO fouling prevention method 0 inspection freq (react cycles) Type of inspec 11on RO replacement freq (no.a) Genera 1 sresen{ concerns Number of failures in 1984 railure causes-l. -2. -3. Overpressure ever occurred 7 Overpressure amount (psig) Last overpressure Overpressure causes-l. *2. Other comments TABULATION OF PSL of 7 > f H IJ KL n 20000 300 12 yes 312 363 270 S/5 no 2 no 20 270 34100 300 6 yes 196 162 5.9/1.6 yes 2 yes 0 165 10000 100 6*6 no 105 no 5 no none 90 6000 235 5.91 yes 158 232 10/10 yes 10 yes not available 232 3700 206 6 yes 228 212 180 180 20000 220 2*611 *8 Yes(for 6" ROs ) 237 200 6'-210i8*-225 2 no none 200 KBA rev buckling Continental 1 SS 316 none yes Crosby Pinholing press, gauge not vented every batch never never water spray 4X per year visual <12 prescoredfbulged Osaco E-0B57-01 4 SS 316/TFE/SS316 special holder no graphita/braas cracking/reacts with VCM tattle-tale gauge none atm reverse buckling BS&B S-90 22 nickel J bolts yes * all others premature failure once/year rare none none Close to vessel none 12 24 prescored+buigad Fika.Poly S-0 150 1 316 SS none no reversing Not allowed by law if hydrostat possible. Pressure ind. none BV BS&B SS/TFE special holder no pressure ind. none rev. acting insert Cont manta 1 -KBA 3 3I6SS/TFE special holder yes PI none 2-4 X per year only once Uash every batch 1 v i sua J 2-6 S0X of all ROs SOX of all ROs RO on cooled nozzle daily vi sua 1 6(due to 1 eaks ) _ once in 3 yrs coo 1ed noz z1e 2-3 v i sua 1 9 Plugs below RO 5 Poor quality RO no Cannot inspec t 0-5 press/vac fle*mg high temp. no none none overpressure no :Good experience with Continental discs Most failures due to pressure/vac cycling :Corrosion of SS Rl led to failure. No problems with nickel discs. rPressure test if vessel removed from service. Satisfied none none none 5-20 Faulty manufacture 0-5 faulty manufacture yes 215 1962 Back-up pressure Fouling Vacuum supported discs susceptible to fouling. no :Use PI to detect pressure above RO :Cool nozzle under PO to prevent PO 1 yner nation. no CTL019997 TABULATION OF TT^P I | | I I-onpa"* Oes i 3t> l ion N 0 P QR 5 :* Pressure Considerations ea::jr Sire (US6) Rat : ng (psig> (in. > :*-ies .`th SV 7 =-T*t 3 t 72F t pa ig ) 2es . ;** Bur a t T (F ) a-r **. 9 9 rjrit T ( ps ig ) hsn. *`sc tur ; ng Range-Over/under ( X ) ssei.i! nanj fee tuning range 7 ?-rtt *.ole- a nee (X) isei.ii buT'st tolerance 7 r.- sicacit* refl'n due to RO (X) 5/ #*. ting ( PS IQ > { 6600 zse 4 no 176 274 10/0 yes 10 yes none - 7250 312 6 yes 276 175 256 S/0 no 5 yes - 256 5300 - 6 yes - 175 2S0 5/5 yes 0 250 ; 20000 224 6 yes - 190 211 0/0 no 5 no 1 .4 21 1 6600 217 0 no 277 158 250 11 no - 84S0 217 8 no 277 158 250 I1 no - : -- He-u'ac tu-i ng and Installation *i0 '.se tan.4ctur er **an:-r of aiscs oer location 2`is: Material >isr orientation device ora*e requirements used ? L'isrt not r*econnended-type -reason -ee* detection device **ent lho3 for space above RO ten* oast i-,*t ion "ren monitoring freq for space --ea-.ncy s* RO le.k. "-es^eney ;f RO oin-hole. 4 iv*i i ng prevention nethod 3- ."ssectipn freq (react cycles) os :1 inspection 3j 'talace"ent freo (no.s) r-^na-e. " 'etri Cc"*:erns of 'silu^ea in 1984 *a:._rs Ca.jes-I . -2. plain Sigri-n 1 Oraphite none no Elfab-Hughes Cannot install between flanges. - - none once/nonth visual 24 Scored BS10-6FN or S-90 1 SS J bolts yes BS&B RB90 RO nay reverse against knives without rupture pressure gauge - atn every batch - disc location daily visua1 1000-2000 batches Rev buckling Johnson flatthey 1 nickel arrow on unit no none - P6 with ind nanuel valve atn every batch 2/yr never none t visua1 at failure none 0 Tension problens none 0 Wrong installation, handling or knife damage 0-S per react. Oaforned by cleaning Wrong joints Prescored*bulged bu1ged Fike Poly 50 6 nickel disc tao no reverse buckling 9S&B t ype BU 1 316SS none none graphite ,rev.buck. Engineering dept doefouling,hydrostatic not allow then. overfill P6 and alarn nanual valve atn continuous none in 3 yrs none in 3 yrs reactor coating 150 v i sua1 24 Alu fol 1 under dt sc 4 Curvature QduQe 4 batches.Re-use t f inspect ion OK bulged 8510 type 6'/ 1 31655 none none graohite fouling * Alu-foil under disc '150 replaced 150 Occasional plugoage none none none none none 1 t' irtssu-e ever occurred T -e-renu-e amount .**. :erp-essure 1 .e't'tisure causes-l. -? , (psig ) yea 284 1980 Bad housing no ^Tension freo installation in o metal 5S housing. :Exhaust pipe should be larger than inlet pipe. Bad experience with 6S1B RB90(see above) no Interested in disc systems that prevent wrong installations, work for liquid and for vapour, and can be cleaned without RO danage. no ye no 305 1975 overfilled CTL019998 TABULATION OF pg 4 of 7 Company Designation Set Pressure Coneideretioni Reactor Size (US6) Vessel Rating (psig) RO Size (in.) In Series with SV 7 RO Burst P 9 72F (psig) OesIon Burst T (F > Burst P 9 Burst T (psig) Manufacturing Reno*-over/under ( X ) Special manufacturing range 7 Burst tolerance (X) Special burst tolerance 7 SV capacity red`n due to RO (X) SV setting (psig) RO Manufacturing end Installation RO Type Manufacturer Number of discs per location Oise Materiel Oise orientation device Torque requirements used ? Oiscs not recommended-type -reason Leek detection device Vent method for space above RO Vent destination Press monitoring freq for apace Frequency of RO leaks Frequency of RO pin-holes RO fouling prevention method RO inspection freq (react cycles) Type of inspection RO replacement freq (no.e) 6enera1 Present concerns Number of failures in 1964 Failure causes-1. -2. -3. Overpressure ever occurred 7 Overpressure amount (psig) Last overpressure Overpressure causes-1. Other comments T U V uX Y 2000 300 3 yes 169 tee 2/2 no 2 no 0 too 4000 300 3 yes 189 180 2/2 no 2 no 0 180 no 10/5.2 no 5 no 0 yes 10.9/5.7 no 5 no NOA 13200 240 8 no 135 232 2/2 no 24000 200 18 yes 195 183.5 190 0/3 no 5 no 20 200 reverse buckling Continentel-Zap 3I6SS holder guide rings yes none pilot valve pilot valve atm every 2 weeks none teflon liner 10 press, test 10 cycles reverse buckling Continental-Zap I 3I6SS holder guide rings yes pilot valve pilot valve atm once every 2 wks teflon liner to pressure test 10 cycles Oual Presc.* bulge Proquip OV80 2 SS/TFE/SS Speciel holder yes nickel-sealed Pinhollng due to P fluctuations. P6 and alarm 10 psig rel. vlv. atm none since *85 none since *85 water spray I visual 6-12 Pres bulge w/ VS Proquip 0V80 2 31 6SS/Incone 1/31ESS vent side marked yes reverse buckling Corrosion of knife blades. P switch alarm 10 psig Nupro RV atm 15 sec none none Fouling inhibitor 400 Visua1<lampmirror) 8 Rev buck/km fe Continenta1-Zap 8 31GSS none no P alarm switch manual valve atm continuous <I per year Only once TFE 1 ined R0 500 visual in place on failure Prescored bulged BS&B 77-37-009-45 4 nickel J bolt s no Tell-tale P switch excess flow valve atm none Fouling inhibitor 10-15 v i sua1 12 Installation of disc holder on reactor 5-20 bad holder mi shandling corrosion yes 190 I 984 fouling Installation of disc and holder 5-20 Bad holder Handlihg of unit Corrosion yes 190 1984 Fouling -Follow manufacturer's instruct ions. -Bench P test every disc before use. i -Most important to assure even torquing of disc in hoider and of holder in f tenges. -Follow manufacturer ' s 1 ns true tions. -Bench P test every disc before use. -Most important to assure even torquing of disc in holder and of holder in f langes. TFE pinching during installet ion. >20 Ptnholing of Ni RGs Pinching of TFE line Installation damage 0 rs Inspection freq. Ou1 Satisfied knives. Corrosion none 0-5 Hydrostatic overfjli no Nickel sealed dual element ROs not recommended due to turt1ebacking. TFE discs require careful installation no yes 30 no 1984 Dull knife b 1 ades Valve leak under R0 in a dual assembly Must install properl CTLO19999 TABULATION OF pg 5 of 7 Company Designation Sat Pressure Considerations Reactor Size (US6> l i Vessel Rating (psig) RO 51ze <in. ) In Series with SO 7 RO Bunt P 72F <psig> Oesion Burst T (F 1 Bunt P * Bunt T (psig ) Manufacturing Range-over/under(X) Special manufacturing range ? Burst tolerance (*) I I Special burst tolerance 7 5V capacity red'n due to RO (1) SO setting (ptig) Z 16000 270 12 yet 312 363 270 2/2 no s no 0 270 4300 290 B yea 207 167 200 0/0 yea 5 no IS 210 AA 18600 300 12 yes 295.5 190 221 0/5 no 5 no IS 2S0 4000 227 4 no 227 0/0 yes 5 no " 4300 250 4 no 249 0/5 no 5 no - I AB 14000 232 no 180 225 ** - AC 16000 300 10 yes 263/283 196 205-215/260-276 no no none 215/2SS AO 16510 300 12 yes 190 250 5/5 no 5 no none 231 RO ftanuf ac tur i ng and Installation RO Type Manufacturer Number of discs per location Oise Material Oise orientation device Torque requirements used 7 Oisca not recommended-type 'reason Leak detection device Vent method for space above RO Vent destination Press monitoring freq for space Frequency of RO leaks Frequency of RO pin-holes RO fouling prevention method RO inspection freq (react cycles) Type of inspect ton RO replacement freq Imo.s) Reverse acting knife Preacored + bulged Rev buck. bulged Continental K8A BS&B 6FN 8S&B-S90 8S&B-BV 1 16 16 12 3I6SS Ni Ni Ni Knives prevent error Olac Tab Oise tab Oise teb yea Yea yes no aluminum,silver Type OV/ BV under SV HC1 corrosion -fragmentation -cycling P tattletale gauge P switch ind P switch <- excess flow valve low P relief valve <- <- atm atm atm atm - - -- "2/yr rarely never never "2/yr never never never antifoulant.water spray HPU wash 100 to 1 year visual 12 -------- 6- 12 reverse buckling bulged rev buck.(unscored) BS&B RB-90 BS&B Elfab Hughes RK76 2*2 2 1 Ni nickel 3I6SS none sandwich links Disc tag yes yea no - reverse buck 11ng graphite.scored - Premature failure in fragmentation cycling service. excess flow valve P switch alarm P gauge excess flow valve 10 psig RV 10 psig RV - atm atm very seldom 1 /yr never very seldom none causing P never none inhibitor coating inhib11or coating 800 300 130 t v i sua1 v i sua1 randomly each year 12 12 sanerel Present concerns Number of failures in 1994 Failure causes'!. -2. Overpressure ever occurred 7 Overpressure enount (psig) Last overpressure Overpressure causes-l. -2. Other comment s Nozzle plugs under discs. 2 ? no 'Oamage by HPU wash 'Improper torqutng 6 -10 Oamage by HPU Improper torquing No - 6FN end S90 ROs ere prone to damage by HPU - Nozzle plugs were common until inhibitor used none 0 - not recently 3 pioho 1 e leaks -handling hydrostats -de f orna tion 0 no Mirufuze piping between RO and reactor. -Paper gaskets allow l eak-11ght seals Detween RO ana ho 13er. -2 ROs in series are unsatis tactor t Cue to the shock-wave effect of tre 'irn St SC Dwrslirg, CTL020000 TABULATION OF USES pg 6 of 7 1K AF AS lo-csny Designation set Pressure Conslderations :ssctor 5ixe (US6 > .tisel Rating s0 Sue (psig) ( i n. ) I- Series with SV 7 =3 Burst P I 72F C-esign Burst T (psig) (F ) Bwrst P 0 Burst T (psig) Manufacturing Range-Over/under(X > Ssacial manufacturing range 7 5-wTst tolerance (X) Special burst tolerance 7 j; capacity red'n due to RO (X) 3*> setting (psig) RO Manufacturing and Installation S-j Type "jno f ac turer Numoer of discs per location Cite Material One orientation device Torque requirements used 7 Discs not recommended-type -reason Ltali detection device vent method for space above RO '.tnt dest mat ion -"ess monitoring freQ for space :**eQuency of RO leaks Frequency of RO pin-holes -0 fouling prevention nethod -j inspection freq (react cycles) ' O! o f l nspec 11 on replacenent freq <mo.s) 6e- e^a 1 ^-esent concerns somber of failures in 1904 ; tlure causes-I. -2. -3. C/erpressure ever occurred 7 Overpressure amount (psig) .set overpressure "*erpressure ceuaes-1. -2. I `her comment s 4500 - 6 no - 122 221 9.3/5 no - - - 10000 B no - 100.4 220.5 9.3/S yea _ N/A N/A 18000/30000 200/225 6/8 yes 228 176 215 0/0 no S none 10 psig under bulged BS&B OV 2 INC/TFE/3I6SS J bolts none N/A bulged BS&B-OV 2 INC/TFE/3I6SS J bolts no prescored rev 1 B5&B S90 47 nickel none yea 5S chloride cracking red balKln project) P gauge ~ excess flow valve water wash I v i sue 1 3 water wash I visua1 6 negliQible once none none 12 prenoture failure 0-5 uni noun no no Inspect incoming ROs. Burst test one disc from each lot received. Install in holders and test to 90X of burst P in shop. On 1y Qua lifted mechanics to do instellet ions. AH AI AJ 16000 200 2X6 / 2X8 yes 189.198.200 ,200 200 185.195.200.200 0/0 no 5 no 10 18S. 195.200.200 10.9/5.7 no 5 no no data 10600 335 12 no 160 273 6/3 no 5 no N/A N/A Prescored rev buck 8S&B S90 4 nickel none yes SS chloride cracking Prescored bulged Proquip OV80 2 31B5S/INC/3IS5S vent side narked yes reverse buckling corrosion of knives conventional domed Marston Excelsior I Aluminum special holders no composite discs P gauge excess flow valve atn none none disc material I leak check 6 P switch alarm 10 psig RV atn every 15 sec none never inhibitor coating 400 visual!lampmirror ) 6 none none atn N/A <1 per yr N/A inhibitor coa11ng 1 v l sua 1 80 batches -prenature failures -overpressure 5-20 -process damage -unknown no Damage Cu".ng installation none no none 5-20 Punctured by lump no "Inspect and protect disc after every batch. -Disc should be far enough away from iiQuid level to prevent damage during agitation. CTL020001 TABULATION OF Company Designation Sat Pressure Cons 1 derat ions Reactor Size (US6 ) Vessel Rating (psig) RO Size (in. ) In Series with 5V 7 RO Burst P 9 72F (psig) Design Burs t T (FI Burst P 0 Burst T (psig) flanu f ac tur i ng Range-over/under ( Z ) Special menufacturing range 7 Burst tolerance (Z) Special burst tolerance 7 SV capacity red'n due to RO (Z) SV setting (psig) *0 flanufactur mg and Installation RO Type Menu f aclurer Number of discs per location Oise Material OiSC orientation device Torque requirements used 7 Oiscs not recomnended-type reason Leak detection device Vent method for space above RO Vent destination Press monitoring freq for space Frequency of RO leaks Frequency of RO pin-holes RO fouling prevention method RO inspection freq (react cycles) Type of inspection RO replacement freq (no.s) 6eneral Present concerns Number of failures in 1364 Failure causes~l. -2. Overpressure ever occurred 7 Overpressure amount (psig) Last overpressure Overpressure causes-l. -2. Other comments i AL confid confid 4-8 yes 90-95Z of VPR 0/0 yes S no <1X 90-I00Z of VPR AM (VCH plant - data - - - - prescored + bulged BS&B 6FN >6 nickel none no vacuum supp't/knife - leakage -no good for hydrostat red ball ind red ball t St atm N/A over 6 no.s none since *84 water spray 3-5 days visual 6 rev buck-k m fe Cont mental 50-100 nos11y mono 1 none yes P switch bleed valve sal don unknown N/A yearly no pattern Reverse 1 wit hou t rupture. 0-5 0-5 fatigue of material Poor design no no -Never use discs with knives in f1anges. -Oo not use ROs with vacuum supp'l -Replace ROs on preventive basis. -Use water spray to -Have found some discs reversed or dented on VCM spheres. 'Moving towards prescored ROs. keep RO clean. pq 7 of 7 ) CTL020002