Document EvyzpJj0geqxoxoeng7rYZ0k0

contract Lab Program Bata Package for DuPont Env. Remediation Svcs. IV ORGANICS DATA PACKAGE Madison - g w Monitoring-1996 Annual Water Samples ected on 09/17/96 - 09/18/96 . 2583205-2583211, 2583823-2583828 PA Cert. # 36-037 NY Cert. # 10670 NJ Cert. # 77011 Prepared by. 'uCn f4'$L Quality Assurance Review /D-H-7h Delivery Date_________If)- I'l-tfbj Lancaster Laboratories A Thermo Analytical Laboratory N36822 Pike, P0 Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681 Lancaster Laboratories A division of Thermo Analytical Inc. La Reference List for 806 # f h d o i with a Package Type of IV-O iim Sample Mummer 2583205 2583806 2583207 2583208 2583209 2583210 2583211 2583823 2583824 2583825 2583826 2583827 2583828 Sample code BRASS BRA4D BR4DD BRS4S BRS3D BRASS BRASS BRA2D BRA2S BRAIO BRA1S BRAF1 BRAT2 Client Sample Description FMN-BRA-4S Water Sample FMN-BRA-3D Unspiked Water Sample FMN-BRA-38 Water Sample FMM-BRA-TBLK-1 Water Sample FMN-BRA-2D Water Sample FHN-BRA-28 Water sample FMN-BRA-1D water sample FMN-BRA-lS Water 8ample FHM-BRA-FBLX-1 Water Sample FHN-BRA-TBLX-2 Water Sample Lancaster uooratones 2425 New Holland Pike PO Box 12425 lanC5Stc,r. PA 17605-2425 717-656-2300 Fax. 717-656-263' Shipping Address: Lancaster Laboratories 2425 New Holand PikeLancaster, PA 17601 717-656-2300 Fax. 717-656-268' DUP050307975 TABLE OF CONTENTS A. Case Narrative-Conformance/Nonconformaiice Suminary....... ....................1 B. chain-of-custody Record.................... 4 C. Volatiles Data..................................................................................................................13 1. QC Summary...................... 14 2. Sample Data............................ 29 3. Standards Data.......... ...................................................................................96 4. Raw QC Data................................................................................................... 198 A DUP050307976 Case Narrative Conformance/Nonconformance Summary l DUP050307977 Lancaster Laboratories A thermo Analytical Laboratory. Where quality is a science. LANCASTER LABORATORIES VOLATILES by GC/MS LL NUMBERS: SAMPLE CODE: 2583205 2583206 2583207 2583208 2583209 2583209 2583209 2583210 2583211 2583823 2583824 2583825 2583826 2583827 2583828 BRASS BRA4D BR4DD BRS4S BRS3D BRS3DMS BRS3DMSD DRA3S BRATB BRA2D BRA2S BRAID BRA1S BRAF1 BRAT2 LABORATORY SUBMITTED QC: VBLKG24 VBLKI93 VBLKI95 VBLKG24 VBLKE93 VBLKI95 CASE NARRATIVE CLIENT: DUPONT SDG: FMD01 MATRIX SOIL WATER X X X X X X X X X X X X X X X COMMENTS UNSPIKED MATRIX SPIKE MATRIX SPIKE DUP CLIENT BLANK CLIENT BLANK CLIENT BLANK X METHOD BLANK X METHOD BLANK X METHOD BLANK SAMPLE PREPARATION: No problems were encountered during the sample preparation for the VOA fraction. ANALYSIS: The method used for analysis was EPA CLP OLM03.1 SOW. No problems were encountered during the analysis of these samples. QUALITY CONTROL and NONCONFORMANCE SUMMARY: Only client requested compounds are addressed in this narrative. All QC was within specifications. DATA INTERPRETATION: No interpretation is necessary for the data submitted. Lancaster Laboratories 2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681 A subsidiary of Thermo Process Systems Inc., a Thermo Electron company % DUP050307978 Lancaster Laboratories A Thermo Analytical Laboratory Where quality is a science. CASE NARRATIVE Case Narrative Reviewed and Approved by: / Wj a ktfLg. Date /C s "> C- ihn F. Morton, M.S., GC/MS Volatiles Lancaster Laboratories 2425 Mew Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681 A subsidiary of Thermo Process Systems Inc., a Thermo Electron company t> DUP050307979 Chain-of-Custody Record DUP050307980 DU P050307981 DUP050307982 5-157 X3, 10-9W ANALYZING LAB COPY DUP0503 07983 5-157 X3, 10-91 an al y zin g l ab c o p y DUP050307984 AM M V*7IM f2 I A MSNewHdland WtiiicMter. PA TOOtSSM Sample Administration Receipt Documentation Log Client/Project:__________ Date of Receipt:__ i -- / ^& Time of Receipt:__________ ft 0 Source Code: __ _____ ^I COC Seal: Pre^t / Not Present on cooler Broken / li^ct Package: Cl^d / Not Chilled Unpacker Emp. No.: ---------------- Temperature of Samples Thermometer ID: #1 /6 /D 3 Thermometer ID: #2 Corrected Temo.: B^t^e / Air e>v *7 W^jle / Dry Ice / ice Packs Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs Ice Present? /N #3 Ice Present? Y / N #4 Thermometer ID: Thermometer ID: Corrected Temo.: Corrected Temp.: Bottle / Air Bottle / Air Wet Ice / Dry Ice / Ice Packs Wet Ice / Dry Ice / Ice Packs Ice Present? Y / N Ice Present? Y / N Paperwork Discrepancy/LTnpacking Problems: Sample Administration Chain of Custody Name Date Time Reason for Transfer y-nr-w mZl. f'/A / fl f | // Uppaekmg-- Klace in Storage )or Entry t*fOO Remove from Storage^ Place in Storage or Entjy Entry j Rev. 2174 09/09/96 DUP0503 07985 JSNewHolUnd H Uncww. Sample Administration Receipt Documentation Log Client/Project: _ Date of Receipt: Time of Receipt: Source Code: __ PfM/fl CO JEd. COC Seat: Pr^s^nt / Not Present on cooler Broken / Injj^Ct Package: Cl^filpd / Not Chilled Unpacker Emp. No.: Thermometer ID: Corrected Temp.: B<(^ie / Air #1 j 0 f O'} 1\ Wejtj^e / Cffy Ice / Ice Packs Ice Present? $) / N #3 Thermometer ID: Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs Ice Present? Y` / N Temperature of Samples #2 Thermometer ID: Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs tee Present? Y / N #4 Thermometer ID: Corrected Temp.: Bottle / Air Wet ice / Dry Ice / Ice Packs Ice Present? Y / N Paperwork Discrepancy/Unpacking Problems: % Sample Administration Chain of Custody 1 Name Date Time Reason for Transfer | Cml XCaX-. bnI rrzQxs*t U> 1 * Ai A) i-n-% 1em Unpackina 1/66 < Place in Storage) or )soc Remove from Storage ^ Place in Storage or Entry Entry . Entry Rev. 2174 09/09/96 DUP050307986 3425 NewHolland Lancaster PA 17601-SS94 Locked Storage Chain of Custody Original Sample Client/Project: P)i, PflnT"" F~n\i Fpy** A.irTTi an ^.Vi/a: 2 - Preservative: H~C, L,___________ Matrix: IaJ Ll ,'__________ Sample # Range of Entry Group: Pi<T D.f)I!____________ - Of ~P f/'.oA > _________ SDG: P M P 0 } Bottle Type: W`0 aPs it La,1' .. Sample Number(s) Released Received Date of Time of in Custody By By Transfer Transfer Reason for Change of Custody a vf3aas'-// Z&320&-U 2c<r-// -2573UOS - ii oJSg'S^os-n P5054)S -if JSTOos-li n tt M. 'h' SfjJ $*&<'} /Ot) 9//9M Oft3 $ 2-1 HaU- P/^tsc-iu ^ oA ifj a 9//9/9^ cfsrv /^ vUH ..... ~(pl ZyT[*M/\ S Cii. vi.j c-- TL-.W,J \1b %*iKt WZc Vii'A"-C 66 -5T or *-"**- T>e*f>fc 21 ifo Sxt>r<ua^ !<h . y&-* z Vo* Ata-utf's /I ir -3o * j5g% v Cam-pUiXy 3T tftvnawI7C `ifptfx ir.eo l/a&mu&Sfs / Sc**7Kb SI Cj J-UWM. Ttyfc Zf yyk 174, S'reraBP. .0 VC*. jWZ/3,'3 u QixuSile.biry Dist., Extr., or Digest Chain Created (X) `r/^Kv- 2016 Rev. 09/05/95 ii Page__[_ of DUP050307987 *25 NewHolland Pika UneasiK,IJ60I-S99* Locked Storage Chain of Custody Original Sample Client/Project: Du PfisTf' UprnpAt/t (iOi.\ St>c\ , For~f }V grl/i .%Gs> ___________ _ Preservative: N Os'JL,___________ Matrix: lOU____________ SDG: FM D Q 1 Sample # Range of. Entry Group: <35'? 3?33-3 P"__________ Bottle Type: 4# <yJ Sample Number(s) in Custody ^91% ai-a* ^i 25^597-Z -29 F5b 3sra-3-^J Released Received Date of Time of By By Transfer Transfer 7a (0-r SA AtFu~^ 9-f^% yjos sH`Uo 3'AO'3C. OGlO Ti^./iy iLo D"S-lp--3vi Vfava gif T Kelly Ai T Kelly ?>4o q-lQ-tL oC^S 9'5o-^C, o^oc 340 \Rpt 3t <?'3fc-9fc 0 3l S Dept 2.1 S7 0-vtnew- 3forru^t. t7C y%i/% f5-oo Jscpt 2 i / 70 Snr^Hft. iV-Zo ofiiZ^c/4 jtemM qz* Fh 5// c 0r, tf0 Reason for Change of Custody S F~ -fVc\w5-f<> + o De-O-f 3. * ^ <; 5 tUV-4 q e yv< Sc K;e v \ 0 CD t x /q -s' 7c- V-CIvv^ ru Sfolrgyu Vfe- ArtaXtrsiS Rftucw. to ofc^v^t. i/u/j # 7/5 6 Dist., Extr., or Digest Chain Created (X) ^ Sfr3S>3-9-$- e?% ~i $f6! 2016 Rev. 09/05/95 ------- 2__ Page I of DUPO50307988 Volatiles Data 13 DUPO50307989 QC Summary DUP050307990 2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY Lab Name: LANCASTER LABS Contract: ______ . Lab Code: LANCAS Case No,: ______ SAS No.: _______. SDG No.: FMD01 :--------8NE ' ' sNci ` SMC2 " SMC3.. oTfcfiR.. fS? SAMPLE NO. (TOL)# (BFB)# (DCE)# OUT 01 ':ViLNS24 02 BRA2D 03 BRA2S 04 BRAID 05 BRA1S 06 BRAF1 07 BRAT2 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 100 99 100 102 94 96 97 103 100 104 107 100 100 105 93 92 94 95 90 91 90 0 0 0 0 0 0 0 SMC1 (TOL) Toluene-d8 SMC2 (BFB) = Bromofluorbenzene SMC3 (DCE) = 1,2-Dichloroethane-d4 QC LIMITS (88-110) (86-115) (76-114) f Column to be used to flag recovery values * Values outside of contract required QC limits D System Monitoring Compound diluted out page 1 of 1 FORM II VOA-1 OLM03.0 15 DUP050307991 2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY Lab Name: LANCASTER LABS Contract: ______ . Lab Code: LANCAS Case No.: _______ SAS No.: ______ . SDG No.: FMD01 ----- gpjj---------- - SMC1 SM<S2" "s mc '3... 0TMER ToT SAMPLE NO. (TOL)# (BFB># (DCS)# OUT 01 VBLKI&3 02 BRATB 03 BRS3D 04 BRS3DMS 05 BRS3DMSD 06 DRA3S 07 BRS4S 08 BR4DD 09 BRA4D 10 VBLKI95 11 BRASS 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 101 101 102 100 97 99 102 102 100 104 102 98 99 97 98 98 98 98 102 97 100 99 94 90 94 94 92 94 95 94 94 95 94 0 0 0 0 0 0 0 0 0 0 0 SMC1 SMC2 SMC3 (TOL) = Toluene-d8 (BFB) = Bromofluorobenzene (DCE) = 1,2-Dichloroethane-d4 QC LIMITS (88-110) (86-115) (76-114) # Column to be used to flag recovery values * Values outside of contract required QC limits D System Monitoring Compound diluted out page 1 of 1 FORM II VOA-1 OLM03.0 16 DU P050307992 3A WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: LANCASTER LABS Contract: ______. Lab Code: LANCAS Case No.: . . . SAS No.: . Matrix Spike - EPA Sample No.: BRS3D s d g No.: _____ COMPOUND 1,1-Dichloroethene Benzene Trichloroethene Toluene Chlorobenzene "SPISE------ -------- 33EHP0S------ "US------- " 55- ADDED CONCENTRATION CONCENTRATION % l imit s (ug/L) (ug/L) (ug/L) EEC # REC. 50.00 50.00 50.00 50.00 50.00 0.00 0.00 0.00 0.00 0.00 58.99 57.81 56.61 54.80 52.59 118 116 113 110 105 61-145 76-127 71-120 76-125 75-130 COMPOUND 1,l-Dichloroethene Benzene Trichloroethene Toluene Chlorobenz ene SPIKE ADDED (ug/L) MSD CONCENTRATION (ug/L) 50.00 50.00 50.00 50.00 50.00 58.74 58.40 57.26 54.44 53.26 MSD % REC # 117 117 114 109 106 % RPD # 1 1 1 1 1 QC LIEMITS RPD REC. 14 61-145 11 76-127 14 71-120 13 76-125 13 75-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: .0 out of 5 outside limits Spike Recovery: o out of 10 outside limits COMMENTS: ___________________________________________ FORM III VOA-1 OLM03.0 17 DUP050307993 4A VOLATILE METHOD BLANK SUMMARY EPA SAMPLE NO. Lab Name: LANCASTER LABS Lab code: LANCAS Case No.: ______ Contract: SAS No.: VBLKG24 SDG No.: Lab File ID: >GSPB1 Lab Sample ID: VBLKG24 Date Analyzed: 09/25/96 Time Analyzed: 01:04 GC Column: DB624 ID: 0.53 (mm) Heated Purge: (Y/N) N Instrument ID: HP03460 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD: Bp F SAMPLE NO. 01 BRA2D 02 BRA2S 03 BRAID 04 BRA1S 05 MRA2S 06 MRA2SMS 07 MRA2SMSD 08 BRAF1 09 BRAT2 10 MRA1S 11 MRA1D 12 MRA2D 13 TB3FM 14 MRA4S 15 MRA3S 16 MRA3D 17 MR3DD 18 MRAFB 19 MRTB4 20 21 22 23 24 25 26 27 28 29 30 COMMENTS: ESI SAMPLE ID 2583823 2583824 2583825 2583826 2585279 2585279 2585279 2583827 2583828 2585276 2585277 2585278 2585280 2585281 2585282 2585283 2585284 2585285 2585286 LAB FILE ID >GSP01 >GSP02 >GSP03 >GSP04 >GSP05 >GSP06 >GSP07 >GSP08 >GSP09 >GSP10 >GSP11 >GSP12 >GSP13 >GSP14 >GSP15 >GSP16 >GSP17 >GSP18 >GSP19 page 1 of 1 FORM IV VOA TIME ANALYZED 01:57 02:30 03:02 03:34 04:05 04:36 05:06 05:39 06:11 06:42 07:13 07:44 08:17 08:50 09:22 09:55 10:27 11:00 11:33 18 QLM03.0 DU P050307994 4A VOLATILE METHOD BLANK SUMMARY EPA SAMPLE NO Lab Name: LANCASTER LABS Contract VBLKI93 Lab Code: LANCAS Case No.: ______ SAS No.: ______ . SDG No.: ___ Lab File ID: >ISJB2 Date Analyzed: 09/19/96 GC column: DB624 ID: 0.53 (mm) Lab Sample ID: VBLKI93 Time Analyzed: 08:44 Heated Purge: (Y/N) N Instrument ID: HP03046 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD: 01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 COMMENTS: EPA SAMPLE NO. BHATB BRS3D BRS3DMS BRS3DMSD DRA3S BRS4S BR4DD BRA4D ElB SAMPLE ID 2583211 2583209 2583209 2583209 2583210 2583208 2583207 2583206 LAB FILE ID >ISJ10 >ISJ11 >ISJ12 >ISJ13 >ISJ14 >ISJ15 >ISJ16 >ISJ17 TIME ANALYZED 10:34 11:04 11:35 12:11 12:41 13:12 14:11 14:41 page 1 of 1 FORM IV VOA OLM03.0 19 A DUP050307995 iA 4A VOLATILE METHOD BLANK SUMMARY EPA SAMPLE NO. Lab Name: LANCASTER LABS Contract: VBLKI95 Lab Codes LANCAS Case No.: ______ SAS No.t SDG No. Lab File ID: >ISOB3 Lab Sample ID: VBLKI95 pate Analyzed: 09/24/96 Time Analyzed: 15:43 GC Column: DB624 ID: 0.53 (mm) Heated Purge: (Y/N) N Instrument ID: HP03046 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD: ---------- ggg------------ SAMPLE NO. SAMPLE ID FILE ID TIME. ANALYZED 01 BRA5S 2583205 >ISO01 16:23 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 A 26 27 ' 28 29 30 COMMENTS: page 1 of 1 FORM IV VOA OLM03.0 20 DU PO50307996 SA " VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK BROMOFLUOROBENZENE (BFB) Lab Name: LANCASTER LABS - Contract: _______. Lab Code: LANCAS case No.: _______ . SAS No.: _______. SDG No.: Lab File ID: >GSMT3 BFB Injection Date: 09/24/96 Instrument ID: HP034S0 BFB Injection Time: 01:08 GC Column: DB624 ID: 0.53 (mm) Heated Purge: (Y/N) N m/e ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE 50 8.0 - 40.0% Of mass 95 75 30.0 - 66.0% of mass 95 95 Base peak, 100% relative abundance 96 5.0 - 9.0% of mass 95 173 Less than 2.0% of mass'" 1*74 174 50.0 - 120.0% of 'mass 95 ........................ 175 4.0 - 9.0% of mass 174 176 93.0 - 101.0% of mass TTZ 177 5.0 - 9.0% of mass 176 26.7 49.0 100. 6.6 0.0 ( 0.0)1 70.7 5.0 ( 7.1)1 69.4 ( 98.2)1 3.9 ( 5.7)2 l-Vaiue is % mass 174 ! 2-Value "is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS: EPA SAMPLE NO. LAB SAMPLE ID ESI FILE ID DATE ANALYZED TIME ANALYZED 01 VSTD010 02 VSTD020 03 VSTD050 04 VSTD100 05 VSTD200 06 VBLKG22 07 FTWAS 08 F8WAS 09 F6WAS 10 DU-P- 11 F8WASDL 12 DU-P-DL 13 3-------- 14 5------------------- 15 T------B 16 3--------DL 17 F6WASMSD 18 F6WASMS 19 20 21 22 010 ppb IC 020 ppb IC 050 ppb IC 100 ppb IC 200 ppb IC VBLKG22 2585266 2585227 2585228 2585229 2585227 2585229 2585230 2585231 2585232 2585230 2585228 2585228 >GSMI1 >GSMI2 >GSMI3 >GSMI4 >GSMI5 >GSMB1 >GSM01 >GSMQ2 >GSM03 >GSM04 >GSM05 >GSM06 >GSM09 >GSM10 >GSM11 >GSM12 >GSM13 >GSM14 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 01:40 02:12 02:44 03:17 03:49 04:50 05:33 06:03 06132 07:02 07:37 08:07 09:41 io:i3 10:42 11:21 11:53 12:41 page 1 of 1 FORM V VOA OLM03.0 21 DUP050307997 5A VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK BROMOFLUOROBENZENE (BFB) Lab Name: LANCASTER LABS Lab Code: LANCAS Case No.: ______ Contract: ______ . SAS No.: ______. SDG No.: _______ . Lab File ID: >GSFT1 Instrument ID: HP03460 BFB Injection Date: 09/24/96 BFB Injection Time: 23:59 GC Column: DB624 ID: 0.53 (mm) Heated Purge: (Y/N) N m/e ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE 50 8.0 - 40.0% of mass 95 75 30.0 - 66.0% of mass 95 95 Base peak. 100% relative abundance 96 5.0 - 9.0% of mass 95 173 Less than 2.0% of mass 174 174 50.0 - 120.0% of mass 95 175 4.0 - 9.0% of mass 174 176 93.0 - 101.0% of mass IY4 177 5.0 - 9.0% of mass 176 27.1 50.1 100. 6.9 .4 ( .6)1 70.2 5.0 ( 7.1)1 68.6 ( 97.7)1 4.5 ( 6.6)2 l-value is % mass i>4 2-Value is % mass i7e THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS: EPA SAMPLE NO. La b SAMPLE ID LAB FILE ID DATE ANALYZED TIME ANALYZED 01 VSTD050 02 VBLKG24 03 BRA2D 04 BRA2S 05 BRAID 06 BRA1S 07 MRA2S 08 MRA2SMS 09 MRA2SMSD 10 BRAF1 11 BRAT2 12 MRA1S 13 MRA1D 14 MRA2D 15 TB3FM 16 MRA4S 17 MRA3S 18 MRA3D 19 MR3DD 20 MRAFB 21 MRTB4 22 050 ppb CC VBLKG24 2583823 2583824 2583825 2583826 2585279 2585279 2585279 2583827 2583828 2585276 2585277 2585278 2585280 2585281 2585282 2585283 2585284 2585285 2585286 >GSPS1 >GSPB1 >GSP01 >GSP02 >GSP03 >GSP04 >GSP05 >GSP06 >GSP07 >GSP08 >GSP09 >GSP10 >GSP11 >GSP12 >GSP13 >GSP14 >GSP15 >GSP16 >GSP17 >GSP18 >GSP19 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 00:26 01:04 01:57 02:30 03:02 03:34 04:05 04:36 05:06 05:39 06:11 06:42 07:13 07:44 08:17 08:50 09:22 09:55 10:27 11:00 11:33 page 1 of 1 FORM V V0A OLM03.Q 22 DUP050307998 5A VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK BROMOFLUOROBENZENE (BFB) Lab Name: LANCASTER LABS Contract: Lab Code: LANCAS Case No.: ______ SAS No.: SDG No.: Lab File ID: >IGKT2 BFB Injection Date: 08/20/96 Instrument ID: HP03046 BFB Injection Time: 19:52 GC Column: DB624 ID: 0.53 (mm) Heated Purge: (Y/N) N m/e ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE 50 8.0 - 40.0% Of mass 95 75 30.0 - 66.0% of mass 95 95 Base peak, 100% relative abundance 96 5.0 - 9.0% of mass 95 173 Less than 2.0% of mass 174 174 50.0 - 120.0% Of mass 95 175 4.0 - 9.0% of mass 174 176 93.0 - 101.0% of mass 173 177 5.0 - 9.0% of mass 176 26.4 55.3 100. 7.2 0.0 ( 0.0)1 56.6 4.5 ( 7.9)1 55.5 ( 98.1)1 3.8 ( 6.9)2 l-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS: EPa SAMPLE NO. EH SAMPLE ID La b FILE ID DATE ANALYZED TIME ANALYZED 01 VSTD010 02 VSTD020 03 VSTD050 04 VSTD100 05 VSTD200 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 010 PPB IC 020 PPB IC 050 PPB IC 100 PPB IC 200 PPB IC 5?IGKI1 >IGKI2 >IGKI3 >IGKI4 >IGKI5 08/20/96 08/20/96 08/20/96 08/20/96 08/20/96 20:25 20:59 21:41 22:15 22:46 page 1 of 1 FORM V VOA OLM03.0 28 DUPO 50307999 5A VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK BROMOFLUOROBENZENE (BFB) Lab Name: LANCASTER LABS Contract: ______ . Lab Code: LANCAS Case No.: ______ SAS No.: ______ . SDG No.: _______ . Lab File ID:, >ISJT1 Instrument ID: HFO3046 GC Column: DB624 ID: 0.53 fmm) BFB Injection Date: 09/19/96 BFB Injection Time: 06:10 Heated Purge: (Y/N) N m/e ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE 50 8.0 - 40.0% of mass 95 75 30.0 - 66.0% of mass 95 95 Base peak, 100% relative abundance 96 5.0 - 9.0% of mass 95 173 Less than 2.0% of mass 174 174 50.0 - 120.0% of mass 95 175 4.0 - 9.0% of mass 174 176 93.0 - 101.0% of mass 174 177 5.0 - 9.0% of mass 176 1-Value is %..mass 1?4 26.9 57.9 100. 6.6 0.0 ( 0.0)1 58.0 4.8 ( 8.4)1 56.1 ( 96.8)1 3.9 ( 7.0)2 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS: EPA SAMPLE NO. LAB SAMPLE ID es b : FILE ID DATE TIME ANALYZED ANALYZED 01 VSTD050 02 VBLKI93 03 BRATB 04 BRS3D 05 BRS3DMS 06 BRS3DMSD 07 DRA3S 08 BRS4S 09 BR4DD 10 BRA4D 11 12 13 14 15 16 17 18 19 20 21 22 050 PPB CC VBLKI93 2583211 2583209 2583209 2583209 2583210 2583208 2583207 2583206 >ISJS1 >ISJB2 >ISJ10 >ISJ11 >ISJ12 >ISJ13 >ISJ14 >ISJ15 >ISJ16 >ISJ17 09/19/96 09/19/96 09/19/96 09/19/96 09/19/96 09/19/96 09/19/96 09/19/96 09/19/96 09/19/96 06:34 08:44 10:34 11:04 11:35 12:11 12:41 13:12 14:11 14:41 page 1 of 1 FORM V VOA OLM03.0 24 DUP0503 08000 5A VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK BROMOFLUOROBENZENE (BFB) Lab Name: LANCASTER LABS Lab Code: LANCAS Case No-: ______ Lab File ID: >ISOTl instrument ID: HP03046 GC Column: DB624 ID: 0.53 (mm) Contract: ______ . SAS No.: ______ . SDG No.: _______ . BFB Injection Date: 09/24/96 BFB Injection Time: 11:10 . Heated Purge: (Y/N) N m/e 50 75 95 96 173 174 175 176 177 ION ABUNDANCE CRITERIA 8.0 - 40.0% of mass 95 30.0 - 66.0% of mass 95 Base peak, 100% relative abundance 5.0 - 9.0% of mass 95 Less than 2.0% of mass 174 50.0 - 120.0% of mass 95 4.0 - 9.0% of mass 174 93.0 - 101.0% of mass 174 5.0 - 9.0% of mass 176 1-Value is % mass 174 % RELATIVE ABUNDANCE 21.5 49.6 100. 7.0 1.1 ( 1.8)1 64.2 4.9 ( 7.6)1 62.8 ( 97.8)1 4.2 { 6.7)2 2-vaiue is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS: Ip a SAMPLE NO. es b SAMPLE ID : LAB FILE ID 5EPI ANALYZED TIME ANALYZED 01 VSTD010 02 VSTD020 03 VSTD050 04 VSTD100 05 VSTD200 06 VBLKI95 07 BRA5S 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 010 PPB IC 020 PPB IC 050 PPB IC 100 PPB IC 200 PPB IC VBLKI95 2583205 >ISOIl >IS0I2 >IS0I3 >IS0I4 >IS0I5 >ISOB3 >IS001 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 11:35 12:08 12:50 13:23 13:56 15:43 16:23 page 1 of 1 FORM V VOA QLM03.0 25 DUP050308001 8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: LANCASTER LABS Contract: ______ . Lab Code: LANCAS Case No.: _____ SAS No.: ___________ SDG No.: ______. Lab File ID (Standard): >GSPS1 Date Analyzed: 09/25/96 Instrument ID: HP03460 Time Analyzed: 00:26 GC Column: DB624 ID: 0.53 (mm) Heated Purge: (Y/N) N 12 HOUR STD UPPER LIMIT LOWER LIMIT ISl(BGM) AREA # 58132 116264 29066 RT # 9.49 9.99 8.99 IS2(d f E) AREA # RT # 243476 11.09 486952 11.59 121738 10.59 1S3(CBZ) AREA # RT # 197202 15.36 394404 15.86 98601 14.86 EPA SAMPLE NO. 01 VBLKG24 02 BRA2D 03 BRA2S 04 BRAID 05 BRA1S 06 MRA2S 07 MRA2SMS 08 MRA2SMSD 09 BRAF1 10 BRAT2 11 MRA1S 12 MRA1D 13 MRA2D 14 TB3FM 15 MRA4S 16 MRA3S 17 MRA3D 18 MR3DD 19 MRAFB 20 MRTB4 21 22 47273 45203 43616 42390 46112 46326 45165 46550 45345 45012 46147 45607 42125 43375- 43050 44476 43668 43617 44189 43139 9.50 9.49 9.46 9.45 9.48 9.49 9.49 9.50 9.46 9.45 9.48 9.48 9.49 9.43 9.45 9.46 9.46 9.46 9.48 9.45 187620 184177 172338 163927 180206 181876 174760 180523 182909 170584 176866 175880 153258 166648 163107 169366 167569 165520 167898 165161 11.10 11.08 11.05 11.05 11.08 11.08 11.09 11.10 11.06 11.05 11.07 11.08 11.07 11.04 11.04 11.05 11.06 11.06 11.07 11.05 153010 148674 136114 132526 145332 149856 141875 143435 143510 136060 144085 142240 124991 133567 133232 137466 137313 134757 134641 132325 15.37 15.37 15.33 15.33 15.35 15.35 15.37 15.37 15.33 15.33 15.35 15.36 15.36 15.31 15.32 15.33 15.34 15.32 15.36 15.32 151 (BCM) = Bromochloromethane 152 (DFB) = 1,4-Difluorobenzene 153 (CBZ) = Chlorobenzene-d5 AREA UPPER LIMIT - +100% of internal standard area AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = +0.50 minutes of internal standard RT RT LOWER LIMIT = -0.50 minutes of infernal standard RT # Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII VOA OLM03.26 DUP050308002 SA VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: LANCASTER. LABS Contract: _. t .ain code: LANCAS Case No.: ______ . SAS No.: ___________ SDG No.: _______. Lab File ID (Standard): >ISJS1 Date Analyzed: 09/19/96 Instrument ID: HP03046 Time Analyzed: 06:34 GC Column: DB624 ID: 0.S3 (mm) Heated Purge: (Y/N) N IS1(BCM) AREA # IS2(DFB) RT # AREA # IS3(CBZ) RT # AREA # RT # 12 HOUR STD UPPER LIMIT LOWER LIMIT 30709 61418 15355 8.34 8.84 7.84 129120 10.01 258240 10.51 64560 9.51 94592 14.33 189184 14.83 47296 13.83 EPA SAMPLE NO. 01 VBLKI93 02 BRATB 03 BRS3D 04 BRS3DMS 05 BRS3DMSD 06 DRA3S 07 BRS4S 08 BR4DD 09 BRA4D 10 11 12 13 14 15 16 17 18 19 20 21 22 39611 40404 39376 39018 40297 38676 38771 39747 40307 8.35 8.36 8.35 8.36 8.35 8.38 8.36 8.35 8.38 163966 168853 165349 162767 167429 163613 163565 166824 167994 10.02 10.02 10.03 10.02 10.01 10.05 10.04 10.03 10.04 121256 124072 122020 121783 125468 121255 121552 123866 124864 14.33 14.31 14.33 14.32 14.32 14.34 14.33 14.34 14.35 151 (BCM) = Bromochloromethane 152 (DFB) = l,4~Difluorobenzene 153 (CBZ) = Chlorobenzene-d5 AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = +0.50 minutes of internal standard RT RT LOWER LIMIT = -0.50 minutes of internal standard RT # Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII VOA OLM03 DUP050308003 8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: LANCASTER LABS Contract: ______ . Lab Code: LAMCAS Case No.: _____ SAS No.: _________ SDG No.: _______. Lab Rile ID (Standard): >lSOI3 instrument ID: HPQ3046 Date Analyzed: 09/24/96 Time Analyzed: 12:50 GC Column: DB624 ID: 0.53 (mm) Heated Purge: (Y/N) N ISl(BCM) AREA # " IS2CDFB).. RT # AREA # IS3(CBZ) RT # AREA # RT # 12 HOUR STD UPPER LIMIT LOWER LIMIT 30984 61968 15492 8.17 8.67 7.67 125072 9.84 250144 10.34 62536 9.34 97357 14.15 194714 14.65 48679 13.65 EPA SAMPLE NO. 01 VBLKI95 02 BRA5S 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 18842 35115 8.19 8.20 73204 139655 9.85 9.86 55305 14.18 106918 14.18 151 (BCM) "= Bromochloromethane 152 (DFB) == 1,4-Difluorobenzene 153 (CBZ) = Chlorobenzene-dS AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = +0.50 minutes of internal standard RT RT LOWER LIMIT = -0.50 minutes of internal standard RT / Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII VOA OLMO30S DUP050308004 Sample Data DUP050308005 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract: BRA5S Lab Code: LANCAS Case No.: ______ SAS No.: SDG NO.: Matrix: (soil/water) WATER Lab Sample ID: 25S3205 Sample wt/vol: 5.0 (g/mL) ML Lab Pile ID: >IS001 Level: (low/med) LOW Date Received: 09/18/96 % Moisture: not dec. _______ Date Analyzed: 09/24/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0 Soil Extract Volume: _______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: fug/L or ug/Kq) UG/L Q 74-87-3------------------ Chloromethane 75-01-4------------------ Vinyl Chloride 74-83-9----------------- Bromomethane 75-00-3----------------- Ch 1 oroethane 75-35-4-----------------1,1-Dichloroethene 67-64-1------------------ Acetone 75-15-0------------------Carbon Disulfide 75-09-2------------------ Methylene Chloride 75-34-3-----------------1,1-Dichloroethane 540-59-0---------------1,2-Dichloroethene (total) 78-93-3-----------------2 -Butanone 67-66-3------------------ Chloroform 107-06-2----------------1,2-Dichloroethane 71-55-6------------------ 1,1,1-Trichloroethane 56-23-5------------------Carbon Tetrachloride 71-43-2------------------ Benzene 79-01-6------------------ Trichloroethene 78-87-5------------------1,2-Dichloropropane 75-27-4------------------ Bromodichloromethane 10061-01-5-----------cis-l, 3-Dichloropropene 10061-02-6------trans-1,3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane 124-48-1---------------- Dibromochloromethane 75-25-2----------------- Bromof orm 108-10-1------- --------4-Methyl-2-Pentanone 108-88-3---------------Toluene 12 7 -18-4---------------Tetrachloroethene 591-78-6----- ---------2 -Hexanone 108-90-7----------------Chlorobenzene 100-41-4---------------Ethylbenzene 1330-20-7--------------Xylene (total) 100-42-5----------------Styrene 79-34-5----------------- 1,1,2,2-Tetrachloroethane FORM I VOA 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u OLMO3.0^0 DUP050308006 -m-rot t o m c h r o ma t o g r a m Data File: >ISQ01::D4 Name: BRA5S 25832U5 Mi sc: ~SJL WL %L 1 + > Quant Output File: Instrument ID: #1962631AB &5 *5 $''1SQB3 /'ISO01::D? HPCI3 046 id File: 1A6590::DB Title: 3/9U SOU Water/'Med Soil ID File for Inst. HP03Q46 Last Calibration: 951122 10:44 Last Qcal Time: 960924 12:50 Operator ID: Quant Time : Injected at: SJL-176 960924 16:47 960924 16:23 31 DUP050308007 QUANT REPORT Llperetor ID: SOL-1/6 Uutput Files ~iSU01s sD7 Uata File: >1SQ0I::U4 Name: BRASS 2583205 mac: ~S0L |WL JSC =! +> Wuant #1962631AB &5 Revs 5 7 Qu ant Tlme: Injected at: Dilution Factor: Instrument ID: `ISQ83 Page 1 VC.U924 it- * A.- 960924 16:23 i . 0U000 HP03046 lu Files IA639B::DB iitie: 3/90 SOW Water/Med Soil Last Calibration: 951122 10:44 ID File for Inst. HP03U46 Last Qcal Time: 960924 12:50 Compound 1) 15) i?) 29) 51) 41)) *8ramaehforomethane I,2-Dichloroethane-d4 *154-DiF1uorobenzene *Chlorobenzene-d5 toiuene-d8 4-BromoFluorobenzene * Compound is IB I'D R.'l . Q ion 8.20 9.15 9.86 14.10 12.0B 15.90 128.0 65.0 114.0 117.0 98.0 95.0 Area 35115 63490 139655 106918 123922 9B150 *---O Tt C Un its 50.00 46.76 50.00 50.00 5U . 84 49.53 UG/L UG/L UG/L UG/L UG/L UG/L 9/ 91 87 85 y6 81 32 DUP050308008 Lancaster Laboratories Quantitation Report-GC/TIS Volatiles Lift: SI <5 S 3 2 O 5 SO l-- File: "ISuai Injected: 16:23 09/24/96 Sample: BRASS 2333203 Dilution Factor: 1.0 Initial Uolume/Ut.: 3.0 Standard: "ISOli Inst. 1^03046 Batch: I962631AB Final Volume/Ut.t 5.0 flethod: 7194 Hatrix/level: UL Blank: l'iSUB3 $ Internal Standaras R.I. (V-RT) Sean Dion Areal*/-*Area) Cone. UC Flag tone Units = uq.'L TX. BramoehIoromethane 17. 1,4-Bifluorobenzene 21. Chisrobfinzene-db * = RETENTION TIME OUT OF RANGE 8.2041.0324) 550 128 35115( 13) 50.08 9.8561.0178) 692 114 139655( 12) 50.00 14.181.0300) 1064 117 1069181 10) 50.00 * * INTERNAL STANDARD AREA OUT OF RANGE NC - NOT ABLE TO CALCULATE--NO STANDARD. Xf Surrogate Standards R.T. IV-RRT) Scan Dion Area Cone. ffitee. Q RHaiesaBaaftaBsacaBaB*a*as>anM(taai iia>aitaaBMiaatataaaiaaaasaaaKMBaa8BBnaiaaasi8aaaaBnaaasBaaBssaas8XBB& 15. 1,2-Dichloroethane-d4 9.14?(-.0Q1) 631 65 31. Toluene-dfl 12.08C-.0003 683 98 40. 4-Bromofluorobenzene 15.90I-.001) 1212 95 # - RELATIVE RETENTION TIME OUT OF RANGE * - REC OUT OF RANGE 63490 46.76 94 123922 50.84 102 98150 49.53 99 0 SURROGATES DILUTED OUT NC COULD NOT CALCULATE Cone. Quantitaticn t target Compounds R. t. (+/-SRT) Scan Own Area Cone.A Conc.B Blank 0 Limit 3SBaBBBBttBBBBma*B3BBBBBB**B:EBBBmBB*BB*BBBmBB*am3**mBmwBBBBBwBBBBBBSBB:B**BBBB**BBBBBBmBBBBBMB* Ch Ioromethane 10 Vinyl Chloride Uromomethane Chloroethane 1.1- Qichlorostherie 10 ID 10 10 Acetone Carbon Disulfide 10 ID Methylene Chloride 1.1- Dichloroethane 10 10 1.2- Dichloroethene (total) 10 2-Butanone 10 Chloroform 10 1.2- Bichloroethane 10 1,1,1-Trichloroathane 10 Car&on letrachloride 10 Benzene 10 Tnchloroethene 10 1.2- Dichloropropane 10 bromodichIoromethane 10 cis-l,3-Dichloropropene 10 trans-1,3-Dichloropropene 10 1.1.2- Trich loroethane 10 sssasss: ssaessssmasxsssassatsttsmssxasBSttKaag essBSseatsasac&sssssssasaesssxsBasss&ssaat&assssscsBeBsiaararcaBisssKs.sssa isasses ft = RAW CUNC. 6 - CONC. MULTIPLIED BY DILUTION FACTOR E - CONC. OUT OF CAL. RANGE * - RELATIVE RETENTION TIME OUT OF RANGE Lab Chronicle: .Ent. by ,,Ver. by PAGE 1 UF 2 DUP050308009 Lancaster Laboratories Quantitation Report-GC/HS Volatiles' LLl*: 2 9 O 3 2 O E5 SJL Fslei AiSUUl injected: 16:23 U9/24/96 Sample: BRA5S 2583285 Dilution Factor: 1.0 initial Uoiume/Ut.! 5.8 Standard: AISUI3 Inst. HP03046 Batch: 1962631A8 Final VeUme/Ut.: 5.8 flethod: 7156 ttatrix/iewel: UL Blank: A1SQB5 t 1argot Compounds R.T.C+/-RRT) Scan Qion Area Cone.A Conc.B Cane. Blank 8 Quantitation Limit 27. Dibromochlororaethane 2B. Brantsform 38. 4'-flethyl-2-Fentanone 32. Toluene 35. ietrachioroathene 34. 2-Hexanone 55. Chlorobenzene 36. Ethylbenzene 58. Xylene (total) 39. Styrene 41. 1,1,2,2-letrachloroethane aaaasaaaaaassaaaaaaaaaaaasaaaa! A = m COfC. B = DISC. nULf(PLIED BY DILUTION FACTOR II) IB 1U 10 10 18 10 10 10 10 10 as3E*3ta;xB'SaaiassssBBKaaascBst: E CUNC. OUT OF UAL. RANGE * = RELATIVE RETENTION TIME OUT OF NANCE Lab Chronicle: ,,Ent. by DUPO 50308010 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract: BRA4D Lab Code: LANCAS Case No.: _______ SAS No.: SDG No.: Matrix: (soil/water) WATER Lab Sample ID: 2583206 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >ISJ17 Level: (low/med) LOW Date Received: 09/18/96 % Moisture: not dec. _______ Date Analyzed: 09/19/96 GC column: DB624 ID: 0.53 (mm) Dilution Factor: l.o Soil Extract Volume: ______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3----------------- Ch1oromethane 75-01-4------------------ Vinyl Chloride 74-83-9-----------------Bromomethane 75-00-3------------------ Chloroethane 75-35-4------------------ 1,1-Dichloroethene 67-64-1------------------ Acetone 75-15-0---------------Carbon Disulfide 75-09-2------------------Methylene Chloride 75-34-3-----------------1,1-Dichloroethane 540-59-0----------------lr2-Dichloroethene (total) 78-9 3-3-----------------2-Butanone 67--66--3---------------Chloroform 107-06-2--------------1,2 -Dichloroethane 71-55-6----------------- 1,1,1 -Tr i chloroethane 56-23-5------------------Carbon Tetrachloride 71-43-2------------------Benzene 79-01-6------------------Trichloroethene 78-87-5----------------- 1,2-Dichloropropane 75-27-4-----------------Bromo d i ch loromethane 10061-01-5----------- cis-1,3-Dichloropropene 10061-02-6----------trans-1,3-Dichloropropene 79-00-5------------------1,1,2-Trichloroethane 124-48-1----- ---------- Dibromochloromethane 75-25-2------------------Bromoform 108-10-1---------------4-Methyl-2 -Pentanone 108-88-3---------------- Toluene 127-18-4---------------- Tetrachloroethene 591-78-6----------------2-Hexanone 108-90-7----- ---------- Chlorobenzene 100-41-4----------------Ethylbenzene 1330-20-7--------------Xylene (total) 100-42-5----------------styrene 79-34-5------------------ 1,1,2,2-Tetrachloroethane FORM I VOA 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 V 10 u ----------------------------------------------------------------- -------------------------- _ OLM03.0*>'J DUP050308011 TdTfiL ION CHROMATOGRAM Data File: >ISJ17::03 Quant Output File: Name: BRA4D 2583206 Instrument ID: Nisc: ~TLN gWL XC =1 *1962631AA &5 *5 $~ISJB2 /*'IS017::07 HPQ3Q46 Id File: IA639Q::DB Title: 3/-90 SOW Water7Med Soil ID File for Inst. HPD3046 Last. La Iibrat ion: 951122 10:44 Last Qcal Times 960919 06:34 Operator ID: TLN-262 Quant Time : 960919 15:06 Injected at: 960919 14:41 36 DUP050308012 QUANT REPORT Uperator ID: TLN-262 Output File: '"*ISJ17::D7 Data File: >1BJ1?::D3 Name: BRA4D 2533206 mac: "TLN JjOWL S4C =1 +> Quant =11=1962631AA &5 Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: *5 $'"13082 Page 1 96U919 15:U6 960919 14:41 1.UOUUU HPU3Q46 ID File: IA6390::DB Title: 3290 SOU! Water/Tied Soil ID File for Inst. HP03Q46 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 1) 15 ) 17) 29 ) 51 )' 40 ) ^Bromochloromethane 1,2-Dichloroethane-d4 *1,4-Difluorobenzene *Ch16robenzens-d5 To luene-dS 4-Qromofluorobenzene * Compound is 1STD R.T. Q ion 8.38 9.33 10.04 14.35 12.25 16.09 128.0 65.0 114. 0 117.0 98.0 95.0 Area 40307 87236 167994 124864 148480 100430 Cone Units 50.00 46.97 50.00 50.00 50.20 48.60 UG/L US/L UG2L UG7L UG^l UG2L q 92 90 89 84 97 74 37 DUP050308013 Lancaster. Laboratories Quantitation Report-GC/MS Volatiles III*: 2583206 Hlei ''1SJ17 Injected! 14:41 89/19/96 Sample: 8RA4D 2583206 Dilution Factor: 1.0 Initial Uoluma/Ut.: 5.0 Standard: AISJS1 Inst. HP03046 Batch: 1962631AA Final Volume/tlt.: 5.0 Method: >156 Matrix/level: UL Blank: '13^82 t Internal Standards R.T. (*/-GT) Scan Qion ftreaU/-)iArea) Cone. SC Flag Cone Units = ug/L 1. Oroaochloromathane 17. 1.4-Difluorobenzene 29. Chlerobenzana-d5 0 - RETENTION TIKE OUT OF RANGE 8.386(.641?) 570 128 403071 31) 58.UO 10.041.0293) 713 114 1679941 30) 56.08 14.35(.(1267) 1884 117 12B64( 32) 98.08 * - INTERNAL STANDARD AREA OUT OF RANK NC - NOT ABLE TO CALCULATE--NO STANDARD. S Surrogate Standards R.T. (+/-RRT) Scan Qion Area Cone. SRec. 15. l,2-Dichloroatbane-d4 9.334C-.001) 652 65 31. Toluena-dB 12.251.0810) 903 98 40. 4-Bromofluorobenzene 16.09C.0804) 1233 95 # RELATIVE RETENTION TIME OUT OF RANGE * - XREC OUT OF RANGE 87236 46.97 94 148480 50.20 100 100430 48.60 97 D SURROGATES DILUTED OUT NC - COULD NOT CALCULATE Cone. Uuantitation $ Target Compounds R.T.C+/-KRT) Seen Qion Area Cone.A Cone.if Blank Q Limit x5acea>ssass&BB3!BBaBstEiaaBBSfl98BOSBasssRBnKaBCBSWRnts>anmBaBnstcamMnMBsaaBBiWiBnoasseaaRSi:isas8isss>MSKS .2 Chloromethane ID 3. Vinyl Chloride 10 4. Broraomethane &j Chtoroethane .6 1.1-DichloroBthene 1U 10 10 1. Acetone .8 Carbon Disultide 18 lu 9. Methylene Chloride .11 1.1-Dichloroethane .12 1.2-Dichloroethene (total) 10 18 10 13. 2-Butanene 18 14. Chloroform 10 16 1.2-Dichloroethane 18. 1,1,1-Triehloroathane 18 10 19. Carbon Tetrachloride .20 Benzene .21 Tnchloroethene .22 1.2-Dichloropropane 23. Uromodichloromethane 2a. cis-l,3-Dichloropropene 25. trans-l,3-0ichloropropene 26. l,l)2-Trichloroethane 1U 10 18 10 18 10 10 10 saeaaassssBsase&sasaaasvasessajgtetKatssiasBaaeea&eaesaicattSBssassssssaaBsasssaa&sssesas ft RfiW C0NC. B - C0NC. MULTIPLIED BY DILUTION FACTOR E C0NC. OUT OF CAL. RANK t RELATIVE RETENTION TIME OUT OF RANGE Lab Chronicle: ,,Ent. by .Ver. by PAGE 1 OF 2 ICO I DUP050308014 Lancaster Laboratories Quantitation teport-SC/MB Uolatilas LLi#: 2! "5 3 3 2 O *. Tl__M File; A1J17 injected: 14:41 89/19/96 Sanpla! BRS4D Dilution tactor: 2583206 1.1) Initial Volume/Ut.: 5.0 Standard: A1SJS1 Inst. HPD3Q46 Batch: 1962631fift Finai yolune/tlt.: 5.0 Rethod: 7156 Hatrix/leval: III Blank: ASSJB2 * larget Compounds R.T.U/-KRT) Scan Qion Area Cone.ft Cone.8 Cone. Blank Q Quantitation Limit B8usBsBBSBnuHniaaaa8saiaac5smisimBSsaB3iaiss8aatssKnBtaBUUnHS8smnaKKsniBuiSRBiMssamtia3Stsnc8BSB*s*n& 27. Uibromochloromethane ~----- -------------------------------------------------------------------------------- ----------------------- 11) . 28. Bronoform 30. 4-flettiyl-2-Pentanone 32. Toluene 33. letrachloroothene 34. 2-Hexanone --;------- ;----------------------------------------------------------------------------------------- --------------------------------------------------------------------------- --------------------------------------------- ----------- '------------------- ------------- --------------- ------------------------------- ----------------------------------- ----------------------------------- ------------------------------- ------------------------------- --------------------------- ------------------------------ ~---------- --------------------------- ------ - io 10 10 18 10 35. Chlorobenzene ' 36. Ethylbenzene ' -------------- ------ ---------------- ----------------- --------------------------------------------------------------------- --------------- -------------- ------- ------------ -----------'--------- ---------- i-- -------- *---------- 18 '10 38. Xylene Uotell 39. Styrene 41. 1,1,2,2-tetrachloroethane ----------------------- ----------------------------------------------- ------------------------------------------------------------- ----------- --------------------------------------------- ------------- --------------------------------------------------- ------------------------ ;------------------------------------------------------------------------------ 18 10 18 ssBsaKss&saBaBBaBBBBBBauBmaBBBBmBaauEaBBsmaaaBSBmsaBBBBaanaBSSBSSBasBBBBBBBamsBBBBBBBBsxBBBmanamBBaasBBBaBsamBBBBaBBmBBaaBaamBBBBBmBm ft KAO CONC. B = CONC. MULTIPLIED BY DILUTION FACTOR E CUNC. OUT OF CflL. RANGE 4 * RLLftTUJE ROBmuN TIME BUT OF RANGE Lab Chronicle: Ent. by, eft 3 DUP050308015 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Lab Code: LANCAS Case No.: ____ Contract: SAS No.: BR4DD SDG NO.: Matrix: (soil/water) WATER Sample wt/vol: 5.0 (g/raL) ML Level: (low/med) LOW Lab Sample ID: 2583207 Lab Pile ID: >ISJ16 Date Received: 09/18/96 % Moisture: not dec. ______ Date Analyzed: 09/19/96 GC Column: DB624 ID: 0.53 Dilution Factor: 1.0 Soil Extract Volume: ______ (uL) Soil Aliquot Volume: ______ (UL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3-----------------Chloromethane 75-01-4------------------Vinyl Chloride 74-83-9--------Bromomethane 75-00-3------------------Chloroethane 75-35-4-----------------1/ 1-Dichloroethene 67-64-1------------------ Acetone 75-15-0--------- ---------Carbon Disulfide 75-09-2-----------------Methylene Chloride 75-34-3---------------1,1-Dichloroethane 540-59-0----------------1,2-Dichloroethene (total) 78-93-3----------------- 2-Butanone 67-66-3------------------ Chloroform 107-06-2--------------- 1,2-Dichloroethane 71-55-6------- --------1,1,1-Trichloroethane 56-23-5------------------Carbon Tetrachloride 71-43-2------------------ Benzene 79-01-6------------------ Trichloroethene 78-87-5----------------1,2-Dichloropropane 75-27-4-----------------Bromodichloromethane 10061-01-5-----------cis-1,3-Dichloropropene 10061-02-6--------- -trans-rl, 3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane 124 -48-1------- ----Dibromochloromethane 75-25-2------------------ Bromoform 108-10-1---------------- 4-Methyl-2-Pentanone 108-88-3---------------- Toluene 12 7-18-4--------- -------Tetrachloroethene 591-78-6--------------- 2-Hexanone 108-90-7---------------- Chlorobenzene 100-41-4---------------- Ethylbenzene 1330-20-7--------------Xylene (total) 100-42-5----------------Styrene 79-34-5--------- ---------1,1,2,2-Tetrachloroethane 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FORM I VOA OLM03.0 40 DUP050308016 Data File: >ISJ16::D3 Quant Output File: Name: BR4DD 25832 07 Instrument ID: Mi sc: ~TLN @WL KC 1 +> # 1962631AB &5 *5 $'VISJB2 /'ISJ'16::D7 HP03EJ46 Id Files 1A6390::DB Titles 3/90 SOU Water/Med Soil ID File for Inst. HP03046 Last Calibrations 951122 10:44 Last Deal Times 960919 06:34 Operator IDs TLN-262 Quant Time : 960919 14:35 Injected at: 960919 14:11 41 DUP050308017 QUANT REPORT Page 1 Uperator ID: TLN-262 Output File: '"'IS316;:D? Data File: >1SO16::Q3 Name: BR4D0 2563207 mac: ~TLN WUIL % *> Quant #I962631Aft &5 Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: *5 AISJIB2 960919 14:35 960919 14:11 1.00U0U HP03046 ID File: IA6390::OB Title: 3/90 BOW Ulater/Med Boil ID File for Last Calibration: 951122 10:44 Inst. HP03046 Last Qcal Time: 960919 06:34 Compound 1? 15) 17) 29 ) 31 ) 40 ) *Bramochloromethane 1 /2-Di Ohio roe thane-d4 *1,4-Di fluorobentene *Chlorofaenzone-d? To tuene-d8 4-8romofluorobenzene * Compound is l&TD R.T. Q ion 8.35 9.32 10.03 14.34 12.22 16.06 128.0 65.0 114.0 117.0 98.0 95.0 Hrea 39747 86127 166824 123866 149489 104525 Cone Units 30.00 47.02 50.00 50.00 50.95 50.99 UG/L UG/L UG/L UG/L UG/*'L UG/L q 92 90 87 84 97 77 42 DUP05030801 8 Lancaster Laboratories Quantitation Raport-GC/ftS Volatiles LLMM 25832 07 Tl--IN tiie: *15016 Injected! 14:11 09/19/96 Sample: BR4DD 2583207 Dilution tactor: 1.0 Initial Uolufee/Ot.: 5.0 Standard! *ISJS1 inst. I03046 Batch: I962631flfl Final Uialume^Ut.: 5.0 Method: 7156 Matrix/level: WL Blank: *15052 $ Internal Standards R.T. (+/-RT) Scan Dion Area(+/-XArea) Lone. DC Hag Cone Units = ug/L sBu&e8MCS8sasE8Bsssi8WBBaasimasaasmtaaTCMfuatMiBsiiiummansBiMcwRiuniBcsaBSBswMnans8snB<iBe**sNaaaiBBsx 1. Bromochlororaethane 17. 1,4-Oifluorobenzena 29. Chlorobenzene-dS * RETENTION TIME OUT OF RAISE 8.5541.8150) 569 128 39?4?( 29) 5B.U0 Id.Q3(.fll32) 713 114 166824( 29) 50.00 14.34(.0122) 1884 117 123B66< 31) 50.0U * * INTERNAL STANDARD ARBI OUT OF RANGE NC - NOT ABLE TO CALCULATE--NO STANDARD. 4 Surrogate Standards R.T. l*/-RRT) Scan Oeo o Area Cone. XRec. 0 15. l,2-f)iehloroethane-d4 9.3181.0018) 652 65 31. Toluene-d8 12.221.0000) 902 98 40. 4-Bromafluorobenzene 16.06(-.008) 1232 95 # * RELATIVE RETENTION TIME OUT Iff RANGE * SREC OUT OF RANGE 86127 47.02 94 149489 50.95 102 104525 50.99 102 D - SURROGATES DILUTED OUT NC COULD NOT CALCULATE Cone. Quantitation $ target Compounds R.T.(+/-HRT) Scan Qion Area Cone.A Conc.B Blank Q Limit ^rr^Tf,^r.tBrTtTrrtttTt.w^y>ta,gB:T1rfff.Mi!!.Miea^Mmai-acgaiegaigMtKggaatMiMamaKtKaiaBiauaameaMggaaaiititBsmoiKwBBttat8 2. Chloroaethane 3. Uinyl Chloride --------------------------------------- ------------------------- *------------------------------------------------------------------------------- -------------- ------------------------------ ------------------------------------- 10 10 4. tiromofflethane ------------------------<----------------------------------------------------------------------------------------------------- 18 5. Chloroethane 6. 1,1-Dtehloroethene --------------------------------- ----------------------------- _-------------------------------------------- --------------- 10 -------- -1-TM------- ---------- ------- -------- ------- -------------- ---------------------------10 7. Acetone 3. Carbon Uisuifide 9. Methylene Chloride 11. l.l-Dichloroethene -------------------------------------------------- -------- -------- --------- ---------- ------------------------------- 18 12. 1,2-Dichloroethene (total) ---------------------------------------------------------- :------------------------------------------------------------------ 10 13. 2-Butanone ------------------------------------ *------------------------------------ -------------------------------------------------- 10 14. Chloroform ------------------------------------------------------------------- ---- ------------------------------------------------ 10 16. 1,2-Dichtoroethane 15. 1,1,1-Tr ich toroethane 19. Carbon tetrachloride 20. Benzene ------------------------------------------------ -------------------------------------------------------------------- --- 10 21. Irichloroethene 22. 1.2-Dichlorcpropane 23. Bromodicnloromathane 24. cis-l,3-Dichloropropene ------------------------------------------------------------------------------------------------------------------------------------ 10 25. trans-l,3-Dichioropropene ----------------------------------------------------------------------------------------------------------------- 1----------- 1(1 26. 1,1,2-Trichloroethane sa=saasaBsesas8SBaasrttCssessaBS3B&ttSBeBSSKSBBa8BBttssssaaBeS8S3msaaKVSessSKOB3cttBBCSas8%esassssSBSSBSSsaDBBa_sseBSasxass.ss:s;3.18D8ESSsms A - RAW CQIC. B - C0NC. MULTIPLIED BY DILUTION FACTOR E CQNC. OUT OF CAL. RANGE * RELATIUE RETENTION TIME OUT OF RANGE Lab Chronicle: ;Ent. by. ------------------:------------------------------------------------------------------------------:----------------------------------------------------------------------------------------------:------------------------------------------------------------------------------------------------------------------------------------------------- PftEE 1 OF 2 DUP050308019 Lancaster laboratories Quantitation Report-GC/flS Uolatiles LLl#: 2^032 07 Tl__N Files '"ISO16 Injected: 14*.II 09/19/94 Sample: BR40B 2583207 Dilution Factor: 1.0 Initial Uolune/Ut.: 5.0 Standard: "ISJSl inst. HP03846 Batch: IH2631AA Final Dolune/Ut.: 5.0 Method: 7156 Matrix/lavel: VIL Blank: *15082 $ Target Compounds R.T.(*/-RRT) Scan Qiort Area aaaica*6s***:am*misaiem***J*aa*****a*a***a********f*****i 27. Qibromach loronethane ------ -------------------- -------------- ------------ --------- 38. 4-ttethyl-2-Pentanone 32. Toluene 33., letrachloroethane 34. 2-Hexanene 35. Chlorobenzene 36. Ethylbenzene 38. Xylene (total) 39. Styrene 41. 1,1,2,2-Tetrachloroethane --------------------------------------------------------------------------- ----------------------- ------------------------------- --------- ----------------- ----------------------------------------. ------------ --------- ---------------------------;------------------------------------- ---------- -------- -------------------------------- -------------------------------.------------------------ ---------------------------------------- -------------------- --------------------- -------------------- Cone.A lone.8 Cone. Blank Q Quantitation Limit 10 10 ID 10 la 10 10 18 10 10 10 A = RAD OJfC. B - tOC. MULTIPLIED BY DILUTION FACTOR E = CISC. OUT OF CAL. RANGE * = RELATIVE RE1ENT1UN TIME OUT OF RANGE Lab Chronicle: ,,nt. by 44 DUP050308020 ' 1A . VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract: ______ BRS4S Lab Code: LANCAS Case No.: ______ . SAS No.: _____ _ SDG No.: Matrix: (soil/water) WATER Lab Sample ID: 2583208 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >ISJ15 Level: (low/med) LOW Date Received: 09/18/96 % Moisture: not dec. .. Date Analyzed: 09/19/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0 Soil Extract volume: . ' (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) tXG/L Q 74-87-3----------------- Chloromethane 75-01-4------------------Vinyl Chloride 74-83-9-----------------Bromomethane 75-00-3------------------Chloroethane 75-35-4--------- -------- 1,1-Dichloroethene 67-64-1-----------------Acetone 75-15-0------------------carbon Disulfide 75--09--2-------------- Methylene Chloride 75-34-3------------------1, l-Dichloroethane 540-59-0----- ----------1,2-Dichloroethene (total) 78-93-3---------------2-Butanone 67-66-3------------------ Chloroform 107-06-2---------------1,2-Dichloroethane 71-55-6------------------1,1,1-Trichloroethane 56-23-5----------------Carbon Tetrachloride 71-43-2------------------Benzene 79-01-6-----------------Tr ichloroethene 78-87-5------------------1,2-Dichloropropane 75-27-4------------------Bromodichloromethane 10061-01-5----------cis-1,3-Dichloropropene 10061-02-6-----------trans-1,3-Dichloropropene 79-00-5------------------1,1,2-Trichloroethane 124-48-1-- ----- --Dibromochloromethane 75-25-2----------------- Bromof orm 108-10-1----------------4-Methyl-2-Fentanone 108-88-3----------------Toluene 127-18-4----------------Tetrachloroethene 591-78-6------ ---------2-Hexanone 108-90-7--------------Chlorobenzene 100-41-4---------------- Ethylbenzene 1330-20-7------------Xylene (total) 100-42-5--------------- Styrene 79-34-5-------------- ir 1 2,2-Tetrachloroethane FORM I VOA 10 u 10 u 10 D 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 tr 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 D 10 u 10 u 10 u 10 u 10 u 10 u OLM03.o45 DUP050308021 Data File: >18315::D3 Names BR84S 2583208 Mi sc: ~TLN gWL HC =1 +> Quant Output File: Instrument IDs #I962631AA &5 *5 $AISJB2 ''IS315::D7 HF'03046 Id Fj les IA639D::DB Titles 3/90 SQW Water/Med Soil ID File for Inst. HPO3046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLN-262 Quant [irae : 960919 13:36 Injected at: 960919 13:12 46 DUP050308022 QUPNT REPORT Page 1 tip erstor ID: TLN-262 Quant Output File! 'MSJlSi: : D7 Data Fites >1S315:s 03 Name: BRS4S 25832OS til sc: "TLN .{WL; *C =1 ** ,#1962631AA &9 Revs 7 Quant Time Injected at Dilution Factor Instrument ID *5 ' ISJB2 960919 13:36 960919 13:12 1.00UGU HP03046 ID .Files 1A639Q::DB . Title: 3790 SOW Water''fled Soil ID S- i le for Inst. HP03046 Last Calibration: 951122 10:44 Last deal Time 960919 06:34 Compound 1) 15) 17) 29 ) 31) 41) J *8romocti loromethane 1,2-Dichloroeth8ne-d4 *1,4-Difluorobenzene *Chlorobenzene-dS To 1uene-d8 4-Sromofluorobenzene * Compound is ISTD R.T. Q ion 8.36 9.32 10.04 14.33 12.23 16.07 128.0 65.0 114. 0 117.0 98.0 95.0 ftrea 38771 84719 163565 121552 146327 99086 Cone Units 50.00 47.42 50.00 50.00 50.82 49.25 UG7L UG7L UG7L UG/L UG7L UG/'L q 9a 89 87 85 96 75 47 DUP050308023 Lancaster Laboratories Quantitation Report-GC/MS Volatiles LLM: 2583200 TL.N File: "IS315 injected: 13:12 09/19/96 Sample: BRS4S 2583208 Dilution Factor: 1.0 Initial Vniurae/Ut.: 5.8 Standard: ''TSJS1 Inst. HP83846 Batch: I962d31ftfl Final Uolume/Ut.: 5.0 Method: 7156 Natrix/level: UL Blank; AlSJd2 * Internal Standards R.T. (*/-RT) Scan Uion ftrea(*/-SArea) Cone. QC Flag Lone Units = ug/L issBessaas*eBBBaBBSs*BBBBBBBBBaBaaBBBS*BBsBBBaBBBBmBBBBBaBBmBmBBBBmBmBBBBBBBBm*BBBmBBB**aBmaBBBBBmi>airs=mB*B==BB=BBm**: 1. Bromochloromsthane 17. 1,4-Difluorobenzane 29 . Chlorobenzene-dS # RETENTION TltlE OUT DF RANGE 8.365(.0262) 566 128 38771( 26) 50,88 10.84(.O246) 718 114 163565( 27) 58.88 14.33(.81968) 1079 11? 121552( 29) 50.00 * INTERNAL STANDARD AREA OUT OF RANGE NC NOT ABLE TO CALCULATE--!*) STANDARD. Surrogate Standards R.7. (V-RRO Scan Qian SSSSSSBSISSS 15. 1.2-Uvchloroethane-d4 9.318C-.808) 64B 65 31. Toluane-dS 12.23(.0006) 898 98 48. 4-Bromofluorobenzene 16,0?(.B807) 1228 95 * = RELATIVE. RETENTION TIME OUT OF RANGE * = *REC OUT OF RANGE Area Cone. XRec. Q laiaBisiisxstwKCissismsauiisxi! 84719 47.42 95 146327 58.82 102 99886 49.25 98 D SURROGATES DILUTED OUT NC COULD NOT CALCULATE Cone. Quantitation $ target Compounds R.T.U-/-KRD Scan Qion Area Conc.A Lonc.B Blank 0 Limit BBBBSBBBSBBSSBBBKSBBBSBBBSSBBSBSBBBBBBBBBBBBBBBBBBBBSBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBaBBBBBBBBBBBBBSBBBBBBBBBBBBBBBttSSBBBBSBBBBBBBBB 2. Chloromethane 3. Vinyl Chloride 4. Bromoaethane 5. Cbloroethane 6. 1,1-Dichloroethene 7. Acetone 8. Carbon Disulfide 5. ttethylane Chloride 11. l.l-D:chloroethane 12. 1,2-Dichloroethane (total) 13. 2-Butanona 14. Chloroform 16. 1,2-Dichloroethane 18, 1,1,1-Tnchloroe thane 1?. Carbon Tetrachloride 2U. Benzene 18 18 18 10 18 10 18 18 18 18 18 10 18 10 18 18 21. Irichloroethene 22. 1,2-Dichloropropane 23. Broir.odicnloromethane 24. cis-l,3-Dichloropropene 23. trans-l,3-Dichloropropene 26, 1,1,2-Trichloroethane ssssssasrsssttsssassstsssssss&sassatBStBxeteMfissetsseassatrsstsssesssttSBatBatssflKtssss 18 10 18 10 18 10 sastssssscssscsssessssBSsa A = RAW CONC. B = CONC. MULTIPLIED BY DILUTION FACTOR E * EMC. OUT OF CAL. RANGE * - RELATIVE RETENTION TIME OUT OF RANGE Lab Chronicle: _Ent. by. Pag e i o f 2 _Ver. by --^ g.... DUP050308024 Lancaster Laboratories Quantitation Report-GC/MS Uolatiles Lilts St E? S 3 22 O S T l--i'-'l :Hlie: "'1SJ15 Injected: 13:12 89/19/96 Sanple: BRS4S 2583208 Dilution Factor: 1.0 lmttai DdltlraB^Ut.s 5.0 Standard: A1SJS1 Inst. HPD3046 Batch: I962631flfl Final Uoluaa/Ut.: 5.8 Method: 7156 Matrix/level: Blank: A1S382 Cone. Quantitation # target Compounds R.T.H/-RRTJ Sean Qian Area Conc.fi Lone.8 Blank Q Limit 39sastnanaiasiERSralBi&^aatM8XB:BSKS&asaBSBteCBasamtMlBas3imHSlinBB*KsKlBKBM*MKSliVsaiatKKMgMttSSttBaHKnasisaiKMalieesssv 27. Dibromochloromethane 10 28. Bramaform 18 38. 4-ftethyl-2-Pentanone 10 32. Toluene 33. tetrachloroethene 18 1 34. 2-Hexanone 35. Chlorobenzene 36. Ethylbenzene ID 10 10 38. Xylene (total) 10 39. Styrene 10 41. 1,1,2.2-letrachloroethane 10 asseeesBB8msssa8BesssBBsccaBseisssmaBtianmats>ei*sHMass88ini8aiBMtanMumBnBBraaBBBasn8scsBsases3BsiBS8{iBeMe* fl RAW CGNC. 8 = LU1C. MULTIPLIED 8 DILUTION PACTUR E * CUNC. OUT UF CfiL. RANGE # = RELflTlDE HETEMT1UN TIME UUI UF RANGE Lab Chronicle: .Ent. by Analyst; Auditor; A *r JDates ll~t)ate: .. ?/?!% Uer. by PAGE 2 Iff 2 40 DUP050308025 . . 1A ^ VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE MO Lab Name: LANCASTER LABS Contract: 1 Lab Code: LANCAS Case No.:___ SAS No.: BRS3D SDG No.: Matrix: (soil/water) WATER Lab Sample ID: 2583209 Sample wt/vol: 5.0 (g/mL) ml Lab File ID: >ISJll Level: (low/med) LOW Date Received: 09/18/96 % Moisture: not dec. _ Date Analyzed: 09/19/96 GC Column: DB624 ID: 0.53 Dilution Factor: 1.0 soil Extract velum? ______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) 0g /l q 74-87-3------------------chloromethane 10 u 75-01-4------------------Vinyl Chloride 10 u 74--83--9-------- --Bromomethane 10 u 75-00-3-----------------Chloroethane 10 u 75-35-4---------------- -1,1-Dichloroetheme 10 u 67-64-1------------------ Acetone 10 u 75-15-0------------------ Carbon Disulfide 10 u 75-09-2-------- --Methylene Chloride 10 u 75-34-3----------------1,1-Dichloroethane 10 u A 540-59-0----------------1,2-Dichloroethene (total) 10 u 78-93-3---------------2-Butanone 10 u 67-66-3-----------Chloroform 10 u 107-06-2---------------1,2-Dichloroethane 10 u 71-55-6-----------------1,1, l-Trichloroethane 10 u 56-23-5-- ----- ----Carbon Tetrachloride 10 u 71-43-2------------------Benzene 10 u 79-01-6---------------- -Trichloroethene 10 u 78-87-5------------------1,2-Dichloropropane 10 u 75-27-4-------------Bromodichloromethane 10 u 10061-01-5----------- cis-1,3-Dichloropropene 10 u 10061-02--6----------- trans-1,3-Dichloropropene 10 u 79-00-5----------- ------1,1,2-Trich1oroethane 10 u 124-48-1--------------- Dibromochloromethane 10 u 75-25-2------------------Bromoform 10 u 108-10-1--------------- 4 -Methyl-2 -Pentanone 10 u 108-88-3----------------Toluene 10 u 127-18-4----------------Tetrachloroethene 10 u 591-78-6----------- --2-Hexanone 10 u 108-90-7----------------Chlorobenzene 10 u 100-41-4---------------Ethylbenz ene 10 u 1330-20-7--------------Xylene (total) 10 u A 100-42-5----------------Styrene 79-34-5------------ 1,1,2,2 -Tetrachloroethane 10 u 10 u FORM I VOA 50OLM03.0 DUP050308026 TOTOL ION CMROMCTOSRClII Data Filet >ISJ11::D3 Name: BRS3D 2583209 Misc: ~TLN @WL %C =1 +> Quant Output Files Instrument ID: #I962631AA *5 *'"ISJB2 ^IS311::D7 HP03046 Id file: 1A6390::DB Title: 3/90 SOUi Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLM-262 Quant lime : 960919 11:29 Injected at: 960919 11:04 5i DUP050308027 QUANT REPORT Uperator ID: TLN-262 Output Fi le; ''"ISJll: :D7 Data File! >iSJll:sD3 Name: E3RS3D 2583209 mac: ~TLN (jlWL. KC =1 +> Uuant #1962631AA &5 Ke u>: 7 Qu ant Ti me Injected at Dilution Factor Instrument ID *5 $'N1S3B2 Page 1 y609iv ii:2y 960919 11:04 1.ou uoo HP03046 ID File: IA6390:::DB Title; 3790 BOW Water/fled Soil ID File Last Calibration: 951122 10:44 For Inst. Last HPC3046 Qcal Time: 960919 06:34 Compound 1) 15 ) 17) 29 > 31 ) 40 ) Bromoch16 romethane 1,2-Dichloroethane-d4 *1,4-Dif1uorobenzene *Chlorobenzene-d5 'l o iuene-dB 4-Bromo Fluorobenzene * Compound is tSTD R.T. Q ion 8.3? 9.30 10.03 14.33 12.22 16.06 126.0 65.0 114.0 117.0 98.0 95.0 Area 39376 85646 165349 122020 147990 97619 Cone Units 5U.- 00 47.20 50.00 50.00 51.20 48.34 Uc-'L uc/c UG/L UG7L UW7|_ UG7L A 9j90 89 84 97 76 5S DUP050308028 Lancaster Laboratories Quantitation Report-SC/ftS Volatiles LL.I4: 25832 O V TI_M hie! "1SJ11 injected! 11:84 09/19/96 Cample: BRS5D 25B320? Dilution factor: 1.0 Initial Volume/ldt.: $.0 Standard: AISJS1 Inst. HP03046 Batch: 1962631AA Final Volume/Ut.: 5.0 Bethod: 7156 ftatrix/level: UL Blank: AlSJli2 V internal Standards SS8) 1. JBrosochloromethane 17. 1,4-Uifiuorobenzene 29. Chlorobenzene-d5 - RETENTION TIME OUT OF RANGE R.T. ( ART) Sean Qion Area(+/-*ftrea) Cone. UC Flag Lone Units = ug/c 8.35U.8124) 566 128 39576( 28) 50.08 18.O5C.0117) 718 114 165349( 28) 50.00 14J3C.8817) 1088 117 122028C 29) 58.09 * - INTERNAL STANDS AREA OUT OF RANGE NC * NOT ABLE TO CALCULATE---NO STANDARD. * Surrogate Standards R.T. CV-RRT) Scan (lion Area Cone. XRee. It s8sassQSccasssMBas*iisesBsttBss8S3assaeacuMSicscHKMua8*HsassntBMaBtiiBMn8aa8stnw8>aiUHUsBMasra8as8 15. l,2-Uichloroethane-d4 9.394C-.9U0) 648 65 51. Toiuene-dB 12.22C.8886) 89? 98 48. 4-Qrowjfluorobenzane 16.06C.0906) 1229 95 4 * RELA'I WE RETENTION TIME OUT OF RANGE * - *REC OUT OF RANGE 85648 47.20 94 147990 51.28 182 97619 48.34 9? D - SURROGATES DILUTED OUT NC COULO NOT CALCULATE Cone. Quantitation target Compounds R.1.U/-RRTJ Scan Cion Area Cone.A Conc.b Blank Limit tsaaaniinsnauaiRinnininnainnimniBnnnnnnnminmnnuniBntunninnKonin 2. Ubloromethane 3. Vinyl Chloride 4. Bromomethane 5. Chioroethane 6. 1,1-Dichioroethane 7. Acatone S. Carbon Disulfide 5. Methylene Chloride 11. l.-l-Biciiloroetbane 12. 1,2-Dichloroethene ttotal) 15. 2-Butanone 14. Chloroform 16. 1,2-Oichloroethane 10. 1,1,1-Triehloroethane IV. Carbon ietrachlonde 21). Benzene 21. Snchloroethene 12. 1,2-Dichloropropane 23. arotnodichloromethane 24. cis-l,3-Diehloropropene 25. trans-l,5-Dichtoropropene 18 10 111 10 18 18 18 18 10 18 10 10 1U 10 iu 10 10 18 18 18 18 26 1,1,2-Trich to roe thane --------------------------------------------------------------- ------------------------------------------------------------ 18 sssaMassass9SS8e9Saeefts3s^Sess8aSSS9ssttBSSga8S1B9SSSeaSSSS3QS^BseSaS~eM(!|SeSBttSSSBSXSSSBsasCSS:ra3ne3as98XSeSSSSaSesssBseS8S.asaas A = RAW CUNC. B - COUC. MULTIPLIED BY DILUTION FACTOR E - CONE. OUT OF CAL. RANGE * = RELATIVE RETENTION TIME OUT OF RANGE Lab Chronicle: JEnt. by PASt 1 UF 2 Ver. by _________ K %} a V DUP050308029 Lancaster Laboratories Quantitation Report-GC/fB Volatiles LLl$: 2585209 TLN Hie: A1SJ11 Injected: 11:04 0949/96 liampie: BRS3D 2583269 Dilution Factor: 1.0 initial Uoluie/Ut.: 5.8 Standard: Inst. HP03046 Batch: 194263188 Final Volune/Ut.: 5.0 Method: 7156 flatrix/level: Blank: AISJti2 target Compounds R.1.(*/-RK0 Scan Qion Cone. Quantitation Area Lone.A Conc.B Blank Limit MraBsaxascmaBssKattsesttnKSBeetKriBttBafivsMstfcsinBnBs 27. DibroaiochlsrOBiethane ------------ ---------------------------- ---------------------- 3tt. 4-nethj)l-2-Pentanone ------------------------------ :------- ------------------------------ 32. loluene TM------------------- ------------------------------ 33. letrachloroethene --------------------------------------------- .---------- ------- 34. 2-Haxanona ------------------------------------------ ---------------------- 35. Chlorobenzene ------------------------------ -------------------------------------- 36. Ethylbenzene ------------------------------- ------------------------------------ 38. Xylene (total) ------------------------------------ --------------- ---------------- 39.. Styrene ------------------------------------------ 41. 1.1.2,2-Set rachloroethane -------------------- :--------- *---------------------------------------------------------------------;-------- Baaaai3sstsBa8:cc8aBBseBaaaa23s;8B8BBBaB38ss*n8SSBnr3uat8BaBBit8iB8BBnBBn8*BBesnnsBSsoi**8CtMai 1U 111 16 la 10 lit 10 111 10 11) A t LOtC. B CDHL. MULT IfLIS) BY DlLtltlON FACTOR E * LUC. BUT OF CfiL. SftfffiE * * RELATIVE HElLMTlUN UflE UUf OF RANGE Lab Chronicle: _Ent. by Analyst: Auditor: iAO-Ctt'& _Date: ^^-Date: ijjlfcik _Ver. by PAGE 2 OF 2 54 DUP050308030 1A VOLATILE ORGANICS ANALYSIS DATA SHEET SPA SAMPLE HO Lab Names LANCASTER LABS Lab Code: LANCAS Case No.: ______ Contract: ______ . SAS No.: ______ . DRA3S SDG No. : Matrix: (soil/water) WATER Lab Sample ID: 2583210 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >ISJ14 Level: (low/med) LOW Date Received: 09/18/96 % Moisture: not dec. . Date Analyzed: 09/19/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0 Soil Extract Volume: ______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3------------------ Chloromethane 75-01-4------------------Vinyl Chloride 74-83-9------------- --Bromomethane 75-00-3------------------chloroethane 75-3 5-4 --------------1, l-Dichloroethene 67-64-1------------------Acetone 75-15-0----- -------------Carbon Disulfide 75-09-2------------------Methylene chloride 75-34-3------------------1,1-Dichloroethane 540-59-0----------------1,2-Dichloroethene (total) 78-93-3------------------2-Butanone 67-66-3------------------chloroform 107-06-2--------------1,2-Dichloroethane 71-55-6----- ------------1,1,1-Trichloroethane 56-23-5------------------carbon Tetrachloride 71-43-2-------- --------- Benzene 79-01-6------------------Trichloroethene 78-87-5------------------ 1,2-Dichloropropane 75-27-4-----------------Bromodichloromethane 10061-01-5------------cis-1,3-Dichloropropene 10061-02-6----------- trans-l, 3-Dichloropropene 79-00-5-----------------1,1,2-Trichloroethane 124-48-1----- --------- -D ibromochloromethane 75-25-2------------------ Bromoform 108-10--1---------------4-Methyl-2-Pentanone 108-88-3------------- Toluene 127-18-4----------------Tetrachloroethene 591-78-6----------------2-Hexanone 108-90-7----------------Chlorobenzene 100-41-4----------------Ethylbenzene 1330-20-7--------------xylene (total) 100-42-5----------------Styrene 79-34-5----------------1,1,2,2-Tetrachloroethane 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FORM I VOA OLMG3. Cjjj g DUP050308031 Data File! >ISJ14::D3 Quant Outpuf Fi1e: 'MSJ14::D? Names DRR3S 2583210 Instrument IDs HPG3046 flisc: ~TLN gML C =1 +> #I962631AA &3 *5 $'"1S3B2 Id F.i le s 1A6390: :DB Title: 3^90 SOW Uater/'Med Soil ID File for Inst. HPG3046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLN-262 Quant lime : 960919 13:06 Injected at: 960919 12:41 56 DUP050308032 QUANT REPORT Page 1 Operator IDs TLN-262 Output File: rtISJ14ssD7 Data File! >1S314:-D3 Nfime ! 0RA3S 2583210 (i;isc: ~TLN (jjfWL.. %C "1 + > Quant #1$>6263lAA &5 Rev! 7 Quant Time! in jected at: Dilution Factor: Instrument ID: *5 $-'IS3B2 96U9I9 13 : Ltd 960919 12:41 1.0 0 U 0 0 HP03G46 ID File: IA6390: iBlS: Title ! 5790 EOU) Water/Fled Soil Last Calibration: 951122 10:44 ID File for Inst. Last HP03046 Qcal Tima: 960919 06:34 Compound 1) 15) 17) 29) 31) 40) ^Bromoch iorometbane 1,2-Dichloroethane-d4 *1;4-Difluorobenzene *Chlorofaenzene-d? Toluene-d8 4-Bromofluorobenzene * Compound is (STD R.T. Q ion Area 8.38 9.33 10.05 14.34 12.24 16.07 128.0 65.0 114. 0 117. 0 98.0 95.0 38676 83628 163613 , 121255 142624 97919 Corec Units 5 0.00 46.92 50.00 50.00 49.66 48.79 UG/L UG/L UG/L UG/L UG/L UG/L q 94 8B 87 85 9tl 77 57 DUP050308033 Lancaster Laboratories Buantitatien Report-SC/MS Volatiles LLt 2583210 TL.N files A1SJ14 Injected: 12:41 09/12/26 Sample: DRA3S 2583210 Dilution Factor: 1.0 Initial Volune/Wt.f 5.0 Standard: "ISDSl Inst. HP0J046 Batch: 1962631m Final Volume/Ut.: 5.0 Method: 7126 tlatrix/level: UL Blank: "ISJua i Internal Standards R.T. C*/-RT) Scan Dion fireaCV-XArea) Cone. liC Flag Cone Units = ug/L sasHsmBiraasa3x*a38nEsBi&8:8XBm*Baist9BrtttaBKKaMLBrtaNBaDBmBassataKMSinsanBaBBBmBBMBIBRBWMMBSmiBBBIB8SBIBZ88aBBBBB88BBBBBa*BB8BaS*BnaB8a* 1. Bromochloramethane 17. 1,4-Difluorobenzene 2y. Chiorobenzene-d5 # RETENTION TIME OUT OF RANGE 8.3761.8376) 560 128 38676C 26) 58.00 10.B5t.03ai) 704 114 1636131 27) 5O.0O 14.34C.0184) 1073 117 121255C 28) 50.00 * * INTERNW. STANDARD AREA OUT OF RANGE NC NOT ABLE TO CALCULATE-NO STANDARD. i Surrogate Standards R.T. <*/-RRO Scan 9 ion Area Cone. SKee. U 15. I.2-Dichloroethane-d4 9.330C-.080) 642 65 31. Toluena-dS 12.24C.0OD7) 892 98 40. 4-Braiwfluorobenzene 16.07I-.008) 1221 95 * RELATIVE RETENTION TIME OUT OF RANGE * *REC OUT OF RANEE 83628 46.92 142624 49.66 97919 48.79 0 - SURROGATES DILUTED OUT 94 99 98 1C - COULD NOT CALCULATE Cone. Quantitation n $ Target Compounds R.T.C+/-RRT) Scan Oion 3sDsssea*B83*s8saac8aacsrvs8ttiisa8sssss9sssssB8iBa8tSBn8SHt! Area Cone, ft 8888B8B1 Cone,8 Blank Q Limit ia*SB8mssaBi 2. Chloromethane 3. Vinyl Chloride 4. Bromomethane 5. Chlsroethane 10 is 18 10 6. 1.1-Uichloroethene 7. Acetone 18 10 8. Carbon OisulFide 9. Methylene Chloride 18 10 11. 1,1-Oichleroethane 18 12. 1,2-Dichloroethene (total) A 13. 2-8utanone 14. Chloroform' 10 18 10 16. 1.2-Qichioroethane 18 18. 1,1,1-Trichloroethana 10 19. Carbon Tetrachloride 20. Benzene 10 ID 21. Triehlaroethene 18 22. 1,2-Biehloropropane 23. Bromodichloromethane 10 lu 24. cis-l,3-Dichloropropene 25. trans-1.3-Uichloropropene 10 10 26. 1,1,2-Trichloroethane 10 ft * RAW core. B * CISC. MULTIPLIED B1 DILUTION FACTOR E - CQNC. OUT OF CAL. RANGE i - RELATIVE RETENTION TIME OUT OF RANGE Lab Chronicle: Ent. by. PACE 1 OK 2 *' --os- DUP050308034 Lancaster Laboratories Quantitation Report-GC/WS Volatiles Lilts 25&32 1Q TLN File: "(SJ14 injected: 12:41 09/19/96 Sample: DRAJS 25B3210 Dilution hector: 1.0 initial Volims/Ut.: 5.0 Standard: A1SL)S3, Inst. HPA3046 Batch; mi&Jlfifi Final Uoiune/Ut.: 5.11 Method: 7156 Matrix/level: UL Blank; AISJB2 Cone. Quantitation # Target Compounds R.T.(v-RRT) Sean Qion Area Cone,A Lone.8 Blank Q Limit aBtaaa*a*BO***c**mtt******|t***J****t**a*****aMa3a(****dia*KJtatti*****a*MttuaB*a*Mm******a***x3ca= 27. OibromochloromethaOB ----- ----------- ------------------------------------------------------- ------ 18 28. Bromoform JO. 4-Plethy1-2-PentanonB ----------------- -------------------------------- ------------- -- ---------------------- ~------ ----------------------- ------------- ------------------------------------------ *-------------------- ---------`--t ------- ----------- -- 10 111 32. Toluene , ------------------- ----------- --------------------------- ------------------ -- 10 ii. Tetrachloroethene ------~~-------- -- ------------------- -------------- - "IB 34. 2-feKdnone ----------------------- ---------------------- --------------*------------------------------ ---18 35. Chlorobenzene -- --------- -----------*- 1 36. Ethylbenzene .. ------------ ------------ ----------- --------------------------- ------------ ---------------- IB 38, Xylene (total) ---------------- -- ---------------------- ------------ ------------ ---.------------------ ,-- ----------------- -- iu 39. Styrene -- ---------------------- -- ---------------------------- ------------------------------ -------------- 10 41. 1,1,2,2-Tet rach loroet hane ------------------------------------- ------ ------ ----------------------- ------------------------------ 1U 3tsisa3aea3acsBasaitaaa8ota:saasBsetBSBMBUisaKiuaiiKSMaxiimiiMBmnt!UBSMBaaatffsmnBmsaaMssraaattaattta8mBma*sa*B8mBxaisttx ft = RfiU CONC. 8 * COMC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT IF CAL. RANK * - RELATIVE RETENTION TIME OUT OF RANGE PAGE 2 OF 2 oJ^'. )D DUP050308035 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract: ______. BRATB Lab Code: LANCAS Case No.: ______ SAS No.: ______. SDG No.: Matrix: (soil/water) WATER Lab Sample ID: 2583211 Sample wt/vol: 5.0 (9/mi) ml Lab Pile ID: >ISJ10 Level: (iow/ffied) LOW Date Received: 09/18/96 % Moisture: not dec. ' Date Analyzed: 09/19/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0 Soil Extract Volume: ______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3---------------- Chloromethane 75-01-4------------------Vinyl Chloride 74-83-9------- -----------Bromomethane 75-00-3--------- --------Chloroethane 75-35-4------------------1,1-Dichloroethene 67-64-1------------------Acetone 75-15-0------------------carbon Disulfide 75-09-2------------------Methylene Chloride 75-34-3-----------------1,1-Dichloroethane 540-59-0----------1---- 1,2-Dichloroethene (total) 78-93-3----------------- 2-Butanone 67-66-3--------- ---------Chloroform 107-06-2----------------1,2-Dichloroethane 71-55-6-----------------1,1,1-Trichloroethane 56-23-5--------- --------Carbon Tetrachloride 71-43-2-----------------Benzene 79-01-6------------------Trichloroethene 78-87-5-----------------1,2 -Dichloropropane 75-27-4-----------------Bromodichloromethane 10061-01-5------------cis-1,3-Dichloropropene 10061-02-6--------trans-1,3-Dichloropropene 79-00-5------------------1,1,2 -Trichloroethane 12 4 -48-1---------------Dibromochloromethane 75-25-2----------------- Bromof orm 108-10-1-------------- -4-Methyl-2-Pentanone 108-88-3----------------Toluene 12 7-18-4----------------Tetrachloroethene 591-78-6----------------2 -Hexanone 108-90-7---------------Chlorobenzene 100-41-4----------------Ethylbenzene 1330-20-7--------------Xylene (total) 100-42-5---------------- Styrene 79-34-5------------------1,1,2,2-Tetrachloroethane FORM I VOA 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 5OLM03.0 DUP050308036 Data File: >IS310::D3 Name: BRFitB 2983211 Hisc: "TLN gUL %C = 1 + > Quant Output File*. Instrument 10: #I962631AA 6.5 *5 $AISJB2 '"IS.KIO: :D? HP03Q46 id File: 1A6390::DB Title' J/'yp SOW Water/Tled Soil ID File for Inst. HPG3046 Last Calibration: 951122 10:44 Last Deal Time: 960919 Q6.*34 Operator 10: TLN--262 Quant Time : 960919 11:06 Injected at: 960919 10:34 60 DUP050308037 QUANT REPORT Page 1 Qnerator IDs ILN-262 Output File: '''ISJ1Q s :D7 Data File: >iSJ10::D3 Names SRATB 2583211 Hi sc: ~TLN WL C =1 +> Quant #1962631Aft &5 kew: *5 7 Quant Time: In j ected at: Di lution Factor: Inst rument ID: 1SJ82 >'6 0viy il s U6 960919 10:34 1 . U U !J U u ' HP03046 ID- Files IA63^D;s -:DB' Titles 3-"90 S(ilQ Water/Necl Soil Last Calibration: 951122 10:44 ID File for Inst . Last HP03U46 Qcal Times 960919 06:34 Compound 1) 13) 1?) 29) 31) *0) *0romochior6methane 1 J,2-Dicftioroethane-d4 *1,4-Difluorobenzene *Lhlorobenzene-d5 Taiuene-d8 4-Bramofluorobenzene * Compound is iSTD R.T. Q ion 8.36 9.30 10.02 14.31 12.22 16.03 128.0 65.0 114. 0 117.0 98.0 95.0 Area 404U4 84059 168853 124072 147845 101420 Lone Units 3U . 00 45.15 90. U0 50.00 50.31 49.39 UG/L UE/L UG/L UG7L UG-'L UG2L q 92 91 88 84 y i> 78 61 DUP050308038 Lancaster Laboratories Quantitation Rfcport-GC/MS Uelatilas LLI*: 2 S? O 3 2 X X TUN File; "lbilU Injected: lit:>4 uy/19/96 Sample: BRATS 2983211 Dilution Factor: 1.8 initial Uolusie/Ut.: 9.0 Standard: AiSJSl Inst. HP03Q46 Batch: 1962631AS Final Uolune/Wt.: 9.0 Method: 7196 Hatnx/level: WL Blank: AlSJU # internal Standards R.T. t*/-RT) Sean Dion AreatV-XArea) Cone. UC Flag Cone Units * ug/L ^ffq|ffiyi'mi!ffTrB]B8Ti'^wp'W^|i'gq:agBMe=ffaMe!MeBaiBlilBaiiBgaBBaBBBBBBBBBB8iBaBBBBaBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB**MaineiaasKessvastssatgsiasawBsssa 1. Brotsoehioromethane 17, 1.4-Difluorobenzene 29, Chlorobenzene-dt* * - RETENTION TIME DOT OF RANGE 8.3611.0224) 970 126 48404( 32) 98.80 10.02t.0093) 713 114 1688931 31) 90.00 14.31t-.014) 1082 117 124872( 31) 90.00 * - INTERNAL STANDARD AREA OUT OF RANGE NC K NOT ABLE TO CALCULATE--NO STANDARD. 4 Surrogate Standards R.T. t+/-RRi) Scan Dion Area Cone. sftec. 6 se:am>uc.U3sioa!S>imnn>ema><niaitEnnnniminnnnnn>n>nn>nnn>nnn<ni>aaisnunxnaii 19. l,2-B!ehloroethBrte-d4 9.3O2<-.002> 691 69 >1. loiuene-dti 12.22t.0013) 902 98 48. 4-BrqKpHuorobenzene 16.U3t-.00il) 1230 99 * RELAIIUE RETENTION TIME GUT BF RANGE * - KREC OUT OF RANGE 84099 49.19 vu 147849 90.31 101 1&1420 49.39 9V 0 SURROGATES DILUTED CUT NC COULD NOT CALCULATE $ target Compounds R.T.(*/-RRT) Scan Qion Cone, Uuantitation Area Conc.A Conc.B Blank (I Limit 2. Chloromethane 3. Utnyl Chloride 4. Bronomsthane b. Chioroethane 6. 1,1-Dichtoroethena 7. Acetone 8. Carbon Disulfide 9. Methylene Chloride 11. 1,1-Uichloroethane 12. 1,2-Uichloroethene Itotal) 13. 2-8utanone 14. Ch lorotons 16. 1,2-Uichloroethane IB. 1,1.1-Trichtoroethane 19. Carbon tetrachloride 20. Benzene 21. frichloroethene 22. 1,2-Dichloroprapane 23. Bromadichtaromethane 24. cts-l?3-Dichloropropene 2b. trans-l,i-Cuchloropropene 26. 1,1,2-lrichlorosthane 3BsBBssB8BSBsasBssBssss8BBSBBass&SBSasassBassaKB8BaBBSssBa888BassBBBBBBttB8aBesB8BBBBBBBSt8asssBBasssaaB:BSBSsms: lit 10 1U 18 10 10 18 10 10 10 18 18 18 10 10 10 18 10 10 10 18 10 A = RAW C01C. B CQNC. MULTIPLIED BY DILUTION FACTOR E CONC. OUT OF CAL. RANGE # = RELAT1UE RETENTION TIME OUT OF RANGE Lab Lhronicie: tnt. by _0er. by PAGE 1 OF 2 DUP050308039 Lancaster Laboratories Quantitation Report-GL/tlS Uolatilea LL1*: 2 3 3 2 X X TLN File: AlSJllf injected! 10i34 09/19/96 taample: CttftTB 2583211 Dilution factor! 1.1) inttial (to lume/Ut.: 5.0 Standard: A1SJS1 Inst. HP83046 Batch: 1962631AA Final Uolum/Ut.: 5.0 Metnod: )l% ttatrix/leveli UL Blank! A1SJB : Target Compounds R.M*/*RRi> Scan Sion Area Lone. A Uonc.t) Cone. Blank U Quantitation Limit BBBBIMKt 22. Uibrorcochtoromsthane 10 28. Bromoform 10 30. 4-fletftyl-2-F'entanone 1U 32. toluene ID 33. (etrachloroethena 10 34. 2-Hexanone 10 35. Chlorobenzene 10 36. Cthylbanzena 10 38. Xylene (total) 1U 39. Styrene 10 41. 1.1,2,2-1et r achloroetbane 10 aaaaaeaass*SBa*e*as**aBsa**c***MM**aa*axs*aBMBBmBM*BnBM*aa*aa*a***asa*a*attaBaa*saaaa ft = RftU tunc. B * UUfC. nuLflftLSBi BY DILUTION tftCTOR E = CUNC. UUl UF COL. RtoiLE * = RELATIUE RtltNTIUN "11ME UUl OF RAN1 Lab Chronicle! JEnt. by Analyst Auditor n ..ob. *44- Dates _^2_Date! j/lflfL tier. by PA0E 2 OF 2 A <* 06 DUP050308040 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract: BRA2D Lab Code: LANCAS Case No.: ______ SAS No.: SDG No.: Matrix: {soil/water) WATER Lab Sample ID: 2583823 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >GSP01 Level: (lqw/med) LOW Date Received: 09/19/96 % Moisture: not dec. _______ Date Analyzed: 09/25/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0 Soil Extract Volume: _______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ucr/L or ug/Kgr) UG/L o 74-87-3------------------ Chioromethane 75-01-4------------------- Vinyl Chloride 74-83-9------------------ Bromomethane 75-00-3 ---- -------- Chloroethane 7 5-35-4------------------1, l-Dichloroethene 67-64-1---------- -------- Acetone 75-15-0------------------- Carbon Disulfide 75-09-2------------------- Methylene Chloride 75-34-3------------------- 1, l-Dichloroethane 540-59-0----------------- 1,2-Dichloroethene (total) 78-93-3------------------- 2-Butanone 67-66-3------------------- Chloroform 107-06-2---------------- 1,2-Dichloroethane 71-55-6------------------ 1,1/ 1-Trichloroethane 56-23-5------------------- Carbon Tetrachloride 71-43-2------------------- Benzene 79-01-6------------------ Trichloroethene 78-87-5------------------ 1,2 -Dichloropropane 75-27-4--------------------Bromodichloromethane 10061-01-5----------- cis-1,3-Dichloropropene 10061-02-6------------trans-l, 3-Dichloropropene 79-00-5-----------------1,1,2-Trichloroethane 124-48-1----------------- Dibromochloromethane 75-25-2------ -----Bromoform 10 8 -10-1-------- -------- 4 -Methyl-2 -Pentanone 108-88-3----------------- Toluene 127-18-4----------------- Tetrachloroethene 591-78-6----------------- 2-Hexanone 108-90-7----------------- Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-42-5----------------- Styrene 79-34-5------------------- 1,1,2,2-Tetrachloroethane 10 u 10 u 10 u 10 u 10 u 10 u 10 u 3J 10 u 10 u 10 u 10 u 10 u 10 u 10 D 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FORM I VOA 4OLM03.06 DUP050308041 THTiftL i-: flRR0MTftf*R$'^ " . 4.00 3iiU0yiH. 'Tie 5$3*c S&OOOO-J : :J . i*/ 40000-] ' 4: 2CS0(k M I. rjpOOO" onrtrirL 40000- 1 .i V s J2. I t 0E2i 4- io ? . J. A.Jt i.= PUL 120 0 *> :T I0 f! !L 16 16 30 Do. la Fite: > GSF!) 1 : : 04 Quant Output File: /'GSFfll : : FM Name : BSR2D 2583823 Instrument ID: HP0346Q Mias : ~SHM gW:,, %C *> #098268IftA S^GSPBl &5 *5 =1 Id Fi le : Ifi'4390 : : DB Title : 3/9H Water/Med Soil ID File for Inst. HK"346s.: Last Calibration: 951207 01:53 Last ycal Time: 360925 0i::26 Operator II:: SftM-983 Quant Time : 960925 02:22 Injected at: 9BM92-5 01:57 65 DUP050308042 Cy. ; ,nU IlH*' FUal<'U' fVJ- ":' f'aj- - Operator ID : SAM'963 Output File : ''GSP01: : FM Data File: > GeHO1: : Haros : Bf;-'2D 25838 Id d Hist 1 -'SftM UL %C +> yuant Rev: #(2962681ftA S^GSPBl ? ytiant Tawe ; 1 ejected at Dilution Factor: Instr unient ID: &5 *5 .. =1 Ht<>-925 U: 2 9k .132S< ! I : b' ' i . ' :::. u 0 H- -:4t.: ID File: IP 390::DB . Title 3/90 'UaterVMed Soil ID File Last. Ca l i far at icri: 351 20? 01:59 for Inst.. HPOS'-'SO Last. Qcsi Tarr.e: 9hH325 U0:26 (lompoand 1) 9; 15} 1?! 29 > 31 > 10) *Bromochlororoethane Me thylene CbIo ride 1 J>2-Dichloroethane-d4 *1,4-Difluor obenzene *Ch 1 o r o be.ns e ne - d5 Toiuene-d8 4-Bromofluorobenzene * Compound as ISTD R.T. Q ion 3.49 S . 85 10.40 11 . 08 15.37 13.26 1? . 09 128.0 84.0 65.0 114.0 11?. 0 98 . o 95.0 fires d Li S 342? S'? bn 6 184:17? 148674 1913159 125190 Cone Units 5 0.0 0 3.19 4b . 06 5 00 5U . 00 4? 47 4 9.82 ug, L uq ' L. uq/L u.g/'L _* ' i_j ug/L l j g Ej . c M ,,' 99 3 OV 99 S3 66 DUP050308043 {grRgNi? feTRBffSRD S.FECTRLm rru >i5r0**3n a He'fhyi--^ n- * Chior-i (JOT 49 84 Srsn 403| HI 1 i'i . | 10000-j rI r4WuJ|Li n 8b` L Trnrrr J DO rrrr 150ri-yt.'i r'T*'-0rr0r _J Sftt1Pi_E SPFCTPLIrt <BfiCt=8R0>JMn SiJBTRSOTFD p l ie ; i!M?5'P01 BSH2U 2b&383 &c k fib 794. SUB 49 / Si Scan 40 6 . mitt. j-100 SQiP L 1& SO 1, 100 150 SAMPLE SPECfSUM (UHSLTERED> ffi l b yespdi Bm&o 583823 [Spl fib 794. 49 i{ 84 50ihj jJ 50 100 150 ecr , . nL ' eoo Scats 420 6.85 min. 100 07 "r*,rrt 200 Fils .'^SSPOi 4-r * 7--41? 7 80 Cn 40(4 rJt. v*""\ / / -j-x-,-; ~n-r- 7.0 Fills N3SPQ1 SS.7-S1." am 2o 4 F \ J/ V.. 0-^*4=4r 6.8 ' 7.0 Fiis >6SPG1 83.7-84.7 an 4004j //*\\ 1/ O-Hfri.u 6.8 \ ,T?- 7 .0 File >SSPvi 85.7-66.7 an D.-r.a File: >GSFU1 i s D4 Quant Output File: ''GKFOl : : FM Name: BRP2D 2583823 Instrument ID: HPU34S0 Mi sc : ~SHM @Wi. %C + > #CH626Blftfl S^GSPBl 65 *5 =1 Quant Time: 960925 02:22 Quant ID Pile: IM39U : DB In igcted at: 9SU925 01:57 Last Calibration: 95 1207' 1:1:59 Bast Qcal Time; 960925 00:26 Compound No : Compound Name : Scan Number : Retention Time: Quant Ion : Area : Concentration : o-walue : 9 Methylene Chloride 420 S.S5 rnm. 84.0 3427 3.13 ug/L 32 67 DUP050308044 Lancaster Laharatones Quantitation Report-GIL'ME Ooistiles LL1I; '!!-: File! AGSP0I Injected: 01:57 (19/25/96 Sample: BRH2D " 2593823 Dilution Factor' Initial Uoiume/Bt.: 1.0 5.0 Standard: AGSPS1 Inst. 89(13460 Batch; G962681AA Final Dclune/Ut.: 5.B Method; 7156 Katri5./leuEl: Ii. Blank. -'GSl'Bl 1 Internal Standards R.T. <*/-RT) Scan Qion Areal+/-$ftrea) Cone. ESS -s----;.-s;---,-----Btssr 53assistetss-cas ================= ======== ======= ================== =========: Flag Con: Units = ug/ 1. BromcchioroTfiethane 17. 1,4-fiiflucrebenzene 29. Chlorobenzene-d5 9.48B(-.B01) 11.08S-.005) 15.37C.0072) 647 7B4 1152 128 114 117 45203(-22) 1841771-241 14BG74C-25) 50.00 5U.80 50.00 1 RETENTION TIME OUT OF RANGE * INTERNAL STANDARD AREA OUT OF RANGE NC - NO? ABLE TO CALCULATE--NO STANDARD. I Surrogate Standards R.T. (+/-RRT) Scan ftion Area Cone. tEec. Q 15. l,2-Dichloroethane-d4 10.40.000) 725 65 3). Toluene-dB 13.261-.000) 971 88 40. 4-Bromofluorobenzene I7.83C-.000) 1380 85 I = RELATIVE RETENTION TIME OUT OF RANGE * = TREC OUT OF RANGE 67856 46.06 92 15B159 49.4? 99 125140 49.82 100 D = SURROGATES DILUTED OUT NC = COULD NOT CALCULATE Target Compounds R.T.H/-RKT) Scan Qion Area Cone.A Conc.B Cone. Blank Q Quantitation Limit 2. Chloronsethane 3. Omul Chloride 4. Bromotnethane 5. Chloroethane 6. 1,1-Dichloroethene ?. Acetone B. Carbon Disulfide S. Methylene Chloride 11. 1,1-Uichloroethane 12. l//-Diehlnroethene (total) 13. 2-Butanune 14. Chloroform 16. 1,'2-Dichloraethane 18. 1,1,1-Tnchloroethane 19. Carbon Tetrachloride 20. Benzene 21. Trichloroethene 22. 1,2-Dichloropropane 23,. Bromcdichlaromethane 24. cis-l,3-Dichloroprapene 25. trans-l,3-Dichloropropene 26. l.lj2-Trichloroethane -------------------------------------------------------------------------- :----------------------- ------------------------------------------------------------------------------------------------------------------------------------------------- -- ------------------------------------------------- 4-------------------------------------------------------------------------- 6.851 .0001 420 84 3427 3.188 3J ----------------------------------------------------------------------------------------------------------------------------- ----------------------------------------------------------------------------------------------------------------'-------------------------------------------------------------------------------------------------------------------------- .------------ -------------------------------------------------------------------------------------------- ------------------------------------------------------------------------------------------------------------------------------------------------------------ 10 111 10 1U 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 A = RAW CQNC. B = CONC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CAL. RANGE I = RELATiUE RETENTION TIKE OUT OI RANGE Lab Chronicle: tnt. bp PAGE 1 OF 2 Uer, by _______ 68 DUP050308045 ':' Lancaster Laboratories . Quantitation Eaport-GC/MS ttoiatiiss LLiff: Si '~zn & % r-n FiLe: "GSPOl Injected:01:57 <W:25/9& Sample: BSA2D 2583S23 Dilution Factor; 1,0 Initial I'olume/liSt.: 5,0 Standard: "GSPS1 Inst. HP03460 Batch; G9S2681ftft Final Uolume/Ut ; 5.0 Method: 7156 Matrix,-level: SL Blank: -'GSPBl 1 Target Compaunas 8 ? f-.-Sk'.'J Scan Qion Area Conc.fi Ccnc.B Cent. Blank Q Quantitation Limit 27, Dibromochlorofflethane 2fi Bromotoriri 30 `S-Methyl-2-Fentanone 3V. Toluene 33, Tetrachloroelhene 34, 2-Hexannne ,. 35, Chlorobenzene 3K. Ethylbenzene 38. Xylene (total) ,3M, Styrene 41, 1,1,2,2-Tetrachloroethane tssrestsesttsaasrasassareiesaataas ft = Ml CONC. 8 = CONC. MULTIPLIED BY DILUTION FfiCTOE E = CONC. OUT OE CAL. RANGE 10 10 10 Ilf 10 10 10 10 10 10 10 i = EELfiTlUE RETENTION TIME OUT OF EHNGE Lab Chronicle; _______________ ' __________________________ Ent,. by 65 DUP050308046 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract BRA2S Lab Code: LANCAS Case No.: _______ SAS No. : _______ . SDG NO.: _______ . Matrix: (soil/water) WATER Lab Sample ID: 2583824 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >GSP02 Level: (low/med) LOW Date Received: 09/19/96 % Moisture: not dec. _______ Date Analyzed: 09/25/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: l.o Soil Extract Volume: _______ (uL) Soil Aliquot Volume: _______ <uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3------ ---------- Chloromethane 75-01-4------------------- Vinyl Chloride 74-83 -9------------------ Bromomethane 75-00-3------------------- Chloroethane 75-35-4------------------- 1,1-Dichloroethene 67-64-1------------------- Acetone 75-15-0------------------- Carbon Disulfide 75-09-2------------------- Methylene chloride 75-34-3------------------ 1,1-Dichloroethane 540-59-0----------------1,2-Dichloroethene (total) 78-93-3------------------- 2-Butanone 67-66-3--------------- -Chloroform 107-06-2----------------- 1,2-Dichloroethane 71-55-6------------------- 1,1,1-Trichloroethane 56-23-5------------------- Carbon Tetrachloride 71-4 3-2---------- -------- Benzene 7 9-01-6------------------ Trichloroethane 78-87-5------------------- 1,2-Dichloropropane 75-27-4------ ------ --Bromodichloromethane 10061-01-5---------- -cis-l,3-Dichloropropene 10061-02-6-------------trans-1,3-Dichloropropene 79-00-5------------------ 1,1,2-Trichloroethane 124-48 -1----------------Dibromochloromethane 75-25-2------------------- Bromoform 108-10-1-------- --~4-Methyl-2-Pentanone 108-88-3----------------- Toluene 127-18-4----------------- Tetrachloroethene 591-78-6---------------- 2 -Hexanone 108-90-7------------ --Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-42-5----------------- Styrene 79-34-5------------------ 1,1,2,2-Tetrachloroethane FORM I VOA 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u OLM03.C)7 0 DUP050308047 TON >fc>? Vc r 80000n 40OQO-j 320000-j 2C2:0C'C4 I 18000CH 4 160000^ 140000-j ISQOCHH 1000004 4 80000-j Si'C'OC"FI 4QQQ0j 20000-j j Cm= I400 .___ ___i. gJep?" gflftSSgc TIC SCO V$CTT ftUL 1200 a jj =gC 5 T<Tc65= 3 mok iI I iT jc S j! <Mi m! ii n a 1--1rC~' 1--iFf r 14 --r~ if. If 2t0 Dr. t. a F=.Le: >GSF02 : : D4 Quant Output File: ''GSFU2 ! : FM Name: BRA2S 2583824 Instrument ID: HPQ346G Mi sc : ~SH @JilL %C + > #G9H2681fift S^GSPBl &b *5 =1 Id File: IH4390::DB Title: 3/Sli Uater/Med Soil ID File Last Calibration: 95120? 01:59 tor Inst. HPH34fc>l! Last yeal Time: 860925 00:26 Operator ID: Quant Time : Injected at: SPlM-BBB 960925 02:55 960925 02:30 71 DUP050308048 Ooerator ID: SAM-9H3 Out pu t f'l ie : ''GSHU2 ; : FM Do * a File: > CS H i] 2 : : D4 Newift : BRH2S 25838V4 M 1 S C ' ~SPM &JL 'SC +> yuant #0962681 HP Hev: 7 ont Time : Injected at: Dilution Factor: Instrument ID: &5 *5 =1 i.i j- p O ? er, n ? s u St- i!S2w :j 2 : 3 U i . o 0;; o o Hi- -346 ir, Fi Is : JP439U : : DH Title : 3790 tdater^'Med Soil ID File Last Calibration: 951207 01 : 59 For Inst . HP0346 0 . Last. Qcal Time.: 961ISV5 0 0 : 2 r- Compound 1> lb i 17) 9W \ 31) 4H ) *BroTnoc hloromet hane 1 .2.-Die hior oet hane-d4 *1 ,4-DiflQDrobenseris *Cb 1 orc benzene-d5 To 1uene-d8 4 Kromofluorobensene * Compound is 1 STD R . T . Q ion 9.46 10.37 11 . 05 IS .33 13.24 17.05 128.0 65.0 114.0 117.0 98.0 95-0 Area 43616 66262 172338 136114 144153 119975 Cone lira t s 5 0.0 0 46.75 50.00 5i: . 0 0 49.88 5 V . 17 ag.*'L ug/L ug/L ug.-'L ug7L ug.-''L q yu a ri 95 92 98 84 t-J DUP050308049 Lancaster Laboratories Quantitation Report-GC/MS Volatiles LLH: File: AGSP02 Injected: 82:30 19/25/96 Sample: BKA2S 2583B24 Dilation Factor: 1.8 Initial Qoiame/lilt.: .5.0 Standard: AGSFS1 Inst. HP034S8 Batch: G962681HA Final Uolume/lOt.: 5.0 Method '/156 Matrix/levei: Blank: %`bi'Bi S internal Standards R.T. (+/-RT3 Scan Qian Areal+z-tArsa) Cone. QC Hag. Cone Unit;. = an 'L ssssB%ss3Sssss3Ss&3asaails=ssBS8ssssssBSSSS=sss$3asss99Sss8SS:a9seseeas8sesB*HasssBaBcssac9BBsasa&aa&esessssBssssssBaeaa9a&ssssss = :; 1. Bromochloromethane 17. 1,4-Difluorobensene 9.465I-.0253 646 12S 11.05(-.04B) 782 .114 43S16C-25) 172338C-23) 50.00 50.00 29. Chlorobenzene-d5 8 = RETENTION TINE OUT OF RANGE 15.33t--. 029 > 1150 11? 13S114C-31) 50.130 * = INTERNAL STANDARD AREA OUT OK RANGE NO = NOT ABLE TO CALCULATE--NO STANDARD. f Surrogate Standards R.T. (+/-RSTS Scan Qion Area Cone. %Rec. 15. l,2-Dichloroethane-d4 10.37(.OUOOi 724 65 33. Toluene-dB 13.241.00823 970 96 40. 4-BroTiiofluorohenzene 17.05(-.0903 1298 95 8 * BELATIUE RETENTION TIME OUT OF RANGE * = iC OUT OF RANGE 66262 46.75 94 144153 4S.B8 100 119975 52.17 IU4 D = SURROGATES DILUTED OUT NO = COULD NOT CALCULATE 8 Target Compounds R.T.(+/-RRT3 Scan Qion Area Cone,A Conc.B Cone. Blank Q Quantitation Limit 2. Chloromethane 3. Oinyl Chloride 4. Bromomethane 5. Chloroethane 6. 1,1-Dichloroethene 7. Acetone 8. Carbon Disulfide 8. Methylene Chloride 11. 1,1-Dicbloroethane 12. 1,2-Dichloroethene (total) 13. 2-Butanone 14. Chloroform 16, 1,2-Dichloroethane 16. Ijl.l-Tricbloroethane 15. Carbon Tetrachloride 20. Benzene 21. Trichloroethene 22. 1j2-0ichioropropane 23. Bromschchioronethane 24. cis-l,3-Dichlorapropene 25. trans-l,3-Dichioropropene 26. 1,1,2-Tnchloroethane ------------------------------- :-------------------------------------------------------------------------------------------- ---------------------------------------------------------------------------------------------------- ;-----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------.------------------------------------ --------------------------------------------------------------------------------------------------------------------.----------------------------------------------------------------------------------------------------------------------------- ----------------------------------------------------------------------------------------------------------------------------- . ------------------------------------------------------------------------------------------------------------------------------------ 1(3 10 10 10 10 10 10 A RAN CCC. B = CONC. MULTIPLIED BY DILUTION FACTOR E CUNC. OUT OF CAL. RANGE 8 = RELATIVE RETENTION TIME CUT OF RANGE Lab Chronicle: _____________________________________________________________________________________ Ent, bu PAGE 1 OF 2 Uer. by _____ r4f-Z;S DUPO 50308050 Lancaster Laboratories Quantitation Repori-GC/llS Udatiies LLli; *JcJ* ^ *~Tj fcS IrJ! 1M File: -GSP02 Injected: 02:36 G3/25.'S6 Sample: 8Rfl2S 2583823 Dilation Factor: 1.0 Initial (lolmfe/Ut.: 5.0 Standard: ''GSPS1 Inst. HP03460 Batch: ($6268IftA Final Uoiume4Jt.: 5.0 Target Compounds R.T.lv-RR?) Scan Qion Area Method: 7158 Matrix/leoei: (it. Blank: "GSPB1 Cone.ft Cone.B Cone. Blank Q Quantitation Limit 27. Dibrcmochloromethane 28. Bramoi-onts 30.. 4-Methyl-2-Pentanone 32. Toluene . 33. Tetrachlornethene 34. 2-Hexanone 35. Chlorobenzene 36. Ethylbenzene 38. Xylene (total) 39.. Styrene 41. 1,1,2,2-Tetrachloroethane --------------------------- --------------------------------------------------------------------------------------------- -- -----------------------------------;------------------ ;---------------------------------- ----------------------------------------------------------------- ;--------------- 1------------------------------ --------------------------------------------------------------------------------- 1-------------------------------------------------------------------- ----------*--------------------------------------------------------------------------------------------- -------------------------------------------- ;------------------------------------------ ----------------------------------------------------------------------------------------------------------------------------------------------- -------------- :------------ ----------------------------------------------------------------------------------------------------------------------------- 10 10 16 10 16 10 16 1(1 10 10 18 ft = HAli CONC. B = CONC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CflL. RANGE i KELflTSUE RETENTION TIME OUT OF RANGE Lab Chronicle: Ent. by DUP050308051 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract BRAID Lab Code: LANCAS Case No.: _______ SAS No.: _______ . SDG No.: _______ . Matrix: (soil/water) WATER Lab Sample ID: 2583S25 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >GSP03 Level: (low/med) LOW Date Received: 09/19/96 % Moisture: not dec. _______ GC Column: DB624 ID: 0.53 (mm) Date Analyzed: 09/25/96 Dilution Factor: l.o Soil Extract Volume: _______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3------- --------- Chloromethane 75-01-4------------------- Vinyl Chloride 74-83-9---------- -------- Bromomethane 75-00-3------------------ ch1oroethane 75-35-4------------------ 1,1-Dichloroethene 67-64-1------------------- Acetone 75-15-0------------------- Carbon Disulfide 75-09-2---------- -------- Methylene chloride 75-34-3------------------- 1,1-Dichloroethane 540-59-0------ 1,2-Dichloroethene (total) 78-93-3---------- ---------2-Butanone 67-66-3------------------- Chloroform 107-06-2-------- ---------1,2 -Dichloroethane 71-55-6---------- -------- 1,1,1-Trichloroethane 56-23-5------ -------------Carbon Tetrachloride 71-43-2---------- ------ Benzene 79-01-6------------------- Trichloroethene 78-87-5---------- ---------1,2 -Dichloropropane 7 5-27-4---------------- Bromodichloromethane 10061-01-5-- ------ cis-1,3-Dichloropropene 10061-02-6------------trans-l,3-Dichloropropene 79-00-5------------------ 1,1,2 -Trichloroethane 124-48-1----------------- Dibromochloromethane 75-25-2------------------- Bromoform 108-10-1--------------- 4 -Methyl-2-Pentanone 108-88-3------------ --Toluene 127-18-4--------- -Tetrachloroethene 591-78-6-----------------2-Hexanone 108-90-7----------------- Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7-------------- Xylene (total) 100-42-5----------------- Styrene 79-34-5------------------ 1,1,2,2-Tetrachloroethane 10 U 10 u 10 u 10 u 10 u 10 u 10 u 3J 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 tr 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FORM I VOA OLM03. 0 _ DUP050308052 Data File. X3SF03: : D*; yuan! Output File! AGHHQ3 : ; I'M Name: RRH1D 2582825 ' Instrument ID: HP034K0 Mi sc : ~SdM @(Jl. %0 +> #CaK2681fM-: $~<3SPB1 S.5 *5 =1 Id E'; Is' IM39Q : ' DB Title : 3/yil Uat.er/'Mp.d So: i ID File Last Calibration: 951207 0.1:59 for Inr.t . HPU348!) Last Qeal Time: H8U925 UU: 26 Operator ID: Q'lnnt Time : Injected at: SfTS=9S3 Sfci 11925 03:27 98HS25 03:0V. 76 DUP050308053 QMMNT PLFORT f1 /i'!p:eratnr ID:: SWM=483 Quant Output ,F) ie : ''GAP 17 3 : : FM Data Ftlia > LIS P 0 3 ! L>9 :: 2;5H282S/ ' -SAM @UL %C +; *G9S26S1AA Rev! 7- ycant T-'t w Inje.a+.ed a- ' Dilution Factor' Instrument IS!,' ' &5 *5 = 1 9S;t923 ; 1 ' 3 >','4'.7 U : !iy 1 . 1.1 n *.p ,i ij Hu' '' 46 = iy Ft !.; . IA A 3 9 C ! ! DH Title : 3790 fOater/Hed Soil ID File for Inst ; HP 03 96 0 Lost Ca 11 briatapn ; &5:T2 Bp 01! 59 Last Qcai T iw: 9 1I9 2 3 0 0 : 76 Compound : i) :S> i s :> 17 > 29 ) 31 ) -til > *Br omcchlor OTethar=e MctHplene Chloride . 1 .. 2- Dichiorciet hane-- d4 *1 . 4-Di f liiorohensiftne *Chlorobenzene-d5 Tc. Iuerft-d8 4-Sromofluorobensnne * Comprand is 1ST!) R.T. Q ion 9.45 6.82 10.37 11 . Q5 15.33 13.24 17. 05 12S . 0 .89.0 65.0 114.0 117.0 98.0 95.0 ftrea 423 9 0 331 a 65314 163927 132326 144071 1J 9970 Cone 0 n its 5U . do 3 . 26 Q? - 42 *"< 1 i ou 3 U . CL! b `.1 . 2 U t*. 36 t i-j L> UQ.'L ug/L uqv'I, u*3 .''L uq-.'-'L i.in .-'L l**1 "*! 94 99 99 91 H\ ' 34 11 DUP050308054 Hrn.UHKw ;rr t,'L - i ii.g VirH'^0%? ' j t4fc- .4.5* >?:? * "'ien^ cr*. x cv-1 .: CuC i<r pin 4>j.* i . *1- JV I i`t * ,iOp;OC^ '. k t : ? . :; 4 : T tTif--JjUii M. ew j-iccj i\ ?00 ^ariF.i. e fF-.TFiirl (RfSr.KGRC'iftin SCBTFa.'.Trp , C i-jV-e* : iiRwuyOk o$y I )ri Rfc> .. SUB Tc- Jd nir* ! '"it C" i <JWV1 H. ti-jcu-i! .y ! SOS f 1 L ^04- i 5c: i 00 iBC- goo SflfWtE SPFVTRMF .UNSI.TEREOT iFiia ::&s.03;:sftKiD "582825 I Dp * fib oi?0._ Scan 414 6.30 in i ii . ] | ^| [- IC'Oj tI SOT ! j ! i 40 4 ru- i File >SSPSS ,! i 8`T I/ ! o-i^.4-,,,..,. !e l -- ___ Kile 1SSD&S -84 .T ! 40C-, / }^ 6.8' j..,---^. File >6SP0S S5.F--36." ! i ! 4.V.0.-v} ^rj' ! i V. C! = an! Data File: ' G5F0':5 : ; DC Quant Output File: ''GAFtiS ' : Fit Mime : BRAID 2582B25 Instrument ID: HPU3c60 Misc : ~Sf-m (3Di:.. %C *) #t39626lHA $-sGSPBl &6 *5 =1 Quant Time: 960925 03:2? Quant ID Fi le: 1DM390: : DB Injected at: 9611925 03:02 Last Calibration: 95120? 01:59 Last Qcal Time; 9611925 DU: 26 Compound No Compound Name1., scan Numiner Retention Time Quant Jon Area Concent.r at i nn o-uaJ ue <3 Met'hii j ene Chloride 4! 1 C ' fc . 92 mm . 8 -'! . 0 3310 3.28 ug/L 78 DUP050308055 . l.ancasfRr tahinratoriBR Sjnanf statinn Rp.nnrt-Rn/IIK Uniat Up." !! 14! ?* > "9 FI 1? ^ r-r Filft! AfSPIIi In jfintp.d: 81:8? 119/99/94 Ra.-nr.lRl RRam IhluHnn Factnrl 9501095 l.fl Initial Un liina/ldt.! 5.11 Standard: /'SKPS1 Inst. HPK14f.ll Hatch! B94?481fV) Fins! UnhimR/tlt.: 5.11 tlathnd! 7154 flat riv/laua!! Rlar.1;: "fiSPRI Internal Standards R.T, I+/-RT5 Scan t}trm flreat +/-8flren t Rnr.r.. ==========s:===:===ts===:s:s=t::=:=::5J=:=ssssasssssaessssxssat#wn===sss ======= SSSSSSSSSS5SS9S69S========; !?: Fta.j I'nnr. Units = ii,-/i 1. Hrnmnr.hlcrrasBthane 1/. 1 ,4-Hi f hinrnhanrp.nfi 9.4541-.H14) 11.1151-.I1T9) m\ 198 777 il4 4919111-97) 141997!-Ill 58.1111 58.811 99. IThlnrnhttn7Rnfi-rf5 t = k f t f h i k in t mf n':s rs r mk f ' 15.TK-.fl98) 1145 117 11959ft(-y5) 58.111! * = IMFHNfi! STANIK ARRA SUIT HI RW NT. = HITT AHIF TJI i:a: SIISI ftTI--KIT STAWitfW. $ FtiirrnqatR Standards R.l. H/-RRT) Scan fjinn firea F.nnc. SRar. a I*;. 1 j?-flir.hlnrnRthanfi-ri4 18.171.81114) 719 45 1'.. Tnit:p.na-riH 11.94! .11089) 9*5 90 411, 4-Rrnmnf InornhenTBUR 17.1151-.811111 1991 95 t SFlfiltur RFrFSTtfiN I!(l IS IT II RAN * = r: ran nr 45114 144871 47.4? S') *^*| 95 1!!'/ 119478 51.14 1117 n = stewKRTKSi rnimm ran w: = misi) uni it a ii't s a ii- 1arnaf Cnropnunrts R. 1.1 t7-SRl1 Scan flsr.n flraa Cnr.r .3 I.ann.R f.nnr.. Hlar.k I1. (ThlnrniiiRfhanR ----------------------------------------------- ----------------------- 1. Utny! rhlnriria ----------------------------------------------------------------------- 4. Brnninmethanfi 8. nhinrnalhana --------------------------------------------------------------------------------------------------------------------------------------------- 4. 1 .t-Oirhlhrnp.thanR 7. ftr.atnr,R -------------------------------------------------------------------------------------------------------------------------------------------------- 5. narhnr. Disul f i rtn ----------------------------------------------------------------------- 9. tV.thylar.R lli-.lnriria 11. 1,1-nichlornethane 4.891 .am I 414 B4 1118 i. VP. f IV. 1 -hlr.r.-p.rhRnF. (t,stall 1?. ?~Rntannne 14. f>.lnrnf.-.nri If,. 1 ;9-!)ir.H Inrnp.fhana IB. 1 ,1,1-Tr >r.h inrnp.thana 19. Carbnn 1atrar.hlnrtdB V:i. Ranrana. 91. Trichlnmathfine 99. 1 .V-Dirh lr.rnnrnr.ana ?i. Flrninriir.hlnrnmp.thanp. V4. r.is-l .l-lhr.hlftrnr.rnnRnR A 95. trsns-1 jT-Oir.hlnrnnrnpp.np. 94. 1 .I .'V-TrichlnrnfifhanR A fi = lift!.' CT!!:. F: = IT1S2:. WiTlH U tl f!Y D!I !t", HIM FftiiTlIk' f = !lf!:. I!!!T 13 ['.ft! . KftNFi! RSTftityr wiFHiinn t ih f rs::: ra- r j ^k f !ah nirnnictr.! ______________________________________________________________________________ FfiKh i nr' v _______________________F-,t. hy ifep. t. *icc.- DUP050308056 ! ar.r.sstF.r tahfiratr.rip.f, Eltiar.t ifatinn ftannrt-KK/Ttii Ur.lafilea I! li! ? ci- I--I "-5 !--I T' P"! S-Ilp.: A(SPR5 tnjRr.ffiri: DHfi? )// Sample: RBfil.!) WHjfiVh fti lijtian Factnr! 1,0 Initial Ur,!ii7iia/U(.! 5.JI Standard: AKSPSl Inst. Hatch! GYiWfiSIAft F:fls! Uhliime/fit.: <i.!! nsthe.a I ?1W, Rsfrix/lflue!: IT Blank: ''RSPR1 Vi Tsrqet Caratimintis S.J.f/-BRT) Scan Qinn ftr'iw flnnc.ft f.nnc.B Dins. Blank g latent 1 tat inr. l imit 7'K Rihrnmr.r.hlnrnmR thane ?l`.. Rrnsnfnrn III. 4-flp.thjit^?-PentannnB v:. I.'.tuene 'V. Ifttrar.hlnrnp.thBnfi T-. V-Hr.vannnfi -* * ----------- ------------------- ----------------------------------------------------------------------------------------------------------- -------`--------------------------------------------------------- ------------------------------------------- --- ----------------------- ---- -------------------------- ---------------------------------------------- ----------------------------------- ---------------------------------- ---r---------------------------------- -------------------- ----------------------------------------- -------------------------------------------------------------------------------*------ ------------------------------------------------------------------------------------------------------ ----------------- 111 111 HI HI HI If! V.. P thiiShenrane IS. Xylene. ttnta 1) IV. Styrene 41. 1,1,? j?-Tetrar.hlnrnBthana -- ---- ------ -------- --------- ------- ------- -------- -------- --------- ----------- ------ --- ------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------ -------------------------- ----------------------------------------------------- 11! Hi HI 111 ft K'Au ratr.. r raw:. ran t ip i if d r y mi iit iiim f firms f = rjiw:. mu iif :at. r p w 4 = n f ir t h if r f t f n t iu n t ih f mu if raw I ah Chrar.iria: fins Iys 11 fiiirittnM r jL__. Dntfil riatR! PfiKF ? Rf ? _Fnt. hy Uar. hy 80 DUP050308057 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract BRA1S Lab Code: LANCAS Case No.: ______ SAS No. . SDG No.: ____________ . Matrix: (soil/water) WATER Lab Sample ID: 2583826 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >GSP04 Level: (low/med) LOW Date Received: 09/19/96 % Moisture: not dec. ' Date Analyzed: 09/25/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: l.o Soil Extract Volume: _______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3------------------- Chloromethane 75-01-4---------- ---------Vinyl Chloride 74-83 -9--------- --------- Bromomethane 75-00-3-------- -----Chloroethane 75-35-4------------------- 1,1-Dichloroethene 67-64-1------------------- Acetone 75-15-0---------- ---------Carbon Disulfide 75-09-2------------------- Methylene Chloride 75-34-3------------------- 1,1-Diehloroethane 540-59-0---------------- 1,2-Dichloroethene (total) 78-93-3------------------ 2-Butanone 67-66-3------------------- Chloroform 107-06-2----------------- 1,2-Dichloroethane 71-55-6----------------1,1,1-Trichioroethane 56-23-5------------------- Carbon Tetrachloride 71-43-2------------------- Benzene 79-01-6----------------- -Trichloroethene 7 8-87 -5-------------1,2 -Dichloropropane 75-27-4------------------- Bromodichloromethane 10061-01-5-------------cis-1,3-Dichloropropene 10061-02-6-------------trans-1,3-Dichloropropene 79-00-5------------------ 1. l, 2-Trichloroethane 124-48-1----------------Dxbromochloromethane 75-25-2------------------- Bromoform 108-10-1----------------- 4 -Methyl-2 -Pentanone 108-88-3-------------- Toluene 12 7-18-4-------------- -- Tetrachloroethene 5 91-7 8-6-----------------2 -Hexanone 108-90-7----------------- Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-42-5---------------Styrene 79-34-5-------- ---------- 1,1,2,2-Tetrachloroethane 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FORM I VOA GLM03. o81 DUP050308058 ITiTai. JTlN nHPntiSTjlRRBM ft ; i s >g*.eriu 35.0-3f'O .P arau. BRi-lfe TIC 400' GOO ,-uyyC^- Z&QQQQ- 34900.5- EiOOOO S 0-0 0004 isoooo-i - c~ 11 r. ri i rU 14Q90gj i:ooa0"| l'JUUOOii j S0030-1| i OOOQO-j 4GOOC4 I GQOQC-j -I <H = S % TO K C*iO 1f JK "rf- os l ` e23 o en \ 1? \ iV i Vi............ -............Il j l ..f!]l..... ... i 10 14 .1 BUL r",C- + 1200 ..,<.. i........ ...--;..... . % cE ? 't i I i!l in l. . ]'S._ _ X* *_ Data File: XJSFG4 : : D4 Quant Output File; ''GSP04: : FM Name: BRP1S 2583826 Instrument ID: HP0346Q Misc : ~SMM @Ud. %C +> #G9fi2881AP S^GSPBl &5 *5 =1 Id File : IA43S0 : : DB Title: 3/30 bJater/Med Soil ID File for Inst. HF0346U Last Calibration: 951207 01:59 Last Qcal Time: 3611325 OU : 26 Op.-rat or ID: SAM983 Quant Time : 960925 03:59 Injected at: 960925 03:34 U hi DUP050308059 O'DPNT REPORT Pago Operator IB: SPtM-98'3 Quant Rev: 7 ijuant Tsrne : 9b 092 r r. - - c Ci Output File: 's 6960 4: ' FM Injected at: 91-': ^ 2 5 i's r- : 3 Data File: > Gf.P04 : ;D4 Dilution Factor: 1 . i.l: riQU Name': BKA1S 2583826, Instrument ID: Hu !34 ir* * 1 fiisc : ~SFtH (3UL %C =) #G962S8 Iftfi S"'GSFB1 as *5 -1 ID tilfc: IPd 39 0 : : DB Title- 3---9 0 b.later.-''Med Soil ID File for Inst . HP03460 Loot C& libra tion: 991307 01 : 59 Last Qc.i 1 Time: 9fc 0925 U !.! -J to Compound 1) lb :> 17) ", LJ I 31 ) 4!! ) tBromoc hi orouie thane 1,2-Bichloroethane-d4 *1,4-Difluarabensene *Chiorobenzene-dS Toluene-dS 4- tfromof iuorobenzene * Compound is. ISTD R -T. Q i on 3.48 1 U - 39 11.08 lb .35 13 .24 17.07 128 . t) 65.0 114.0 117.0 38.0 35.0 rtrea 46112 67358 130206 1.493 32 149636 123157 Cone Units . q 50 . 00 44 - 95 5 0 . 00 50 . 00 47 . 19 cr 16 ug/L UQ ug.-'"L uq-'L US'/L ug-'l. 81 uw1.:i1 32 9 *! 88 89 A DUP050308060 Lancaster Laboratories Quantitation Report-GC/NS Uoiatiies : -4 r Fiie: AGSPiJ4 Injected1 63:34 09/25/96 Sample: BRH1S 2583826 Dilution Factor: 1.8 Initial Ut>Unae/Qt..' 5.0 Standard. AGSPS1 Inst. 8903460 Batch; G9S2681AA Final Uolurac/yt.i 5.0 Met.hoS' 71.56 Matrix/levs 1; 131. Blank AGSPB1 t Internal Standards E.T. ?*/-8T> Scan ftioti Areal+/-%Areai Cone. QC Fiat Cone Units og/L 1. Bromochloromethane 17. 1;4-Difluorobenzene 29. Chlorcbenzene-dS * = RETENTION TIME OUT OF RANGE 9.482(-.U80! 642 128 46112(-21) 50.00 u. oat-, ons 779 114 18828B(-26) 58.00 15.35l-.0125 1146 117 145332(-26) 50.00 * = INTERNAL STANDARD AREA OUT OF RANGE NC = .N0T ABLE TO CALCULATE--NO STANDARD. * Surrogate Standards P.T. 1+/-RET) Scan Qion Area Cone. %8ec. 15. l,2-Dichloroethane-d4 10.39t-.B88) 720 65 31. ToJuene-dB 13.24t-.0O8) 965 9B 40. 4-Broiaofluorobenzene 17.07(-.000) 1234 95 { > RKIATIUE RETENTION TIME OUT OF RANGE * = IREC OUT OF RANGE 67358 44.95 90 ' 145636 47.19 94 123157 50.16 106 D = SURROGATES DILUTED CUT HO = COULD NOT CALCULATE i Target Compounds R.T.I+/-8RT) Scan Qitm Area Cone.A Conc.B Cone. Blank Q Quantitation Limit 2. Chlorcmethane 3. Uinpi Chloride 4. Bromomethane 5. ChJoroethsne 6. 1,1-Dichioroethene 7. Acetone 8. Carbon Disulfide 9. Hcihyiene Chloride 11. 1.1-Biehloroethane IT. l;2-D`.chloroethene (total! 13. 2-Butanone 14. Chloroform 16, l;.2-Dichioroethane 15. 1,1;l-TrichloroEthane 19. Carhon Tetrachloride 20. Benzene 21. Tnchloroethene 22. 1,2-Dichloroprapane 23. Bromodichlororaethane 24. oi3-l,3-Dichloropropene 25. trans-1.3-Dichloropropene 2E. 1.1,2-Trichloroethane -------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------'----------------------------------------------------------------------- ---------------------------------------------------------------------------------------------------- --------------------------------------------------------------------------------------------------------------------------------------------------- ---------- .------------------------------- '---------------------------------------------------------------------- ------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------...........--........... -....................................................------------- ------------------------------------------------------------------------------------------------------------------------------- -------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- ID 10 Hi ID lit 18 10 10 10 10 10 10 is 10 to 10 10 10 10 t*. n>. 10 Hi A * RA!i! CONC. E - CCNC. MULTIPLIED BV DILUTION FACTOR E - C*JNC. OUT OF CAL. RANGE - SELAT'.UE RETENTION TIME OUT OF RANGE Lab Chronicle: Ent. bp --- -------------------------------------------------------------------------___>r bp ^4 PAGE 1 OF 2 - DUP050308061 Lancaster Laboratories Quantitation Repert-GC/HS Volatiles U*I: t=> s 3 i B tH7. ;"-a ; File: 7GSPSI4 Injected: 03:34 0.9/25/96 Sample: . BHflIS 2583828 Dilation factor: 1.0 ; Initial UoluW/tlt.: ; -5.0 Standard: nGSPSl Inst.HH03460 Batch: G962681fifi . Final Ublume/Gt..: 5.0 Method 7156 Hatrix/leuei: U: Blank' ''GBPEi t. Target Compounds B,T.(+/-8RT) Sean Qibn Area Conc.fi Conc.B Cone Blank Quantitation Limit 27. Dibromochloromethane 28. Bromotarm 30. 4-Methyl-2-Pentanofie 32. Toluene 33. Tetrachloroethene ;34. 2-Hetansne 35. Chlorobenzene 36. Ethylbenzene 38. Xylene (total) 39. Sturens 41. 1,1,2,2-Tetraehioroethane ------------------------------ *------------------------------ ---------<-------------;--------------------------------------------------------------------------------------------------------------------------------------------------------------------- -------------------- -------------------- ----------------------------------------------- ------------------- to lc U! ---------------------------------------------------------------------'---------------------------------------------- ------;---------- ;--------------------------------------------------------------------------------------------------------------------------------------------------------------------------- *-------------------------------------------------------- lit 10 10 ----------------------- 7----------------------------------------------------------------------------------------------------------------------------------------- ;----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- 10 10 10 fi = ftfiU CONG. 8 = OONC. MULTIPLIED BY DILUTION FACTOR E CONC. OUT OF CfiL. RANGE S SELATIUE RETENTION TIME OUT OF RANGE Lab Chrom-cie_Ent. by 85 DUP050308062 1A VOLATILE ORGANICS ANALYSIS DATA SHEET SPA SAMPLE NO Lab Name: LANCASTER LABS Contract: ______ . BRAF1 Lab Code: LANCAS Case No.: _______ SAS No.: ______ . SDG No.: Matrix: (soil/water) WATER Lab Sample ID: 2583827 Sample wt/vol: 5.0 (g/fflL) ML Lab File ID: >GSP08 Level: (low/med) LOW Date Received: 09/19/96 % Moisture: not dec. _______ Date Analyzed: 09/25/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0 Soil Extract Volume: _______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3------------------ Chloromethane 75-01-4-------- ---------Vinyl Chloride 74-83-9------------------- Bromomethane 75-00-3-----------------Chloroethane 75-35-4-- -------------- 1, l-Dichloroethene 67-64-1---------- ---------Acetone 75-15-0------------------- Carbon Disulfide 75-09-2------------------- Methylene Chloride 75-34-3-----------1, l-Dichloroethane 540-59-0------ -------- -I,2-Dichloroethene (total) 78-93-3---------- ---------2-Butanone 67-66-3------------------- Chloroform 107-06-2----------------- 1,2-Diehl oroethane 71-55-6------ -------------1, l, l-Trichloroethane 56-23-5------------------- Carbon Tetrachloride 71-43-2------------------- Benzene 79-01-6------------------- Trichloroethene 78-87-5------------------ 1,2-Dichloropropane 75-27-4----------------Bromodichloromethane 10061-01-5------------ cis-l,3-Dichloropropene 100 61-02-6----------- trans-1,3 -Dichloropropene 79-00-5------------------ 1,1,2-Trichloroethane 124-48-1----------------- Dibromochloromethane 75-25-2------------------- Bromoform 108-10-1----------------4 -Methy1-2 -Pentanone 108-88-3------ ---------- Toluene 127-18 -4---------------- Tetrachloroethene 591-78-6----------------- 2-Hexanone 108-90-7----------------- Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-4 2-5----------------styrene 79-34-5------------- 1,1,2,2-Tetrachloroethane FORM I VOA 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 c 10 u 10 c 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u OLM03.08^ &^ DUP050308063 TflT&t frftM r.HKftMCTrtftgfitt [c i i o 3? C51-`SC'C*. t1 ( *.-.O<-. ^W.~tU^-. Vr. il 400 ..-.I.... S^OGOO- s^o^aorl 22OB00- Sfn/QOO- 1O0CW i AOOQfW " ; ' ! I-iOOOOi' : . -1 1S3Q0CH lOiJOOO-i coooc I 40000-11I COOOO-J oi *N. B&ar-, pns^?7 TIC ! ... 801 0 ... I ~san aty,_ sr L00 fPcr & Cfc o! fc: K t ii i a t .:":ici......i..... i I Data File: >GSFQ8 : : D4 Quant Output File: 'vGSi-'U8: : FH Nome : B^HFl 2583827 Instrument ID: HPU'.-MISO Mi sc: ~SMM @UL %C *> #0882 88:1 MO $~GSPS1 &5 *5 =1 Id File : IfVi39 0 : : D8 Title: 3/9 1J Uater/MeC Sell ID File Last Calibration: 9512 07 01:59 for Inst. H-03490 Last !:cal Time: 980925 U ll : 26 Operator ID : SMM=9t: i Quant Ti me : 980925 OS : 0 I n j p. c t e d at : 980928 05 :3 87 DUP050308064 QiJHNT SEF'OET Pc. c--- Uperator ID : SAM"983 Output File : ''GSS-'OS : ; Fm Data File: >CSF08.:;D4 Name: BPMFl 288382/ Misc! ~S0H (at)L %c yuant fteu; #G9K28818 S-NSSHBl 7 yuant `ID me : Injected at ; Dilation Factor: Instrument ID: &5 *5 =1 33113 25 lib ; U3 g K:: 3 2 s f15 3 9 1 . U ! i i! U i.' H`-:!34F1i ID File: IN 4338 :D DE Ta 11 e : 3/90 Ulster/Had Soil ID File L uo t, Cc. 11 fa r atiorri 9512 02 01 ; 59 tor Inst . HP03460 Last Qc-al Time : 9 feU 925 0 0: 2 6 Compound 15 15 ) 17) 29 ) 31 ) 4!J ; *Brq-roochlorometfaane 1,2-Dichloroethane-d4 *114-Dx Fluorobenzene *Cfelorobensene-dS Toluene d8 4-Bromotluorobenzene * Conpounc! is. I STD R.T. Q ion 8 46 128.0 10.37 65.0 11 . 06 114.0 15.33 117.0 13.23 98.0 12.05. 95 0 Hr ea 453 95 6728IJ 18 2 H ll 9 193510 146/07 121223 Cone U Vi j. *t. s 50 . 00 4b .66 5 0.00 5:: . 0U 48.14 5 0.0 U ug/L uo/L uo .-'L ug/L ug-'L ug/L. q 'dli' qQ 92 9 98 86 88 DUPO 50308065 Lancaster Laboratories Quantitation Report-GC'ES Uoiatile: Lit: a r- File: ''GSHUS Injected: 05:33 09/25/96 Sample; MFi 258382? Dilation Factor: 1.8- Initial Uoluwe/Ut.: 5.0 Standard: AGSPSi Inst. HP034&U Batch: G962681RA Final Uotune/(Jt.: 5.0 Method: ?'b Matrix/leoel: 6); Blank: AGSHB1 t Internal Standards 8.T. (+/-RT) Scan Qion ftreal+/-$Area) Gone. ijC Flag Cone Units = cg/l 1. Bromochloromethane 17. 1,4-Difluorobenzene 29. Chlorobenzene-d5 f - RETENTION TIME OUT Of 8RNSE S.46U-.U29) S42 128 45345C-22) 50.00 11.06(-.S33) 77S 114 182909(-25) 50.00 15.33(-.fl33) 1146 117 1435101-27) 50.00 * - INTERNAL STANDARD RHER OUT OF RANGE NC = NOT ABLE TO CALCULATE--NO STANDARD. # Surrogate Standards R.T. (V-R8?) Scan Qion Rrea Cone. tRec. y aaBSs&3SBBBSSS9a:sssss=ss=BssB5S&r: 15. l,2-Dichloroeihane-d4 10.371.00(10) ?20 65 31. Talaene-dH 13.23 (.00111) 966 98 40. 4-Bromofluorobenzene 17.USt-.DOO) 1294 95 ? = EELRTIUE RETENTION TIME OUT OF RANGE * tREC OUT OF RRNSE 67280 45.86 91 146707 48.14 86 121229 50.00 100 D = SURROGATES DILUTED OUT NC = COULD NOT CftLCULHTE Target Compounds R,T.t+/-RKT) Scan Qion Rrea Cone.fl Cone.B Cone. Blank 0 Quantitation limit 2. Chloromethane 3. Uirtyl. Chloride 4. Bromomethane 5. Chioreethane 6. 1,1-Dichloroethene 7. Acetone 8. Carbon Disulfide 9. Methylene Chloride 11. 1,1-bichloreethane 12. 1 ;2-Di.chloroethene (total i 13. 2-Butanone 14. Chloroform 16, 1 ;5-Dichloroethane IK. 1,1,1-Trichloraethane 19. Carbon Tetrachloride 20. Benzene 21. Trichioroethene 22. l;2-Diehiorr.propane 23. Sromcdiehioromethane 24. ets-1,3-Dichiorapropene 25. trans-l,3-Dichloropropene 26. i;i,2-Tri.chLoroethans 10 10 10 18 10 10 16 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 fl = 8RU COKC. B = case. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CfiL. RANGE RELflTJUE RETENTION TIME OUT OF RANGE Lab Chronicle: ______________________________________________________________Ent. by _____ ----------------------------------------------------------------------------------------------Uer. by PRGE 1 OF 2 DUP050308066 Lancaster Laboratories Quantitation Report-GC/H9 Volatiles U.U L? If) & 3 fc-: t-:s -4 t File: ''SSPlffi Injected: (15:39 09/25/98 Sample: BRAF1 2583827 Dilution Factor: 1.8 initial Volume/tlt.: 5.8 Standard: WSl Inst. HFU34S0 Batch: G3626S1HA final Uclrnne/Ut.: 5.0 I Target Compounds 77, Bibromochloromethane ?K. Bromororm 36. 4-Methyl-2-Perrtanone 32. Toluene 33. Tetrachloroethene 34. 2-Hexanone 35. Chlorobenzene 36. Ethylbeiaene 38. Xylene !total) 39. Styrene 41. 1,1,2,2-Tetrachloroethane R.T.I+/-RBT) Scan (Jion Area Method: 7158 Matrix/leuel: 8.. Blank: '"GSKBi Cone. A Cone.B Cone. Blank Q Quant itat ion Li it =^= :0 u 10 Il ls lii 10 ID 10 10 10 H . RHlii cone. & CONC. MULTIPLIES! BY DILUTION FACTOR E = CONC. OUT OF CAL. RANGE = RELATIVE RETENTION TIME OUT OF RANGE Lab Chronicle: _Ent. by Ver . by Anaiust: -2ZZv _Date: Auditor: _________________ _________________________ Date: ............ .............................. PAGE 2 OF 2 90 DUP050308067 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract: _______. BRAT2 Lab Code: LANCAS Case No.: ______ SAS No.: SDG No.: Matrix: (soil/water) WATER Lab Sample ID: 2583828 Sample wt/vol: 5..0 (g/mL) ML Lab File ID: >GSP09 Level: (low/med) LOW Date Received: 09/19/96 % Moisture: not dec. _______ Date Analyzed: 09/25/96 GC Column: DB624 ID: 0.53 (mm} Dilution Factor: 1.o Soil Extract Volume: _______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3------------------- Chloromethane 75-01-4------------------- Vinyl Chloride 74-83-9------------------ Bromomethane 75-00-3-- ----------- Chloroethane 75-35-4------------------- 1,1-Dichloroethene 67-64-1------------------- Acetone 75-15-0------------------- Carbon Disulfide 75-09-2------------------- Methylene Chloride 75-34-3------------------- 1,1-Dichloroethane 540-59-0----------------1,2-Dichloroethene (total) 78-93-3------------------- 2-Butanone 67-66-3------------------Chloroform 107-06-2----------------- 1,2-Dichloroethane 71-55-6----------- --1,1,1-Trichloroethane 56-23-5------*------------ Carbon Tetrachloride 71-43-2------------------- Benzene 79-01-6------------------- Trichloroethene 78-87-5------------------ 1,2-Dichloropropane 75-27-4------------------ Bromodichloromethane 10061-01-5-------------cis-1,3-Dichloropropene 10061-02-6-------------trans-1,3-Dichloropropene 79-00-5------------------ 1,1,2-Trichloroethane 12 4-48-1----------------- Dibromochloromethane 75-25-2------------------- Bromoform 108-10-1-------- ---------4-Methyl-2-Pentanone 108-88-3----------------- Toluene ' 12 7-18-4-----------------Tetrachloroethene 591-78 -6----------------2 -Hexanone 108-90-7----------------- Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-42-5----------------- Styrene 79-34-5------------------- 1,1,2,2-Tetrachloroethane 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FORM I VOA OLM03. o9i A DUP050308068 rriTq \ in?* nwRiTMBTnfi**s" 40 s' ! SfetfOCOi ; --40000-] IH ! C0QCv-j Ii l*0000-j it-uoucH I4GG00-1 12Q0Q0\ j. X O 0 000~ tl{ b'JOOOi 40000i :o c c *;h f fV Tic 3 I 4 *NI _ n11 j, pul l?oo iU l. iT i* Usxa Fiie ; >CBFOS : : D") yuant Output File; '"GS5FUS : : FM Name : BRRT2 2583828 Instrument ID; HP03';1S0 Muc: ~SRM (cil.Jl, %V +> 'IGHS2B81HH S''GHFHi *5 =1 Id File ; IW-i9 0 : : UB Tit le : 3-"SI l Water .'Med Soil ID File Last Calibration: 951207 01:59 for Inst, Hf 1346 0 Past ycal Time: ybl!S25 0 0:26 Operator IP: SMM-98* Quant Time : 960925 06:36 Injected at: 960925 06:11 9 /j DUP050308069 ""iv* yi!.4NT RKKORT Operator ID` SttM-983 Output File: ''GSP09 : : Fh Data File : >CSf09 : : U4 Name ; BKHT2 2bK382W Mi sc i ' SAM (3UL %C +> yuant Rev: ftG96268IHA S'-GSFBl y iguant `Lme : 1 r.jer, ted at : D11 u t ion Factor Ins trament II'1' &5 *5 = 1 Ft: ,- :'5 08-36 9- Or. 2 5 l.ifcl : L i i ; = ! l 1. H- 0346-. ID File : If' 4 3 9 U : : DB Title: 3/90 tiater/Med Soil ID File Last Calibration: 35120!/ 01:59 For Inst. HPO 3'16 0 Las t ftcal Time : 98 0929 0 0 :26 Compound 1) 15 ) 17) O U % 31 ) <31! I *br otnoohlor omet hane 1 /i-DichlorGethane~d4 *1}4-Difluorobensene *C:.ior o benzene ~d5 Toiuene-dB 4- dr OTr.o r iuor obenzene * Compound is- I STD R.T. Q ion S . 45 128.0 1 L! . 36 .65.0 11 . 05 114.0 lb . 33 117.0 13.22. 38.0 17.05 95.0 fH 65 3 45 ! i ! 2 65688 170584 136116 0 13ybbl 12U231 ( y'.i nc i.inrts 50 . 00 . 31 5U . 00 5o.au ' > ci . O 0 52.311 un.'L uq ag/L u g 1., <L: Ij j_i ag/u q 8 8 9 y ."r .H 9 DUP050308070 Lancaster Laboratories Quantitation Report-GC/HS Oolatiies LLit; li? rn fc-:e; v; s h Fite' '`GSRllS Injected: OS; 11 03/25/36 Sample: BKAT2 " 2583328 Dilation Factor: Initial Ur. lune/OR.: 1.0 5.0 Standard: /'GSFS1 Inst. 8603480 Batch: G962681HA Final Onlonse/IOt.: 5.0 Method: 711& Matrix/level: Blank: "GSHBl 8 Internal Standards R.T. t+/-RT! Scan Qion Areas*/-flrea) Cone. yC Frag Cone Units * u -j -'l 1. Bromochioromethane 1?. 1.4-DifIuorobenzene 28. ChLoroberzene-dS S = RETENTION TIME OUT OF RANGE 9.453t-.037) 645 128 45012(-23! 50.00 11.05!-.040) 782 114 l?0584t-3D) 50.00 15.33t-.029) 1150 117 136O60(-31) 50.00 * = INTERNAL STHNDHRD AREA OUT OE RANGE NC = NOT ABLE TO CALCUl ATE-h :.' STANDARD i Surrogate Standards R.T. (+/-RRT) Scan Qian Area Cone. tRec. Q 15. l/2-Bichioroethane-d4 ia.3St.oao2) 723 65 31. Taluene-dB 13.22l-.081) 963 96 48. 4-BroraofIuorobenzene 17.tlSL-.a08) 1298 95 i - RKLATIOE RETENTION TINE Ol!T OF RANGE * = %REC OUT OF RANGE 65688 44.91 90 139551 48.30 97 120231 52.30 105 D = SURROGATES DILUTED OUT NO = COULD NOT CALCULATE t Target Compounds R.T.(*/-RRT) 2. Chloromethane 3. Oir.yl Chloride 4. Bramomethane 5. Chioroethane 6. 1jl-Dichloroeinene 7. Acetone 8. Carbon Disulfide 9. Methylene Chloride U. 1,1-Sichloroethane 12. l}2-Dichloroethene (totalJ 13. 2-Butanone 14. Chloroform 16. 1,2-Dichloroethane 18. 1^,1-Tnchloroethane 18. Carbon Tetrachloride OIL BenzEne 21. Trichloroethene 22. 1,2-L'ichioropropane 73. Bromod ichloroaethane 24. cis-1jS-Dichicropropene 25 trans-1,3-Dzchloroprcpene ?E. 1 ,2-Trich.Ioroethane ------------------------------------------ ---------- ------ ------------------- -- Scan Qion Area Co.nc.fl Conc.O Cone. Biank Q Quantitation Limit 10 10 10 10 10 It 10 10 10 10 10 10 10 10 10 IS 10 10 10 lti 10 10 P. = RAF! CON". t - CONC. MULTIPLIED BY DILUTION FACTOR E = OONC. OUT OF CAL. RANGE I = RELATIUE RETENTION TIME OUT Of RANGE Lab Chronicle:Ent. by _______________________________ _________________________________________________________________Cer. by 0 A RAGE i OE 2 DUP050308071 Lancaster Laboratories Quantitation Report-GC/MS Uctaiiie: ! =: fi *!_ File: "6SKS9 Injected: 86:11 83/25-'96 Sample- BHAT2 " 258382k Dilution Factor: Initial Uclame/Ot.: 1,8 5.8 Standard: "SSPSl Inst. HHII34B0 Batch; G962S81RR Final Uciune/Ut.: 5.0 Method. ?'.56 Matrix.-'lew! C; Blank- "GSKS1 t Target Compounds R.T.t*/-KR?l Scan- Qion ftrea Cone.ft Cone.B Cone. Blank anti tat; or. Lioiiit 27. Dibromochlcransethane 28. Bromoform 30. 4-Methyl-2-Pentanone 32. Tnitiene 33. Tetrachloroethene 34. 2-Bexanone 35. Chlorobenzene 38. Ethylbenzene 38. Xylene I totalJ 38. Styrene 81. 1 ,l,2j2-Tetrachloroethane ---------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------:------------------------------------------------------------------ 1------------------------------------------------------------------------------------ 1------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------ ----------------- .................... ll: .......................... ............. 18 ----------------------------------------- ly ............ ...................................... It! ---------------------------------------------- .y ft - m CONC. B COSC. MULTIPLIED BY DILUTION FACTOR E CONC. OUT OF CftL. BHNSE Lab Chronicle: RELftTiOE RCTar-lON TIME OUT OF BUNGE tnt. by 95 DUP050308072 Standards Data 9( DUP050308073 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: LANCASTER LABS Contract: ______ . Lab Code: LANCAS Case No.: ________ . SAS No. _______ . SDG No.: _______ Instrument ID; HP03460 Calibration Date(s): 09/24/96 09/24/96 Heated Purge; (Y/N) N Calibration Times: 0140 0349 GC Column: DB624 LAB "FIEimn-------------- RRF 50= >GSMI3 ID: 0.53 (mm) RRF 10= >GSMI1 RRF100= >GSMI4 RRF 20= >GSMI2 RRF200= >GSMI5 COMPOUND RRF 10 RRF 20 RRF 50 RRF100 RRF200 --f-- SKF RSD Dichlorodifluoromethane 2.648 Chloromethane Vinyl Chloride 1.601 9if 1.512 Bromomethane if 1.025 Chloroethane .863 Trichlorofluoromethane 1.392 Furfuran 1.549 Ethyl Ether .905 Acrolein 1,1-Dichloroethene .158 9t 1.082 Freon 113 2.244 Acetone .418 Methyl Iodide 3.589 Carbon Disulfide 3.350 Allyl Chloride 2.237 Methylene Chloride 2.082 t-Butyl Alcohol .088 Acrylonitrile .243 Methyl t-Butyl Ether 2.842 1,2-Dichloroethene (total) 1.353 n-Hexane 1,1-Dichloroethane 1-Propanol 1.533 ifc 2.773 .002 2-Butanone .411 Propionitrile .089 Ethyl Acetate 1.490 Methacrylonitrile .318 Tetrahydrofuran Chloroform Cyclohexane .312 if 2.967 2.012 1,2-Dichloroethane * 1.971 Vinyl Acetate .055 1,1,l-Trichloroethane * .490 J 2.285 1.179 1.143 .904 .680 1.274 1.252 .764 .132 .944 1.831 .285 3.601 2.630 1.654 1.489 .074 .191 2.396 1.167 .992 2.211 .003 .314 .070 1.110 .266 .232 2.525 1.359 1.716 .051 .450 2.196 1.095 1.091 .755 .593 1.215 1.179 .697 .118 .914 1.813 .248 3.594 2.564 1.571 1.210 .065 .182 2.241 1.125 1.117 2.142 .003 .300 .066 .996 .236 .193 2.485 1.401 1.614 .046 .448 2.221 1.033 1.039 .711 .558 1.258 1.218 .716 .132 .876 1.822 .253 3.579 2.607 1.689 1.112 .066 .194 2.372 1.106 1.162 2.068 .003 .301 .069 1.055 .255 .220 2.385 1.444 1.562 .049 .451 2.221 1.061 1.083 .662 .387 1.176 1.233 .734 .143 .885 1.725 .254 3.663 2.685 1.761 1.151 .074 .211 2.406 1.144 1.082 2.130 .004 .326 .076 1.179 .271 .234 2.396 1.431 1.534 .052 .444 2.314 1.194 1.173 .811 .617 1.263 1.286 .763 .137 .940 1.887 .292 3.605 2.767 1.782 1.409 .073 .204 2.452 1.179 1.177 2.265 .003 .330 .074 1.166 .269 .238 2.552 1.529 1.679 .050 .456 All other compounds in OLMOl.8 must meet a minimum RRF of o.oio. 8.2 19.6 16.4* 18.5* 28.5 6.5 11.6 10.9 10.8 8.9* 10-.8 24.8 .9 11.9 14.8 28.7 12.3 11.7 9.3 8.5 17.7 12.7* 20.4 14.0 12.2 16.6 11.3 18.7 9.4* 17.8 10.5* 6.4 | 4.1* 1 page 1 of 3 FORM VI VOA OLM03.0 97 DUP050308074 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: LANCASTER LABS Contract: _______ . Lab Code: LANCAS Case No.: '. SAS No. _______ . SDG No.: _______ Instrument ID: HP03460 Calibration Date(s): 09/24/96 09/24/96 Heated Purge: (Y/N) N Calibration Times: 0140 0349 GC Column: DB624 ID: 0.53 (mm) LAB FILE ID: RRF 50= >GSMI3 Rr F 10= >GSMIl ERF100= >GSMI4 Er f 2o= >g s mI2-------RRF200= >GSMI5 COMPOUND RRF 10 RRF 20 RRF 50 RRF100 RRF200 --s-- KKF RSD Carbon Tetrachloride 1 t .501 Isobutyl Alcohol Benzene 1 .008 * .861 n-Heptane .227 n-Butanol Trichloroethene .006 k .409 l? 2-Dichloropropane .429 Dibromomethane .324 1,4-Dioxane .003 n-Propyl Acetate Bromodichloromethane .547 4k .731 2-Nitropropane .092 2-Chloroethyl Vinyl Ether .197 cis-l,3-Dichloropropene * .594 trans-1,3-Dichloropropene * .507 1,1,2-Trichloroethane * .366 Dibromochloromethane * .689 Bromoform * .609 trans-1,4-Dichloro~2-Butene .123 4-Methyl-2-Pentanone Toluene .418 * 1.151 Ethyl Methacrylate .444 Tetrachloroethene .529 2-Hexanone .255 1,2-Dibromoethane Chlorobenzene .631 b 1.001 1,1,1,2-Tetrachloroethane .433 Ethylbenzene Xylene (total) j .398 k .502 Isoamyl Acetate Styrene .426 ib .883 Cumene 1.280 Cyclohexanone .012 .459 .007 .721 .157 .005 .389 .351 .290 .003 .461 . 656 .081 .175 .522 .444 .319 .672 .608 .115 .324 .999 .416 .488 .209 .609 .918 .412 .350 .430 .370 .780 1.068 .011 .467 .006 .701 .201 .005 .380 .331 .275 .002 .428 .652 .065 .172 .511 .435 .305 .663 .606 .104 .296 .976 .402 .511 .201 .574 .889 .405 .351 .434 .345 .797 1.144 .010 .455 .006 .688 .201 .005 .379 .319 .333 .002 .442 .641 .081 .180 .515 .448 .299 .646 .593 .104 .335 1.043 .492 .528 .222 .629 .883 .531 .349 .436 .367 .798 1.231 .010 .445 .006 .685 .177 .005 .373 .323 .311 .002 .465 .624 .085 .191 .509 .436 .294 .628 .606 .100 .362 1.075 .512 .503 .251 .660 .901 .507 .338 .408 .389 .756 1.197 .011 .465 .006 .731 .193 .005 .386 .350 .307 .003 .469 .661 . 083r .183 .530 .454 .317 .660 .604 .109 .347 1.049 .453 .512 .228 .621 .918 .457 .357 .442 .380 .803 1.184 .011 4.6 14.2 10.1 13.9 12.0 3.6' 12.9 7.8 15.8 9.9 6.3' -12.0 5.9 6.86.6 9.2 3.6' 1.1' 8.8 13.4 6.5 10.5 3.4' 10.8 5.1 5.2' 12.5 6.5' 8.0' 8.0 6.0' 6.9 7.9 ..tyi All other compounds in OLMOl.8 must meet a minimum RRF of 0.010. page 2 of 3 FORM VI V0A OLM03.0 98 DUP050308075 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: LANCASTER LABS Contract: _______ . Lab Code: LANCAS Case No.: '. SAS No. _____ SDG No.: _______________ Instrument ID: HP03460 Calibration Date(s): 09/24/96 09/24/96 Heated Purge: (Y/N) N Calibration Times: 0140 0349 GC column: DB624 ID: 0.53 (mm) LAB FIOTHd ! RRP 50= >GSMI3 RRF 10= >GSMll RRP100= >GSMI4 Rr E 20= >GSMI2 RRF200- >GSMI5 COMPOUND RRF 10 RRF 20 RRF 50 RRF100 RRF200 --r~ KKF RSD 1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane 2-Chlorotoluene Pentachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl Chloride 1,2-Dichlorobenzene 1,2-Dibromo-3-Chloropropane .728 .164 .366 .390 .891 .992 .754 .879 .148 .642 .149 .319 .372 .780 .900 .719 .789 .148 .598 .137 .335 .374 .841 .925 .669 .795 .124 .621 .145 .357 .485 .904 .990 .728 .870 .136 .651 .143 .349 .484 .897 .980 .751 .892 .150 .648 .148 .345 .421 .863 .958 .724 .845 .141 1,2-Dichloroethane-d4 1.472 1.584 1.494 1.470 1.500 1.504 Toluene-d8 .971 1.104 1.059 1.110 1.116 1.072 4-Bromofluorobenzene * .766 .899 .856 .873 .817 .842 I ,r Compounds with required minimum RRF and maximum %RSD values. All other compounds in OLM01.8 must meet a minimum RRF of 0.010. 7. 6 7. 0 5. 4 13. 9 6. 1 4. 4 4. 8 5. 8 7. 9 3. 1 5. 7 6. 2 page 3 of 3 FORM VI V0A OLM03.0 99 DUP050308076 TOTAL ION CHROMATOGRAM File >6Snil 35.0-300.o'amu. VStOOlO TIC 400 rI 800 80000- 260000- 010 ppb IC"SAn 7.C OWL *1 +OCEC 1200 1 1600 .x--i,,.. -E-..i__i. i t'r 20 22 Data File: >GSMI1::D5 Quant Output File: AGSMI1::FM Name: VSTD010 010 ppb IC Instrument ID: HP03460 Misc: -SAM %C @WL =1 +DCE05Y-W Id File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960910 21:25 Operator ID: SAM-983 Quant Time : 960924 02:06 Injected at: 960924 01:40 100 DUP050308077 Operator ID: SAM-983 Output File: ~GSMI1::FM Data File: >GSMI1::D5 Name: VSTD010 010 ppb- ic Misc: -SAM %C @WL =1 +DCE05Y-W QUANT REPORT Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: Page 1 960924 02:06 960924 01:40 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst HP03460 Last Calibration: 951207 01:59 Last Qcal Time 960910 21:25 Compound 1) 2) 3) 4) 5) 6) 7) 8) 9) 10) 11) 12) 13) 14) 15) 16) 17) 18) 19) 20) 21) 22) 23) 24) 25) 26) 27) 28) 2 9) 30) 31) 32) 33) 34) 35) 36) 37) 3 8) 39) 40) *Bromochloromethane Dichlorodifluoromethane Chloromethane Vinyl Chloride Bromomethane chloroethane Trichlorofluoromethane Furfuran Ethyl Ether Acrolein 1,1-Dichloroethene Freon 113 Acetone Methyl Iodide Carbon Disulfide Allyl Chloride Methylene Chloride t-Butyl Alcohol Acrylonitrile Methyl t-Butyl Ether trans-l,2-Dichloroethene n-Hexane l,l-Dichloroethane 1-Propanol cis-l,2-Dichloroethene 2-Butanone Propionitrile Ethyl Acetate Methacrylonitrile Tetrahydrofuran Chloroform Cyclohexane l,2-Dichloroethane-d4 1,2-Dichloroethane *1,4-Difluorobenzene Vinyl Acetate 1,1#1-Trichloroethane Carbon Tetrachloride Isobuty1 Alcoho1 Benzene R.T. Q ion 9.48 128.0 3.06 85.0 3.28 50.0 3.52 62.0 4.07 94.0 4.29 64.0 4.84 101.0 5.50 68.0 5.43 59.0 5.68 56.0 5.86 96.0 5.94 101.0 5.99 43.0 6.14 142.0 6.27 76.0 6.60 41.0 6.83 84.0 7.16 59.0 7.30 53.0 7.39 73.0 7.37 96.0 7.88 57.0 8.11 63.0 8.38 59.0 9.10 96.0 9.12 43.0 9.20 54.0 9.25 43.0 9.45 67.0 9.57 42.0 9.62 83.0 10.01 56.0 10.39 65.0 10.51 62.0 11.07 114.0 8.24 86.0 9.90 97.0 10.17 117.0 10.39 41.0 10.49 78.0 Area Cone Units 52918 50.00 ug/L 28026 10.66 ug/L 16944 12.84 ug/L 16000 12.07 ug/L 10850 12.55 ug/L 9189 12.60 ug/L 14733 7.94 ug/L 16392 12.08 ug/L 9581 13.16 ug/L 8348 52.99 ug/L 11451 11.30 ug/L 47499 17.37 ug/L 4427 16.30 ug/L 37980 6.76 ug/L 35457 10.60 ug/L 23674 15.73 ug/L 22036 17.47 ug/L 4644M. 258E-37 ug/L 12843 57.71 ug/L 30083 12.45 ug/L 13839 11.46 ug/L 16223 13.58 ug/L 29349 12.04 ug/L 262 90.12 ug/L 14795 12.25 ug/L 4349 11.85 ug/L 4693M. 261E-37 ug/L 15774 16.83 ug/L 8414M. 467E-37 ug/L 3307 17.05 ug/L 31404 11.31 ug/L 21291 14.28 ug/L 15579 9.32 ug/L 20860 11.78 ug/L 220675 50.00 ug/L 2408 11.19 ug/L 21605 10.87 ug/L 22107 10.33 ug/L 4409 228.08 ug/L 37984 12.82 ug/L q 59 98 96 99 86 91 95 78 70 86 91 97 90 69 100 82 87 93 95 89 94 95 100 93 90 96 88 94 88 98 82 93 93 87 95 99 91 101 DUP050308078 QUANT REPORT Page 2 Operator ID: SAM-983 Output File: ~GSMI1::FM Data File: >GSMI1::D5 Name: VSTD010 010 ppb IC Misc: -SAM %C @WL =1 +DCE05Y-W Quant Rev: 7 Quant Time: Injected at: Dilution Factor: instrument ID: 960924 02:06 960924 01:40 1.00000 HP0346D ID File: IA439Q::DB Title: 3/90 Water/Med Soil ID File for Inst HP03460 Last Calibration: 951207 01:59 Last Qcal Time 960910 21:25 Compound 41) n-Heptane 42} n-Butanol 43) Trichloroethene 44) l{2-Dichloropropane 4 5) Dibromomethane 46) 1,4-Dioxane 47) n-Propyl Acetate 48) Bromodichloromethane 49) 2-Nitropropane 50) 2-chloroethyl Vinyl Ether 51) cis-l,3-Dichloropropene 52) trans-1,3-Dichloropropene 53) 1,1,2-Trichloroethane 54) Dibromochloromethane 55) Bromoform 56) trans-1,4-Dichloro-2-Butene 57) *Chlorobenzene-d5 58} 4-Methyl-2-Pentanone 59) Toluene-d8 60} Toluene 61) Ethyl Methacrylate 62) Tetrachloroethene 63) 2-Hexanone 64) 1,2-Dibromoethane 65} Chlorobenzene 66) 1,1,1,2-Tetrachloroethane 67} Ethylbenzene 68) m+p-Xylene 69) Isoarayl Acetate 70) o-Xylene 71) Styrene 72) Cumene 7 3) Cyclohexanone 74) 4-Bromofluorobenzene 75) 1,1,2,2-Tetrachloroethane 76) l,2,3-Trichloropropane 77) 2-Chlorotoluene 78) Pentachloroethane 79) l,3-Dichlorobenzene 80) 1,4-Dichlorobenzene 81) Benzyl Chloride R.T. Q ion 10.91 71.0 11.39 56.0 11.48 130.0 11.79 63.0 11.98 93.0 11.99 88.0 12.06 43.0 12.21 83.0 12.53 41.0 12.64 63.0 12.85 75.0 13.66 75.0 13.93 97.0 14.51 129.0 16.60 173.0 17.35 53.0 15.35 117.0 13.06 43.0 13.25 98.0 13.34 91.0 13.79 69.0 14.16 164.0 14.28 43.0 14.69 107.0 15.40 112.0 15.51 131.0 15.55 106.0 15.71 106.0 15.80 70.0 16.31 106.0 16.32 104.0 16.84 105.0 16.97 55.0 17.08 95.0 17.26 83.0 17.33 110.0 17.59 126.0 18.23 167.0 18.70 146.0 18.83 146.0 19.03 91.0 Area Cone Units 10021 11.22 ug/L 3444 217.99 ug/L 18046 10.97 ug/L 18914 12.31 ug/L 14295 8.86 ug/L 1745 181.59 ug/L 24161 14.20 ug/L 32283 10.53 ug/L 8088 25.15 ug/L 8699 10.58 ug/L 26234 12.30 ug/L 23297 12.80 ug/L 16149 11.60 ug/L 30392 10.15 ug/L 26896 9.60 ug/L 13625M. 18IE--37 ug/L 179841 50.00 ug/L 15035 13.97 ug/L 34909 9.06 ug/L 41383 11.87 ug/L 15983 9.40 ug/L 19023 10.85 ug/L 9185 12.91 ug/L 22691 8.81 ug/L 35995 10.95 ug/L 15561 6.37 ug/L 14316 11.64 ug/L 37084 25.25 ug/L 15324 11.85 ug/L 18051 12.29 ug/L 31749 10.97 ug/L 46040 9.97 ug/L 5261 174.28 ug/L 27567 8.91 ug/L 26179 13.10 ug/L 5901 9.51 ug/L 13172 10.34 ug/L 14011 6.24 ug/L 32049 7.99 ug/L 35679 8.16 ug/L 27112 9.77 ug/L q 81 92 88 79 79 83 95 94 94 86 89 92 95 99 97 93 88 97 92 69 92 98 92 90 89 99 96 93 96 88 93 89 97 96 60 94 86 94 92 90 10 3 DUP050308079 Operator ID: SAM-983 Output Pile: " GSMI1: :FM Data File: >GSMI1::D5 Name: VSTD010 010 ppb IC Misc: -SAM %C @WL =1 +DCE05Y-W QUANT REPORT Quant Rev: 7 Quant Time Injected at Dilution Factor Instrument ID Page 3 960924 02:06 960924 01:40 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last calibration: 951207 01:59 Last Qcal Time: 960910 21:25 Compound 82) 1,2-Dichlorobenzene 83) l,2-Dibromo-3-Chloropropane * Compound is ISTD R.T. Q ion 19.40 146.0 20.61 157.0 Area 31600 5306 Cone Units 8.37 ug/L 9.84 ug/L q Z 8' 10: DUP050308080 Compound No: 18 Compound Name: t-Butyl Alcohol Scan Number: 442 Retention Times 7.16 min Quant ion: 59.0 Area: 4644M Concentration: .00 ug/L q-value: 0 This report was produced by QAREA at: 4:40 AM TUE., 24 SEPT, 1996 104 DUP050308081 Data File: >GSMI1 Name: VSTD010 010 ppb IC Misc: -SAM %C @WL =1 +DCEOSY-W Quant Time: 960924 02:06 Injected at: 960924 01:40 Compound No: 27 Compound Name: Fropionitrile Scan Number: 618 Retention Time: 9.20 min Quant Ion: 54.0 Area: 4693M Concentration: .00 ug/L q-value: 0 Quant Output File: *GSMI1 Instrument ID: HP03460 Quant ID File: IA4390 . Last Calibration: 951207 01:59 This report was produced by QAREA at: 4:41 AM TOE., 24 SEPT, 1996 105 DU P 05030 8082 Data File: >GSMI1 Name: VSTDQ10 010 ppb XC Misc: -SAM %C @WL =1 +DCEQ5Y-W Quant Time: 960924 02:06 Injected at: 960924 01:40 Quant output File: 'GSMIi Instrument ID: HP03460 Quant ID File: IA4390 Last Calibration: 951207 01:59 Compound No: 29 Compound Name: Methacrylonitrile Scan Number: 639 Retention Time: 9.45 min Quant Ion: 67.0 Area: 8414M Concentration: .00 ug/L q-value: 0 This report was produced by QAREA at: 4:42 AM TUE., 24 SEPT, 1996 106 DUP050308083 Data File: >GSMI1 Quant Output File: *GSMI1 Name: VSTD010 010 ppb IC Instrument ID: HP034 60 Misc: -SAM %C @WL =1 +DCEOSY-W Quant Time: 960924 02:06 Quant ID File: IA4390 Injected at: 960924 01:40 A Last Calibration: 951207 01:59 Compound No: 56 Compound Name: trans-1,4-Dichloro-2-Butene Scan Number: 1316 Retention Time: 17.35 min Quant Ion: 53.0 Area: 13625M Concentration: .00 ug/L g-value: 0 This report was produced by QAREA at: 4:43 AM TUB., 24 SEPT, 1996 7 DUP050308084 TOTAL ION CHROMATOGRAM File >6St1I2 36.0-300.0 amu. VSTDQ2Q TIC < I i < 40I 0 1__!_I--I---1--1--801--0X 80000- 020 ppb IC~SRI1 J5C 0WL -1 +DCEC 1200 1 - 1 1 1 , 1600 -i -t-I-, i i 240000220000- Data File: >GSMI2::D5 Quant Output File: A-GSMI2::FM Name: VSTD020 020 ppb IC Instrument ID: HP03460 Misc: -SAM %C @WL =1 +DCE05V-W Id File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 operator ID: SAM-983 Quant Time : 960924 03:07 Injected at: 960924 02:12 108 DUP050308085 QUANT REPORT Page 1 Operator ID: SAM-983 Output Pile: ~GSMI2;:FM Data File: >GSMI2::D5 Name: VSTD020 020 ppb IC Misc: -SAM %C @WL =1 +DCE05Y-W Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 03:07 960924 02:12 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Compound 1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Furfuran 9) Ethyl Ether 10) Acrolein 11) 1,l-Dichloroethene 12) Freon 113 13) Acetone 14) Methyl Iodide 15) Carbon Disulfide 16) Allyl Chloride 17) Methylene Chloride 18) t-Butyl Alcohol 19) Acrylonitrile 20) Methyl t-Butyl Ether 21) trans-lf 2-Dichloroethene 22) n-Hexane 23) 1,l-Dichloroethane 24) 1-Propanol 25) cis-l,2-Dichloroethene 26) 2-Butanone 27) Propionitrile 28) Ethyl Acetate 29) Methacry1onitri1e 30) Tetrahydrofuran 31) Chloroform 32) Cyclohexane 33) 1,2-Dichloroethane-d4 34) 1,2-Dichloroethane 35) *1,4-Difluorobenzene 36) Vinyl Acetate 37) 1,1,1-Trichloroethane 38) Carbon Tetrachloride 39) Isobutyl Alcohol 40) Benzene R.T. Q ion 9.50 128.0 3.08 85.0 3.31 50.0 3.56 62.0 4.10 94.0 4.31 64.0 4.86 101.0 5.52 68.0 . 5.45 59.0 5.70 56.0 5.90 96.0 5.97 101.0 6.02 43.0 6.18 142.0 6.32 76.0 6.63 41.D 6.86 84.0 7.15 59.0 7.32 53.0 7.41 73.0 7.39 96.0 7.91 57.0 8.13 63.0 8.39 59.0 9.12 96.0 9.15 43.0 9.23 54.0 9.26 43.0 9.47 67.0 9.58 42.0 9.64 83.0 10.02 56.0 10.41 65.0 10.52 62.0 11.08 114.0 8.24 86.0 9.93 97.0 10.19 117.0 10.40 41.0 10.51 78.0 Area Cone Units 56711 51841 26736 25924 20500 15420 28904 28402 17329 14919 21421 83090 6455 81690 59650 37520 33783 8369 21710 54346 25729 22506 50154 867 27229 7117 7960 25189 15067 5263 57277 30837 35934 38921 226246 4644 40733 41524 7662 65209 50.00 ug/L 18.40 ug/L 18.90 ug/L 18.24 ug/L 22.13 ug/L 19.73 ug/L 14.54 ug/L 19.52 ug/L 22.21 ug/L 88.36 ug/L 19.73 ug/L 28.36 ug/L 22.18 ug/L 13.57 ug/L 16.64 ug/L 23.27 ug/L 24.99 ug/L . 434E-37 ug/L 91.03 ug/L 20.99 ug/L 19.89 ug/L 17.58 ug/L 19.20 ug/L 278.26. ug/L 21.05 ug/L 18.09 ug/L .412E-37 ug/L 25.07 ug/L .781E-37 ug/L 25.31 ug/L 19.25 ug/L 19.30 ug/L 20.07 ug/L 20.51 ug/L 50.00 ug/L 21.05 ug/L 19.99 ug/L 18.92 ug/L 386.59 ug/L 21.46 ug/L q 72 96 99 96 85 91 97 84 71 97 93 94 86 66 100 88 91 96 91 98 92 95 96 100 98 86 88 98 85 93 96 89 98 85 93 94 91 97 88 94 ios DUP050308086 Operator ID: SAM-983 Output File: AGSMI2::FM Data File: >GSMI2::D5 Name: VSTD020 020 ppb IC . Misc: -SAM %C WL =1 +DCE05Y-W QUANT REPORT Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: Page 2 960924 03:07 960924 02:12 1.00000 HP03460 ID File: IA4390::DB , ^. Title: 3/90 Water/Med Soil ID File for Inst HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Compound 41) 42) 43) 44) 45) 46) 47) 48) 49) 50) 51) 5 2) 53) 54) 55) 56) 57) 58) 59) 60) 61) 62) 63) 64) 65) 66) 6 7) 68) 69) 70) 71) 72) 73) 74) 75) 76) 77) 78) 79) 80) 81) n-Heptane n-Butanol Trlchloroethene 1,2-Dichloropropane Dlbromomethane 1,4-Dioxane n-Propyl Acetate Bromodichloromethane 2-Nitropropane 2-Chloroethyl Vinyl Ether cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane Bromoform trans-1,4-Dichloro-2-Butene *Chlorobenzene-d5 4-Methyl-2-Pentanone Toluene-d8 Toluene Ethyl Methacrylate Tetrachloroethene 2-Hexanone 1,2-Dibromoethane chlorobenzene 1,1,1,2-Tetrachloroethane Ethylbenzene m+p-Xylene Isoamyl Acetate o-Xylene Styrene Cumene Cyclohexanone 4-Bromofluorbenzene 1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane 2-Chlorotoluene Pentachloroethane. 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl Chloride R.T. Q ion 10.93 71.0 11.40 56.0 11.49 130.0 11.81 63.0 11.99 93.0 12.01 88.0 12.06 43.0 12.23 83.0 12.53 41.0 12.65 63.0 12.87 75.0 13.66 75.0 13.93 97.0 14.53 129.0 16.60 173.0 17.35 53.0 15.37 117.0 13.08 43.0 13.27 98.0 13.36 91.0 13.79 69.0 14.18 164.0 14.28 43.0 14.69 107.0 15.41 112.0 15.52 131.0 15.55 106.0 15.73 106.0 15.81 70.0 16.31 106.0 16.32 104.0 16.85 105.0 16.98 55.0 17.03 95.0 17.27 83.0 17.34 110.0 17.60 126.0 18.24 167.0 18.71 146.0 18.84 146.0 19.03 91.0 Area Cone Units 14204 5720 35191 31762 26251 3039 41763 59359 14655 15830 47226 41828 28900 60837 55067 25982 181413 23490 80133 72475 30180 35400 15134 44210 66605 29903 25387 64381 26865 31233 56631 77503 10121 65244 46622 10835 23137 26984 56635 65291 52205 15.51 ug/L 3 53 X4 ug/L 20.87 ug/L 20.17 ug/L 15.87 ug/L 308.46 ug/L 23.94 ug/L 18.89 ug/L 44.45 ug/L 18.77 ug/L 21.60 ug/L 22.42 ug/L 20.24 ug/L 19.83 ug/L 19.18 ug/L . 337E-37 ug/L 50.00 ug/L 21.64 ug/L 20.63 uq/L 20.62 ug/L 17.60 ug/L 20.01 ug/L 21.09 ug/L 17.02 ug/L 20.08 ug/L 12.13 ug/L 20.47 ug/L 43.46 ug/L 20.59 ug/L 21.08 ug/L 19.39 ug/L 16.64 ug/L 332.36 ug/L 20.91 ug/L 23.12 ug/L 17.31 ug/L 18.01 ug/L 11.91 ug/L 14.00 ug/L 14.79 ug/L 18.64 ug/L q 79 98 92 78 85 68 94 94 97 90 89 93 96 98 96 86 89 90 97 99 71 90 99 90 91 88 95 97 93 94 89 96 87 91 93 61 97 80 97 96 92 110 DUP050308087 Operator ID: SAM-983 Output File: AGSMI2::FM Data File: >GSMI2::D5 Name: VSTD020 020 ppb IC Misc: -SAM %C @WL -1 +DCE05Y-W QUANT REPORT Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: Page 3 960924 03:07 960924 02:12 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Compound 82) 1,2-Dichlorobenzene 83) 1,2-Dibromo-3-Chloropropane * Compound is ISTD R.T. Q ion 19.41 146.0 20.62 157.0 Area 57283 10755 Cone Units 15.04 ug/L 19.78 ug/L q 91 92 A fttt 1,, .1 , 111 DUP050308088 Data Files >GSMI3::D5 .. Quant Output Files AGSMI3s:FM Names VSTD050 050 ppb IC Instrument ID: HP03460 Misc: -SAM %C @WL =1 +DCE05Y-W Id File: IA4390::DB Titles 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Operator ID: SAM-983 Quant Time : 960924 03:11 Injected at: 960924 02:44 1 t-J DUP050308089 QUANT REPORT Page 1 Operator ID: SAM-983 output File: -GSMI3::FM Data File: >GSMI3::D5 Name: VSTD050 050 ppb'IC Misc: -SAM %C @WL =1 +DCE05Y-W Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 03:11 960924 02:44 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Mater/Med Soil ID File for Inst HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Compound 1) 2) 3) 4) 5} 6) 7) 8) 9) 10) 11} 12) 13) 14) 15) 16) 17) 18) 19) 20) 21) 22) 23) 24) 25) 26) 27) 28) 29) 30) 31) 32) 33) 34) 35) 36) 37) 38) 39) 40) *Bromochloromethane Dichlorodifluoromethane Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane Furfuran Ethyl Ether Acrolein 1,l-Dichloroethene Freon 113 Acetone Methyl Iodide Carbon Disulfide Allyl Chloride Methylene Chloride t-Butyl Alcohol Acrylonitrile Methyl t-Butyl Ether trans-1,2-Dichloroethene n-Hexane 1,1-Dichloroethane 1-Propanol cis-1,2-Dichloroethene 2-Butanone Propionitrile Ethyl Acetate Methacrylonitrile Tetrahydrofuran Chloroform Cyclohexane 1,2-Dichloroethane-d4 1,2-Dichloroethane *1,4-Difluorobenzene Vinyl Acetate l,l,l-Trichloroethane Carbon Tetrachloride Isobutyl Alcohol Benzene R.T. Q ion 9.51 128.0 3.08 85.0 3.32 50.0 3.57 62.0 4.10 94.0 4.30 64.0 4.85 101.0 5.52 68.0 5.46 59.0 5.71 56.0 5.91 96.0 5.98 101.0 6.03 43.0 6.17 142.0 6.30 76.0 6.63 41.0 6.86 84.0 7.17 59.0 7.32 53.0 7.41 73.0 7.39 96.0 7.90 57.0 8.15 63.0 8.41 59.0 9.13 96.0 9.15 43.0 9.23 54.0 9.27 43.0 9.48 67.0 9.59 42.0 9.65 83.0 10.04 56.0 10.41 65.0 10.54 62.0 11.10 114.0 8.25 86.0 9.93 97.0 10.20 117.0 10.41 41.0. 10.51 78.0 Area Cone Units 59428 50.00 ug/L 130520 44.20 ug/L 65049 43.89 ug/L 64809 43.52 ug/L 44863 46.21 ug/L 35257 43.06 ug/L 72182 34.64 ug/L 70070 45.97 ug/L 41415 50.65 ug/L 35166 198.76 ug/L 54338 47.75 ug/L 215468 70.18 ug/L 14747 48.36 ug/L 213591 33.86 ug/L 152367 40.57 ug/L 93332 55.24 ug/L 71932 50.78 ug/L 19336 .956E-37 ug/L 54084 216.40 ug/L 133186 49.08 ug/L 64345 47.46 ug/L 66367 49.47 ug/L 127274 46.50 ug/L 2420 741.19 ug/L 69283 51.10 ug/L 17844 43.28 ug/L 19479 .963E-37 ug/L 59199 56.23 ug/L 35022 .173E-36 ug/L 11475 52.67 ug/L 147690 47.36 ug/L 83268 49.73 ug/L 88787 47.32 ug/L 95905 48.23 ug/L 237050 50.00 ug/L 10921 47.24 ug/L 106122 49.70 ug/L 110632 48 11 ug/L 17447 840.18 ug/L 166155 52.19 ug/L 5 72 95 98 96 92 93 97 80 77 94 96 95 98 68 100 87 95 98 96 97 93 91 96 100 96 89 94 97 83 82 97 94 98 89 92 92 87 98 85 92 ns DUP050308090 QUANT REPORT Page 2 Operator ID: SAM-983 Output File: AGSMI3::FM Data File: >GSMI3::D5 Name: VSTD050 050 ppb IC ' Misc: -SAM %C 0WL=1 +DCE05Y-W Quant Rev 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 03:11 960924 02:44 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Compound 41) 42) 43) 44) 45) 46) 47) 48) 49) 50) 51} 52) 53) 54) 55) 56) 57) 58) 59) 60) 61) 62) 63) 64) 65) 66) 67) 68) 69) 70) 71) 72) 73) 74) 75) 76) 77) 78) 79) 80) 81) n-Heptane n-Butanol Trichloroethene 1,2-Dichloropropane Dlbromomethane 1,4-Dioxane n-Propyl Acetate Bromodichloromethane 2-Nitropropane 2-Chloroethy1 Vinyl Ether cis-1,3-Dichloropropene trans-l,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane Bromoform trans-1,4-Dichloro-2-Butene *Chlorobenzene-d5 4-Methyl-2-Pentanone Toluene-d8 Toluene Ethyl Methacrylate Tetrachloroethene 2-Hexanone 1,2-Dibromoethane Chlorobenzene 1,1,1,2-Tetrachloroethane Ethylbenzene m-f-p-Xylene Isoamyl Acetate o-Xylene Styrene Cumene Cyclohexanone 4-Bromofluorobenzene 1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane 2-Chlorotoluene Pentachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl Chloride R.T. Q ion 10.93 71.0 11.41 56.0 li.50 130.0 11.82 63.0 12.00 93.0 12.02 88.0 12.08 43.0 12.23 83.0 12.53 41.0 12.65 63.0 12.87 75.0 13.67 75.0 13.94 97.0 14.52 129.0 16.61 173.0 17.36 53.0 15.37 117.0 13.08 43.0 13.27 98.0 13.36 91.0 13.80 69.0 14.17 164.0 14.29 43.0 14.70 107.0 15.42 112.0 15.52 131.0 15.56 106.0 15.73 106.0 15.82 70.0 16.32 106.0 16.33 104.0 16.86 105.0 16.98 55.0 17.08 95.0 17.28 83.0 17.35 110.0 17.61 126.0 18.25 167.0 18.72 146.0 18.85 146.0 19.03 91.0 Area Cone Units 47761 14619 90007 78403 65242 7061 101420 154465 30911 40674 121185 107426 72261 157229 143542 61643 189164 55945 200295 184698 76031 96665 38037 108514 168208 76642 66308 173276 65310 82119 150679 216358 22630 161949 113203 25857 63415 70764 159001 175048 126470 49.77 ug/L 861.41 ug/L 50.96 ug/L 47.52 ug/L 37.64 ug/L 684.03 ug/L 55.50 ug/L 46.91 ug/L 89.48 ug/L 46.04 ug/L 52.89 ug/L 54.96 ug/L 48.30 ug/L 48.91 ug/L 47.71 ug/L . 764E-37 ug/L 50.00 ug/L 49.42 ug/L 49.45 ug/L 50.39 ug/L 42.51 ug/L 52.39 ug/L 50.84 ug/L 40.07 ug/L 48.64 ug/L 29.83 ug/L 51.27 ug/L 112.17 ug/L 48.00 ug/L 53.16 ug/L 49.48 ug/L 44.55 ug/L 712.70 ug/L 49.77 ug/L 53.84 ug/L 39.62 ug/L 47.34 ug/L 29.95 ug/L 37.70 ug/L 38.04 ug/L 43.31 ug/L g 82 98 93 80 85 75 95 95 98 90 88 93 94 95 98 87 92 90 97 92 72 88 96 93 95 91 98 93 89 93 90 94 93 92 93 61 99 81 95 95 93 114 DUP050308091 Operator ID: SAM-983 Output File: ~GSMI3::FM Data File: >GSMI3::D5 Name: VSTDOSO 050 ppb IC Misc: -SAM %C @WL =1 +DCEOSY-W QUANT REPORT Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: Page 3 960924 03:11 960924 02:44 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01*40 Compound 82) 1,2-Dichlorobenzene 83) 1,2-Dibromo-3-Chloropropane * Compound is ISTD R.T. Q ion 19.41 146.0 20.62 157.0 Area 150309 23367 cone Units 37.86 ug/L 41.22 ug/L q g" si 115 DUP050308092 TOTAL ION CHROMATOGRAM Data File: >GSMI4::D5 Quant Output File: AGSMI4::FM Name: VSTD10Q 100 ppb IC Instrument ID: HP03460 Misc: -SAM %C @WL =1 +DCE05Y-W Id File: IA4390::DB Title: 3^90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Operator ID: SAM-983 Quant Time : 960924 03:44 Injected at: 960924 03:17 A - v ,,g 116 DUP050308093 Operator ID: SAM-983 Output File: `"'GSMI4:: FM Data File: >GSMI4::D5. Name: VSTD100 100 ppb IC . Misc: -SAM %C WL 1 +DCEQ5V-W QUANT REPORT Quant Rev: 7 Quant Tine Injected at Dilution Factor Instrument ID Page 1 960924 03:44 960924 03:17 1.00000 HP03460 . ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time 960924 01:40 Compound 1) 2) *Broraochloromethane Dichlorodifluoromethane 3) Chloromethane 4} Vinyl Chloride 5) Broxnomethane 6) Chloroethane 7} Trichlorofluoromethane 8} Furfuran 9) Ethyl Ether 101 Acrolein 11) 1,l-Dichloroethene 12) Freon 113 13) Acetone 14) Methyl iodide 15) Carbon Disulfide 16) Allyl Chloride 17) Methylene Chloride 18) t-Butyl Alcohol 19) Acrylonitrile 20) Methyl t-Butyl Ether 21) trans-l,2-Dichloroethene 22) n-Hexane 23) 1,l-Dichloroethane 24) l-Propanol 25) cis-1,2-Dichloroethene 26) 2-Butanone 27) Propionitrile 28) Ethyl Acetate 29) Methacrylonitrile 30) Tetrahydrofuran 31) Chloroform 32) Cyclohexane 33) 1,2-Dichloroethane-d4 34) 1,2-Dichloroethane 35) *1,4-Difluorobenzene 36) Vinyl Acetate 37) 1,1,l-Trichloroethane 38) Carbon Tetrachloride 39) Isobutyl Alcohol 40) Benzene R.T. Q ion 9.50 123.0 3.07 85.0 3.33 50.0 3.59 62.0 4.10 94.0 4.30 64.0 4.83 101.0 5.52 68.0 5.46 59.0 5.70 56.0 5.90 96.0 5.97 101.0 6.02 43.0 6.18 142.0 6.31 76.0 6.63 41.0 6.87 84.0 7.18 59.0 7.32 53.0 7.41 73.0 7.39 96.0 7.90 57.0 8.14 63.0 8.41 59.0 9.13 96.0 9.15 43.0 9.22 54.0 9.27 43.0 9.48 67.0 9.59 42.0 9.66 83.0 10.03 56.0 10.41 65.0 10.53 62.0 11.09 114.0 8.26 86.0 9.92 97.0 10.19 117.0 10.41 41.0 10.52 78.0 Area Cone Units 60383 268177 124772 125423 85865 67410 151881 147079 86525 79941 105786 439989 30581 432186 314806 203927 134343 40109 117073 286435 127714 140364 249788 5048 139380 36401 41835 127448 77088 26542 288086 174365 177477 188644 240039 23355 216382 218497 34885 330285 50.00 ug/L 89.37 ug/L 82.85 ug/L 82.89 ug/L 87.04 ug/L 81.02 ug/L 71.73 ug/L 94.96 ug/L 104.15 ug/L 444.68 ug/L 91.49 ug/L 141.04 ug/L 98.69 ug/L 67.44 ug/L 82.50 ug/L 118.78 ug/L 93.34 ug/L .195E-36 ug/L 461.03 ug/L 103.88 ug/L 92.71 ug/L 102.97 ug/L 89.81 ug/L 1521.63 ug/L 101.18 ug/L 86.89 ug/L .204E-36 ug/L 119.15 ug/L .375E-36 ug/L 119.89 ug/L 90.92 ug/L 102.49 ug/L 93.08 ug/L 93.36 ug/L 50.00 ug/L 99.77 ug/L 100.08 ug/L 93.84 ug/L 1659.01 ug/L 102.46 ug/L g 77 98 97 98 96 94 99 81 78 93 93 94 97 71 100 86 93 93 94 92 92 93 96 100 96 90 90 98 82 86 95 96 97 86 93 92 92 97 89 92 117 DU P050308094 QUANT REPORT Page 2 Operator ID: SAM-983 Output File: ~GSMI4::FM Data File: >GSMI4::D5` Name: VSTD100 100 PPb 1C ' Misc: -SAM %C 0WL *1 +DCE05Y-W Quant Rev 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 03:44 960924 03:17 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst HPQ3460 Last calibration: 9S1207 01:59 Last Qcal Time: 960924 01:40 Compound 41) 42) 43) 44) 45) 46) 47) 48) 49) 50) 51) 52) 53) 54) 55) 56) 57) 58) 59) 60) 61) 6 2) 63) 64) 65) 66) 67) 68) 69} 70} 71} 72) 7 3} 74) 75) 76) 77) 78) 79) 80) 81) n-Heptane n-Butanol Tr i chi oroetitiene 1,2-Dichloropropane Dibromomethane 1,4-Dioxane n-Propyl Acetate Bromodichloromethane 2-Nitropropane 2-Chloroethyl Vinyl Ether cis-l,3-Dicnloropropene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane Bromoform trans-1,4-D:tchloro-2 -Butene *Chlorobenzene-d5 4-Methyl-2-Pentanone Toluene-d8 Toluene Ethyl Methacrylate Tetrachloroethene 2-Hexanone 1,2-Dibromoethane Chlorobenzene 1,1,1,2-Tetrachloroethane EthyIbenzene m+p-Xylene Isoamyl Acetate o-Xylene Styrene Cumene Cyclohexanone 4-Bromofluorobenzene 1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane 2-Chlorotoluene Pentachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl Chloride R.T. Q ion 10.94 71.0 11.41 56.0 11.50 130.0 11.82 63.0 11.99 93.0 12.01 88.0 12.08 43.0 12.23 83.0 12.54 41.0 12.66 63.0 12.88 75.0 13.67 75.0 13.94 97.0 14.53 129.0 16.61 173.0 17.36 53.0 15.37 117.0 13.09 43.0 13.26 98.0 13.37 91.0 13.79 69.0 14.18 164.0 14.28 43.0 14.69 107.0 15.42 112.0 15.52 131.0 15.56 106.0 15.73 106.0 15.81 70.0 16.32 106.0 16.33 104.0 16.85 105.0 16.98 55.0 17.09 95.0 17.28 83.0 17.35 110.0 17.61 126.0 18.24 167.0 18.71 146.0 18 *84 146.0 19.04 91.0 Area cone Units 96641 99.45 ug/L 27621 1607.26 ug/L 182138 101.83 ug/L 153214 91.70 ug/L 159973 91.14 ug/L 13393M 1281.28 ug/L 212118 114.62 ug/L 307588 92.25 ug/L 77616 221.87 ug/L 86194 96.34 ug/L 247458 106.66 ug/L 223868 113.11 ug/L 143552 94.76 ug/L 310000 95.22 ug/L 284510 93.39 ug/L 124560 .. 152E-36 ug/L 183503 50.00 ug/L 122944 111.95 ug/L 407233 103.64 ug/L 382877 107.68 ug/L 180533 104.06 ug/L 193616 108.18 ug/L 81470 112.26 ug/L 230941 87.92 ug/L 324152 96.62 ug/L 194712 78.11 ug/L 128089 102.09 ug/L 327748 218.71 ug/L 134870 102.18 ug/L 160135 106.86 ug/L 292954 99.17 ug/L 451656 95.87 ug/L 46470 1508.65 ug/L 320456 101.52 ug/L 227858 111.71 ug/L 53128 83.92 ug/L 130884 100.73 ug/L 177941 77.62 ug/L 331810 81.10 ug/L 363384 81.40 ug/L 267298 94.36 ug/L g 80 98 92 81 88 96 92 97 95 88 89 94 93 94 97 89 91 91 98 99 78 88 97 93 90 92 98 95 89 93 93 96 94 90 92 58 99 84 95 96 93 118 DU P 050308095 QUANT REPORT Page 3 Operator ID: SAM-983 Output File: AGSMI4::FM Data File: >GSMI4::D5 Name: VSTD100 100 ppb IC Misc: -SAM %C @WL =1 +DCE05Y Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 03:44 960924 03:17 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Compound 82) 1,2-Dichlorobenzene 83) l,2-Dibrorno-3-Chloropropane * Compound is ISTD R.T. Q ion 19.40 146.0 20.62 157.0 Area 319295 4983B Cone Units 82.90 ug/L 90.62 ug/L g 96 84 DUP050308096 Data File: >GSM14 Name: VSTD100 100 ppb IC Misc: -SAM %C @WL =1 +DCE05Y-W Quant Time: 960924 03:44 Injected at: 960924 03:17 Compound No: 46 Compound Name: 1,4-Dioxane Scan Number: 858 Retention Times 12.01 min Quant Ion: 88.0 Area: 13393M Concentration: 1281.28 ug/L g-value: 96 Quant Output File: ''GSMI4 Instrument ID: HP03460 Qusnt ID File: IA4390 ' Last Calibration: 951207 01:59 This report was produced by QAREA at: 4:47 AM TUE., 24 SEPT, 1996 120 DUP0 50308097 TOTAL ION CHROMATOGRAM Data File: >GSMI5::D5 Quant Output File: AGSMI5::FM Name: VSTD200 200 ppb IC Instrument ID: HP03460 MlSC: -SAM %CI @WL =1 +DCE05Y-W Id File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Operator ID: SAM-983 Quant Time : 960924 04:16 Injected at: 960924 03:49 121 DUP050308098 QUANT REPORT Page l Operator ID: SAM-983 Output File: "'GSMIS: :FM Data File: >GSMX5::D5 Name: VSTD200 200 ppblCMisc: -SAM %C @WL =1 +DCEOSY-W Quant Rev 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 04:16 960924 03:49 1.00000 HP03460 ID File: IA4390::DB Title: 3/90 Water/Med Soil ID File for Inst HF03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Compound 1 *Bromochloromethane 2 Dichlorodifluoromethane 3 Chloromethane 4 Vinyl Chloride 5 Bromomethane 6 Chloroethane 7 Trichlorofluoromethane 8 Furfuran 9 Ethyl Ether io; Acrolein 11 1.l-Dichloroethene 12 Freon 113 13 Acetone 14 Methyl Iodide 15, carbon Disulfide 16 Allyl Chloride 17, Methylene Chloride is; t-Butyl Alcohol 19] Acrylonitrile 20] Methyl t-Butyl Ether 21 trans-l,2-Dichloroethene 22] n-Hexane 23 1,l-Dichloroethane 24] 1-Propanol 25] cis-1,2-Dichloroethene 26] 2-Butanone 27] Propionitrile 28] Ethyl Acetate 29] MethacryIonitrile 30] Tetrahydrofuran 31) Chloroform 32) Cyclohexane 33] 1,2-Dichloroethane-d4 34) 1,2-Dichloroethane 35) *1,4-Difluorofoenzene 36) Vinyl Acetate 37) lf1,l-Trichloroethane 38) carbon Tetrachloride 39) Isobutyl Alcohol 40) Benzene R.T. Q ion 9.50 128.0 3.08 85.0 3.34 50.0 3.58 62.0 4.10 94.0 4.28 64.0 4.84 101.0 5.53 68.0 5.46 59.0 5.70 56.0 5.89 96.0 5.96 101.0 6.03 43.0 6.18 142.0 6.32 76.0 6.62 41.0 6.86 84.0 7.20 59.0 7.32 53.0 7.41 73.0 7.38 96.0 7.89 57.0 8.14 63.0 8.43 59.0 9.13 96.0 9.15 43.0 9.22 54.0 9.27 43.0 9.48 67.0 9.60 42.0 9.64 83.0 10.03 56.0 10.41 65.0 10.53 62.0 11.09 114.0 8.25 86.0 9.92 97.0 10.19 117.0 10.41 41.0 10.51 78.0 Area Cone Units 57852 513973 245542 250682 153149 89513 272249 285271 169891 165366 204786 798368 58672 847690 621367 407545 266336 85918 243622 556879 247474 250446 492976 10310 282002 75329 87904 272820 156959 54100 554524 331139 347154 355078 233932 48334 415759 416626 69979 640812 50.00 ug/L 178.78 ug/L 170.17 ug/L 172.93 ug/L 162.03 ug/L 112.29 ug/L 134.21 ug/L 192.23 ug/L 213.44 ug/L 960.12 ug/L 184.86 ugVL 267.12 .ug/L 197.63 ug/L. 138.06 ug/L 169.96 Ug/L 247.77 ug/L 193.13 ug/L .436E-36 ug/L 1001.35 ug/L 210.80 ug/L 187.50 ug/L 191.76 ug/L 185.01 ug/L 3243.74 ug/L 213.66 ug/L 187.68 ug/L .447E-36 ug/L 26-6.22 ug/L .797E-36 ug/L 255.07 ug/L 182.66 ug/L 203.15 ug/L 190.04 ug/L 183.42 ug/L 50.00 ug/L 211.88 ug/L 197.31 ug/L 183.61 ug/L 3414.84 ug/L 203.98 ug/L q 70 97 98 99 98 94 96 78 75 95 97 96 93 64 100 82 94 94 96 92 93 90 96 100 96 87 91 99 79 88 98 90 97 85 95 91 92 96 88 93 ioo DUP050308099 QUANT REPORT Page 2 Operator ID: SAM-983 Output File: AGSMI5::FM Data File: >GSMI5::D5Name: VSTD200 200 ppb IC Misc: -SAM %C @WL=1 +DCE05Y-W Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 04:16 960924 03:49 1.00000 HP03460 ID File:.IA4390::DB ^, Title: 3>90 Water/Med Soil ID File for Inst HP03460 Last Calibration: 951207 01:59 Last Qcal Time 960924 01:40 Compound 41 n-Heptane 42 n--Butanol 43 Trichloroethene 44 1,2-Dichloropropane 45 Dibromomethane 46 1,4-Dioxane 47 n-Propyl Acetate 48] Bromodichloromethane 49, 2-Nitropropane 50] 2-Chloroethyl Vinyl Ether 51 cis-1,3-Dichloropropene 52 trans-l,3-Dichloropropene 53 1,1,2-Trichloroethane 54] Dibromochloromethane 55] Bromoform 56] trans-l,4-Dichloro-2-Butene 57] *Chlorobenzene-d5 58] 4-Methy1-2-Pentanone 59, Toluene-d8 60] Toluene 61] Ethyl Methacrylate 62] Tetrachloroethene 63] 2-Hexanone 64 1,2-Dibromoethane 65] Chlorobenzene 66] 1,1,1,2-Tetrachloroethane 67] Ethylbenzene 68] m+p-Xylene 69] Isoamyl Acetate 70] o-Xylene 71) Styrene 72) Cumene 73 Cyclohexanone 74) 4-Bromofluorobenzene 75) 1,1,2,2-Tetrachloroethane 76) 1,2,3-Trichloropropane 77 2-Chlorotoluene 78) Pentachloroethane 79) 1,3-Dichlorobenzene 80) 1,4-Dichlorobenzene 81) Benzyl Chloride R.T. Q ion 10.93 71.0 11.41 56.0 11.50 130.0 11.82 63.0 11.99 93.0 12.02 88.0 12.07 43.0 12.24 83.0 12.53 41.0 12.65 63.0 12.87 75.0 13.67 75.0 13.93 97.0 14.52 129.0 16.61 173.0 17.35 53.0 15.36 117.0 13.08 43.0 13.27 98.0 13.36 91.0 13.79 69.0 14.17 164.0 14.29 43.0 14.68 107.0 15.41 112.0 15.51 131.0 15.56 106.0 15.73 106.0 15.82 70.0 16.31 106.0 16.33 104.0 16.85 105.0 16.99 55.0 17.08 95.0 17.27 83.0 17.34 110.0 17.60 126.0 18.23 167.0 18.70 146.0 18.84 146.0 19.03 91.0 Area Cone Units 165593 59373 349386 302209 291358 25833 435294 583534 158439 178885 476251 425486 274964 587790 567345 234387 172695 249995 771123 742685 353699 347155 173610 456010 622593 350002 233777 575648 268601 281804 522081 826826 92886 564555 449931 98801 241181 334267 619886 677213 518907 174.86 ug/L 3545.10 ug/L 200.43 ug/L 185.60 ug/L 170.33 ug/i* 2535.90 ug/L 241.36 ug/L 179.59 ug/L 464.74 ug/L 205.16 ug/L 210.64 ug/L 220.60 ug/L 186.24 ug/L 185.27 ug/L 191.10 ug/L .294E-36 ug/L 50.00 ug/L 241.89 ug/L 208.53 ug/L 221.93 ug/L 216.63 ug/L 206.10 ug/L 254.19 ug/L 184.47 ug/L 197.19 ug/L 149.20 ug/L 197.99 ug/L 408.18 ug/L 216.24 ug/L 199.82 ug/L 187.80 ug/L 186.49 ug/L 3204.28 ug/L 190.05 ug/L 234.39 ug/L 165.83 ug/L 197.23 ug/L 154.95 Jig/L 160.99 ug/L 161.20 ug/L 194.64 ug/L q 79 98 92 81 84 78 93 96 96 87 90 94 95 98 95 87 92 90 93 96 69 89 96 91 94 95 98 87 86 95 90 99 93 79 94 63 99 S3 97 96 90 DUP050308100 QUANT REPORT Page 3 Operator ID: SAM-983 Output File: '`GSMI5:: FM - Data File: >GSMI5::D5 Name: VSTD200 200 ppb IC Misc: -SAM %C @WL =1 +DCE05Y-W Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 04:16 960924 03:49 1.00000 HP03460 ID File: IA4390::DR Title: 3/90 Water/Med Soil ID File for Inst. HP03460 Last Calibration: 951207 01:59 Last Qcal Time: 960924 01:40 Compound 82) 1,2-Dichlorobenzene 83) l,2-Dibromo-3-Chloropropane * Compound is ISTD R.T. Q ion 19.39 146.0 20.61 157.0 Area 616392 103383 Cone Units 170.05 ug/L 199.74 ug/L q 97 80 1-24 DUP0503081 01 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: LANCASTER LABS - contract: ______ . Lab Code: LANCAS Case No.: ______ . SAS No. _______. SDG No.: _______ Instrument ID: HP03046 Calibration Da'te(s) : 03/20/96 08/20/96 Heated Purge: (Y/N) N Calibration Times: 2025 2246 GC Column: DB624 LAB FILE.ID: : RRF 50= >IGKI3 ID: 0.53 (mm) RRF 10= >IGKI1 RRF100- >IGKI4 RRF 20= >I<3KI2 RRF200= >ICJKI5 COMPOUND RRF 10 RRF 20 RRF 50 RRF100 RRF200 ESF RSD sss ssssssssssss =======SSSSSSESSSSS ssasassessas ssssasasssss Diehlorodifluororaethane Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 3.008 1.230 1.236 1* 1.315 .784 .907 2.790 1.143 1.167 1.236 .727 .852 2.718 1.001 1.134 1.190 .721 .893 2.913 1.132 1.230 1.205 .746 .936 2.762 1.093 1.172 1.010 .687 .877 2.838 1.120 1.188 1.191 .733 .893 4.2 7.4 3.7* 9.4* 4.8 3.5 Ethyl Ether Acrolein 1,l-Dichloroethene Freon 113 Acetone Methyl Iodide Carbon Disulfide Allyl Chloride Methylene Chloride t-Butyl Alcohol Acrylonitrile Methyl t-Butyl Ether 1,2-Dichloroethene (total) 1,l-Dichloroethane 2-Butanone Propionitrile Ethyl Acetate Methacrylonitrile Tetrahydrofuran Chloroform Cyclohexane 1,2-Dichloroethane Vinyl Acetate 1,1,l-Trichloroethane Carbon Tetrachloride Isobutyl Alcohol Benzene -.884 .142 1* 1.230 2.767 .4T0 3.163 2.965 1.507 2.141 .115 .245 3.439 1.387 i 2.602 .376 .083 1.417 .325 .254 1 3.137 1.757 * 2.373 .519 * .566 * .421 .007 * .816 .861 .138 1.153 2.342 .360 2.929 2.875 1.435 1.711 .099 .234 3.285 1.313 2.502 .395 .084 1.376 .312 .252 2.986 1.620 2.296 .522 .547 .412 .005 .779 .868 .131 1.150 2.270 .343 2.900 2.949 1.452 1.427 .088 .251 3.260 1.338 2.484 .404 .084 1.320 .326 .278 2.900 1.609 2.257 .556 .526 .398 .006 .748 .873 .148 1.189 2.446 .3743.160 3.365 1.546 1.339 .111 .263 3.257 1.367 2.623 .452 .095 1.440 .355 .315 3.003 1.703 2.299 .583 .552 .420 .008 .791 .836 .152 1.137 2.219 . 3T55 3.032 3.278 1.615 1.340 .114 .275 3.199 1.338 2.597 .449 .101 1.465 .350 .329 2.976 1.643 2.295 .595 .520 .411 . 008 .752 .864 .142 1.172 2.409 .370 3.037 3.086 1.511 1.601 .105 .254 3.288 1.348 2.562 .415 .089 1.403 .334 .286 3.001 1.666 2.304 .555 .542 .412 .007 .777 2.1 6.0 3.2* 9.0 6.8 4.1 7.1 4.8 20.9 11.0 6.3 2.7 2 .1 2 ,5* 8 .1 9 .1 4 ,1 5 ,5 12 .2 2 ,9* 3.7 | 1.8* 6.2 | 3.5* 2.3* 15.2 | 3.6* 1, ............... A * Compounds with required minimum RRF and maximum %RSD values. All other compounds in OLM01.S must meet a minimum RRF of 0.010. page 1 of 3 FORM VI VOA OLM03.0 rr DUP050308102 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: LANCASTER LABS Contract: Lab code: LANCAS Case No.: . iSAS No. SDG No.: Instrument ID: HP03046 Calibration Date(s): 08/20/96 08/20/96 Heated Purge: (V/N) N Calibration Times: 2025 2246 GC column: DB624 ID: 0.53 (mm) LAB FILE ID: RRF 50= >IGKI3 RRF 10= ">fSKn RRF100= >IGKI4 RRF 2o= >1g KI21 RRF200= >IGKI5 COMPOUND RRF 10 RRF 20 RRF 50 RRF100 RRF200 Trichloroethene . 1 if .391 1,2-Dichloropropane .344 Methyl Methacrylate .226 Dibromomethane .395 1,4-Dioxane n-Propyl Acetate .002 .529 B romod1chloromethane k .682 2-Nitropropane .096 2-Chloroethyl Vinyl Ether .206 cis-1,3-Dichloropropene \e .562 trans-1,3-Dichloropropene * .507 1,1,2-Trichloroethane * .335 Dibromochloromethane . * .497 Bromoform * .303 trans-1,4-Dichloro-2-Butene .131 4-Methy1-2-Pentanone Toluene .447 1If 1.230 Ethyl Methacrylate Tetrachloroethene .615 * .417 2-Hexanone .265 1,2-Dibromoethane Chlorobenzene .691 if .933 1,1,1,2-Tetrachloroethane .434 Ethylbenzene * .392 Xylene (total) * .478 Isoamyl Acetate Styrene .448 * .838 Cumene 1.477 1,1,2,2-Tetrachloroethane If .751 1,2,3-Trichloropropane .196 Pentachloroethane .321 1,3-Dichlorobenzene .604 1,4-Dichlorobenzene .733 .367 .334 .229 .387 .002 .524 . 695 .106 .207 .566 .527 .328 .519 .330 .142 .445 1.197 .627 .399 .278 .689 .892 .489 .380 .467 .457 .823 1.429 .753 . 190 .329 . 618 .730 .351 .329 .224 .374 .001 .508 .696 .108 .207 . 564 .524 .323 .541 .343 .143 .436 1.175 .644 .395 .280 .697 .870 .485 .372 .469 .465 .834 1.400 .736 . 189 .326 .648 .732 .368 .346 .236 .379 .002 .560 .741 .128 .227 .598 . 560 .330 .566 .373 .159 .483 1.266 .701 .413 .328 .734 .934 .499 .391 .474 .508 .896 1.443 .730 .192 .322 .658 .743 .348 .350 .236 .377 .002 .561 .734 .131 . 231 . 592 . 555 .1*26 .557 .373 .155 .487 1.243 .719 .394 .334 .745 .928 .490 .369 .453 .516 .863 1.433 .763 .189 .316 .639 .731 KKF .3 65 .341 .230 .382 .002 .536 .710 . 114 .216 .576 .535 .328 .536 .344 .146 .460 1.222 .661 .404 .297 .711 .911 .490 .381 .468 .479 .851 1.436 .757 .191 .323 .633 .734 % RSD 4.8 2.6 2.4 2.2 14.5 4.3 3.7 13.3 5.7 3.0 4.2 1.4 5.3 8.7 7.8 5.1 3.0 7.0 2.6 10.7 3.7 3 * 2' 1.2 2.8' 2.0" 6*5 3.41.9 2.1' 1.5 1.6 3.5 .7 * Compounds with required minimum RRF'and' maximum %RSD values. All other compounds in OLMOI.8 must meet a minimum RRF of 0.010. page 2 of 3 FORM VI VOA 0LM03.0 .26 A DUP050308103 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: LANCASTER LABS Lab Code: LANCAS Case No.: Contract: . SAS No. * SDG No . : Instrument ID: HP03046 Calibration Date(s) : 08/20/96 08/20/96 Heated Purge: (Y/N) N Calibration Times: 2025 2246 GC Column: DB624 ID: 0.53 (mm) LAB FILE..ID": RRF 50= >IGKI3 RRF 10= >IGKI1 RRF100= >IGKI4 Hi'F.20= >IGKI2 RRF200= >IGKI5 COMPOUND RRF 10 RRF 2 0 RRF 50 RRF100 RRF200 HKf * RSD 1,2-Dichlorobenzene .604 .618 .614 .583 .562 .596 3.9 1,2-Dichloroethane~d4 Toluene-d8 4-Bromofluorobenzene 2.166 1.204 .843 2.115 1.184 .830 2.128 1.221 861 2.119 1.233 .868 2.140 1.256 .876 2.133 1.220 .855 1.0 2.2 2.2 * Compounds with required minimum RRF andmaximum %RSD values. All other compounds in OLM01.8 must meet a minimum RRF of 0.010. page 3 of 3 FORM VI VOA OLM03.0 A .27 DUP050308104 Data File: >XGKX1::D9 Name: VSTD010 010 PPB IC Wise: -SJL @WL %C +JCEO =1 Quant Output File: AIGKI1::D7 Instrument ID: HP03046 Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Operator ID: SJL-176 Quant Time : 960820 20:50 Injected at: 960820 20:25 128 DUP050308105 QUANT REPORT Page 1 Operator ID: SJL-176 Output Filei ~IGKI1::D7 Data Files >IGKX1::D9 Name: VSTD010 010 PPB IC Misc: -SJL WL %C +JCEO ' =1 Quant Revs 7 Quant Time Injected at Dilution Factor Instrument ID 960820 20:50 960820 20:25 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time 960710 14:27 Compound 1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) l,l-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene jChloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene ,21) 1,1-Dichloroethane 22) cis-1 2-Dichloroethene 23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,1-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) Methyl Methacrylate R.T. Q ion 8.29 128.0 2.42 85.0 2.52 50.0 2.72 62.0 3.14 94.0 3.31 64.0 3.67 101.0 4.19 59.0 4.42 56.0 4.59 96.0 4.64 101.0 4.71 43.0 4.87 142.0 5.02 76.0 5.30 41.0 5.56 84.0 5.91 59.0 6.05 53.0 6.11 73.0 6.08 96.0 6.85 63.0 7.89 96.0 7.95 43.0 8.03 54.0 8.09 43.0 8.28 67.0 8.39 42.0 8.45 83.0 8.82 56.0 9.24 65.0 9.37 62.0 .9.96 114.0 7.01 43.0 8.72 97.0 9.00 117.0 9.31 41.0 9.32 78.0 10.36 130.0 10.68 63.0 10.90 69.0 Area Cone Units q 39140 23545 9629 9674 10294 6136 7098 6921 5554M 9630 43326 3213 24760 23211 11798M 16758 4502 9587 26921 10700 20371 11015 2947 3243 11095 6361 1991 24558 13754 16954 18577 162514 16863 18389 13680 2732 26513 12721 11168 7356 50.00 UG/L 12.93 UG/L 13.32 UG/L 10.81 UG/L 14.50 UG/L 13.08 UG/L 8.51 UG/L 16.28 UG/L 55.33 UG/L 9.23 UG/L 22.20 UG/L 11.24 UG/L 9.81 UG/L 8.42 UG/L 10.79 UG/L 14.32 UG/L 49.28 UG/L 53.69 UG/L 12.37 UG/L 8.94 UG/L 9.07 UG/L 9.20 UG/L 9.02 UG/L 50.07 UG/L 11.53 UG/L 25.88 UG/L 9.83 UG/L 8.88 UG/L 20.39 UG/L 9.94 UG/L 9.36 UG/L 50.00 UG/L 7.97 UG/L 8.65 UG/L 7.92 UG/L 114.91 UG/L 9.80 UG/L 9.61 UG/L 9.99 UG/L 10.84 UG/L 87 92 95 99 95 95 98 83 99 92 92 75 72 100 97 95 96 90 93 95 96 89 96 97 89 72 97 95 89 90 87 96 89 94 93 90 87 89 38 129 DUP050308106 QUANT REPORT Page 2 Operator ID: SJL-176 Output File: AIGKI1::D7 Data File: >IGKIl::D9 Name: VSTD010 010 PFB IC Misc: --SJL @WL %C +>CEO =1 Quant Rev: 7 Quant Time Injected at Dilution Factor Instrument ID 960820 20:50 960820 20:25 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Ked Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Compound 41) 42) 43) 44) 45) 46} 47} 48) 49) 50) 51) 52) 53) 54) 55) 56) 57) 58 59 60 61] 62] S3, 64] 65; 66; 67 68 69 70] 7i; 72; 73' 74) 75) Dibromomethane 1,4-Dioxane n-Propyl Acetate Bromodlchloroaethane 2-Nitropropane 2-Chloroethyl Vinyl Ether cis-l,3-Dichloropropene trans-l,3-Dichloropropene l,1,2-Trichloroethane Dibromochloromethane Bromoform trans-l,4-Dichloro-2-Butene * Chlorobenz ene-d5 4-Methyl-2-Pentanone Toluene-d8 Toluene Ethyl Methacrylate Tetrachloroethene 2-Hexanone 1,2-Dibromoethane Chlorobenz ene 1,1,1,2-Tetrachloroethane Ethylbenzene m+p-Xylene Isoamyl Acetate o-Xylene Styrene Cumene 4-Bromofluorobenzene 1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane Pentachloroethane 1,3-Dichlorobenz ene 1,4-Dichlorobenzene 1,2-Dichlorobenzene * Compound is ISTD R.T. Q ion 10.87 93.0 10.92 88.0 11.01 43.0 11.11 83.0 11.45 41.0 11.58 63.0 11.78 75.0 12.59 75.0 12.85 97.0 13.42 129.0 15.51 173.0 16.29 53.0 14.26 117.0 12.01 43.0 12.16 98.0 12.25 91.0 12.73 69.0 13.04 164.0 13.23 43.0 13.58 107.0 14.30 112.0 14.43 131.0 14.47 106.0 14.64 106.0 14.78 70.0 15.22 106.0 15.24 104.0 15.75 105.0 15.99 95.0 16.20 83.0 16.25 110.0 17.14 167.0 17.59 146.0 17.73 146.0 18.28 145.0 Area 12834M 727 17194 22177 6223 6687 18265 17145 10888 16150 9847 10608 119727 10704 28830 29444 14729 9993 6334 16536 22339 11593 9379 24549 10722 11445 20058 35367 20174 17991 4685 7683 14468 17551M 14464 Cone Units 10.85 UG/L 75.32 UG/L 10.88 UG/L 8.79 UG/L 15.86 UG/L 10.40 UG/L 9.15 UG/L 9.23 UG/L 10.26 UG/L 8.46 UG/L 7.79 UG/L 24.29 UG/L 50.00 UG/L 12.14 UG/L 10.30 UG/L 9.73 UG/L 10.57 UG/L 9.16 UG/L 12.12 UG/L 11.64 UG/L 9.92 UG/L 10.07 UG/L 9.65 UG/L 20.82 UG/L 10.23 UG/L 9.71 UG/L 9.51 UG/L 13.05 UG/L 10.64 UG/L 11.79 UG/L 11.51 UG/L 9.89 UG/L 10.43 UG/L 12.66 UG/L 10.30 UG/L q 84 99 93 95 83 88 90 96 98 96 91 85 91 95 94 92 98 88 95 82 86 96 96 94 92 86 96 72 96 72 88 86 86 83 130 DUP050308107 Data Pile: >IGKI1 Name: VSTD010 010 PPB IC Misc: ~SJL ML %C +>CEO =1 Quant Time: 960320 20:50 Injected at: 960820 20:25 Quant Output File: "IGKI1 Instrument ID: HP03046 Quant ID Pile: IA6390 Last Calibration: 951122 10:44 Compound No: 9 Compound Name: Acrolein Scan Number: 225 Retention Time: 4.42 min Quant Ion: 56.0 Area: 5554M Concentration: S5.3S TJG/L q-value: 99 This report was produced by QAREA at: 12:00 AM WED. , 21 AUG., 1996 131 DUP0503081 08 MJr\ Data File: >IGKI1 Name: VSTD010 010 PPB IC Misc: ~SJL WL %C +JCEO =1 Quant Time: 960820 20:50 Injected at: 960820 20:25 Compound No: 15 Compound Name: Allyl Chloride Scan Number: 301 Retention Time: 5.30 min Quant Ion: 41.0 Area: il798M Concentration: 10.79 UG/L q-value: 0 Quant Output File: ~IGKIl Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 This report was produced by QAREA at: 12:01 AM WED., 21 AUG., 1996 132 DUP050308109 Data File: >IGKI1 Name: VSTD010 010 PPB IC Misc: -SJL WL %C +>CEO =1 Quant Time: 960820 20:50 Injected at: 960820 20:25 Compound No: 41 Compound Name: Dibromomethane Scan Number: 780 Retention Time: 10.87 min Quant Ion: 93.0 Area: . 12834M Concentration: 10.85 UG/L q-value: 0 Quant Output File: MGKI1 . Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 This report was produced by QAREA at: 12:02 AM WED., 21 AUG., 1996 13 DUP050308110 Data File: >IGKI1 Name: VSTD010 010 PPB IC Misc: ~SJL WL %C +}CEO -1 Quant Time: 960820 20:50 Injected at: 960820 20:25 Compound No: 74 Compound Name: 1,4-Dichlprobenzene Scan Number: 1370 Retention Time: 17.73 min Quant Ion: 146.0 Area: 17551M Concentration: 12.6 6 UG/L q-value: 86 Quant Output File: ~IGKI1 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 This report was produced by QAREA at: 12:02 AM WED., 21 AUG., 1996 134 DUP050308111 TOTAL ION CHROHflTOSRflM File >ISKIS 35.0-300;0 amu. Vggfflfeg 020 PPB IC~SJL 8L JSC +>CEQ . - .8?. .-i- 1SQ0 200000- Data File: >IGKI2::D9 Name: VSTD020 020 PPB IC Misc: -SJL WL %C +}CEO *1 Quant Output File: -'IGKI2::D7 Instrument ID: HP03046 Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Operator ID: SJL-176 Quant Time : 960820 21:24 Injected at: 960820 20:59 13 r DUP050308112 QUANT REPORT Page 1 Operator ID: SJL-176 Output File: AIGKI2::D7 Data File: >IGKI2::D9 Name: VSTD020 020 PPB IC Misc: -SJL @RL %C +>CEO =1 Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960820 21:24 960820 20:59 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time 960710 14:27 Compound 1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromathane 4) Vinyl Chloride 5} Bromomethane 6) Chlotoethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,1-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) carbon Disulfide 15) Allyl Chloride 16) Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene 21) l,l-Dichloroethane 22) cis-l,2-Dichloroethene 23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *l,4-Diluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) Methy1 Methacrylate R.T. Q ion Area 8.28 128.0 2.42 85.0 2.54 50.0 2.74 62.0 3.16 94.0 3.31 64.0 3.68 101.0 4.19 59.0 4.40 56.0 4.61 96.0 4.63 101.0 4.71 43.0 4.86 142.0 5.03 76.0 5.29 41.0 5.56 84.0 5.88 59.0 6.04 53.0 6.11 73.0 6.07 96.0 6.85 63.0 . 7.89 96.0 7.95 43.0 8.04 54.0 8.07 43.0 8.27 67.0 8.39 42.0 8.45 83.0 8.82 56.0 9.24 65.0 9.37 62.0 9.96 114.0 7.00 43.0 8.71 97.0 9.01 117.0 9.32 41.0 9.33 78.0 10.36 130.0 10.68 63.0 10.90 69.0 40292 44973 18428 18807 19916 11715 13739 13379 11153 18575 75483 5804 47207 46336 23129M 27575 7938 18849 52947 20966 40322 21349 6371 6773 22170 12554 4063 48129 26115 34084 37012 165797 34626 36283 27325 4517 51694 24361 22156 15177 Cone Units 50.00 UG/L 23.99 UG/L 24.77 UG/L 20.41 UG/L 27.25 UG/L 24.25 UG/L 16.00 UG/L 31.72 UG/L 108.02 UG/L 17.29 UG/L 37.57 UG/L 19.72 UG/L 18.17 UG/L 16.32 UG/L 20.54 UG/L 22.90 UG/L 84.40 UG/L 102.53 UG/L 23.63 UG/L 17.02 UG/L 17.43 UG/L 17.33 UG/L 18.94 UG/L 101.58 UG/L 22.38 UG/L 49.62 UG/L 19.48 UG/L 16.91 UG/L 37.60 UG/L 19.41 UG/L 18.11 UG/L 50.00 UG/L 16.03 UG/L 16.73 UG/L 15.50 UG/L 186.22 UG/L 18.73 UG/L 18.04 UG/L 19.43 UG/L 21.92 UG/L q 85 97 94 97 93 92 98 89 97 88 91 66 74 100 96 94 99 91 96 96 96 93 95 97 89 75 98 97 89 91 87 97 90 96 90 88 86 89 81 136 DUP050308113 QUANT REPORT Page 2 Operator ID: SJL-176 Output File: AIGKI2::D7 Data File: >IGKI2s:D9 Name: VSTD020 020 PPB IC Misc: -SJL WL %C +JCEO =1 Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960820 21:24 960820 20:59 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Compound 41) Dibromomethane 42} 1,4-Dioxane 43} n-Propyl Acetate 44) Bromodichloromethane 45) 2-Nitropropane 46) 2-Chloroethyl Vinyl Ether 47) cis-1,3-Dichloropropene 48) trans-1,3-Dichloropropene 49) 1,1,2-Trichloroethane 50) Dibromochloromethane 51) Bromoform 52) trans-l,4-Dichloro-2-Butene 53) *Chlorobenzene-d5 54) 4-Methyl-2-Pentanone 55) Toluene-d8 56) Toluene 57) Ethyl Methacrylate 58) Tefcrachloroethene 59) 2-Hexanone 60) 1,2-Dibromoethane 61) Chlorobenzene 62) 1,1,1,2-Tetrachloroethane 63) Ethylbenzene 64) m+p-Xylene 65) Isoamyl Acetate 66) o-Xylene 67) Styrene 68) Cumene 69) 4-Bromofluorobenzene 70) 1,1,2,2-Tetrachloroethane 71) 1,2,3-Trichloropropane 72} Pentach'loroethane 73) 1,3-Dichlorobenzene 74 1,4-Dichlorobenzene 75) l,2-Dichloroben2ene * Compound is ISTD R.T. Q ion 10.87 93.0 10.90 88.0 11.01 43.0 11.11 83.0 11.44 41.0 11.58 63.0 11.77 75.0 12.59 75.0 12.84 97.0 13.41 129.0 15.51 173.0 16.29 53.0 14.26 117.0 12.01 43.0 12.16 98.0 12.25 91.0 12.73 69.0 13.05 164.0 13.23 43.0 13.58 107.0 14.30 112.0 14.43 131.0 14.46 106.0 14.64 106.0 14.76 70.0 15.22 106.0 15.24 104.0 15.75 105.0 15.99 95.0 16.20 83.0 16.25 110.0 17.13 167.0 17.59 146.0 17.72 146.0 13.28 146.0 Area . 25646M 1570 34742 46108 14039 13748 37512 36359 21780 34404 21859 23474 123077 21920 53312 53926 30859 19663 13668 33941 43934 24070 18721 48673 22496 22970 40512 70373 40859 37095 9361 16217 30423 35960M 30448 Cone Units 21.24 UG/L 159.44 UG/L 21.55 UG/L 17.92 UG/L 35.08 UG/L 20.97 UG/L 18.43 UG/L 19.19 UG/L 20.12 UG/L 17.68 UG/L 16.95 UG/L 52.69 UG/L 50.00 UG/L 24.18 UG/L 20.26 UG/L 18.94 UG/L 21.53 UG/L 17.53 UG/L 25.44 UG/L 23.24 UG/L 18.98 UG/L 20.35 UG/L 18.73 UG/L 40.15 UG/L 20.88 UG/L 18.95 UG/L 18.69 UG/L 25.26 UG/L 20.96 UG/L 23.66 UG/L 22.36 UG/L 20.30 UG/L 21.34 UG/L 25.23 UG/L 21.10 UG/L q 83 95 97 96 87 86 89 92 99 97 87 85 91 98 96 90 98 98 95 84 89 96 96 94 93 85 96 73 95 67 87 86 86 86 137 DUP050308114 Data Pile: >IGKI2 Name: VSTD020 020 PPB IC Misc: -SJL @WL %C +JCEO =1 Quant Time: 960820 21:24 Injected at: 960820 20:59 Compound No: 15 Compound Name: Allyl Chloride Scan Number: 304 Retention Time: 5.29 min Quant Ion: 41.0 Area: 23129M Concentration: 20.54 UG/L q-value: o Quant Output File: AIGKI2 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 This report was produced by QAREA at: 12:06 AM WED., 21 AUG., 1996 a O O iOO DUP050308115 . --^ t/uhl Data File: >IGKI2 Name: VSTD020 020 PPB 1C Misc: -SJL @WL %C +}CEO *1 Quant Time: 960820 21:24 Injected at: 960820 20:59 Compound No: 41 Compound Name: Dibromomethane- Scan Number: 783 Retention Time: 10.87 min Quant Ion: 93.0 Area: . 25646K Concentration: 21.24 UG/L q-value: o Quant Output File: ~IGKI2 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 This report was produced by QAREA at: 12:07 AM WED., 21 AUG., 1996 136 DUP050308116 Name: VSTD020 020 PPB IC Wise: -SJL @WL %C +>CEO =1 Quant Time: 960820 21:24 Injected at: 960820 20:59 Instrument ID: HPQ3046 Quant ID Pile: IA6390 Last Calibration: 951122 10:44 Compound No: 74 Compound Name: 1,4-Dichlorobenzene Scan Number: 1372 Retention Time: 17.72 min Quant Ion: 146.0 Area: 35960M Concentration: 25.23 UG/L q-value: 86 This report was produced by QAREA at: 12:08 AM WED., 21 AUG., 1996 DUP050308117 Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HF0304S Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Operator ID: SJL-176 Quant Time : 960820 22:06 Injected at: 960820 21:41 141 DUP050308118 QUANT REPORT Page l Operator ID: SJL-176 Output File: *IGKI3::D7 Data File: >IGKI3::D9 Name: VSTD050 050 PPB IC Misc: ~SJL WL %C +J-CEO ' "1 Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960820 22:06 960820 21:41 1.00000 HP03046 ID File: 1A6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Compound 1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6} Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,1-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene 21) 1,1-Dichloroethane 22) cis-i,2-Dichloroethene 23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32} *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) Methyl Methacrylate R.T. Q ion 8.30 128.0 2.43 85.0 2.54 50.0 2.74 62.0 3.15 94.0 3.30 64.0 3.67 101.0 4.19 59.0 4.40 56.0 4.61 96.0 4.63 101.0 4.69 43.0 4.87 142.0 5.03 76.0 5.28 41.0 5.57 84.0 5.89 59.0 6.03 53.0 6.12 73.0 6.07 96.0 6.86 63.0 7.89 96.0 7.94 43.0 8.03 54.0 8.09 43.0 8.27 67.0 8.38 42.0 8.46 83.0 8.82 56.0 9.24 65.0 9.37 62.0 9.96 114.0 7.01 43.0 8.73 97.0 9.01 117.0 9.32 41.0 9.33 78.0 10.36 130.0 10.68 63.0 10.91 69.0 Area 41532 112891 41562 47096 49439 29955 37077 36034 27161 47778 1SS528 14228 120428 122468 60310M 59254 18312 52092 135406 55563 103174 55539 16797 17485 54830 33891 11529 120463 66811 88376 93746 173525 96530 91344 69021 13175 129773 60832 57035 38891 Cone Units 50.00 UG/L 58.41 UG/L 54.20 UG/L 49.60 UG/L 65.63 UG/L 60.17 UG/L 41.89 UG/L 79.89 UG/L 255.21 UG/L 43.14 UG/L 91.02 UG/L 46.91 UG/L 44.97 UG/L 41.86 UG/L 51.97 UG/L 47.73 UG/L 188.89 UG/L 274.91 UG/L 58.63 UG/L 43.75 UG/L 43.28 UG/L 43.73 UG/L 48.45 UG/L 254.40 UG/L 53.69 UG/L 129.97 UG/L 53.62 UG/L 41.06 UG/L 93.33 UG/L 48.82 UG/L 44.49 UG/L 50.00 UG/L 42.71 UG/L 40.25 UG/L 37.41 UG/L 518.97 UG/L 44.93 UG/L 43.05 UG/L 47.80 UG/L 53.66 Uci/JL <3 83 94 94 96 96 94 95 90 95 92 91 71 72 100 97 93 96 91 95 96 96 91 93 98 88 78 97 96 91 92 88 96 88 96 96 88 S3 88 82 14 DUP050308119 QUANT REPORT Page 2 Operator ID: SJL-176 output File: *IGKI3::D7 Data File: >IGKI3::D9 . Name: VSTD050 050 PPB IC Misc: -SJL WL %C +JCEO =1 Quant Rev: 7 Quant Time Injected at Dilution Factor Instrument ID 960820 22:06 960820 21:41 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time 960710 14:27 Compound 41) Dibromomathan 42) 1,4-Dioxane 43} n-Propyl Acetate 44) Bromoalchloromethane 45) 2-Nitropropane 46) 2-Chloroethyl Vinyl Ether 47) cis-1,3-Dichloropropene 48} trans-1,3-Dichloropropene 49) 1,1,2-Trichloroethane 50) Dibromochloromethane 51) Bromoform 52) trans-1,4-Dichloro-2-Butene 53) *Chlorobenzene-d5 54) 4-Methyl-2-Pentanone 55) Toluene-d8 56) Toluene 57) Ethyl Methacrylate 58) Tetrachloroethene 59) 2-Hexanone 60) 1,2-Dibromoethane 61) Chlorobenzene 62) 1,l,1,2-Tetrachloroethane 63) Ethylbenzene 64) m+p-Xylene 65) Isoamyl Acetate 66) o-Xylene 67) Styrene 68) Cumene 69) 4-Bromofluorobenzene 70) 1,1,2,2-Tetrachloroethane 71) 1,2,3-Trichloropropane 72) Pentachloroethane 73) l,3-Dichlorobenzene 74 1.4-Dichlorobenzene 75) 1,2-Dichlorobenzene * Compound is ISTD R.T. Q ion 10.87 93.0 10.92 88.0 11.01 43.0 11.13 83.0 11,45 41.0 11.59 63.0 11.79 75.0 12.59 75.0 12.86 97.0 13.43 129.0 15.52 173.0 16.30 53.0 14.27 117.0 12.01 43.0 12.17---98-. 0 12.27 91.0 12.74 69.0 13.06 164.0 13.23 43.0 13.58 107.0 14.32 112.0 14.43 131.0 14.48 106.0 14.66 106.0 14.78 70.0 15.24 106.0 15.25 104.0 15.77 105.0 16.00 95.0 16.22 83.0 16.28 110.0 17.15 167.0 17.61 146.0 17.74 146.0 18.29 146.0 Area Cone Units 64864M 3193 88195 120817 37353 35926 97877 94524 56066 93875 59543 61967 126822 55285 154866 148958 81697 50150 35542 88444 110317 61551 47174 123452 58957 59522 105823 177575 109132 93391 24007 41391 82195 92865M 77874 51.33 UG/L 309.83 UG/L 52.27 UG/L 44.86 UG/L 89.17 Uta/ Jj 52.35 UG/L 45.94 UG/ L 47.67 UG/L 49.48 UG/L 46.08 UG/L 44.12 UG/L 132.89 UG/L 50.00 UG/L 59.19 UG/L 52.21 UG/L 46.46 UG/L 55.33 UG/L 43.33 l 64.20 UG/L 58.77 UG/L 46.26 UG/L 50.50 UG/L 45.80 UG/L 98.84 U^i/ L 53.10 UG/L 47.65 UG/L 47.38 UG/L 61.86 UG/L 54.34 UG/L 57.80 UG/L 55.66 UG/L 50.29 UG/L 55.96 UG/L 63.22 UG/L 52.37 UG/L q 74 97 96 96 88 87 90 95 97 98 89 86 89 98 97 96 97 97 94 85 90 95 95 95 93 84 96 74 93 65 84 86 86 85 14 DUP050308120 Data File: >IGKI3 Name: VSTD050 050 PPB IC Misc: ~SJL @WL %C +>CEO =1 Quant Time: 960820 22:06 Injected at: 960820 21:41 Compound No: 15 Compound Name: Allyl Chloride Scan Number: 296 Retention Time: 5.28 min Quant Ion: 41.0 Area: 60310M Concentration: 51.97 UG/L q-value: 0 Quant Output File: -IGKI3 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 This report was produced by QAREA at: 12:13 AM WED., 21 AUG., 1996 144 DUP050308121 Data File: >IGKI3 Name: VSTD050 050 FFB IC Misc: -SJL @WL %C +>CEO =1 Quant Time: 960S20 22:06 Injected at: 960820 21:41 Quant output File: ~IGKI3 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 Compound No: 41 Compound Name: Dibromomethane Scan Number: 773 Retention Time: 10.87 min Quant Ion: 93.0 Area: 64864M Concentration: 51.33 UG/L q-value: 0 This report was produced by QAREA at: 12:14 AM WED., 21 AUG., 1996 145 DUP050308122 Data File: >IGKI3 Name: VSTD050 050 PPB IC Misc: -SJL WL %C +}CEO =1 Quant Time: 960820 22:06 Injected at: 960820 21:41 Compound No: 74 Compound Name: 1,4-Dichlorobenzene Scan Number: 1363 Retention Time: 17.74 min Quant Ion:.146.0 Area: 92865M Concentration: 63.22 UG/L q-value: 86 Quant Output File: ~IGKI3 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 This report was produced by QAREA at: 12:15 AM WED., 21 AUG., 1996 i46 DUP050308123 Data Pile: >IGKI4::D9 Name: VSTD100 100 PPB IC Misc: ~SJL @WL %C +JCEO 1 Quant Output File: *'IGKI4::D7 Instrument ID: KP03Q46 Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Operator ID: SJL-176 Quant Time : 960820 22:40 Injected at: 960820 22:15 147 DUP050308124 QUANT REPORT Page l Operator ID: SJL-176 Output Pile: *IGKI4::D7 Data Pile: >IGKI4::D9 Name: VSTD100 100 PPB IC Misc: -SJL eWL %C +JCEO =1 Quant Rev: 7 Quant Time Injected at Dilution Factor Instrument ID 960820 22:40 960820 22:15 1 00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Compound 1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,1-Dichloroethene ID Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl chloride 16) Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene 21) 1,l-Dichloroethane 22) cis-1,2-Dichloroethene 23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) Methyl Methacrylate R.T. Q ion 8.29 128.0 2.42 85.0 2.57 50.0 2.75 62.0 3.15 94.0 3.31 64.0 3.69 101.0 4.19 59.0 4.41 56.0 4.61 96.0 4.64 101.0 4.70 43.0 4.88 142.0 5.03 76.0 5.30 41.0 5.56--84.0 5.90 59.0 6.03 53.0 6.12 73.0 6.08 96.0 6.86 63.0 7.89 96.0 7.94 43.0 8.02 54.0 8.08 43.0 8.28 67.0 8.38 42.0 8.45 83.0 8.82 56.0 9.24 65 ;0 9.36 62.0 9.96 114.0 7.01 43.0 8.73 97.0 9.00 117.0 9.31 41.0 9.32 78.0 10.35 130.0 10.69 63.0 10.91 69.0 Area Cone Units q 41622 50.-00 UG/L 242456 125.18 UG/L 94245 122.63 UG/L 102406 107.61 UG/L 100293 132.86 UG/L 62102 124.47 UG/L 77955 87.89 UG/L 72675 160.78 UG/L 61799 579.42 UG/L 93948 89.14 UG/L 407263 196.20 UG/L 31137 102.43 UG/L 263039 98.01 UG/L 280107 95.53 OG/L 128700M 110.66 UG/L 11563-4 92.95 UG/L 46120 474.70 UG/L 109431 576.26 UG/L 271132 117.14 UG/L 111234 87.39 UG/L 218346 91.39 UG/L 116354 91.41 UG/L 37628 108.30 UG/L 39595 574.85 UG/L 119853 117.11 UG/L 73821 282.48 UG/L 26204 121.61 UG/L 249991 85.03 UG/L 141736 197.57 UG/L 176412 97.25 UG/L 191367 90.63 UG/L 173227 50.00 .UG/L 201812 89.45 UG/L 191196 84.39 UG/L 145439 78.96 UG/L 33623 1326.71 UG/L 274003 95.03 UG/L 127424 90.33 UG/L 120011 100.75 UG/L 81933 113.24 UG/L 84 98 98 97 95 93 93 86 99 90 92 69 72 100 97 98 96 89 92 96 97 89 97 99 86 76 98 95 89 91 87 95 88 97 93 90 85 88 81 148 ;:r -ti-'-v."-. DUP050308125 QUANT REPORT Page 2 Operator ID; SJL-176 Output File: AIGKI4::D7 Data File: >IGKI4::D9 - Name; VSTD100 100 PPB IC Misc: -SJL 6WL %C +JCEO =1 Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960820 22:40 960820 22:15 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Compound 41) Dibroraoraethane 42) 1,4-Dioxane 43) n-Propyl Acetate 44) Bromodichloromethane 45) 2-Nitropropane 46) 2-Chloroethyl Vinyl Ether 47) cis-1,3-Dichloropropene 48) trans-1,3-Dichloropropene 49) 1,1,2-Trichloroethane 50) Dibromochloromethane 51) Bromoform 52) trans-l,4-Dichloro-2-Butene 53) *Chlorobenzene-d5 54) 4-Methy1-2-Pentanone 55) Toluene-d8 56) Toluene 57) Ethyl Methacrylate 58) Tetrachloroethene 59) 2-Hexanone 60) 1,2-Dibromoethane 61) Chlorobenzene 62) 1,1,1*2-Tetrachloroethene 63) Ethylbenzene 64) m+p-Xylene 65) Isoamyl Acetate 66) o-Xylene 67) Styrene 68) Cumene 69) 4-Bromofluorobenzene 70) l, 1,2,2-Tetrachloroethane 71) 1,2,3-Trichloropropane 72) Pentachloroethane 73) 1,3-Dichlorobenzene 74) 1,4-Dichlorobenzene 75) 1,2-Dichlorobenzene * Compound is ISTD R.T. Q ion 10.86 93.0 10.92 88.0 11.00 43.0 11.12 83.0 11.44 41.0 11.58 63.0 11.78 75.0 12.59 75.0 12.85 97.0 13.43 129.0 15.51 173.0 16.29 53.0 14.26 117.0 12.01 43.0 12.17 98.0 12.26 91.0 12.74 69.0 13.06 164.0 13.23 43.0 13.58 107.0 14.31 112.0 14.43 131.0 14.47 106.0 14.65 106.0 14.76 70.0 15.22 106.0 15.24 104.0 15.77 105.0 15.99 95.0 16.20 83.0 16.26 110.0 17.13 167.0 17.60 146.0 17.73 146.0 18.29 146.0 Area Cone Units 131345M 9289 193973 256625 88531 73565 207262 201620 114338 196123 129391 137372 124656 120424 307471 315640 174698 102887 81801 182978 232932 124372 97554 249994 126590 118124 223314 359813 216351 194470 47988 80235 163998 185253M 145458 104.13 UG/L 902.89 UG/L 115.16 UG/L 95.45 UG/L 211.72 UG/L 114.67 UG/L 97.45 UG/L 101.86 UG/L 101.08 UG/L 96.44 UG/L 96.05 UG/L 295.11 UG/L 50.00 UG/L 131.16 UG/L 105.4-6 UG/L 100.17 UG/L 120.37 UG/L 90.55 UG/L 150.31 UG/L 123.69 UG/L 99.37 UG/L 103.81 UG/L 96.37 UG/L 203.63 UG/L 115.99 UG/L 96.22 UG/L 101.73 UG/L 127.52 UG/L 109.55 UG/L 122.44 UG/L 113.19 UG/L 99.18 UG/L 113.58 UG/L 128.30 UG/L 99.53 UG/L <3 66 97 96 94 86 86 91 92 98 98 86 84 89 96 99 94 96 94 93 86 91 94 95 94 93 84 95 72 93 65 87 86 86 85 149 DUP050308126 Data File: >IGKI4 Name: VSTD100 100 PPB IC Misc: ~SJL @WL %C +>CEO . =1 Quant Time: 960820 22:40 Injected at: 960820 22:15 Comoound No: 15 Compound Name: Allyl Chloride Scan Number: 305 Retention Time: 5.30 min Quant Ion: 41.0 Area: 128700M Concentration: 110.66 UG/L q-value: 0 This report was produced by QAREA Quant Output File: ~IGKI4 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 : 12:20 AM WED., 21 AUG., 1996 I5( DUP050308127 Data File: >IGKI4 Name: VSTD100 100 PPB IC Kisc: ~SJL @WL %C +}CEO =1 Quant Time: 960820 22:40 Injected at: 960820 22:15 Compound No: 41 Compound Name: Dibromomethane Scan Number: 783 Retention Time: 10.86 min Quant Ion: 93.0 Area: 131345M concentration: 104.13 UG/L q-value: 0 Quant Output File: AIGKI4 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 This report was produced by QAREA at: 12:21AM WED., 21 AUG., 1996 151 4 DUP050308128 Data File: >IGKI4 Name: VSTD100 100 PPB IC Kiso: -SJL @WL %C +}CEO =1 Quant Time: 960820 22:40 Injected at: 960820 22:15 Quant output File: AIGKI4 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 Compound No: 74 Compound Name: 1,4-Dichlorobenzene Scan Number: 1372 Retention Time: 17.73 min Quant Ion: 146.0 Area: 185253M Concentration: 128.30 UG/L q-value: 86 This report was produced by QAREA at: 12:22 AM WED., 21 AUG., 1996 15S DUP050308129 Data File: >IGKI5::D9 Name: VSTD200 200 PPB IC Misc: -SJL @WL %C +>CEO =1 Quant Output File: AIGKI5::D7 Instrument ID: HP03046 Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Operator ID: SJL-176 Quant Time : 960820 23:10 Injected at: 960820 22:46 15 DUP050308130 QUANT REPORT Operator ID: SJL-176 Output File: *IGKI5::D7 Data File: >IGKI5::D9 Name: VSTD200 200 PPB IC Misc: -SJL @WL %C +>CEO =1 Quant Rev: 7 Quant Time Injected at Dilution Factor Instrument ID Tn XA39Q:?DB Title* 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time Page i 960820 23:10 960820 22:46 1.00000 HP03046 960710 14:27 Compound 1) *Broraochloromethane 2) Dichlorodifluoromethane 3} Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) i,i-Dichloroethene 11} Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Ally! Chloride 16) Methylene Chloride 17} t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-l,2-Dichloroethene 21) 1,l-Dichloroethane 22} cis-l,2-Dichloroethane 23) 2-Butanone 24} Propionitrile 25) Ethyl Acetate 26} Methacrylonitrile 27) Tetrahydrofuran 28} Chloroform 2 9) Cyclohexane 30) l,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *i,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1/l-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) Methyl Methacrylate R.T. Q ion 8.30 128.0 2.42 85.0 2.58 50.0 2.76 62.0 3.16 94.0 3.29 64.0 3.70 101.0 4.19 59.0 4.41 56.0 4.61 96.0 4.65 101.0 4.72 43.0 4.88 142.0 5.04 76.0 5.30 41.0 5.5S --84.0 5.92 59.0 6.05 53.0 6.14 73.0 6.09 96.0 6.86 63.0 7.90 96.0 7.95 43.0 8.04 54.0 8.09 43.0 8.30 67.0 8.39 42.0 8.46 83.0 8.82 56.0 9.26 65.0 9.37 62.0 9.97 114.0 7.02 43.0 8.74 97.0 9.01 117.0 9.33 41.0 9.34 78.0 10.36 130.0 10.69 63.0 10.91 69.0 Area Cone Units 42601 50.00 UG/L 470730 237.46 UG/L 186279 236.82 UG/L 199740 205.06 UG/L 172150 222.81 UG/L 117100 229.30 UG/L 149368 164.54 UG/L 142425 307.85 UG/L 129868 1189.64 UG/L 193800 170.58 UG/L 756199 355.94 UG/L 62169 199.81 UG/L 516675 188.08 UG/L 558579 186.12 UG/L 275131M 231.13 UG/L 228287 179.28 -UG/L 97179 977.26 UG/L 234538 1206.68 UG/L 545201 230.14 UG/L 221303 169.87 UG/L 442580 180.99 UG/L 234471 179.97 UG/L 76460 215.01 UG/L 85986 1219.69 UG/L 249570 238.25 UG/L 149163 557.66 UG/L 56031 254.06 UG/L 507178 168.55 UG/L 280048 381.40 UG/L 364600 196.36 UG/L 391115 180.97 UG/L 178956 50.00 UG/L 426096 182.81 UG/L 372078 158.96 UG/L 293856 154.43 UG/L 69559 2656.82 UG/L 538592 180.81 UG/L 248933 170.82 UG/L 250372 203.45 UG/L 168682 225.67 UG/L q 81 96 95 98 99 93 97 87 97 91 91 71 72 100 97 99 96 85 91 97 96 39 94 99 84 76 97 95 89 91 87 95 88 97 95 89 84 88 80 154 DUP050308131 QUANT REPORT Page 2 Operator ID: SJL-176 Output Pile: AIGKI5::D7 Data File: >IGKI5::D9 Name: VSTD20Q 200 PPB IC Misc: -SJL WL %C +>CEO =1 Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960820 23:10 960820 22:46 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960710 14:27 Compound 41) Dibromomethane 42) 1,4-Dioxane 43) n-Propyl Acetate 44) Bromodichloromethane 45) 2-Nitroprofcane 46) 2-Chloroethyl Vinyl Ether 47) cis-1,3-Dichloropropene 48) trans-1,3-Dichloropropene 49) 1,1,2-Trichloroethane 50) Dibromochloromethane 51) Bromoform 52) trans-l, 4-Dich.loro-2-Butene 53) *Chlorobenzene-d5 54) 4-Methyl-2-Pentanone 55) Toluene-ds 56) Toluene 57) Ethyl Methacrylate 58) Tetrachloroethehe 59) 2-Hexanone 60) 1,2-Dibromoethane 61) Chlorobenz ene 62) 1,1,1,2-Tetrachloroethane 63) Ethylbenzene 64) m+p-Xylene 65) Isoamyl Acetate 66) o-Xylene 67) Styrene 68) Cumene 69) 4-Bromofluorobenzene 70) 1,1,2,2-Tetrachloroethane 71) 1,2,3-Trichloropropane 72) Pantachloroethane 73) 1,3-Dichlorobenzene 74) 1,4-Dichlorobenzene 75) 1,2-Dichlorobenzene * Compound is ISTD R. II!1 * Q ion 10.86 93.0 10.92 88.0 11.02 43.0 11.13 83.0 11.46 41.0 11.59 63.0 11.78 75.0 12.59 75.0 12.86 97.0 13.43 129.0 15.52 173.0 16.29 53.0 14.27 117.0 12.02 43.0 12.17---98*0 12.26 91.0 12.74 69.0 13.07 164.0 13.23 43.0 13.58 107.0 14.31 112.0 14.43 131.0 14.48 106.0 14.64 106.0 14.78 70.0 15.23 106.0 15.25 104.0 15.76 105.0 16.00 95.0 16.21 83.0 16.27 110.0 17.14 167.0 17.60 146.0 17.73 146.0 18.29 146.0 Area Cone Units 270106M 207.28 UG/L 18835 1772.15 UG/L 401227 230.57 UG/L 525565 189.21 UG/L 187575 434.22 UG/L 165647 234.03 UG/L 423549 192.77 UG/L 413415 202.17 UG/L 233252 199.59 UG/L 398863 189.85 UG/L 267090 191.92 UG/L 278169 578.45 UG/L 126057 50.00 UG/L 245535 264.46 UG/L 633073 214-.7-2 UG/L 626588 196.64 UG/L 362606 247.06 UG/L 198722 172.94 UG/L 168438 306.08 UG/L 375779 251.20 UG/L 467820 197.36 UG/L 247253 204.07 UG/L 185863 181.56 UG/L 475823 383.26 UG/L 259938 235.53 UG/L 228534 184.03 UG/L 435280 196.09 UG/L 722381 253.18 UG/L 441866 221.26 UG/L 384770 239.57 UG/L 95237 222.13 UG/L 159152 194.53 UG/L 322133 220.63 UG/L 368459M 252.36 UG/L 283526 191.84 UG/L q 71 97 96 94 87 87 90 94 99 99 88 81 89 96 99 91 98 94 93 86 91 93 97 91 91 84 95 70 94 61 85 86 86 84 15 5 DUP0 50308132 Data File: >IGKI5 Name: VSTD20Q 200 PFB IC Misc: -SJL @WL %C +>CEO =1 Quant Time: 960820 23:10 Injected at: 960820 22:46 Quant Output File: AIGKI5 Instrument ID: HPQ3046 Quant ID File: IA639G Last Calibration: 951122 10:44 Compound No: 15 Compound Name: Allyl Chloride Scan Number: 304 Retention Time: 5-30 min Quant Ion: 41.0 Area: 275131M Concentration: 231.13 UG/L q-value: 0 This report was produced by QAREA at: 12:26 AM WED., 21 AUG., 1996 15b DUP050308133 Data File: >IGKI5 Name: VSTD200 200 PPB XC Misc: -SJL @WL %C +}CEO =1 Quant Time: 960820 23:10 Injected at: 960S20 22:46 Quant Output File: ~IGKI5 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 Compound No: 41 Compound Name: Dibromomethane Scan Number: 781 Retention Time: 10.86 min Quant Ion: 93.0 Area: 270106M Concentration: 207.28 UG/L q-value: 0 This report was produced by QAKEA at: 12:27 AM WED., 21 AUG., 1996 157 DUP050308134 Data File: >IGKI5 Name: VSTD200 200 PPB IC Misc: -SJL @WL %C +JCEO =1 Quant Time: 960820 23:10 Injected at: 960820 22:46 Compound No: 74 Compound Name: 1,4-Dichlorobenzene Scan Number: 1369 Retention Time: 17.73 min Quant Ion: 146.0 Area: 368459M Concentration: 252.36 UG/L q-value: 86 Quant Output File: -'IGKI5 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 TUi 5 This report was produced by QAREA at: 1:43 PM WED., 21 AUG., 1996 DUP050308135 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: LANCASTER: LABS Contract: _____ Lab Code: LANCAS Case No.: _______ . SAS No. _______. SDG No.: _______ Instrument ID: HP03046 Calibration Date(s): 09/24/96 09/24/96 Heated Purge: (Y/N) N Calibration Times: 1135 1356 GC Column: DB624 LAB FILE ID: RRF 50= >ISOI3 ID: 0.53 (mm) RRF 10= >IS0I1 RRF100= >IS0I4 RRF 20= >ISOI2 RRF200= >I3015 COMPOUND RRF 10 RRF 20 RRF 50 RRF100 RRF200 RRF Dichlorodifluoromethane 2.728 Chloromethane .920 Vinyl Chloride ** 1.071 Bromomethane ** 1.150 Chloroethane .739 Trichlorofluoromethane 1.203 Ethyl Ether .972 Acrolein .204 1,1-Dichloroethene * 1.153 Freon 113 2.462 Acetone .443 Methyl Iodide 4.338 Carbon Disulfide 3.105 Allyl Chloride 1.777 Methylene Chloride 1.421 t-Butyl Alcohol .120 Aerylonitrile .282 Methyl t-Butyl Ether 3.635 1,2-Dichloroethene (total) 1.408 1,1-Dichloroethane * 2.457 2-Butanone .376 Propionitrile .079 Ethyl Acetate 1.393 Methacrylonitrile .405 Tetrahydrofuran .312 Chloroform * 3.150 cyclohexane 1.623 1,2-Dichloroethane * 2.313 Vinyl Acetate .793 1,1,1-Trichloroethane * .631 Carbon Tetrachloride * .522 Isobutyl Alcohol i .007 Benzene * .900 2.147 .788 .799 .864 .548 1.309 .780 .172 .88 6 1.787 .394 3.434 2.428 1.375 1.094 .118 .241 3.244 1.109 1.902 .319 .076 1.435 .350 .325 2.531 1.288 1.982 .754 .547 .462 .007 .724 2.717 .961 1.083 .996 .619 1.463 .868 .176 1.098 2.277 .411 4.169 3.035 1.791 1.253 .112 .258 3.216 1.339 2.345 .402 .099 1.509 .371 .245 2.929 1.596 2.174 .736 .601 .544 .007 .787 2.669 .926 1.091 .980 .551 1.477 .865 .184 1.113 2.236 .423 4.232 3.138 1.806 1.291 .130 .293 3.172 1.355 2 401 .463 .105 1.477 .374 .306 2.951 1.581 2.196 .805 .634 .553 .009 .827 2.418 .859 1.017 .858 .423 1.328 .843 .187 1.076 2.156 . 426 4.028 3.049 1.802 1.202 .143 .292 2.971 1.300 2.371 .492 .107 1.480 .365 .325 2.925 1.616 2.191 .823 .586 .550 .009 .768 2.536 .891 1.012 .970 .576 1.356 .866 .185 1.065 2.183 .419 4.040 2.951 1.710 1.252 .125 .273 3.248 1.302 2.295 .410 .093 1.459 .373 .302 2.897 1.541 2.171 .782 .600 .526 .008 .801 * Compounds with required minimum RRF and maximum %RSD values. All other compounds in OLM01.8 must meet a minimum RRF of 0.010. % RSD 9.9 7.7 12.1* 12.3* 20.0 8.4 8.0 6.7 9.8* 11.4 4.4 8.8 10.0 11.0 9.6 9.6 8.3 7.4 8.8 9.8* 16.8 15.7 3.1 5.3 11.0 7.8* 9.2 1 5.5* 4.6 I 6.0* 7.2* 13.4 1 8.3* 1 page 1 Of 2 FORM VI VOA QLM03.0 i5S DUP050308136 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: LANCASTER LABS Contract: _______. Lab Code: LANCAS Case No.: _______ . SAS No. _______. SDG No.: _______ . Instrument ID: HP03046 Calibration Date(s): 09/24/96 09/24/96 Heated Purge: (Y/N) N Calibration Times: 1135 1356 GC Column: DB624 ID: 0.53 (mm) woo too II II VV i>aW PnH LAB FILE Id : RRF 50= >ISOI3 ' RRF 10= ">18011----------- -------ERF RRF100== >ISOI4 er f ; 3012--------------------3015 COMPOUND RRF 10 RRF 20 RRF 50 RRF100 RRF200 Trichloroethene : r .430 1,2-Dichloropropane .375 1,4-Dioxane .002 n-Propyl Acetate Bromodichloromethane .552 ik .817 2-Chloroethy1 Vinyl Ether cis-1,3-Dichloropropens * trans-1,3-Dichloropropene * * 1,1,2-Trichloroethane * Dibromochloromethane * Bromoform k .255 .642 .614 .410 .756 .587 trans-1.4-Dichloro-2-Butene .168 4-Methyl-2-Pentanone Toluene Tetrachloroethene .490 J 1.337 5t .484 2-Hexanone .276 1,2-Dibromoethane Chlorobenz ene Ethylbenzene .827 3k 1.027 * .440 Xylene (total) * .547 Isoamyl Acetate Styrene .560 * 1.011 Cumene 1,1,2,2-Tetrachloroethane 1 1.530 .937 1,2,3-Trichloropropane .238 1,3-Dichlorobenzene .804 1,4-Dichlorobenzene .974 1,2-Dichlorobenzene .842 .352 .318 .003 .502 .718 .245 .554 .546 .359 .669 .533 .159 .479 1.061 .386 .267 .728 .837 .359 .441 .500 .798 1.246 .828 .207 .637 .751 .684 .404 .336 .003 .543 .746 .237 .591 .550 .352 .683 .547 .159 .461 1.210 .452 .286 .724 .929 .407 .498 .487 .899 1.456 .788 .203 .777 .870 .776 .423 .352 .004 .587 .770 .248 .617 .577 .359 .689 .552 .169 .473 1.322 .481 .314 .757 .963 .426 .513 .510 .920 1.436 .830 .203 .764 .898 .768 .394 .351 . 003 .588 .754 .247 .577 . 556 .357 .690 .557 .160 .480 1.180 .438 .325 .721 .933 .394 .460 .491 .881 1.407 .763 .190 .739 .863 .726 RRF .401 .346 .003 .554 .761 .246 .596 .569 .367 .697 .555 .163 .477 1.222 .448 .294 .751 .938 .405 .492 .510 .902 1.415 .829 .208 .744 .871 .759 % RSD 7.7* 6.2 I 16.5 6.4 | 4.8* 2.5 j 5.7* 4.9* 6.6* 4.8* 3.6* 3.0 | 2.3 j 9.3* 8.9* 8.5 6.0 7.3* 7.7* 8.6* 5.8 j 8.5* 7.4 [ 8.0* 8.6 8.6 9.2 7.8 1,2-Dichloroethane-d4 1.982 1.909 1.933 1.989 1.939 1.951 Toluene-d8 4-Bromofluorobenzene 1.204 1.184 1.140 1.206 1.153 1.177 * .958 .942 .927 .969 .939 .947 L == Compounds with required minimum RRF andmaximum %RSD values All other compounds in OLM01.8 must meet a minimum RRF of 0.010. 1.7 2.5 1.7* 1 page 2 of 2 FORM VI VOA OLM03.0 DUP050308137 TOTAL ION CHROMATOGRAM File > I SOI! 35.0-300.0 Jt_I__L. JL--I_X4. 00 emu. VSTDQ1Q TIC > -80iQ ' 6lO PPB * > IC~TLN 0ML 1..2I0,,,0r__ * 1 5C *1 +>CEC -I__t1_6_I0_0L. 260000- 240000 220000 200000 180000- 160000 140000 120000100000- 80000 60000 40000 2000O Data File: >IS0I1::D9 Name: VSTD010 010 PPB IC Misc: -TLN WL %C =1 +>CEO-V Quant Output File: AISOIl::D7 Instrument ID: HPG3046 Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLN-262 Quant Time : 960924 13:08 Injected at: 960924 11:35 160 DUP050308138 QUANT REPORT Page 1 Operator ID: TLN-262 Output File: ''ISOIl: :D7 Data File: >ISOIl::D9 Name: VSTD010 010 PPB Ic Misc: -TEN @WL %C =1 +JCEO-V Quant Rev: 7 Quant Time Injected at Dilution Factor Instrument ID 960924 13:08 960924 11:35 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,l-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene Chloride 17} t-Butyl Alcohol 18) Aerylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene 21) 1,1-Dichloroethane 22) cis-l,2-Dichloroethene 23) 2-Butanone 24) Propionitrile A 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) l,2-Dichloroethane-d4 A 31) 1,2-Diehloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,1-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene A 38) Trichloroethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane R.T. Q ion 8.18 128.0 2.28 85.0 2.43 50.0 2.61 62.0 3.04 94.0 3.19 64.0 3.58 101.0 4.07 59.0 4.28 56.0 4.46 96.0 4.53 101.0 4.60 43.0 4.73 142.0 4.85 76.0 5.18 41.0 5.44 84.0 5.80 59.0 5.94 53.0 6.01 73.0 5.96 96.0 6.75 63.0 7.79 96.0 7.87 43.0 7.94 54.0 7.98 43.0 8.18 67.0 8.26 42.0 8.35 83.0 8.70 56.0 9.13 65.0 9.24 62.0 9.84 114.0 6.91 43.0 8.61 97.0 8.88 117.0 9.21 41.0 9.20 78.0 10.23 130.0 10.56 63.0 10.83 88.0 Area 35514 19378 6537 7605 8168 5246 8547 6906 7247 8190 34974 3150M 30815 22054 12621M 10091 4275 10002 25820 9646 17455 10355 2672M 2819 9893 7186 2216 22374 11525 14078 16428 136903 21705 17272 14287 2422 24641 11779 10279 814 Cone Units 50.00 UG/L 10.04 UG/L 11.93 UG/L 11.26 UG/L 11.01 UG/L 11.79 UG/L 13.48 UG/L 11.21 UG/L 78.01 UG/L 11.39 UG/L 21.69 UG/L 13.66 UG/L 14.96 UG/L 17.56 UG/L 12.24 UG/L 11.63 UG/L 68.25 UG/L 56.14 UG/L 11.15 UG/L 10.87 UG/L 10.10 UG/L 11.67 UG/L 9.55 UG/L 47.14 UG/L 10.55 UG/L 31.00 UG/L 11.24 UG/L 9.93 UG/L 10.09 UG/L 8.60 UG/L 9.52 UG/L 50.00 UG/L 14.25 UG/L 10.54 UG/L 10.25 UG/L 145.63 UG/L 12.36 UG/L 12.06 UG/L 11.71 UG/L 201.96 UG/L q 96 99 98 99 90 94 93 86 93 96 97 83 71 100 94 87 97 90 96 97 90 92 93 88 94 91 96 91 90 93 88 98 90 98 88 91 90 90 90 161 A DUP050308139 QUANT REPORT Page 2 Operator ID: TLN-262 Output File: AXSOXl::D7 . Data File: >ISOIl::D9 Name: VSTD010 010 PPB IC Wise: ~TLN @WL %C -1 +}CEO-V Quant Rev: 7 Quant Time Injected at Dilution Factor instrument ID 960924 13:08 960924 11:35 1.00000 HP03046 ID File: IA6390: :DEi Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-1,3-Dichloropropene 45) trans-l,3-Dichloropropene 46) 1,1,2-Trichloroethane 47) Dibromochloromethane 48) Bromoform 49) trans-l,4-Dichloro-2-Butene 50) *Chlorobenzene-d5 51) 4-Methyl-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hexanone 56) 1,2-Dibromoethane 57) Chlorobenzene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) Styrene 63) Cumene 64) 4-Bromofluorobenzene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) 1,3-Dichlorobenz ene 68) 1,4-Dichlorobenzene 69) 1,2-Dichlorobenzene * Compound is ISTD R.T. Q ion 10.90 43.0 11.00 83.0 11.48 63.0 11.68 75.0 12.49 75.0 12.75 97.0 13.32 129.0 15.42 173.0 16.20 53.0 14.16 117.0 11.92 43.0 12.06 98.0 12.16 91.0 12.96 164.0 13.15 43.0 13.48 107.0 14.20 112.0 14.37 106.0 14.54 106.0 14.68 70.0 15.13 106.0 15.15 104.0 15.66 105.0 15.89 95.0 16.12 83.0 16.17 110.0 17.50 146.0 17.63 146.0 18.19 146.0 Area 15106 22376 6971 17566 17483 11238 20693 16060 11479 104864 10287 25248 28038 10155 5780 17345 21535 9231 23622 11745 11475 21194 32087 20082 19656 4982 16852 20424 17660 cone Units 10.85 UG/L 10.83 UG/L 12.3 0 UG/L 11.38 UG/L 11.78 UG/L 12.49 UG/L 12.90 UG/L 14.93 UG/L 29.35 UG/L 50.00 UG/L 11.91 UG/L 10.16 UG/L 11.38 UG/L 11.85 UG/L 11.59r-UG/L 11.86 UG/L 11.41 UG/L 11.45 UG/L 23.58 UG/L 12.05 UG/L 11.46 UG/L 11.90 UG/L 10.93 UG/L 11.57 UG/L 12.80 UG/L 12.55 UG/L 12.40 UG/L 13.30 UG/L 13.71 UG/L q 95 95 92 87 91 95 98 95 91 86 91 97 95 97 89 94 87 96 96 94 91 84 96 81 98 67 90 91 86 16 2 DUP050308140 5^ Data File: >IS0I1 Name: VSTD010 010 PPB IC Misc: **TLN @WL %C =1 +JCEO-V Quant Time: 960924 13:08 Injected at: 960924 11:35 Quant Output File: ''ISOU Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 compound No: 12 Compound Name: Acetone Scan Number: 239 Retention Time: 4.60 min A Quant Ion: 43.0 Area: 3150M Concentration: 13.66 UG/L q-value: 83 This report was produced by QAREA at: 3:23 PM TUE., 24 SEPT, 1996 16 DUP050308141 S3rL Data File: >ISOXl Name: VSTD010 010 PPB IC Misc: -TLN WL %C =1 +J-CEO-V Quant Time: 960924 13:08 Injected at: 960924 11:35 Compound No: 15 Compound Name: Allyl Chloride Scan Number: 289 Retention Time: 5.18 min Quant Ion: 41.0 Area: 1262161 Concentration: 12.24 UG/L q-value: 0 Quant Output File: AISOIl Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 This report was produced by QAREA at: 3:24 PM TUE., 24 SEPT, 1996 164 DUP050308142 A Data File: >IS0I1 Name: VSTD010 010 PPB IC Misc: ~TLN @WL %C -1 +>CEO-V Quant Time: 960924 13:08 Injected at: 960924 11:35 Quant Output File: AIS0Ii Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 Compound No: 23 Compound Name: 2-Butanone Scan Number: 520 Retention Time: 7.87 min Quant Ion: 43.0 Area: 2672M concentration: 9.55 UG/L q-value: 92 This report was produced by QAREA at: 3:25 PM TUE., 24 SEPT, 1996 105 DUP050308143 TOTAL ION CHROMATOGRAM Data File: >ISOI2::D9 Name: VSTD020 020 PPB IC Misc: ~TLN @WL %C =1 +JCEO-V Quant Output File: -ISOI2: :D7 Instrument ID: HP03046 Id File: IA639Q::DB Title; 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TIN-262 Quant Time : 960924 13:17 Injected at: 960924 12:08 166 DUP050308144 QUANT REPORT Page 1 Operator ID: TLN-262 Output File: ''ISOI2::D7 Data File: >ISOI2::D9 Name: VSTD02Q 020 FPB IC Misc: ~TLN @WL %C ==1 +>CEO-V Quant Rev: 7 Quant Time Injected at Dilution Factor Instrument ID 960924 13:17 960924 12:08 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Sromomethane 6) Chloroethane 7} Trichlorofluoromethane 8} Ethyl Ether 9} Acrolein 10) 1,l-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-l,2-Dichloroethene 21) 1,1-Dichloroethane 22) cis-1,2-Dichloroethene 23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,1-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane Q ion 8.19 128.0 2.29 85.0 2.44 50.0 2.62 62.0 3.06 94.0 3.21 64.0 3.58 101.0 4.10 59.0 4.32 56.0 4.47 96.0 4.54 101.0 4.62 43.0 4.74 142.0 4.85 76.0 5.19 41.0 5.46 -84.0 5.80 59.0 5.95 53.0 6.02 73.0 5.98 96.0 6.76 63.0 7.81 96.0 7.88 43.0 7.95 54.0 8.00 43.0 8.18 67.0 8.29 42.0 8.36 83.0 8.70 56.0 9.13 65.0 9.26 62.0 9.84 114.0 6.92 43.0 8.63 97.0 8.89 117.0 9.22 41.0 9.21 78.0 10.23 130.0 10.56 63.0 10.79 88.0 Area 25596 21981 8066 8184 8849 5613 13404 7982 8804 9068 36585 4033M 35155M 24860 14081M 11202 6018 12339 33212 10851 19471 11844 3262 3872 14692 8968 3327 25912 13183 19544 20293 95328 28753 20875 17629 3274 27594 13416 12114 1391 Cone Units 50.00 UG/L 15.80 UG/L 20.42 UG/L 16.81 UG/L 16.56 UG/L 17.50 UG/L 29.33 UG/L 17.97 UG/L 131.49 UG/L 17.49 UG/L 31.49 UG/L 24.26 UG/L 23.68 UG/L 27.46 UG/L 18.94 UG/L 17.91 UG/L 133.31 UG/L 96.09 UG/L 19.90 UG/L 16.97 UG/L 15.63 UG/L 18.52 UG/L 16.18 UG/L 89.83 UG/L 21.74 UG/L 53.67 UG/L 23.41 UG/L 15.95 UG/L 16.01 UG/L 16.57 UG/L 16.31 UG/L 50.00 UG/L 27.11 UG/L 18.30 UG/L 18.16 UG/L 282.72 UG/L 19.87 UG/L 19.72 UG/L 19.82 UG/L 495.62 UG/L q 98 91 98 97 98 91 99 85 97 96 96 99 100 92 93 98 91 96 96 96 97 87 93 90 71 98 93 89 92 88 97 89 97 98 87 89 90 92 167 DUP050308145 QUANT REPORT Page 2 Operator ID: TLN-262 Output File: ~ISOI2::D7 Data File: >ISOI2::D9 Name: VSTD020 020 PPB IC Misc: ~TLN GW!. %C -1 +}CEO-V Quant Rev: 7 Quant Time Injected at Dilution Factor Instrument ID 960924 13:17 960924 12:08 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03Q46 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-1,3-Dichloropropene 45) trans-1,3-Dichloropropene 46) 1,1,2-Trichloroethane 47) Dibromochloromethane 48) Bromoform 49) trans-l,4-Dichloro-2-Butene 50) *Chlorobenzene-d5 51) 4-Methyl-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hexanone 56) 1,2-Dibromoethane 57) Chlorobenz ene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) styrene 63) Cumene 64) 4-Bromofluorobenzene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) 1,3-Diehlorobenzene 68) 1,4-Dichlorobenzene 69) 1,2-Dichlorobenzene * Compound is ISTD R.T. Q ion 10.90 43.0 11.00 83.0 11.47 63.0 11.67 75.0 12.48 75.0 12.74 97.0 13.31 129.0 15.40 173.0 16.18 53.0 14.15 117.0 11.90 43.0 12.05 98.0 12.15 91.0 12.94 164.0 13.12 43.0 13.46 107.0 14.18 112.0 14.35 106.0 14.52 106.0 14.66 70.0 15.11 106.0 15.13 104.0 15.65 105.0 15.88 95.0 16.09 83.0 16.16 110.0 17.49 146.0 17.61 146.0 18.17 146.0 Area 19135 27380 9342 21137 21670 13678 25496 20309 15191 75567 14492 35786 32063 11665 8061 21990 25299 10854 27213 15105 13337 24130 37652 28488 25024 6250 19248 22707 20678 Cone units 19.75 UG/L 19.02 UG/L 23.67 UG/L 19.67 UG/L 20.97 UG/L 21.83 UG/L 22.82 UG/L 27.11 UG/L 55.78 UG/L 50.00 UG/L 23.28 UG/L 19.99 UG/L 18.06 UG/L 18.88 UG/L 22*43 UG/L 20.86 UG/L 18.61 UG/L 18.69 UG/L 37.70 UG/L 21.50 UG/L 18.48 UG/L 18.80 UG/L 17.79 UG/L 22.78 UG/L 22.62 UG/L 21.85 UG/L 19.65 UG/L 20.52 UG/L 22.28 UG/L <3 96 95 89 86 92 93 96 98 90 83 89 97 99 98 94 94 91 99 97 93 95 85 99 81 93 63 88 86 86 168 DUP050308146 5^ Data Pile: >IS0I2 Name: VSTD020 020 PPB IC Misc: ~TLN eWL %C =1 +}CEO-V Quant Time: 960924 13:17 Injected at: 960924 12:08 Quant Output File: 'IS0I2 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 Compound No: 12 Compound Name: Acetone Scan Number: 242 Retention Time: 4.62 min Quant Ion: 43.0 Area: 4033M Concentration: 24.26 UG/L q-value: 0 This report was produced by QAREA at: 3:29 PM TTJE. , 24 SEPT, 1996 169 DUP050308147 9-34-% Data Pile: >1S0I2 Name: VSTD020 020 PPB IC Misc: -TLN @WL %C =1 +JCEO-V Quant Time: 960924 13:17 Injected at: 060924 12:08 Quant Output File: ~ISOI2 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 Compound No: 13 Compound Name: Methyl Iodide Scan Number: 252 Retention Time: 4.74 min A Quant Ion: 142.0 Area: ' 35155M Concentration: 23.68 UG/L q-value: 99 This report was produced by QAREA at: 3:29 PM TUE., 24 SEPT, 1996 170 DUP050308148 Data Files >IS0I2 Quant Output File: AISOI2 . A Name: VSTD020 020 PPB IC Misc: ~TLN @WL %C -1 +J-CEO-V Instrument ID: HP03046 Quant Time: 960924 13:17 Quant ID File: IA6390 A Injected at: 960924 12:08 Last Calibration: 951122 10:44 Compound No: 15 compound Name: Allyl Chloride Scan Number: 291 Retention Time: 5.19 min Quant Ion: 41.0 Area: 14081M Concentration: 18.94 UG/L q-value: 0 This report was produced by QAREA at: 3:30 PM TUE., 24 SEPT, 1996 171 DUP050308149 TOTAL ION CKR0MAT06RAM Data File: >ISOl3::D9 Quant Output File: "ISOIS^D? Name: VSTD050 050 PPB IC Instrument ID: HP03046 Misc: ~TLN @WL %C =1 +JCEO-V =1 Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLN-262 Quant Time : 960924 13:25 Injected at: 960924 12:50 1j L **7*(30 DUP050308150 QUANT REPORT Page 1 Operator ID: TLN-262 Quant Rev: 7 Quant Time Output File: AISOI3::D7 Injected at Data File: >IS0I3::D9 Dilution Factor Name: VSTD050 050 PFB IC Instrument ID Misc: ~TLN WL %C =1 +}CEO-V =1 960924 13:25 960924 12:50 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,l-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-l,2-Dichloroethene 21) 1,l-Dichloroethane 22) cis-l,2-Dichloroethene 23} 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane R.T. Q ion 8.17 128.0 2.28 85.0 2.43 50.0 2.59 62.0 3.02 94.0 3.16 64.0 3.55 101.0 4.06 59.0 4.28 56.0 4.43 96.0 4.49 101.0 4.59 43.0 4.70 142.0 4.82 76.0 5.16 41.0 5.41 84.0 5.77 59.0 5.90 53.0 6.01 73.0 5.96 96.0 6.74 63.0 7.77 96.0 7.84 43.0 7.91 54.0 7.97 43.0 8.16 67.0 8.28 42.0 8.34 83.0 8.68 56.0 9.12 65.0 9.23 62.0 9.84 114.0 6.89 43.0 8.60 97.0 8.88 117.0 9.20 41.0 9.20 78.0 10.22 130.0 10.55 63.0 10.79 88.0 Area Cone Units 30984 50.00 UG/L 84170 49.97 UG/L 29789 62.30 UG/L 33557 56.94 UG/L 30847 47.68 UG/L 19178 49.39 UG/L 45341 81.96 UG/L 26909 50.05 UG/L 27269 336.44 UG/L 34032 54.23 UG/L 141074 100.30 UG/L 12732 63.27 UG/L 129170 71.89 UG/L 94045 85.81 UG/L 55507M 61.68 UG/L 38836 51.28 UG/L 17408 318.57 UG/L 39903 256.70 UG/L 99636 49.32 UG/L 40057 51.76 UG/L 72665 48.18 UG/L 42952 55.50 UG/L 12457 51.04 UG/L 15300 293.23 UG/L 46741 57.13 UG/L 28767 142.22 UG/L 7581 44.07 UG/L 90745 46.16 UG/L 49437 49.59 UG/L 59899 41.95 UG/L 67354 44.73 UG/L 125072 50.00 UG/L 92070 66.16 UG/L 75122 50.18 UG/L 68021 53.41 UG/L 11466 754.65 UG/L 98416 54.02 UG/L 50590 56.68 UG/L 41988 52.37 UG/L 4280 1162.32 UG/L q 94 99 98 98 95 93 94 89 99 95 98 70 69 100 99 94 96 90 94 98 97 85 95 97 87 73 98 95 89 92 88 98 91 98 85 87 87 89 79 iJL O DUP050308151 QUANT REPORT Page 2 Operator ID: TLN-262 Quant Rev: 7 Quant Time Output File: 'ISOI3: :D7 Injected at Data File: >ISOI3::D9 Dilution Factor Name: VSTD050 050 PPB IC Instrument ID Misc: -TLN @WL %C =1 +JCEO-V =1 960924 13:25 960924 12:50 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-1,3-Dichloropropene 45) trans-l,3-Dichloropropene 46) 1,1,2-Trichloroethane 47) Dibromochloromethane 48) Bromoform 49) trans-l,4-Dichloro-2-Butene 50) Chlorobenzene-d5 51) 4-Methyl-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hexanone 56) 1,2-Dibroraoethane 57) Chlorobenzene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) Styrene 63) Cumene 64) 4-Bromofluorobenzene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) l,3-Dichlorobenzene 68) 1,4-Dichlorobenzene 69) 1,2-Dichlorobenzene * Compound is ISTD R.T. Q ion 10.89 43.0 10.99 83.0 11.47 63.0 11.67 75.0 12.48 75.0 12.74 97.0 13.31 129.0 15.40 173.0 16.18 53.0 14.15 117.0 11.90 43.0 12.05 98.0 12.15 91.0 12.95 164.0 13.13 43.0 13.46 107.0 14.20 112.0 14.36 106.0 14.52 106.0 14.67 70.0 15.11 106.0 15.13 104.0 15.66 105.0 15.88 95.0 16.09 83.0 16.15 110.0 17.49 146.0 17.62 146.0 18.17 146.0 Area 67905 93249 29687 73922 71562 44027 85449 68352 49759 97357 44860 110984 117846 43996 27876 70448 90431 39605 98618 47408 48472 87530 141745 90222 76705 19776 75650 84660 75556 Cone Units 53.41 UG/L 49.38 UG/L 57.32 UG/L 52.42 UG/L 52.77 UG/L 53.56 UG/L 58.29 UG/L 69.54 UG/L 139.26 UG/L 50.00 UG/L 55.92 UG/L 48.13 UG/L 51.53 UG/L 55.29 UG/L 60.22 UG/L 51.88 UG/L 51.62 UG/L 52.93 UG/L 106.05 UG/L 52.37 UG/L 52.13 UG/L 52.93 UG/L 51.99 UG/L 55.99 UG/L 53.81 UG/L 53.65 UG/L 59.95 UG/L 59.38 UG/L 63.19 UG/L q 97 95 88 88 91 95 97 97 89 86 90 95 98 98 97 94 85 96 96 94 92 85 98 82 91 67 89 89 88 174 DUP050308152 Data File: >IS0I3 Name: VSTD050 050 PPB IC Misc: ~TLN WL %C =1 +}CEO-V *1 Quant Time: 960924 13:25 Injected at: 960924 12:50 Quant Output File: "ISOI3 instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 Compound No: 15 Compound Name: Allyl Chloride Scan Number: 287 Retention Time: 5.16 min Quant Ion: 41.0 Area: 55507M Concentration: 61.68 UG/L q-value: 0 This report was produced by QAREA at: 3:36 PM TUE., 24 SEPT, 1996 .j u <J ii'it&U; DUP0503081 53 TOTAL ION CHROKflTOeRPm Data File: >XSGI4::D9 Name: VSTD100 100 PPB IC Misc: -TLN WL %C +JCE0-V -1 Quant Output File: AISOI4::D7 Instrument ID: HP03046 Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLN-262 Quant Time : 960924 13:50 Injected at: 960924 13:23 i: 1hf.ili.TM-'.;'#fc.: I 176 t d* 4lUV *< V DUP050308154 QUANT REPORT Page 1 Operator ID: TLN-262 Output File; ~ISOI4::D7 Data File: >ISOI4::D9 Name: VSTD100 100 PPB IC Wise: ~TLN @WL %C +J-CBO-V =1 Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 13:50 960924 13:23 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time : 960919 06:34 Compound 1) *Bromochloromethane 2) Dichiorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,l-Dichloroethene 11) Freon 113 12) Acetone 13} Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16} Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-l,2-Dichloroethene 21) 1,l-Dichloroethane 22) cis-1,2-Dichloroethene 23) 2-Butanone 24) Prop ionitrile 25} Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) l,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37} Benzene 38) Trichlotoethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane R.T. Q ion 8.18 128.0 2.28 85.0 2.43 50.0 2.61 62.0 3.03 94.0 3.17 64.0 3.55 101.0 4.08 59.0 4.28 56.0 4.45 96.0 4.52 101.0 4.60 43.0 4.72 142.0 4.83 76.0 5.16 41.0 5.43 84.0 5.79 59.0 5.92 53.0 6.00 73.0 5.96 96.0 6.74 63.0 7.78 96.0 7.84 43.0 7.91 54.0 7.98 43.0 8.16 67.0 8.27 42.0 8.34 83.0 8.70 56.0 9.12 65.0 9.25 62.0 9.84 114.0 6.89 43.0 8.61 97.0 8.88 117.0 9.19 41.0 9.20 78.0 10.24 130.0 10.57 63.0 10.80 38*0 Area Cone Units 32401 50.00 UG/L 172957 98.19 UG/L 60025 120.04 UG/L 70707 114.73 UG/L 63525 93.89 UG/L 35691 87.89 UG/L 95718 165.46 UG/L 56022 99.64 UG/L 59632 703.55 UG/L 72145 109.94 UG/L 289732 196.99 UG/L 27380 130.12 UG/L 274221 145.94 UG/L 203319 177.41 UG/L 117035M 124.37 UG/L 83654 105.64 UG/L 42045 735.77 UG/L 94868 583.60 UG/L 205574 97.30 UG/L 84835 104.82 UG/L 155594 98.66 UG/L 90864 112.27 UG/L 30015 117.60 UG/L 34060 624.23 UG/L 95738 111.91 UG/L 60550 286.26 UG/L 19801 110.08 UG/L 191240 93.02 UG/L 102483 98.31 UG/L 128913 86.34 UG/L 142327 90.38 UG/L 129247 50.00 UG/L 207987 144.64 UG/L 163983 106.01 UG/L 142896 108.58 UG/L 28113 1790.52 UG/L 213877 113.61 UG/L 109388 118.59 UG/L 90864 109.67 UG/L 11498 3021.66 UG/L q 97 99 99 98 92 97 97 86 98 94 98 71 71 100 98 98 96 89 93 97 98 86 97 97 86 72 98 95 90 92 85 96 92 96 91 87 88 88 85 177 DUP050308155 QUANT REPORT Page 2 Operator ID: TLN-262 Output File: ',ISOl4::D7 Data File: >ISOI4::D9 Name: VSTD100 100 PPB IC Misc: -TLN @WL %C +)CEO-V =1 Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 13:50 960924 13:23 1.00000 HP03046 ID File: 12*6390: :DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-1,3-Dichloropropene 45) trans-l,3-Dichloropropene 46) 1,1,2-Trichloroethane 47} Dibromochloromethane 48} Bromoform 49} trans-l,4-Dichloro-2-Butene 50) *Chlorobenzene--d5 51) 4-Methy1-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hejianone 56) 1,2-Dibromoethane 57} Chiorobenz ene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) Styrene 63) Cumene 64) 4-Bromofluorobenz ene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) 1,3-Dichlorobenzene 68) l,4-Dichlorobenzene 69) l,2-Dichlorobenzene * Compound is ISTD R.T. Q ion 10.89 43.0 11.01 83.0 11.48 63.0 11.67 75.0 12.49 75.0 12.75 97.0 13.32 129.0 15.41 173.0 16.19 53.0 14.16 117.0 11.91 43.0 12.06 98.0 12.16 91.0 12.96 164.0 13.13 43.0 13.48 107.0 14.20 112.0 14.37 106.0 14.54 106.0 14.67 70.0 15.12 106.0 15.14 104.0 15.66 105.0 15.89 95.0 16.11 83.0 16.17 110.0 17.50 146.0 17.63 146.0 18.19 146.0 Area 151671 199052 64170 159532 155208 92848 178145 142643 109109 99855 94445 240894 264087 96039 62798 151196 192360 84978 210645 101788 102538 183720 286845 193449 165681 40460 152661 179375 153412 Cone Units 115.44 UG/L 102.01 UG/L 119.90 UG/L 109.48 UG/L 110.76 UG/L 109.30 UG/L 117.61 UG/L 140.43 UG/L 295.50 UG/L 50.00 UG/L 114.79 UG/L 101.85 UG/L 112.59 UG/L 117.66 UG/L 132.26 TJG/L 108.56 UG/L 107.06 UG/L 110.73 UG/L 220.86 UG/L 109.64 UG/L 107.51 UG/L 108.32 UG/L 102.58 UG/L 117.06 UG/L 113.32 UG/L 107.02 UG/L 117.94 UG/L 122.66 UG/L 125.10 UG/L q 97 96 90 88 92 96 98 98 89 84 90 97 99 98 97 94 85 95 95 91 93 81 98 82 92 62 91 90 87 178 DUP050308156 Data File: >IS0I4 Name: VSTD100 100 PPB IC Misc: ~TLN @WL %C +}CEO-V =1 Quant Time: 960924 13:50 Injected at: 960924 13:23 Quant Output File: AIS0I4 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 Compound No: 15 compound Name: Allyl Chloride Scan Number: 287 Retention Time: 5.16 min Quant Ion: 41.0 Area: 117035M Concentration: 124.37 UG/L q-value: 0 This report was produced by QAREA at: 3:39 PM TUE., 24 SEPT, 1996 JL # DUP050308157 TOTAL ION CHROMATOGRAM Data File: >ISOI5::D9 Name: VSTD200 200 PPB IC Mise: -TLN @WL %C +>CEO-V =1 Quant Output File: AISOI5::D7 Instrument ID: HP03046 Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLN-262 Quant Time : 960924 14:23 Injected at: 960924 13:56 180 DUP050308158 QUANT REPORT Page 1 Operator ID: TLN-262 Output File: AISOI5::D7 Data File: >ISOI5::D9 Name: VSTD200 200 PPB IC Misc: ~TLN @WL %C +}CEO-V =1 Quant Rev: 7 Quant Time Injected at Dilution Factor Instrument ID 960924 14:23 960924 13:56 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcai Time: 960919 06:34 Compound 1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,l-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene 21) l,l-Dichloroethane 22) cis-l,2~Dichloroethene 23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,1-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane R.T. Q ion 8.19 128.0 2.28 85.0 2.45 50.0 2.61 62.0 3.04 94.0 3.17 64.0 3.57 101.0 4.09 59.0 4.30 56.0 4.45 96.0 4.52 101.0 4.62 43.0 4.72 142.0 4.84 76.0 5.18 41.0 5.43 84.0 5.84 59.0 5.93 53.0 6.03 73.0 5.97 96.0 6.76 63.0 7.80 96.0 7.85 43.0 7.94 54.0 7.98 43.0 8.18 67.0 8.27 42.0 8.36 83.0 8.71 56.0 9.13 65.0 9.25 62.0 9.85 114.0 6.91 43.0 8.62 97.0 8.89 117.0 9.21 41.0 9.22 78.0 10.23 130.0 10.57 63.0 10.80 88.0 Area Cone Units 34578 50.00 UG/L 334455 177.92 UG/L 118801 222.63 UG/L 140669 213.88 UG/L 118622 164.29 UG/L 58558 135.12 UG/L 183719 297.58 UG/L 116651 194.41 UG/L 129044 1426.64 UG/L 148758 212.41 UG/L 596527 380.05 UG/L 58852 262.07 UG/L 557135 277.83 UG/L 421692 344.79 UG/L 249270M 248.22 UG/L 166208 196.67 UG/L 98815 1620.35 UG/L 201750 1162.96 UG/L 410933 182.26 UG/L 177567 205.58 UG/L 328000 194.89 UG/L 182049 210.77 UG/L 68000 249.65 UG/L 73866 1268.53 UG/L 204719 224.23 UG/L 126273 559.40 UG/L 44949 234.14 UG/L 404627 184.42 UG/L 223499 200.90 UG/L 268236 168.35 UG/L 303088 180.34 UG/L 137478 50.00 UG/L 452398 295.77 UG/L 322036 195.71 UG/L 302671 216.21 UG/L 63292 3789.72 UG/L 422244 210.87 UG/L 216744 220.92 UG/L 193131 219.14 UG/L 23785 5876.42 UG/L q 92 99 99 99 94 97 98 85 98 95 98 68 71 100 97 97 96 91 94 98 97 85 94 97 84 81 99 93 91 91 87 94 91 98 93 88 84 88 85 131 t "*"-"iTWwtr jrlBifiniirfn^jOT^ DUP050308159 QUANT REPORT Page 2 Operator ID: TLN-262 Output File: AISOI5::D7 . Data File: >ISOI5::D9 Name: VSTD200 200 PPB IC Misc: -TLN @WL %C +)CEO-V =1 Quant Rev: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960924 14:23 960924 13:56 1.00000 HP03046 ID File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-l,3-Dichloropropene 45) trans-l,3-Dichloropropene 46) 1,1,2-Tfichloroethane 47) Dibromochloromethane 48) Bromoform 49) * trans-l,4-Dichloro-2-Butene 50) *Chlorobenzene-d5 51) 4-Methyl-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hexanone 56) 1,2-Dibromoethane 57) Chlorobenzene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) Styrene 63) Cumene 64) 4-Bromofluorobenzene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) 1,3-Dichlorobenzene 68) 1,4-Dichlorobenzene 69) 1,2-Dichlorobenzene * Compound is ISTD R.T. Q ion 10.90 43.0 11.01 83.0 11.48 63.0 11.68 75.0 12.50 75.0 12.75 97.0 13.32 129.0 15.40 173.0 16.19 53.0 14.16 117.0 11.92 43.0 12.06 98.0 12.17 91.0 12.96 164.0 13.13 43.0 13.48 107.0 14.20 112.0 14.37 106.0 14.54 106.0 14.68 70.0 15.12 106.0 15.14 104.0 15.66 105.0 15.89 95.0 16.10 83.0 16.16 110.0 17.49 146.0 17.62 146.0 18.18 146.0 Area 323088 414379 135993 317275 318054 196142 379544 306469 220053 108763 208644 501828 513395 190592 141304 313481 405697 171511 423289 213728 199948 383419 611983 408620 331906 82477 321589 375273 315996 Cone Units 231.19 UG/L 199.64 UG/L 238.89 UG/L 204.70 UG/L 213.39 UG/L 217.07 UG/L 235.56 UG/L 283.64 UG/L 560.28 UG/L 50.00 UG/L 232.82 UG/L 194.79 UG/L 200.96 UG/L 214.38 UG/L 273.23 UG/L 206.65 UG/L 207.30 UG/L 205.18 UG/L 407.46 UG/L 211.35 UG/L 192.47 UG/L 207.54 UG/L 200.93 UG/L 227.00 UG/L 208.42 UG/L 200.30 UG/L 228.11 UG/L 235.60 UG/L 236.58 UG/L q 96 94 88 88 92 95 97 98 90 85 91 96 99 99 98 93 85 94 95 91 91 84 96 79 95 63 88 88 85 18 o DUP050308160 Data File: >IS0I5 Name: VSTD200 200 PPB IC Misc: ~TLN @WL %C +}CEO-V =1 Quant Time: 960924 14:23 Injected at: 960924 13:56 Quant Output File: 'IS0I5 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44 Compound No: 15 Compound Name: Allyl Chloride Scan Number: 288 Retention Time: 5.18 min Quant Ion: 41.0 Area: 249270M Concentration: 248.22 DG/L q-value: 0 This report was produced by QAREA at: 3:43 PM TOE., 24 SEPT, 1996 i8S DUP050308161 a 9n t \ L: flic* i H'-.- j ? L< i * L)U it : c* ' '/ U r 'LiiAi <a !o ' tSij Z-'O . uJ r i i lOt" i = t > "'r' L> S' jJ ^ sx z.'O i s Date: *61112^ lUbb Las t La 1 ib Da ten 9 b X i.22 1 i.i 5 4-4 t ^ i L* 7 " / O L` ' x` A J. j J `Z- Li La i i d S- ; J e ! OftJ1-. io : B 4C a l i'll i i Lj01 ? i ii 60/ < Lv I n G o v 1 ,'r r- n - I.! -< H i t s Lomp ound i !"> i rr* 4 a '* a t;c? 3 H a k KS" iO p ; 7i p 5. i i ; xy .-....in blopc be <s it ivity . i.i V 'J u 4U . t)0 . `J l ) i.i J O . U00uuuu Jfi L Li D X i* 3 Ct 1 o r. He T r,c a l g r. o r e max check HijtO U: 0 & i :vi 0 t h O G Uuantitate Using Un its oV 4one Bunch i ng ; : : ; ; r r- ! rr,p . p OU i"i 03 i ^ J. >_o rr pound i a ri X ~L.il' v"iiu'- i G P u> in . r ri <r L"> i o r n*e t hgOg " '1 / L C * ; or ic:e -- t_-; G rn O '>*' T h a i"i - ' _*- , o - f - e 1 i ~ L.1 1- ~h i oroetnene C e * Or* l - aD oU jBLiii I dS ' \ 7. V * L n J o r i- ~j t i- a -1, V-L>i ch ioroe thene - i , ,-m : I-. 1 Ol' 0 5 t "! a JO c - f C 1 5 - i , Z ~ Liich ioroethene 7 ' -- L< *J V on r> l r, i C- r G V o r m : - j - 4 i c- r* i g r 0 5 t r..=>r.e- a A J X -L; icn i oroethane ` -1t l U O ! C< D 5- n Z r .e > i . 1 . x - > r iCi i ioroethane ,,.0 '* " Pi : s t r oc: or V` 0 - : L? i. i~ Z Pi - : ; r- y c-ic- r v e. t n ar r e x j >:! " ij 1 Oh i Ci rop r opan. " ' C*?' C':'>Gv i C- i"> - O r C' "n t h o 5 - U ich ! crop r opens. ! " ' O " i ; * ' " * *- G p r c p* 6 r, e ' ' 2 > i. ; i. " 1 r * cn { o ros thsns * ; ; b OiVtCiC h j C't' C: .:;t5 tr r? a '* 0 - : u-p *" Tu~ i or rf: ' ' *' ~ i : ' " e i- Z 5 r, 0 - r " ;; * ny ; ~ cl { '' !"i't 3 i~r o n 5 G - r; :r " Retention 'i i me . ype .1 1 1 4 M . \ K X .* I t1J ;> t 'l J ti J tn > :) t rj .> <; i) . j CT J L> (T) Zj t'5 ) Vi i t1J i ij tn > -* 'j t1} iy i. j ) C'! ) \) ti) i) f i ;= b} f: d . 1 ' 2 A^ C 3.02; i.i o t 4. 43 t 4 . - i 4.82 ( i.; 5.96t 6 . L-tL. ?. 77 (. 7. B . 3 41 V . J. V x 9.23 1. y. B41 Si . 6 0 t B . - v y . 2oc X L'l X. JL *L i a. *? 5> t in . vv i. X i 6 /' *. 22.; 14.74t i .i . * i l 1 .40 s. i *. 11.9 Ui i 2 . *J l> : j . !'- 1 . U U l ) . 29B J . 1' . 370 } . B/} . 3 43 .1 . 3oi .390) > {.' i_i i_ . 729 ) . Uw ' . 9b 1) . lj u 1 .020 ) 1 . i j, O 1.13 0 > X L) U ? L ,>4 . Li Sr f .9 33 ) I . 39 ) 1.U72) i 1 X/) 1.IB6 ) 1.20Vi 1.299) 1 , 'S' _/ 1.969i X . ; 1 L* . . tf 41 ) r 1"> x! - . !;! 9 fc! I * )m - i , J L* t.' d u .96143 i # Li Li S? L* 4 . 9999B . 6 iw' D 1. 0 9 B 3 7 . 41 i,. '' 2 3.0 3 9 2 B i . 293 2 1.33999 X . 4':" x >4 1.3 3999 . tVX v. '? 2.92B77 i . V3 i2 2.173B3 X r U U L* :.j U . 6UU63 . b4>o .7B6B7 . 4 1.5 **- 4 ` l .33971 . 9 91U4 . w <Z> .39201 O _ .2. J .946 9 0 X . Li U Li !J .4oU7B i . i '''' 1 - 2 ! 04h NL --X i_ i - r*i c . ii . L; U 90.00 Li . U u 90.00 90. U 9U . 0U vo . o 9U . U0 7- Li . u * 9 0.0 0 " *3 . Li ; 9U . 0U 3U . Uii 9 0.00 9U . U0 90 . UU 7 SJ . L L 9 0.0 0 9 0 . U !- 9U . 0U 90 . U 9 0.00 y o' 9 0.0 U -- 9M 9U . 00 L * L) 90. UU L- . U i.; 90 . U0 > L . U 4 !! , J i 51 DUP050308162 He s Gn :` t Uj c i;-.l uv 36 ; 1 * . ij 1. Ul*> ) -y >eiu -r yr 5 n 5 "- t:i_ orr.o s' 1 uo rooei'iZene T !'5C" i O r C'c 7 !"i L6-v.pour.c- 13 i (. i ! ' * tb ; -S 1 ^ . IX t j- y * x ; l1? . UiJ 16 1. U6fcS i . .- c. .1 . 122 O tj L* 4y yah a. u u *? u. U L' DUP050308163 7A VOLATILE CONTINUING CALIBRATION CHECK Lab Name: LANCASTER LABS Contract: _______. Lab Code: LANCAS Case No.: ________. SAS No.: _______ . SDG No.: _______ . Instrument ID: HP03460 Calibration Date: 09/25/96 Time: 0026 Lab File ID: >GSPS1 Init. Calib. Date(s): 09/24/96 09/24/96 Heated Purge: (Y/N) N Init. Calib. Times: 0140 0349 GC Column: DB624 ID: 0.53(mm) COMPOUND Chloromethane Vinyl Chloride Bromomethane Chloroethane 1,1-Dichloroethene Acetone Carbon Disulfide Methylene Chloride 1,2-Dichloroethene (total) 1,1 -D ich loroethane 2-Butanone Chloroform l,2-Dichloroethane 1,1,1-Trichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-i,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane Bromoform 4-Methyl-2-Pentanone Toluene Tetrachloroethene 2-Hexanone Chlorobenzene Ethylbenzene Xylene (total) Styrene Mi n Ma x SEF RRF 50 RRF %D %D ====== sasasasassiSB cnsrassss ===== a=g-- 1.194 1.173 .811 .617 .940 .292 2.767 1.409 1.179 1.355 1.297 0.100 .765 0.100 .697 .962 0.100 .284 2.805 1.189 1.214 -13.5 -10.6 25.0 5.6 25.0 -12.9 -2.3 25.0 2.6 -1.4 ,15.6 -3.0 2.265 .330 2.552 1.679 .456 .465 .731 .386 .350 .661 . 530 .454 .317 .660 .604 .347 1.049 .512 .228 .918 .357 .442 .803 2.356 0.200 .399 2.612 0.200 1.678 0.100 .472 0.100 .458 0.100 .735 0.500 .385 0.300 .337 .646 0.200 .530 0.200 .453 0.100 .297 0.100 .628 0.100 .582 0.100 .313 1.021 0.400 .493 0.200 .205 .871 0.500 .366 0.100 .441 0.300 .777 0.300 -4.0 25.0 -20.9 -2.3 25.0 .0 25.0 -3.4 25.0 1.4 25.0 -.6 25.0 .2 25.0 3.7 2.2 25.0 -.0 25.0 .3 25.0 6.3 25.0 4.9 25.0 3.6 25.0 9.8 2.7 25.0 3.7 25.0 10.2 5.1 25.0 -2.6 25.0 .2 25.0 3.2 25.0 "--AiE ilsl 'oirtjhgegr^scro...m......p...o'"uj njds1 m'-l -uxs-t me. et a minimum RRF of o.oio. page 1 Of 2 FORM VII VOA OLM03.Q 136 A. DUP050308164 7A VOLATILE CONTINUING CALIBRATION CHECK Lab Name: LANCASTER LABS Contract: _______. Lab Code: LANCAS Case No.: _______ . SAS No.: _______ . SDG No.: _______ . Instrument ID: KP03460 Calibration Date: 09/25/96 Time: 0026 Lab Pile ID: >GSFS1 Init. Calib. Date(s): 09/24/96 09/24/96 Heated Purge: (Y/N) N Init. Calib. Times: 0140 0349 GC Column: DB624 ID: 0.53(mm) COMPOUND 1,1,2,2-Tetrachloroethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene .. SET" RRF RRF 50 RRF .648 .587 0.300 1.504 1.625 1.072 1.062 .842 .845 0.200 "MAX %D %D 9.3 25.0 -8.0 1.0 -.3 25.0 page 2 of 2 FORM VII VOA OLM03.0 i8 DUP050308165 X h Tw L T fttv C H M ^ 11 iri S? *3* ,,v* ^ -F I vc: mono Tic- 80*:- one, ,,pr 13.-, t a V- l e : SGBF31 : : l^i Name : USTDUSO 050 ppb M- -.c : ~SOM %C IdWi, =1 +> CC &t *5 Quant Output File! ''GSHS1 : : Ff. I ns t r ume nt IB ! HPtll-^KO Id Fi Le: IM-'l390 : ! UB T* -3. ie : 3,'"90 Water/Mad Sot 1 ID 1' i i c da st. Ca libration: 951 2 0 ? 01 : 59 f o r I n.r. t. . H > '!! 3 4b i Last. Qcal Time : yyijyiM 02 Operator ID : Quant Tx me i .1 njectcd 3 T. I 96 l!H25 9KI1H25 01) i52 0U ! 26 188 DUP050308166 Ope r at or ID' 983 Or-* pu* File: i'Cstpsi i : Ftf beta File; >09931 : : D4 Name ; OSTDOS'U Ohil ppfi H-sc ; ~i5HM SsC yWL ~1 *> CC 8.5 *5 OFMNT ijuant Re'.' y yu.-int Tune j. f _ t <-- < (? .i ci u Dilution Factor I r.t r urn e n t ] 1! CjfC- : u' I C 1jI J 1 s; :: i i; H- ' ID File; IH4330 : : DB Title: 3,'90 LJater/Med Boil ID File La;:.* Co .! i far at ion : 95120? 01:59 for Inst, HP034SG Last Qcal Time 9n0H29 02 : 44 Compound 1) 2J 3 'i 41 5j 6 -5 /X 8 9) 'Mi. ii 3 3) l --I ? 15) 16 17 ) `I LJ i y .i *j 11 ^ 2i ' 2V ' '} 1 * : /\ . *Bromochlorcimethane Ch;nromnthane Cimil Chloride Brnrnomi" thane Chloroet ha-ne 1 * .! - D x c h 1 c r o e t he ne Pice tone Car bon Du sulfide Methylene Chloride tr nns- 1 > 2 - iJichloroethcne 1 ,i-l'ichicroethnne t . - 1,2--Uichloroet' \ene But. arinne Ch ! q i*p form 1 ,2-Etichloroethane -d4 1 .,V-D:.ohicroethane *1. ; 4-Di f luornbensene 1 ;. 1 / l-Trschlorort.hane Carbon Tetrathloride Benzene Trichloroethene 1 ;V-LO chloropropane Bromodic h lor-met ha ne - - - d -2 Tl ^ ~ U 1 - ^ ~ R , T. Q ion 9.49 3.29 3.53 4.0? 4.28 c*. _> ,. 99 b ,i x. s' Fi .. 84 . .."ji tJU i x1 xL 12 13 9 , 63 10 40 1!! . 52 11 . 09 9 . 32 10 . 18 1 0 . 49 11 . 48 11 .80 12 o -> r *"i "v 128 . SB 62 . 9"-'! 64 96 43 . 0 76 . n 84 . 0 96 . 0 63 . c 36 43 83 . 0 65 0 67 . 0 11 4 . 0 97 . 0 117 0 78 . 0 13 U . 0 .0 83 . 0 Area Co nc 8- u e, o -i `~i 78265 445 0 0 40512 5 5 919 5 16539 168083 691 23 65.2 97 136887 74881 -> I; -j cl C; 15 183 0 34447 97567 243 -176 1 'J 48 19 111674 l-'9U3ii 93803 8 2 099 157386 1 . U > 1 W ___ 50 00 6 '! 89 59 5!! 70 58 58 c . 23 t-. .71 49 12 C.. 1 : .7? .j J . 0 2 5 29 6 6 42 5 J. .55 b 4 . 37 5V . 00 L., 0 . 0 0 5 v . 67 *4 0 . 12 . 45 t2. 0 . 73 5 il .97 4 y . 59 ..j.y ... ug-'L ug/L ug -'L uo/i. ug. 'L uq/., ug'L ug-'L ug 'L ug ' ug - uq..--L ug--'L ug--'L uq- 'L ug-- I i ug.-- ti ug 1. ug.. 7it-J Ug- 'L uq. 'L 56 c 98 c;7 94 Cl I Mci |i!!: y9 yu y& 96 ci O 9b 96 83 y1 88 98 91 95 82 9^ 75 ' 'J -* ` ' > 1../ 1 23 811; y :l yV ; 0- * r a ns -1,3-Dichloroprope ne i . x>2-Triehioroethane iibromoc h10r omet hane B;nmoform *Ch10 r 0 be nsene-d5 4 Me t hy J - 2 - 8 e n t an 0 ne? Toluene- d8 T;i i uenc Tetrachloroethe ne 13.67 13.94 14- 52 16.61 15.36 13.07 13.26 13.36 1 4.16 75 97 5 v9 173 117 43 yfc: 91 164 0 il 0 0 0 0 0 0 0 114 8 5 6 723 46; 152677 14 i 8 2 0 197202 61734 2099-0 2 01272 9 77 ns 5 4 . *7 -Zi ug-'L 4K . 74 u q 7 L 47 . 33 aq/L 4:-: . 10 ijq/L 5 0 . 0 0 uq.-'L 57 . 3f/ ug-'L 5 0 . 14 UC; ''L C. * ! *7 V uq/L '-i 8 . 26 u g' L DUP050308167 94 94 93' 3G 92 9S l_J L. 9C QUMNT REFUK? Or<r:rat.-.r III: SHM~983 Oat pat F3. 1 : ~UHPS1 : : FM D.-vf.e. F'.Je: > CHFF/i : : D4 Home; USTUOSO 05 0 ppb Mt-ic : "Sf-'M %C- U1. =1 + > CC Quant kew: 7 Qr-.-mt Time : in'acted ,nt 1) i lutio n F a c t n r ; Instruinerit if 1 3n': yt-!f HFi: U !.1 : fc SI! !!*;! ID File: If-l '!:^9 0 : : DB Title: Uator/Med. Sc 1 ID File Oast Calibration: 95120? Q1 :t>9 for Inst . HK0346M Last ^cal Time : 9k 0324 02 : <=*4 Compound 4:? 1,1 ^2,2-Tetrachloroethane * Compound is 1.5TD R.T. Q ion 17.28 88.0 Area 115852 Cone Units 4K . 06 i.iq "i. 9i; 19( DUP050308168 Quant ID File: IA4330::DB Title: 3/90 Uater/Med Soil ID File for Inst. HP03460 Last EDIT Date: 960725 11:46 Last .Calib Date: 951207 01:59 Last Qcal Date: 960925 00:26 Calib File: CB3904::DB Qcal File: y'G5PSl: 14906 :FM /. RT Window C+min -%) Max Hits/Compound Minimum Area Peak/Base Peak Ratio Up Slope Sensitivity Down Slope Sensitivity .2000 5 50 40.00 .2000000 .0000000 % Subtraction Method Ignore max check Auto Qdel Method Quantitate Using Units of Cone Bunching 2 NO 5 AREA ug/L -1 Number of Compounds! 41 Comp No . Compound Name Retention Time (Type > Min. (Rel) R.F . Cone . 1) *Bromoc hloromet hane 2) Chloromethane 3) Uinyl Chloride 4) Bromomethane Cl) ; CT) XT) CT) 9.49 C 3.29C 3 .53C 4.07C 1.000) .347) .372) .429) l.ooooo 1.35493 1.29701 .76550 50.00 50.00 50.00 50.00 5) Chloroethane 6) 1,1-Dichloroethene XT) CM) 4.2SC 5.86 C .451) .618) . 69690 .96152 50.00 50.00 7) Acetone CT) 5 .93 C .631) .28434 50.00 8) Carbon Disulfide CT) 6 .27C .661) 2.80539 50.00 9) Methylene Chloride CT) 6.84C .721) 1.18907 50.00 10) trans-1,2-Dichloroeihene CT) 7.37C .777) 1.21425 50.00 11) 1,1-Dichloroethane CT) 8.12C .855) 2.35648 50.00 12) cis-1,2-Dichloroeihene -CT) 9.12C .961) 1.21425 50.00 13) 2-Butanone . CT) 3.13C .962) .39889 50.00 A 14) Chloro form A 15) 1,2-Dichlaroethane~d4 16) 1,2-Dichloroethane . CT) CS> XT) 9.63C 1.015) 10.40C 1.096) 10.52C 1.108) 2.61181 1.62470 1.67837 50.00 50.00 50.00 17) *1,4-Difluorobenzene A 18 ) 1,1,1-Trichloroethane CD 11.09C 1.000) CT) 9.92 C .895) 1.00000 .47158 50.00 50.00 19 ) Carbon Tetrachloride CT) 10.18C .918 ) .45846 50.00 20) Benzene (M) 10.49C .946) .73531 50.00 21) Trichloroethene CM) 11.48C 1.036) .38527 50.00 22) 1, 2-Dichloropropane CT) 11.80C 1.064) .33717 50.00 23) Bromodichloromethane CT) 12.22 C 1.102) .64821 50.00 24) cis-1,3-Dichloropropene CT) 12.87C 1.161) . .53004 50.00 25) trans-1,3-Dichloropropene CT) 13.67C 1.233) .45272 52.10 26) 1,1,2-Trichloroethane CT) 13.94C 1.257) .29714 50.00 27) Dibromochloromethane 28 ) Bronio form 29 ) *Chlorobenzene-d5 <T) CT) CD 14.52 C 1.309) 16.61C 1.438 ) 15.36C 1.000 ) .62789 .5e248 1.ooooo 50.00 50.00 50.00 30) 4-Methyl-2-Pentanone . CT) 13.07( .851) .31305 50.00 31) Toluene-dS CS) 13.26 C .863) 1,06170 50.00 32) Toluene CM) 13.36 C .870) 1.02064 50.00 33 ) Tetrachloroethene CT) 14.16C .322) .43319 50.00 34) 2-Hexanone (T) 14.29 C .930 ) .20467 50.00 35) Chlorobenzene CM) 15.41C 36) Ethylbenzene XT) 15.5SC ' 37) m+p-Xylene CT) 15.73C -38) - o-Xylene -- --......................- ------------------- --tTi - -16.32 C 39) Styrene . CT) IS.33 C 40) 4-Broroofluorobenzene CS) 17.09C 41) 1,1,2,2-Tetrachloroethane CT) 17.28C 1.003) 1.013) 1.024) 1.062) 1.063) 1.113) 1.125) .87102 .36642 .44111 - -*-4414-1.77717 .84478 .58748 50.00 50.00 100 .d|)91 -------- -O-j-0Q--_ 50.00 5U .00 50,. 00 * Compound is 1STD J V)C L t'.y *| {, .-r ' * `A lJ DUP050308169 7A VOLATILE CONTINUING CALIBRATION CHECK Lab Name: LANCASTER LABS Contract: T,ab Code: LANCAS Case No.: _______. SAS No.: _______ . SDG No.: Instrument ID: HP03046 Calibration Date: 09/19/96 Time: 0634 Lab File ID: >ISJS1 Heated Purge: (Y/N) N Init. Calib. Date(s): 08/20/96 Init. Calib. Times: 2025 08/20/96 2246 GC Column: DB624 ID: 0.53(mm) COMPOUND Chloromethane Vinyl Chloride Bromomethane Chloroethane 1,l-Dichloroethene Acetone Carbon Disulfide Methylene Chloride 1,2-Dichloroethene (total) 1,l-Dichloroethane 2-Butanone Chloroform l,2-Dichloroethane 1,1,l-Trichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane Bromoform 4-Methyl-2-Pentanone Toluene Tetrachloroethene 2-Hexanone Chlorobenzene Ethylbenzene Xylene (total) Styrene WF MlN RRF 50 RRF 1.120 1.188 1.191 .733 1.172 .370 3.086 1.601 1.348 2.562 .415 3.001 2.304 .542 .412 .777 .365 .341 .710 .576 .535 .328 .536 .344 .460 1.222 .404 .297 .911 .381 .468 .851 .772 .951 0.100 1.044 0.100 .627 1.013 0.100 .325 1.769 1.222 1.249 2.434 0.200 .394 3.173 0.200 2.430 0.100 .598 0.100 .509 0.100 .728 0.500 .357 0.300 .321 .755 0.200 .564 0.200 .542 0.100 .329 0.100 .586 0.100 .393 0.100 .412 1.174 0.400 .409 0.200 .238 .900 0.500 .384 0.100 .478 0.300 .849 0.300 MAX %D %D 31.1 19.9 25.0 12.3 25.0 14.5 13.6 25.0 12.2 42.7 23.7 7.3 5.0 25.0 5.1 -5.7 25.0 -5.5 25.0 -10.4 25.0 -23.6 25.0 6.3 25.0 2.2 25.0 6.0 -6.3 25.0 2.1 25.0 -1.3 25.0 -.2 25.0 -9.3 25.0 -14.2 25.0 10.4 3.9 25.0 -1.2 25.0 20.0 1.2 25.0 -.9 25.0 -2.0 25.0 .2 25.0 All other compounds must meet a minimum RRF of0.010. page 1 of 2 FORM VII VOA OLM03.0 19 S DUP050308170 7A VOLATILE CONTINUING CALIBRATION CHECK Lab Name: LANCASTER LABS Contract: _______. Lab Code: LANCAS Case No.: _______. SAS No.: _______. SDG No.: Instrument ID: HP03Q46 Calibration Date: 09/19/96 Time: 0634 Lab Pile ID: >ISJS1 Heated Purge: (Y/N) N Init. Calib. Date(s): 08/20/96 Init. Calib. Times: 2025 08/20/96 2246 GC Column: DB624 ID: 0.53(mm) COMPOUND Mf ur RRF 50 RRF %D ~T3S3? %D 1,1,2,2-Tetrachloroethane .757 .732 0.300 3.3 25.0 1,2 -Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene 2.133 2.304 1.220 1.184 .855 .828 0.200 -8.0 2.9 3.2 25.0 page 2 of 2 FORM VII VOA OLM03.0 19 S DUP050308171 T0TOL JON CHROHftTGSRAH Data File: >ISJS1::D3 Name: OSTDU50 U50 PPB CC Hi sc: ~SAH |3WL 9SL =1 + > Quant Output File: 'S1S3S1::D7 instrument ID: HP03046 Id File: 1A6390::OB Title: 3/90 SOW Water/hed Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960917 12:33 Operator ID: SAM=983 Quant Time : 960919 06:58 Injected at: 960919 06:34 194 DUP050308172 QUANT REPORT Page 1 Liperator ID: SAM=y83 Uutpu t File: '' 1SJS1: : D7 (Js t a File: )iSJSI::D3 Na me: MSID050 05 0 PPB CC nisc: -BAM |SWL %L =1 + > Quant Key: 7 Quant Time: In jected at: Dilution Factor: Instrument ID: 960919' 0b: 58 9609191 06:34 1. . 0 LI U U 0 HP03046 ID File: IA6390::DB 1 11 ie : 3790' 8L!W Ulater/Msd Soil ID File for Inst . HP03U46 Last Calibration: 951122 10:44 Last Qcal Time: 960917 12:33 Compound 1.) JLi S 3) 4? t?> 6) 7) 8) V> ID) ii / 12 > 17 ) 14) 1*7 ) 16 ) 17 ) 18) 19) 20) A 1J 22) 23 J 24) 2"? ) 26 ) 27 5 28 5 29 3 30 ) 31) 32 ) 33 3 34 ) 33 2 ) 37) 38 ) 39 ) ^0 ) *t)rornoch lor owe thane Chlorome thane Vinyl Chloride Br omomethane Chloroethane 1,1-Cichloroethene Acetone Carbon Disulfide Methylene Chloride trans-l,2-Dichloroethene 1 ,l-Dichloroethane cls-1,2-Dichloroethene 2-Uutanone Chloroform 1,2-Oichloroethane-d4 1,2-Dichloroethane *1,4-Difluorobenzene X,1,1-Trichloroe thane Carbon Tetrachloride Benzene 1richloroethene 1,2-Dichloropropane Hromodichloromethane cis-l,3-Dichloropropene t rans-1,3-Dich1oropropene 1,1,2-Tr ichloroethane Uibromochloromethane Bromoform *Lh 1o robenzene-d5 4-Methy 1-2-Pentanone !o1uene-dB To 1uene letfachloroethene 2-Hsxanone Chlorobenzene E_t hy lbenzene m+p-Xylene o-Xylene St yrer.e 4-Bromofluorobenzene R.T. Q i on 8.34 2.57 2.74 3.17 3.31 4.65 4.77 5.05 5.61 6.13 6.91 7.94 7.99 8.50 9.29 9.41 ID. 01 8.77 9.05 9.37 10.40 10,72 11.17 11.83 12.63 12.90 13.48 15.57 14.33 12.05 12.21 12.31 13.10 13.27 14.36 14.53 14.70 15.28 15.31 16.05 128.0 50. 0 62.0 94. 0 64. 0 96. 0 43.0 76.0 84.0 96. 0 63.0 96.0 43.0 83.0 65.0 62.0 114.0 97. 0 117. 0 78.0 130. U 63.0 83. 0 75.0 75.0 97. 0 129.0 173.0 117. 0 43.0 98.0 91.0 164. 0 43.0 112.0 106.0 106.0 106.0 104,0 95.0 Area 3 0/09 23696 29205 32062 19244 31098 9972 54310 37527 35489 74735 41219 12095 97426 70/54 74628 129120 77270 65/39 94034 46U/3 41386 974/0 72787 72/94 42432 75663 50739 94592 38970 112029 111095 3866 0 22489 85105 36349 92874 45175 80336 78276 Lone Units q 50.00 UG/L yli 41.67 UG/L 99 42.56 UG/L 95 56.05 UG/L 96 49.97 Uls/L. V5 42.96 UG/L 90 38.34 UG/L 68 27.06 UG/L 100 44. 41 UG/L 97 41.34 UG/L 96 46.48 UG/L 9S 48.01 UG/L 96 37. 49 UG/C 96 50.95 UG/L 98 55.0 0 UG/L 87 52.72 UG/L 93 .50.00 UG/L 86 53.72 UG/L 90 51.72 UG/L 98 43.43 UG/L 90 46.79 UG/L 84 43.92 UG/L 94 5 0.22 UG/L 95 46.45 UG/L 87 49.68 UG/L 90 46.69 UG/L 96 51.38 UG/L 97 50.13 UG/L 99 50.00 UG/L 85 39.37 UG/L 90 47.32 IJG/L 98 44.43 UG/L 99 46.93 UG/L 97 37.71 UG/L 96 46.46 UG/L , . 86 45.68 UG/L 19 b>94 93.52 u g /l 95 45.49 UG/L 91 46.20 UG/L 84 49.29 UG/L 75 DUP050308173 QUANT REPORT ('age Operator ID: SAM=983 Uutput File: '"'1SDS1 ::D7 Data Filet >ISJS1::D3 Name: OSTDObti 05 0 PPB CC Misc : -SAM WL S6C "1 +> Quant Reu>: 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960919 06:58 96 UV19 06 :34 1. 00000 HP03 U46 ID File: 1A639U::D6 Title: 3/9 0 SOU Water/Med Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960917 1 2:33 Compound 41) 1,i,2,2-Tetrachloroethane * Compound is IS I'D R.T. Q ion 16.26 83.0 Area 69249 Cone On i ts 43.39 UC/L q 95 196 DUP050308174 yuant ID File: IA6390::DB title: 3/90 SOW Water/Med Soil ID File for Inst HPQ3U46 Last EDIT Date: 960129 11:59 Last Caiib Date Last Ueal Date: 960919 06:34 Caiib File Ocal File: 'MSJS1:14906:D7 951122 10:44 CA39U6::D8 R) Window C+min -%) : flax Hi ts/Compound : Minimum Area : Peak7Base Peak Ratio : Up Slope Sensitivity : Down Slope Sensitivity: .2000 5 90 40.00 .2000000 .01)00000 % Subtraction Method Ignore max check : Auto Wdel Method : Quantitate Using : Units of Cone : Bunching : NO 5 AREA UG/L -1 Number of Compounds: 41 Comp No . Compound Name Retention Time C Type) Mxn. CRe 1 ) R.F. Cone . 1) 2) 3) 4> 5) 6) /> a> 9) 10) 11) 12) 13) 14) 15 ) 16 ) 17) 18) ly) 20) 21) 22) 23) 2 4) 25) 26) 27) 28) 2y) 30) 31) 32) 33) 34) 35) 36 ) 37) 38 ) 3V ) 40 ) *Bromoeh loromethane Chloromethane Uiryl Chloride Bromomethane Chloroethane 1,1-Dichloroethene Acetone Carbon Disulfide Methylene Chloride trans-1,2-Dichloroethene 1,1-Dichloroethane cis-1,2-Dichloroethene 2-Butanone Ch loroform 1,2-Dichloroethane-d4 1,2-Dichloroethene *1,4-Di 1- luorobenzene 1,1,1--T richloroethene Carbon Tetrachloride Benzene Tr ich loroethene 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene t rans-1,J-Dichloropropene 1,1,2-Trich1o roethane Dibromochloromethane Bromoform *Chlorobenzene~d5 4-Me t hy1-2-Pentanons loluene~d8 To luene 1 et rachloroethene 2-Hexanone Ch lorobenzene EthyIbBnzene rn + p-Xy lane o-Xylene Styrene 4-Bromofluarobenzene C I) 8.34C 1.000) <T) 2.57C .308) (T ) 2.74C .329) CT) 3.17C .381) IT) 3.31 ( .398) (M) 4.65C .558) n) 4.77C .572) (T) 5.05C .605) tT) 5.61C .672) (T) 6.13C .735) m 6.91C . 829) CT) 7.94C .953) <T) 7.99 ( .958) CT) 8.50C 1.020) CS) 9.29C 1.114) CT) 9.41C 1.128) C I ) 10.01C 1.000) CT) 8.77C .876) CT) 9.05 C . y U4) CM) 9.37C .936) CM) 10.40C 1.038) CT) 10.72 (. 1.071) IT) 11.17C 1.115) CT) 11.83 C 1.181) CT) . 12.63 C 1.262) CT) 12.90C 1.288) ( T) 13.48 C 1.346) CT) 15.57C 1.555) C I ) 14.33 C 1.0UCI) CT) 12.05 C .841) CS) 12.21C .852) CM) 12.31( CT) 13.1UC .859) .yi4) CT) 13.27C .926) CM) 14.36 C 1.U02) CT) 14.53 C 1.014) C7 ) 14.70C 1.026 ) - CT)-/- 15.2SC 1.067) CT) 15.31C 1.U68 ) CS> 16.05C 1.120) i.aouuo .77163 .95102 1.04406 .62666 1.01267 .32473 1.76854 1.222U2 1.24895 2.43365 1.24895 .39386 3.17256 2.304U2 2.43017 1.00000 .59844 .50913 .72827 .35682 .32052 .75488 .'36372 .542U9 .32862 .58599 .39296 1.ooouo .41198 1.10434 1.17446 .40870 .23775 .89971 .38427 .47758 .47758 .84929 .82751 50.00 50.00 50.00 50.00 50.00 50.00 50.0U 50.00 50.00 50.00 50.00 50. 00 50.0U 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 52.0 0 50.00 50. UO 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 100 . Ut) 5 Ol TM (Ml 5 0-Lttf 50.00 41) 1,1,2,2-letrachloroathans * Compound is ISTD CT) 16.26 C 1.135) .73208 50 . OU DUP0503081 75 Raw QC Data i9S DUP050308176 TOTAL ION CHROMATOGRAM Data File: >GSMT3::D4 Quant Output File: '"GSMT3::FM Name: BFBJUN2S 50nG BFB Instrument ID: HP03460 Misc: -SAM %C =1 2uL 25ppm BFBJUN28 Id File: IDBFB::DB Title: TUNER Last Calibration: : Last Qcal Time: 920618 19:58 Operator ID: SAM-983 Quant Time : 960924 01:15 Injected at: 960924 01:08 i99 DUP050308177 m/z 50 75 95 96 173 174 175 176 177 GC/MS PERFORMANCE STANDARD Bromofluorobenzene (BFB) Ion Abundance criteria % Relative Abundance Base Appropriate Peak Peak 8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance 5-9% of mass 95 Less than 2% of mass 174 50-120% of mass 95 4-9% of mass 174 93-101% of mass 174 5-9% of mass 176 26.69 49.05 100.00 6.62 0.00 70.67 5.02 69.37 3.93 26.69 49.05 100.00 6.62 0.00 70.67 7.10 98.16 5.67 Injection Date Injection Time Data File Scan 09/24/96 01:08 >GSMT3 138 status Ok Ok Ok Ok Ok Ok Ok Ok Ok INSTRUMENT HP03460 2oe DUP050308178 3/90 CRITERIA ANALYSIS DATE/TIME 9/24/96 1:08 INSTRUMENT HP03460 >GSMT3 138 BFBJUN28 50nG BFB -SAM %C -1 2uL 2Sppm BFBJUN28 SUB NRM ENH File; >GSMT3 Scan #: m/z Int. m/z 36.05 37.05 38.05 39.05 44.05 45.05 46.95 48.15 49.05 50.05 51.05 1.98 9.84 7.70 3.03 1.17 1.63 2.55 .77 6.19 26.69 7.76 52.05 54.95 55.95 57.05 60.15 61.10 62.10 63.00 68.10 69.00 70.10 138 Retn. time: 4.56 Int. m/z Int. m/z .47 .43 2.12 2.89 1.30 5.26 4.76 3.18 11.56 11.00 .48 72.20 73.00 74.00 75.00 76.10 78.00 79.00 80.00 80.90 87.00 88.00 .32 91.00 4.70 92.00 15.03 93.00 49.05 94.00 4.12 95.00 .45 96.00 2.39 96.90 .77 103.85 2.49 115.85 5.84 116.75 5.27 129.75 Int. m/z .52 172.60 2.50 174.00 3.53 175.00 10.24 175.90 100.00 176.90 6.62 207.05 .24 207.95 .31 209.05 .16 280.85 .27 281.15 .09 Int. .23 70.67 5.02 69.37 3.93 .17 .27 .34 .48 .13 32366.,IS THE AREA OF MASS 95 THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK APEX (SCAN 138.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING SCAN 127.00 WHICH IS PRIOR TO THE BFB PEAK. 201 DUP050308179 TfiTOL Tfir-J r.HROtlQTfipBJtt r.-- "OC* . 0 SLKJ-- BCf** ''JrJ3 C>0r: J B' ''" TIC 40 SO ISO Ifc'.O , . t I , l.'l-l....... . B ,l..,l -L .1--1--J..I....... I,..,U.I . ! c'-`i - 0f r ft 0 0O'* ?40C0 i ! c 00 00-` ioOUu-i % 1200 CH 40C1*:-. 4 V i ! i- . ...................ri-rr-rf-TT-v y* 4- 4 - 4 T i-s 5.f Data F lie: >GHTl : : B4 ' Quant Output Files Nam: BFBJSIN28 SOnG HFB Instrument ID: Mt s c : ~SHM %C "'I 2uL 25ppm BFHJUNVH ' 0 'r, y T1::FM HPO :*i <s h 0 Id tile: iDBFB::DB Title: TUNER Laot Co i xbr otiori: : Last Qua ! Tim"; : 9 2 :lti 18 19: 5t: Operator ID Quant Time Injected at SftH-982 SHIfSat Cltl : o? 98L924 28:59 202 DUP050308180 m/z 50 75 95 96 173 174 175 176 177 GC/MS PERFORMANCE STANDARD Broraofluorobenzene (BFB) Ion Abundance Criteria % Relative Abundance Base Appropriate Peak Peak 8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance 5-9% of mass 95 Less than 2% of mass 174 50-120% of mass 95 4-9% of mass 174 93-101% of mass 174 5-9% of mass 176 27.10 50.07 100.00 6.87 .42 70.19 5.01 68.55 4.52 27.10 50.07 100.00 6.87 .60 70.19 7.13 97.66 6.59 Injection Date: 09/24/96 Injection Time: 23:59 Data File: >GSPT1 Scan: 141 Status Ok Ok Ok Ok Ok Ok Ok Ok Ok INSTRUMENT HP03460 DUP050308181 3/90 CRITERIA ANALYSIS DATE/TIME 9/24/96 23:59 INSTRUMENT HP03460 >GSPT1 141 BFBJUN28 50nG BFB -SAM %C =1 2uL 25ppm BFBJUN28 SUB MEM ENH File: >GSPT1 Scan #: m/z int. m/z 36.05 37.05 38.05 39.05 40.05 44.05 45.05 47.05 47.85 49.05 50.05 1.61 9.65 7.51 2.77 .05 1.14 1.55 2.46 1.15 5.96 27.10 51.05 51.95 56.05 57.05 59.95 61.00 62.10 63.00 68.00 69.00 141 Retn. time: 4.59 Int. m/z Int. m/z 7.86 .21 1.23 3.11 1.09 5.21 3.84 3.04 10.57 9.93 70.00 71.90 73.00 74.10 75.10 76.00 77.10 77.90 79.00 80.00 .90 .45 4.60 15.55 50.07 4.05 .44 .65 2.12 .87 80.90 81.90 86.90 88.00 92.00 93.00 94.00 95.00 96.00 116.95 Int. m/z 2.30 118.95 .60 147.90 4.96 172.80 5.73 174.00 2.63 175.00 3.26 175.90 9.65 176.90 100.00 206.95 6.87 208.05 .54 281.15 Int. .32 .20 .42 70.19 5.01 68.55 4.52 .95 .61 .74 31066.,IS THE AREA OF MASS 95 THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK APEX (SCAN 141.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING SCAN 130.00 WHICH IS PRIOR TO THE BFB PEAK. 2G4 DUP050308182 TOTAL ION CHROMATOGRAM Data File: >IGKT2::D2 Quant output File: *IGKT2::D7 Name: BFB 2uL 50ng BFB Instrument ID: HP03046 Misc: -SJL %C -1 2uL (25ppm) BFBJUN28 Id File: IDBFB::DB Title: Last Calibration: : Last Qcal Time: <none> Operator ID: SJL-176 Quant Time : 960820 20:01 Injected at: 960820 19:52 20 DUP050308183 m/z so 75 95 96 173 174 175 17 6 177 GC/MS PERFORMANCE STANDARD Bromofluorobenzene (BFB) Ion Abundance Criteria 8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance 5-9% of mass 95 Less than 2% of mass 174 50-120% of mass 95 4-9% of mass 174 93-101% of mass 174 5-9% of mass 176 % Relative Abundance Base Appropriate Peak Peak 26.46 55.31 100.00 7.23 0.00 56.57 4.49 55.49 3.83 26.46 55.31 100.00 7.23 0.00 56.57 7.93 98.10 6.90 Status Ok Ok Ok Ok Ok Ok Ok Ok Ok Infection Date: 08/20/96 Injection Time: 19:52 Data File: >IGKT2 Scan: 133 INSTRUMENT HP03046 206 DUP050308184 3/90 CRITERIA ANALYSIS DATE/TIME 8/20/96 19:52 INSTRUMENT HP03046 >IGKT2 133 BFB 2uL 50ng BFB -SJL %C =1 2uL (25ppm) BFBJUN28 SUB NRM ENH File: >IGKT2 Scan #: m/z Int. m/z 35.95 37.05 38.05 39.05 44.05 44.95 48.05 1.40 7.SO 7.01 .72 .30 1.09 .33 49.10 50.10 51.10 56.00 57.10 59.90 61.00 133 Retn. time: Int. m/z Int. 6.32 26.46 7.94 .94 4.10 1.13 5.66 62.10 63.10 68.00 69.05 73.05 74.05 75.05 5.63 3.70 12.49 11.70 5.14 17.26 55.31 4.50 m/z 76.05 79.05 86.95 88.00 92.00 93.10 94.10 Int. m/z 4.71 2.79 4.68 3.74 2.33 4.04 11.09 95.10 96.10 174.00 175.00 176.00 177.00 Int. 100.00 7.23 56.57 4.49 55.49 3.83 18754. IS THE AREA OF MASS 95 THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK APEX (SCAN 13 3.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING SCAN 123.00 WHICH IS PRIOR TO THE BFB PEAK. A DUP050308185 TOTCtl TON CHROHOTOSRfiM Bata Files > 1S2JT1: :D2 Quant Output File! ''ISJT1::D7 Name: BF-tJ 2uL 50ng Bf B instrument IDs HP03U46 nisc: ~Sn %C = 1 2uL (25ppm) BFB0UN28 id File;, lDBF 8: :OB f 11 1 e : Last Calibration! : Last Qcal Time: <none> Uperator lu: SftF1=9B3 Buant Time : 960919 06:19 Injected at: 96CJ919 06:10 DUP050308186 m/z 50 75 95 96 173 174 175 176 177 GC/MS PERFORMANCE STANDARD Bromofluorobenzene (BFB) Ion Abundance Criteria % Relative Abundance Base Appropriate Peak Peak 8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance 5-9% of mass 95 Less than 2% of mass 174 50-120% of mass 95 4- 9% of mass 174 93-101% of mass 174 5- 9% of mass 176 26.90 57.89 100.00 6.63 0.00 57.99 4.84 56.13 3.93 26.90 57.89 100.00 6.63 0.00 57.99 8.35 96.79 7.01 Injection Date: 09/19/96 Injection Time: 06:10 Data File: >ISJT1 Scan: 137 Status Ok Ok Ok Ok Ok ok ok Ok Ok INSTRUMENT HP03046 to DUP050308187 3/90 CRITERIA ANALYSIS DATE/TIME 9/19/96 6:10 INSTRUMENT HP03046 >ISJT1 137 BFB 2UL 50ng BFB -SAM %C *=1 2uL (25ppxa) BFBJUN28 SUB NRM ENH File: >ISJT1 Scan #: xa/z Int. m/z 36.05 37.05 38.05 39.85 43.95 44.95 49.10 1.72 8.41 4.20 .33 .92 1.16 6.69 50.10 51.10 57.10 60.00 61.00 62.00 63.10 137 RetH. time: Int. m/Z Int. 26.90 8.16 3.70 .94 6.44 5.69 4.01 68.00 69.05 73.05 74.05 75.05 76.05 76.85 13.41 12.12 5.37 18.19 57.89 5.58 .37 4.54 m/z 78.95 80.95 86.95 88.00 92.00 93.00 94.00 Int. m/z 3.04 95.10 3.70 96.10 3.70 174.00 3.95 175.00 2.81 176.00 4.50 177.00 12.23 Int. 100.00 6.63 57.99 4.84 56.13 3.93 20955.,IS THE AREA OF MASS 95 THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK APEX (SCAN 137.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING SCAN 126.00 WHICH IS PRIOR TO THE BFB PEAK. MJL DUP050308188 TOTAL ION CHROHRTOGRAH__________________________________________________ . File >ISOTi 35.0-300.0 amu. BFB 2uL 50ng 8FB ~TLN 7.C 1 uL <5f Data File: >IS0T1::D4 Quant Output File: AISOTl::D7 Name: BFB 2uL 50ng BFB Instrument ID: HP03046 Misc: -TLN %C ==1 2uL (25ppm) BFBJUN28 Id File: IDBFB::DB Title: Last Calibration: : Last Gcal Time: <none> Operator ID: TLN-262 Quant Time : 960924 11:18 Injected at: 960924 11:10 2: DUP050308189 m/z 50 75 95 96 173 174 175 176 177 GC/MS PERFORMANCE STANDARD Bromofluorobenzene (BFB) Ion Abundance Criteria % Relative Abundance Base Appropriate Peak Peak Status 8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance 5-9% of mass 95 Less than 2% of mass 174 50-120% of mass 95 4-9% of mass 174 93-101% of mass 174 5-9% of mass 176 21.53 49.65 100.00 7.04 1.14 64.17 4.90 62.76 4.21 21.53 49.65 100.00 7.04 1.78 64.17 7.63 97.80 6.71 Ok Ok Ok ok Ok Ok ok Ok ok Injection Date: 09/24/96 Injection Time: 11:10 Data File: >IS0T1 Scan: 76 INSTRUMENT HP03046 DU P050308190 3/90 CRITERIA ANALYSIS DATE/TIME 9/24/96 11:10 INSTRUMENT HP03046 >IS0T1 76 BFB 2uL 50ng BFB -TLN %C =1 2uL (25ppm) BFBJUN28 SUB NRM ENH File: >IS0T1 Scan # m/z Int. m/s 36.05 37.05 38.05 39.15 44.05 45.05 46.95 49.05 50.05 51.05 1.78 6.79 5.56 2.60 .52 1.05 .71 4.93 21.53 6.36 55.05 56.05 57.10 60.00 61.10 62.10 63.00 67.10 68.00 76 Retn. time: Int. m/z Int. 1.58 1.90 2.69 1.29 4.52 4.27 2.77 .56 10.97 69.00 70.10 73.00 74.00 75.00 76.00 77.00 78.00 79.00 10.33 .77 4.07 14.61 49.65 3.97 .65 .21 2.00 4.38 m/z 81.05 81.95 83.15 87.05 87.95 91.05 92.05 93.05 94.05 Int. m/z 2.45 95.05 .62 96.05 .40 116.80 3.65 142.95 3.66 172.95 . 44 173.95 2.27 174.95 3.52 175.95 10.61 176.95 Int. 100.00 7.04 .16 .47 1.14 64.17 4.90 62.76 4.21 29721..rS THE AREA OF MASS 95 THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK APEX (SCAN 76.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING SCAN 67.00 WHICH IS PRIOR TO THE BFB PEAK. fj JLO DUP0 50308191 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract: VBLKG24 Lab Code: LANCAS Case No.: ____ SAS No.: SDG No.: Matrix: (soil/water) WATER Lab Sample ID: VBLKG24 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >GSPB1 Level: (low/med) LOW Date Received: _______. % Moisture: not dec. Date Analyzed: 09/25/96 GC Column: DB624 ID: 0.53 Dilution Factor: l.o Soil Extract Volume: (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3----------------- Chioromethane 75-01-4-------- --------Vinyl Chloride 74-83-9------------------ Bromomethane 75-00-3------------------ Chloroethane 75-35-4------------------ 1,1-Dichloroethene 67-64-1------------------ Acetone 75-15-0------------------ Carbon Disulfide 75-09-2------------------ Methylene Chloride 75-34-3-------------------1,1-Dichloroethane 540-59-0--------------- 1,2-Dichloroethene {total) 78-93-3----------------- 2 -Butanone 67-66-3------------------ Chloroform 107-06-2---------------- 1,2 -Dichloroethane 71-55-6--------- --------- 1,1, l-Trichloroethane 56-23-5------------------ Carbon Tetrachloride 71-43-2------------------ Benzene 79-01-6----------------- Trichloroethene 78-87-5----------------- 1,2 -Dichloropropane 75-27-4----------- ------- Bromodichloromethane 10061-01-5------------ cis-i,3-Dichloropropene 10061-02-6------------ trans-1,3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane 124 -48-1------------- Dibromochloromethane 75-25-2------------------ Bromoform 108-10-1--------------- 4 -Methyl-2 -Pentanone 108 -88-3--------------- Toluene 127-18-4---------------- Tetrachloroethene 591-78-6---------------- 2-Hexanone 108-90-7---------------- Chlorobenzene 100-41-4-- --------- Ethylbenzene 1330-20-7-------------- Xylene (total) 100-42-5---------------- Styrene 79-34-5------------------ 1,1,2,2-Tetrachloroethane 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FORM I VOA OLM03.Q DUP050308192 =:o ooo-; J -i 400 ve il*: 200000-' ii i . Ki'nnr.4 i >000*V; -Hit eoooc-j i i 40000-j j 1 s l', ll I<SIti [I j......:---. 4 -a 3 3i? ii-- `S JL 17 55 J i* n i !iw ;-....-------r--T--1-- 6 8 10 x> c Ca\J 1 fc m X. w - . i i 16 16 0 L)-, u Fi ie: > GSPUl : ; DP Norris i JBLK 02 4 OBLK.02 4 MiOC ! -ir, @WL =1 + > Qaant Output F; le ; instrument ID : 831. HR "tlSHBI : ;FK p p n 'i c.; jj I d F i le ! I 9 D * DB T i 1 e : .3 4 U tiJa t <sr /Mncl Sot l' ID F ilc ii a s *t Cal ibrat.ion : 95 i 2 O'? 01:53 f or Inst. HF 0348 Last- Qcal Ti me : 360925 0 Op;..: r a lf.r ID: Quant i' i me ; i, I ; Jj 5 ted at : SRM~983 9 6 U 9 2 5 01 : 29 9fe'i!25 01 : 04 oi Si-1 DUP050308193 Kh *">]?! Ope rotor ID: SflH-W83 Output File : 'NSSHHl : s FM Data Fi 1 : >(..3PB1: : 1)8 Marne : UHLK.G24 UFUCG24 Hiac i ~Sf4M %C jctlilL "1 + > Oaarit Kev 1 *K396 2 68 IFlPi &5 *5 T*' * : .riant Tme : In.jester a r - Dilut i on Factor Inst ruiner.t I !: W ... : V 1 1 ;f*y -j : ID Fxif?: IR4390 : iDF Title: 3,'SO Uater/Med Soil ID File Last Ca!lbrationt S5I207 01:59 for Inst . HP 03 46 0 Last ^JjC-Ctl. *1 i Tii r2 ! 9- ;?y2b Compound 1) 15 : 17) 29 ) 31) 40 5 rrBroTnochloroTnethane 1 ;.V-Diohloroethane-d4 *1p4~Difluorobenzene *Cb 1 o r o be. ns e ne - d.5 Toluene-dB 4- Hromot lanraberisene * Compound xs ISTD R .T. Q j on 9.50 1U . 42 11.10 15.37 13,27 17.09 128 . 0 65 U 114.0 117.0 8B . 0 95 0 Fir ea 472 73 7120b 18762 0 153010 162,-48 137840 vpnc 3 lj . Ij 0 *4 o b 3 1j . 0 0 5 ' ' 0 0 50 . 09 5 : 36 lO i.(!| i.O O-i ~s 4 DUP050308194 Lancaster Laboratories Quantitation keport-GC/MS Ooiatiies LUI: KJ JH JL.K -3 - -! r- File: -SSPB1 Injected: 01:04 09/25/96 Sample: UBUCG24 UBLKG24 Dilation Factor: 1.0 Initial De luTie/llt..: .5.0 Standard: AGSPSl Inst. H8U34t;u Batch: G9S2681HA Final Dolaue/Ut.: 5.0 Method-: 7156 Matrix/Ieuei: liL. Blank; f Internal Standards R.T. (+/-RT) Scan Qion Area(*/-tArea) Cone. QC Fiao Con: Units * ug-'L 1. Bromochloromethane T'. 1.4-Dirluorobenzene 29 Chiarobenzene-d5 t = r e t e n t io n t ime OUT OF RANGE 3.5014.011.2) 644 128 47273(-13! 50.00 11.101.OB/?) 781 114 187820(-23! 5ll. 0U 15.371.0077) 1148 117 153Q10C-22) 50.00 * - INTERNAL STANDARD AREA OUT OF RANGE NC * NOT ABLE TO CALCULATE--NO STANDARD. S Surrogate Standards R.T. (+/-BET) Scan Qion SSSSS5S 15. l,2-Dichloroethane-d4 10.421.00031 723 S5 31. Totuene-dfl 13.275.00U5) 968 98 40. 4-Broaofluorobenzene 17.03(-.000) 1296 35 } = RELttTiOE RETENTION TIME OUT OF RANGE * = *RC OUT OF RANGE Area Cone. .%Rec. Q 71206 46.36 33 162748 50.09 100 132840 51.38 1A t? v D = SURROGATES DILUTED OFT NC = COULD HOT CALCULATE S Target Compounds R.T.(+/-8RT.1 Scan Qion Area Cone.A Conc.B Cone. Blank Q Quantitation Limit 2. Chloromethane 3- U-.nyJ Chloride 4. SroiBMiethane 5. Chlornethans S. 1,1-Bichioroethene 7. Acetone 8. Carbon Disulfide 3. Methylene Chloride 11. 1,1-Dichlaroethane 12. 1,2-Dschloroethene (total) 13. 2-Butanone IT. Chloroform 16. 1,5-Dichloroethane 18. 1.1,1-Trichloroethane 19. Carbon Tetrachloride 20 Benzene 21. Trichloroethene 22. 1,2-Biehioropropane 23. Bromodichioromethane 29. cis-lj3-Cichloropropene 25. trars-l,3-Diehloropropene 28. 1 >1 ,2-Tnchloroethane ------------------------------------- --------------------- :---------------------------------------------------------------------------------------------------*---------------- --------------------------------------------------------------------------- ----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- --------------------------------- -------------------------------------------------------------------------------------------------------------------------------- 18 18 ID id 10 1U 10 18 10 10 10 1C 30 111 10 111 10 111 10 10 10 111 ft RAW CONC. 8 = CONC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CAL. RANGE * SVi.ftTJ.OE RETENTION TIME OUT OF RANGE Lab Chronicle: Ent. by PAGE 1 OF 2 Uer. bu ' asir-*4: ri-- DUP050308195 Lancaster Laboratories Quantitation Heport-GCvMS Uoiaiiies LLU: U'fciLK File: AGSPB1 Injected: 01014 119/25/96 Sample: (JBL1CG24 UBUCG24 Dilution Factor: 1.0 Initial Uoiurae/(i)t.: 5.0 Standard: AGSPS1 Inst. HP!i346C Batch: G362S8lftft Final Uolame/ldt.: 5.0 Method: 71Sfc Matm/Ievei. li!!, Blank: I Target Compounds 27. Dibromochloromethane 29. Bros form 30. 4-Methyi-2-Pentanone 32. Toluene 33. Tetrachloroethene 34. 2-Hexanone 35. Chlorobenzene 30. Ethylhensane 38. Xylene (total) 33. Styrene 41. 1,1,2,2-Tetrachloroethane Cone. R.T.f+/-RRT) Scan Qion Area Cone, ft Conc'.B Blank 0 issssssssssssssssssssaKzassnsaiasirssasssavesseesBteeesssssseassssissssssssasess' Quantitation Limn 10 11! IS 10 10 10 IB 113 in ft = Bull C0NC. B = CUNC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CftL. RANGE I * RELATIVE RETENTION TIME OUT OF RANGE Lab Chronicle: Erst, by Uer. by Analyst: A Auditor: .Date: Date: PAGE 2 OF 2 DUP050308196 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABS Contract: VBLKI93 Lab Code: LANCAS Case No.: _______ SAS No.: SDG No.: Matrix: (soil/water) WATER Lab Sample ID: VBLKI93 Sample wt/vol: 5.0 (g/mL) ML Lab Pile ID: >ISJB2 Level: (low/med) LOW Date Received: . % Moisture: not dec. _______ Date Analyzed: 09/19/96 GC column: DB624 ID: 0.53 (mm) Dilution Factor: l.o Soil Extract Volume: _______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L O 74-87-3------------------ Cb.lorometh.ane 75-01-4------------------ Vinyl Chloride 74-83 -9----------------- Bromomethane 75-00-3------------------ Chloroethane 75-35-4-------------------1,1-Dichloroethene 67-64-1------------------ Acetone 75-15-0------------------ Carbon Disulfide 75-09-2------------------ Methylene Chloride 75-34-3---------- -------- 1,1-Dichloroethane 540-59-0-------------- 1,2-Dichloroethene (total) 78-93-3------------------ 2-Butanone 67-66-3------------------ Chloroform 107-06-2---------------1,2 -Dichloroethane 71-55-6----------------- 1,1,1-Trichloroethane 56-23-5------------------ Carbon Tetrachloride 71-43-2------------------ Benzene 79-01-6------------------ Trichloroethene 78-87-5------------------ 1,2-Dichloropropane 75-27-4----------------- Bromodichloromethane 10061-01-5----------- cis-l, 3-Dichloropropene 10061-02-6------------ trans-1,3-Dichloropropene 7 9 -00-5------------------ 1,1,2 -Trichloroethane 124-48-1---------------- Dibromochloromethane 75-25-2----------------- Bromoform 108-10-1--------------- 4-Methyl-2-Pentanone 108-88-3---------------- Toluene 127-18-4--------------- Tetrachloroethene 591-78-6--------------- 2 -Hexanone 108-90-7--------------- Chlorobenzene 100-41-4---------------- Ethylbenzene 1330-20-7-------------- Xylene (total) 100-42-5---------------- Styrene 79-34-5------------------ 1,1,2,2-Tetrachloroethane 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FORM I VOA OLM03.QwI9 DUP050308197 TfiTcu. rnM cHBOMaroecflH Data File: >ISJB2: : D4 Quant Output File: /s ISJB2: : D7 Name: U8L.K193 UEJLKI93 instrument ID: HP03046 ruse: ~TLH WC %C = 1 +> #1962631AA &5 *5 id File: 1A6390: :L>B 'lit let 3/90 SOU Water/Med Soil ID File for Inst. HPQ3046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLN-262 Quant Time : 960919 09:09 Injected at: 960919 08:44 09f DUP050308198 QUANT REPORT Uperator 1U: Tl .Nt -262 Output File: 1S3B2 5 : D? Uat a File: >ib JB2 : :U4 Name: UBL.KI93 UBLKI93 msc: ~1LN 1QL %L =1 +> Quant #196263lRft &5 Kev: *5 7 Quant Time: Injected at: Di lut ion Factor: Instrument ID: Page 1 960919 09:UV 960919 OB:44 1 . uuuuu HP03046 1L> File: IA639Q::DB litie: 3^90 BUUI Weter/Med Boil ID File For Inst. HH03U46 Last Calibration*. 951122 10:44 Last Qcal Time: 960919 06:34 Compound 1? 15 ; 191 29) 31) 40) *tiromocti lo remethane 1 ,2-DicFi 1 oroetFiane-d4 *1,4-Uifluorobenzene *Ch1orobenzene~d5 loiuena-d8 4-Bromofluorobenzene * Compound is IBID R.T. Q ion B. 35 128 . U 9. 30 65.0 10. 02 114.0 14. 33 117. 0 12. 22 98.0 16. 05' 95.0 Area 59611 86141 163966 121256 143591 98437 Cone Units 80.00 47.19 50. 00 50.00 50.69 49.05 UC2 C UtC'L US/L UL/L LIG/L ue/L q V3 89 88 85 95 78 OOf*iHij DUP050308199 Lancaster Laboratories Uuantitation Report-GC/MS Volatiles LLl*: UBL.K 193 T L_M I-lie: AiSJU2 Injected: 08:44 09/19/96 Sample: VBLK193 VBLK193 L)i lution factor: 1.0 initial Volume/Dt.: 5.0 Standard: A1SJS1 inst. HP03046 Batch: 1962631AA Final Volume/Ut.: 5.0 Method: 7156 Matrix/level: tIL Blank: t internal Standards R.l. HART) Scan Ition AreaHV-Jifirea) Cone. UL Flag Lone Units = ug/L asse**KB*aa^maaa!**aTOm*Kaa* e***aa* **a W** **** *^******** ****w** * *******m***********st,,**s**t!ss*:a*"*,s, 1. Bromoehloromethane 8.3541.0159) 563 128 396111 29) 50.06 17. 1,4-Difluorobenzene 2V. Cblorobenzene-d5 10.021.0026) 14,53(-.001) 706 107? 114 117 1639661 27) 1212561 28) 50.00 30.00 * = RETENTION TIME DUT OF RANGE * * INTERNAL STANDARD AREA OUT OF RftRGE NC NOT ABLE TO CALCULATE--N0 STANDARD. $ Surrogate Standards K.T. H/-RRI) Scan Dion Area Cone. Wise. a >s9gssKiiniu>a9:uunntniannunuin>iian>3ninninimnn>un>iun>ciKi::uniE9>:an>nnuni: 13. l,2-l)ichloroethana-d4 9.2951-.U02) 644 65 31. Totuene-d8 12.22l.006S) 896 98 40. 4-Broaafiuorobenzene 16.05t-.000) 1225 95 4 - RELATIVE RETENTION TIME BUT OF RANGE * * 5SREC OUT OF RANEE 86141 47.19 94 145591 50.69 101 98437 49.05 98 D - SURROGATES DILUTED OUT NC COULD NOT CALCULATE * target Compounds 2. Ctiloromethane 3. Vinyl Chloride 4. Broisoaeihane 9. Chlornethane 6. 1,1-Dichtoroethene Acetone li. Carbon Disulfide V. Methylene Chloride 11. 1,3-Dicfttoroethane 12. 1,2-Dichloroethene (total) 15. 2-tlutanone 14. Chloroform 16. 1,2-Dichloroethane IB. 1,1,1-Trichloroethane IV. Carbon letrachloride 211. tlanzene 21. Irichloroethene 22. 1,2-Dtchloropropane 25. Bromodichlorousthane 24. cis-l,3-Otchioropropane 22. trans-l,3-Oichloropropene 26. 1,1,2-Trichloroethane R.T.H/-RKI) Scan Qion Area Cone.A Cone.8 Lone. Blank U Uuar.t l tat lor. Limit 10 10 1(1 10 iu 10 ID 10 10 18 10 10 10 10 10 10 10 10 10 10 111 10 A > RfM CONC. 8 CONC. MULTIPLIED BY DILUTION FACTOR E - CONC. OUT OF CAL. RANGE 4 RELATIVE RETENTION TIME OUT OF RANGE Lab Chronicle: .Ent, by PAGE 1 Of 2 Oer. by___QMSiS1-Ji DUP050308200 Lancaster Laboratories Quantitation Report-GC/MS Uolatiles LLI#: UB1__K 193 .M Fiie: A1SJB2 injected! U8i44 09/19/56 Sample: UBCKI95 UBLK193 Uilution l-actor: 1.8 Initial Uolume/Ut.: 5.0 Standard: A1S3S1 Inst. HP03046 Batch! I962631ftft Final Itolime/Ut.: 5.0 Method: 7156 ttatrix/level! UL Blank: t target Compounds R. I.IV-RRI) Scan ctee **s^sesstsHss*a:tta**ie*** *atamawsMarassamsaiat*ataeatwa*M*ai 27. UibroiFiOChSoroifiethane ------------------------------------ Qion Brea Cone.ft Conc.B Coni:. Blank Q Quantitation Limit MtBWUSMtlMftffmMSIUtltlHUmnUIRRXaMSCSSHBBlS -------------------------------------------------------- Ill 28. uroaoform 38. 4-rtetnyl-2-P,entanone 32. toluene Ji. letrachloroethene 34. 2-Haxanone 35. Chlorobenzene i6. Lthytbenzene ill. Xylene (total) i9. Styrene 41. l,l,2,2-t8trachloroethsne ------------------------------------ ------------------------------------ 1U ------------------------------------ 10 -------------------------------- --- 10 ---------------- --------------------------------- ------------------- 10 10 ------------------------------------ 10 ------------------------------------ 10 -------------------- -------------- id ------------------------------------ 10 aaSBBB*inSBS1IBaBliBSKXBBBtaaCBBBBBEaRC8B*BRBleBB*BBBSXaaaSaSXasaXBBSBBBaBBC3 RAR CONC. B = CUMC. MULT1PLIED BY DILUTION FACTOR E = CUiC. OUT OF CAL. RANGE T = RELAT1UE RETENTION TINE UUT OF RANGE Lab Chronic la: JEnt. by Bar. by Analyst! Auditor: ..... ---------------------------- Date; _____4//q/n, ________________________.__________2kSO*t>: ?/lf/& PAGE 2 OF 2 23 DUPO 50308201 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract: VBLKI95 Lab Code: LANCAS Case No.: _______ SAS No.: SDG No. Matrix: (soil/water) WATER Lab Sample ID: VBLKI95 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >ISOB3 Level: (low/med) LOW Date Received: _______. % Moisture: not dec. _______ Date Analyzed: 09/24/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0 Soil Extract Volume: _______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3----------------- Chloromethane 75-01-4------------------ Vinyl Chloride 74-83-9------------------ Bromomethane 75-00-3------------------ Chloroethane 7 5-3 5-4---------- -------- 1,1-Dichloroethene 67-64 -1----------------- Acetone 75-15-0------------------- Carbon Disulfide 75-09-2------------------ Methylene Chloride 75-34-3----------------- 1,1-Dichloroethane 540-59-0---------------- 1,2-Dichloroethene (total) A 78-93 -3------------------ 2-Butanone 67-66-3------------------ Chloroform 107-06-2--------------- 1,2 -Dichloroethane 71-55-6------------------ 1, If 1-Trichloroethane 56-23-5------------------ Carbon Tetrachloride 71-4 3 -2----------------- Benzene A 79-01-6------------------ Trichloroethene 78-87-5-----------------112-Dichloropropane 75-27-4----------------- Bromodichloromethane 10061-01-5------------ cis-1,3-Dichloropropene 10061-02-6-----------trans-1,3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane 124-48-1---------------- Dibromochloromethane 75-25-2----------------- Bromoform 108-10-1------------ --4 -Methyl-2-Pentanone 108-8 8-3---------------- Toluene 127-18-4---------------- Tetrachloroethene 591-78-6--------------- 2 -Hexanone A 108-90-7----------------- Chlorobenzene 100-41-4---------------- Ethylbenzene 1330-20-7-------------- Xylene (total) A 100-42-5---------------- Styrene 79-34-5---------- --------1,1,2,2-Tetrachloroethane 10 u 10 u 10 u 10 u 10 u 10 u 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 U 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u FORM I VOA OLMQ3.0'*'* DUP050308202 T0TO!. TON CHROKPTOeRPM___________ ______ _____ File' >1 SOBS 35.0-300.0 *mu. VBLK195 WU<TW 400 800 "SUL SUL SC =1 > #] 1200 LSCfQOO*} i60ooo4 ft Data File: >IS0B3::D4 Quant Output File: ^1S0B3::D7 Name: UQLKi95 U8LK195 Instrument ID: HP03046 disc: "SJL $Wl *SC 1 +> #I96263lftB &5 *5 id File: 106390::DB Title: 3/90 SOUS Ufater/Med Soil ID File for Inst. HP03046 Last Lalibration: 991122 10:44 Last Goal Time: 96U924 12:50 Operator ID: SJL-176 Quant Time : 960924 16:07 Injected at: 960924 15:43 235 DUP050308203 QUANT REPORT Page 1 Operator- ID: SOL-176 Uutput FT let IS0B3: : D7 Data File: >ibUB3::U4 Name: UBLKI95 UBLKI95 ruse: "SOL jaJWL ssc *1 +> Quant #1962&31AB &5 Reu: *5 7 Quant Time: Injected at: Dilution Factor: Instrument ID: 960724 16: U > 960924 15:43 1 . UUUUU HPG3046 iU File: IAfc390::DB Title: 5790 SCj Q Water/'fled Soil ID File For Inst. HPD3046 Last Calibration: 951122 10:44 Last Qcal Time: 960924 12:50 Compound 1) l`>) 17) 27) 31) 4U) ^Bromochloromethane 1,2-Diehloroethane-d4 *1,4~0ifluorobenzene *Chlorobenzene-d5 loiuene-dQ 4-Bromof luorobenzene * Compound is 1CTD R.T. Q ion a. 19 9.13 9.85 14.18 12.06 15.90 128.0 65.0 114.0 117.0 98.0 95.0 Area 18B42 34766 y 3 21) 4 55305 65343 51399 Cone Un i t.s 50.00 47.72 50. UO 50.00 51.82 50.14 Ub/L UG/L LiG/L UG/L UG.'-'L UG7L q 97 95 82 9y 82 O DUP050308204 Lancaster Laboratories Quantitation Report-C/WS Uolatiles ILl*: t~*fc3L_K 195 GJI-- tile: AlSiJ)3 Injected: 15:4? (I9724/96 Sample: UBLK195 UBLK199 Dilution Factor: 1.0 Initial Volurae/Ut.: 9.0 Standard: 'HSIS13 Inst. HP03046 Batch: 19&2631AB Final Uolume/Ut.: 9.0 Method: 7156 Matrix/level: UL Blank: * internal Standards R. 1. 1+/-RO Scan Clion Areal*/-Sftrea> Cone. sss3ts*ssmtst*SB*stt*ss*3teas*ss*tsM*essB******s****s*************n*! QC Flag Lone Urats = uq/L 1. Bromochloromethane 8.187(.ai9i) 991 128 I8842(-39) 98.80 17. 1,4-Difluorobenzene 29. Chiorobenzene-db * = RETENTION TIME OUT OF RANGE 9.890C.0118) 694 114 73204C-413 90.90 14.181.0292) 1066 117 59389C-43) 90, BIS * * INTERNAL STANDARD AREA OUT OF RANGE 1NC - NOT ABLE TO CALQJLATE-NO STANDARD. * Surrogate Standards R.T. (*/-RRT) Scan Uinn Area Cone. XRac. U S3S8B8S8B88SS8SSBSS8*3E8888BaBBS3B98V8SB88SSXBBS3S8BWIC8BB8BB aBIBIBIXBBBBBBSBBBBIiaBBIBBflBBBBBS:XSBB8S8BaS8BSB8B88B8Sa8a3S8XaBBS8S 19. l,2-Uichloroetbane-d4 9.129(-.081) 632 69 31. Taluene-d8 12.U6C-.0I11) 8B4 98 4U. 4-Broiofluorobenzene 19.98(-.081) 1214 99 4 RELAT1UE RETENTION TIME OUT OF RANGE * SREC OUT OF RANGE 34766 47./2 95 69343 51.82 104 91399 50.14 luu D = SURROGATES DILUTED CUT NC - COULD NOT CALCULATE Cone. Quantitation * target Compounds R.T.(+/-RRT) Scan Uion Area Cone.A Conc.U Blank U Limit ssrsesssssses3&sse33S3BS3ss=B8BC88sae3>B3sr38aBisaxsskaaxa8Bsassss3SSBBBsxQS8V8assasasB3cc8Bi8s*seat:BSSSsssaa:asi:saDsssasss83Kaa3 2. Chloromethane -------------------------------------------------- :--------------------------------------------------------------------- 18 3. Vinyl Chloride ------------------------------------------ ----------------- ---------------------------------------------------------- 10 4. Bromom&thane 9. Chi or oe thane ----------------------------------------------------- ------------------------------------------------------:------------------------------- ---------------------------------------------------------------------------------------------------- 18 10 6. 1,1-Uichlorcethene 7. Acetone -------------------------------------------------------------------------------------------------------------------------------------------------- -------------------- ----------------------- 10 10 8. Carbon Disulfide ---------------------------------------------------------------------------------------------------------------- ---------------- 10 9. Methylene Chloride --------------------------------- *------------------------------------------------------------------------------------- 10 11. 1.1-Qichloroethane --------------------------------------------------- ;------------------------------------------------------------------- 10 12. 1,2-Dichloroethene (total) ---------------------------------------------------------------------- ii. 2-Butanone 14. Chloroform 16. 1,2-Uiehloroethane 18. 1,1,1-Iriehloroethane 19. Carbon tetrachloride 2U. Benzene 21. Irichloroethene 22. 1,2-Diehlorepropane 23. Broiriodi chloromethane 24. cis-l,3-D>chloropropene ----------------------------------------------------------------------------------------------------------------------------- 10 2b. trans-1 fj-U3Chloropropene ---------- ------ ---------------------- ------ -- ------------------------------ ---------------------------------------- 18 26. 1,1,2-1richloroethane ----------------------------------------- --------------------------------------------------------------------------------------- 10 88SSaaB3BX3SeBBBB88eSSSSBSSCSB3S::afiSSSBBS83SSBtt8SSS88SSaBasSSBSBS!:XBSS8SSSSSSSS&SBSSSSS:3SSSSSSSSaSSZZSSBSSSaS&SSSSSSEBtESSSSBSSSS A = RAbJ Ct)C. B = COtC. MULTIPLIED BY DILUTION FACTOR E EffiiC. CUT OF CAL. RANGE * - RELATIVE RETENTION TIME OUT OF RANGE tab Chronicle: Ent, by *r. by PAGE 1 UF 2 DUP050308205 Lancaster Laboratories Uuantstation Report-GC/MS Uolatites LL1#: UBI-- K 1 95 &L3 L_ File: "ISUtSi injected: 15:43 09/24/96 Sample: UBLKl95> UBUCI95 Uilution tactor: 1.0 Initial Voluma/Ut.: 5.0 Standard: 'V1SUI3 Inst. HP03046 Batch: 1962631AB Final Uolurae/ttt.: 5.0 Method: 715a Matrix/level: UL Blank: target Compounds R. T.(V-HRT) Scan Oion Brea Lone.ft lonc.B Cone. Blank U Quantitation Limit 2/. Uibromochloromethane 2B. brotaofora 3U. 4-Methyl-'2-l:'entanane 37. Toluene 33. ietrachloroethene 34. 2-Hexanone 35. Chlorobenzene 36. Ethylbenzene 3B. Xylene (total) 39. Styrene 41, 1,1,2.2-Tetraehloraethane ss***tsseaassBss*ass*sa*iB3*i A fifty tatc. b = LUNC. MULTIPLIED BY D1LUT1UN 1-ftClUR 1U 10 J.U 10 1U 10 1U 10 lu 10 1U * CUNC. OUT UF CftL. RANGE * = RtLftUUE REiENUUN TIME UUT 111 KftNUt Leb Chronicle: Ent. by 228 DUP050308206 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER LABS Contract: BRS3DMS Lab Code: LANCAS Case No.: _______ SAS No.: SDG No.: Matrix: (soil/water) WATER Lab Sample ID: 2583209 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >ISJ12 Level: (low/med) LOW Date Received: 09/18/96 % Moisture: not dec., _______ Date Analyzed: 09/19/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0 Soil Extract Volumes _______ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87-3---------------- -Chloromethane 75-01-4------------- --Vinyl Chloride 74-83-9---------- -------- Bromomethane 75-00-3------------------ Chloroethane 75-35-4------------------ 1,1-Dichloroethene 67-64-1------------------ Acetone 75-15-0------------------ Carbon Disulfide 75-09-2------------------ Methylene Chloride 75-34-3----------------- 1,1-Dichloroethane 540-59-0--------------- 1,2-Dichloroethene (total) 78-93-3------------------ 2-Butanone 67-66-3------------------ Chloroform 107-06-2--------------- 1,2-Dichloroethane 71-55-6----------------- 1,1,1-Trichloroethane 56-23-5------------------ Carbon Tetrachloride 71-43-2---------------- -Benzene A 79-01-6------------------ Trichloroethene 78-87-5------------------ 1,2-Dichloropropane 75-27-4----------------- Bromodich1oromethane 10061-01-5------------ cis-1,3-Dichloropropene 10061-02-6----------- trans-1,3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane 124-4 8-1---------------- Dibromochloromethane 75-25-2------------------ Bromoform 108-10-1--------------- 4 -Methyl-2 -Pentanone 108-88-3---------------- Toluene 127-18-4---------------- Tetrachloroethene 591-78-6---------------- 2-Hexanone 108-90-7---------------- chlorobenzene 100-41-4---------------- Ethylbenzene 1330-20-7----------- Xylene (total) 100-42-5------------Styrene 79-34-5---------------1,1,2,2-Tetrachloroethane FORM I VOA 10 u 10 u 10 u 10 u 59 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 58 57 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 55 10 u 10 u 52 10 u 10 u 10 u 10 u Q9Q OLM03.0 DUP050308207 TClTOt TOW CHROMOTOSRRh Data File: >1SJ12::D3 Quant Output File: AISJ12::D7 Name: BRS3DNS 25832U9 instrument ID: HP03046 flisc: ~TLN @WL %C -1 + > #I962631AA $'"ISJB2 &5 *5 id File: ift6390:sDB Title: 3-'90 SOW Water/Med Soil ID File for Inst. HPQ3Q46 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLN-262 Quant Time : 960919 11:59 Injected at: 960919 11:35 OU DUP050308208 QUANT REPORT Paae 1 Uperator ID: TLN-262 Output File: /SIS012::D7 Data File: >iSJ12::D3 Name: BRS3DMS 2583209 M1 sc: ~TLN (ajUIL %C = 1 + > Quant Reu: #!962631Aft S'"1SJB2 7 Qusnt Tlme: Injected at: Dilution Factor: Instrument ID: &5 *5 960919 11:59 960919 11:35 1. U 0 0 U 0 HP03 046 ID File: IA639G::DB Title : 3290 SOU Water/fted Soil ID File for Inst. HP03046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 1) 6) 15) 17) 20) 21) 29) 31) 32) 35) 40) *8roraochloromethane 1,1-Dichloroethene 1,2-Dichtcroethane-d4 *1,4-Difluorobenzene Benzene Trich loroethene *Chlorobenzane-d5 To luene-d8 To luene Chlorobenzene 4-Bromofluorobenzene * Compound is ISTD R. T. Q ion 8.36 128.0 4.67 96. 0 9.30 65.0 10.02 114.0 9.40 78.0 10.42 130.0 14.32 117. 0 12.22 98.0 12.31 91. 0 14.36 112.0 16.04 95.0 Area 39 U18 46615 84080 162767 137U58 65756 121783 144561 156760 115255 98289 Cone Units 50.00 UbC'L 58.99 UG7L 46.76 U&/L 50.00 UG7L 57.81 UQ7L 56.61 U67L 50.00 US7L 50.11 UG/L 54.80 U/L 52.59 UG7L 48.77 UG7L q 91 92 89 87 88 84 83 96 98 84 76 231 A DUP050308209 Lancaster Laboratories Quantitation Report-GC/MS Uolatiles LLI*: 2 5 8 3 2 0 9 File: AiSvJ12 Lmeeted: 11:35 89/19/96 Sample: BRS3DMS 2583289 Dilution Factor: 1.0 Initial Dolume/Ut.: 5.0 Standard: "tSJSl Inst. HP03046 Hatch: 1962631fift final Volume/Ut.: 5.0 rtethod: ?156 ttatrix/level: UL Dlank: AlSJtri Internal Standards R.T. 1+/-RTJ Scan Dion ftrea(+/-Sflrea) Cone. UL flag Lone Units * ug-'L ==*333diaa3BSKacasms3essaassa**XBUStsaBB33Ks3Bars*n3sssssasssmsxssisssainBSCEBXsm*sssaftassBxmBSKsaKBKaiEBxett2333=3saKaBBxasaisBB3 DUP050308210 Lancaster Laboratories fluentitation Report-GC/ttS Volatiles LLl*i 2 9 e 3 2 Q 9 TLN File: A(SJ12 Injected: 11:35 05/19/% banpla: BRS3BHS 2583209 Dilution Factor: 1.0 Initial Volume/tlt.: 9.B Standard: A1S<1S1 Inst. HPBJ046 Batch: 1962631AA Final Valuae/Ut.: 5.0 Method: 7156 Matrix/level: UL Blank: ALSJH2 $ larget Laapeunds R.T.l*/-RRI) Scan Qion Area Conc.fi tone.B Cone. Blank U Quantitation Limit 2/. Dibromochioroffiethane 28. Bromoform 3D. 4-ftet by l-2-Fentanone 32.. Toluene 12.311 .0811 908 91 156760 54.808 55 yj - letraEhloroethene 34. 2-Hexanone 35. Chlorobenzene 14.361 .800) 1084 X12 115255 52.695 52 36. Ethylbenzene 58. Xylene ltotal! 59. Styrene 41. 1,1,2,2-Tetrachloroethane 8BXSS8SS8eKSSSS8*BaSSBas882Xa8SttSI88>MMSM8B8MmmimCet8laMUSMatmnSSSQUBnn8SS8aSlKSBBW in 10 10 10 10 10 10 10 10 10 111 fl RflW CUNC. B * CUNC, RULl 1PL1ED BY DILUTION FACIUR t - CUNC. OUT IF CAL. RANGE * RELATIVE RETENTION TIME OUT OF RANGE lab Chronic leJ _nt. by DUP050308211 1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABS Contract: BRS3DMSD Lab Code: LANCAS Case No.: _______ SAS No.: SDG No.: Matrix: (soil/water) WATER Lab Sample ID: 2583209 Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >ISJ13 Level: {low/med) LOW Date Received: 09/18/96 % Moisture: not dec. _______ Date Analyzed: 09/19/96 GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0 Soil Extract Volume: ____ (uL) Soil Aliquot Volume: _______ (uL) CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 74-87 -3----------------- Chloromethane 75-01-4---------- -------- Vinyl Chloride 74-8 3 -9----------------- Bromomethane 75-00-3------------------ chloroethane 75-35-4----------------- 1,1-Dichloroethene 67-64-1--------------- Acetone 75-15-0------------------ Carbon Disulfide 75-09-2------------------ Methylene Chloride 75-34-3------------------ 1,1-Dichloroethane 540-59-0--------------- 1,2-Dichloroethene (total) 78-93-3---------------- -2-Butanone 67--66--3------------------ Chloroform 107-06-2--------------- 1,2-Dichloroethane 71-55-6----------------- 1,1,1-Trichloroethane 56-23-5------------------ Carbon Tetrachloride 71-43-2------------------ Benzene 79-01-6------------------ Trichloroethene 78-87-5------- ----------- 1,2-Dichloropropane 75-27-4--------------- Bromodichloromethane 10061-01-5------------ cis-l,3-Dichloropropene 10061-02-6----------- trans-1,3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane 124-48-1----------- --Dibromochloromethane 75-25-2------------------ Bromoform 108-10-1---------------- 4-Methyl-2-Pentanone 108-88-3---------------- Toluene 127-18-4---------------- Tetrachloroethene 591-78 -6--------------- 2 -Hexanone 108-90-7--------------- chlorobenz ene 100-41-4---------------- Ethylbenzene 1330-20-7-------------- Xylene (total) 100-42-5---------------- Styrene 79-34-5----- `------------ 1,1,2,2-Tetrachloroethane 10 u 10 u 10 u 10 u 59 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 58 57 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 54 10 u 10 u 53 10 u 10 u 10 u 10 u FORM I VOA OLM032<8 4 DUP050308212 t o t a l ION CHROflOTOeRfiM Data File: >ISJ13::D3 Quant Output File: '''ISO 13 : : D? [ lame: BRS3DriSO 2583209 Instrument ID: HP03046 nisc: ~TLN WL 5SC =1 +> #I962631AA $^IS0B2 &5 *5 Id File: IA6390::DB Title: 3/90 SOU) Water/'tled Soil ID File for Inst. HP03Q46 Oast Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Operator ID: TLN-262 Quant Time : 960919 12:36 Injected at: 960919 12:11 235 DUP050308213 QUANT REPORT Operator ID: TLN-262 Output File: "'IS.313: : D? Data File: >IB013::D3 Name: 8RS3DMSD 2583209 ruse: ~TLN WL C *1 +> Qu ant Re v: #1962631AA $''ISJB2 7 iQuant Tlme: Injected at: Dilution Factor: Instrument ID: &3 *5 Page 1 96U919 12:36 960919 12: 11 1 . UUU0U HP03046 ID Fi le: 1A6390::DB '< 11 1 e : 3^90 BOW U)ater2F1ed Soil ID File for Inst . HPQ3 046 Last Calibration: 951122 10:44 Last Qcal Time: 960919 06:34 Compound 1? 6) 15) 17) 20) 21) 29) 31) 32) 35) 40) *Bromoch1aromethane 1,1-Dichloroethene 1,2-Dichioroethane~d4 *1,4~Difluorobenzene Benzene Tr ich loroethene *Chlorobenzene-d5 ToIuene-d8 Toluene Chlorobenzene 4-Bromofluorobenzene * Compound is ISTD R.T. Q ion 8.35 4.65 9.30 10.01 9.38 10.41 14.32 12.22 12.31 14.36 16.04 128.0 96.0 65.0 114.0 78.0 130. 0 117. 0 98.0 91.0 112.0 95.0 Area 40297 47939 85333 167429 142425 68413 125468 144106 160454 120237 101642 Cone Units 50 . UO 58.74 45.95 50.00 58.40 57.26 50.00 40.49 54.44 53.26 49.04 UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L q 90 91 89 8? 88 84 85 98 96 87 74 236 DUPO 50308214 Lancaster Laboratories Quantitation Report-GC/MS Uolatiles LL1*: S ^ S 32 0 9* TLN Hie: A1SJ13 Injected: 12:11 119/19/96 Sample*. BRS3WSD 2585209 Uilution factors 1.0 Initial Volume/Wt.: 5.0 Standard*. ''LSJSl Inst. HP03846 Batch: 1962631RA Final Volume/Wt.: 5.0 Method: 7156 Matrix/leyel*. ML Blank: A'lSJt52 * Internal Standards ft.T. IV-RT) Scan Qian Areal+/-XArea) Cone. UL Flag Lone Units = ug/L 1. Bromochloromethane 17. 1,4-Bifluorobenzene 29. Chlorobenzene-d5 i m RETENTION TINE OUT OF RANGE 8.3501.0114) 563 128 482971 31) 50. Ill) 10.8K-.S82) 786 114 1674291 38) 50.80 14.32t-.884) 1877 117 125468( 33) 58.81) * - INTERNAL STANDARD AREA OUT OF RANGE NC * NOT ABLE TO CALCULATE--! STANDARD. Surrogate Standards R.T. (*/-RRT) Scan Cion Area Cone. SRec. U sssasvsBcseBBVEXvMeiBesaaBaassBsaBBB&BsmattaBKSsBinxmaxaxvsHxastsnssatsaaMaaBtiesitHMasBRavnwniiuWMBSssBsaxaBsustBs&asssBBa 15. l,2-Oichlornethane-d4 9.3021-.8B8) 645 65 31. Toluene-dB 12.221.0007) 896 98 40. 4-Bromo fluorobenzene 16.041-.08Q) 1225 95 4 RELATIVE RETENTION TIME CUT OF RANGE * XREC OUT OF RANK 85333 45.95 144186 48.49 101842 49.04 D SURROGATES DILUTED OUT 92 97 9tJ NC COULD NOT CALCULATE Cone. Quantitation f Target Compounds R.T.D/-RRT) Scan Oion Area Cone.A tone.8 Blank Q Limit 5:~3:l!-B.I:-asBBBaBa3e83s*BMSBa8*BBamaBBBBBseaBa8*BBXBnreBe*ata*B*B****B***B**a(s*E8**BBSB8B*88B8*BBnmmBBBB*8n**BBBSBm*BBeB 2. Chloromethane 3. Vinyl Chloride 4. Bromomethane 5. Chloroethane 6. 1,1-Dichloroethene 7. Acetone B. Carbon Disulfide 4.651-.008) 245 96 47959 58.738 59 10 10 1ft 10 lu 10. Ill 9. Methylene Chloride 11. 1,1-Uichloroethane 12. 1,2-Dschloroethene (total) 13. 2-Butanone 14. Chloroform 16. 1,2-Dichloroethane 18. 1,1,1-Trichloroethene 19. Carbon Tetrachloride 20. Benzene 21. Trichloroethene 22. 1,2-Dichloropropane 23. Bromodichioromethane 24. cis-l,3-Dichloropropene 25. trsns-l^-DiehSoropropene 26. 1,1,2-Tnchloroetbane 9.301 .001) 10.411 .001) 652 70 142425 740 130 68413 58.403 57.257 58 57 ssbbsscssstsssscBSsasassesessaeesssBSBasrBisststssBtSB&SBseassssssssssaBStsssssssssdssBsaaeajssaBi 10 la 10 in 10 lft 10 ID 10 11! 10 111 10 10 10 A = RAU CISC. El * COMC. MULTIPLIED BY DILUTION FACTOR - CONC. OUT OF CAL. RANGE * - RELATIUE RETENTION TIME OUT OF RANGE Lab Chronicle*. Ent. by Ver. by_g_^. PAGE 1 OF 2 DUP050308215 -^^ '*uwHn.w--'W'fltfiioiBaiiu,-.as-iiiiiniii-.,,.. ^i,.-^.^,;*,, . . Lancaster Laboratories Quantitation Report-GC/MB Volatiles Lilt: 25832 5* Tl--1^4 tiie: A1SJ13 injected: 12:11 89/19/96 Sanple: BRS3DMSD 2583209 Dilution Factor: 1.(1 Initial Volume/tili.: 5.0 Standard: AiSJSl Inst. HP03046 Batch: I962631AA Final Uolume/Ut.: 5.0 Method: 7156 Matrix/level: UL Blank: A1SJB2 Cone. Quantitation . t target Compounds R.T.l*/-RRf) Scan tlion Area Cone.A Cone.B Blank Q Limit ssEas6asaa83a8ss3BBBSB8eafSiuaais*Mtn8BS88iM*si8seaBaBKaBK>BtasssasB8BS3BsaeBsat8aiia3assKSBsBssss:s*saBss3s 27. Dibromoehioromethane 28. Brosmform ill. 4-ttethyl-2-Pentanone 32. Toluene 33. letrachloroethene 34. 2-Hexanone 35. Chlorobenzene 36. Ethylbenzene 38. Xylene (total) *------------------------------------- -------- --------- -------------------- -------------------- 12.311 .001) 904 91 160454 54.444 54 --------------------------------- *------------------ *---------------------------------------------------------------- --------------------- -----~-------------------- ---------------------------------------------------------- 14.361 .0001 1(180 112 120237 53.257 53 ------------------------------- ----------------------------------------------------- 10 10 10 10 10 41. 1,1,2,2-Tetraefiloroethane ------------------------------- :--------------------------------------------------------------------------------------------- 1U aaaaaaasaa#!sa*aa*aasBsai!*a*jani*:aBeu6*BaB*a*****aa*Ji**sii***aB6iitiKKit**Kamm*05acs**aaaEB3**sa**asa***Bia*a*ffi3Be3a**aoai ft = RAW CUNC. S = CUNC. MULTIPLIED BY DIUJTSUN FACTOR E = CUNC. OLU QF Cftt. RANGE t - KLLftl IDE RETEOT1UN TIME OUT UF RANGE Lab Chronicle: JEnt. by analyst: .Date: Q(lcl Dor. by Auditor: .Date: PfiGE 2 QF 2 238 DUP050308216 ** LANCASTER LABORATORIES INC. LANCASTER LABORATORIES INC. RUNLOG FOR HEWLETT PACKARD GC/MS SYSTEM #HP03460 * * _______ _________________________ First Shift ,, fksu- * _- ________ Second Shift *Third Shift * * <?A-rs (HP4) * * * ' * * * * * * * * * * * * * * * FILE SAMPLE LLI# DATE TIME BATCH >GSMT1 BFBJUN28 >GSMT2 BFBJUN28 >GSMT3 BFBJON28 >GSMI1 VSTD010 >GSMI2 VSTD020 >GSMI2 VSTD020 >GSMI3 VSTD050 >GSMI4 VSTDIOO >GSMI5 VSTD200 >GSMB1 VBLKG22 >GSMB1 VBLKG22 >GSMB1 VBLKG22 >GSM01 FTWAS >GSM02 F8WAS >GSM03 F6WAS >GSM04 DU-P>GSM05 FSWASDL >GSM06 DU-P-DL >GSM07 F6WASMS >GSM05 FSWASDL >GSM07 F6WASMS >GSM06 DU-P-DL >GSM08 F6WASMSD >GSM09 3------->GSM10 5-------- >GSM11 T------B >GSM12 3-------DL >GSM12 3r-----DL >GSM13 FGWASMSD >GSM14 FSWASMS 50nG BFB 09/24/96 00:30 5 OnG BFB 09/24/96 00:48 50nG BFB 09/24/96 01:08 010 ppb IC 09/24/96 01:40 020 ppb IC 09/24/96 02:12 020 ppb IC 09/24/96 02:12 050 ppb IC 09/24/96 02:44 100 ppb IC 09/24/96 03:17 200 ppb IC 09/24/96 03:49 VBLKG22 09/24/96 04:50 52S1T VBLKG22 09/24/96 04:50 G2661 VBLKG22 09/24/96 04:50 G2661 2585266 09/24/96 05:33 G2661 2585227 09/24/96 06:03 G2661 2585228 09/24/96 06:32 G2661 2585229 09/24/96 07:02 G2661 2585227 09/24/96 07:37 G2661 2585229 09/24/96 08:07 G2661 2585228 09/24/96 08:36 G2661 2585227 09/24/96 07:37 G2661 2585228 09/24/96 08:36 G2661 2585229 09/24/96 08:07 G2661 2585228 09/24/96 09:06 G2661 2585230 09/24/96 09:41 G2661 2585231 09/24/96 10:13 G2661 2585232 09/24/96 10:42 G2661 2585233 09/24/96 11:21 G2661 2585230 09/24/96 11:21 G2661 2585228 09/24/96 11:53 G2661 2585228 09/24/96 12:41 G2661 D.F. NOTES u.uu jSi/\ % 0.00 0.00 1.00 1.00 1.OOREPROCESSED1. 1.00 1.00 1.00 1.00 1.OOREPROCESSED!. 1.OOREPROCESSED!. 1.00 1.00 1.00 1.00 2.00 1.00 .40 /'w'vA . 5.00 r<vsf cc.ff&'i . 1.00 2.50 1.00 1.00 ^ <A_ 1.00 1.00 2.50 2.50 t <5 'SliA 1.00 1.00 23S DUP050308217 I ANGASTFR LARDRATriRIFS INF.. RUNI OG FOR HEWLETT PACKARD GC.XMS SYSTEM $KP0346n (HP4) *r First Shift * Second Shift * Third Shif t Sa < * * H II II li II II F f 1. F SAMPLE LI I* DATE TIME BA FCH D. E. saesssasaa sssKssasaHWBsssasssarta sat as as as as asr aa as ssssas s = as as at as ssr as -a as ~ ss as as >r::-.pn > GSPS1 > JhP.PR I >GSPCl! >g s p o ? > GSP03 >GAP04 > GSP05 >g s p o 6 >GSPfl7 >GSP0S >GSP09 >nspin > GSP 11 > RSP12 >GSP13 >g s p i.4 >GSP15 >GSP16 > ESP]7 >GSP18 > GSP19 >GSPX! >GS.X2 > GSPX3 >GSPX4 BFfl.1t.SN78 USTO030 URl KG74 BBA2D 8RA2S BRAID 8RAIS MRA2S MRA2SMS MRA2SMSD BRAF1 BRAT? MRA IS MRA1D MRA20 TB3FM MRftAS MRA IS MPA3D MR3DD MRAFB MRT84 TB96261 T896264 TR9626S TB96269 5 0r.G BFS 09724X96 23 59 030 ppb CC 09X25X96 0 0 26 UR! .KG? 4 09X25X96 01 04 G2681 2583823 09X25X96 01 57 G2681 2583824 09X25X96 0? 30 G2681 2583825 09X25X96 03 02 G2681 2583826 09X25X96 03 34 G2681 2585279 09X25X96 04 05 G2681 2585279 09X25X96 04 36 G2681 2585279 09X25X96 05 06 G2681 2583827 09X25X96 05 39 G2681 2583828 09X25X96 06 11 92681 2 5 P.5 2 76 09X25X96 116 47 G2681 2585277 09X25X96 07 1.3 G2681 2585278 09X25X96 0 7 G26S1 2585280 2585281 09X25X96 08 17 G2681 09X25X96 08 5 0 G76S1 2585282 09X25X96 09 22 G2681 2585285 09X25X96 09 55 132.681 2585284 09X25X96 1 0 27 G2681 2585285 09X25X96 11 00 G2681 2585286 09X25X96 11 33 G2681 TR96261 09X25X96 12 22 G? 681 TB96264 09x25X96 12 55 G2681 TP.96268 09X25X96 13 28 G2681 TR96269 09X25X96 14 0 0 G2681 o. ft n l. no 1. o n 1.00 1.00 1 - 00 1.00 1.00 1.00 1.00 i. o n 1.00 1.00 1.00 1.00 l. no 1 .00 l. no 1.00 1.00 1.00 1.00 1.00 1.00 l. no 1.00 NOTES -*i a * * * 240 DUP050308218 LANCASTER LABORATORIES tf-iC. RUNLOG FOR HEWLETT PflCKARO GC/MS SYS TEH SHP03046 _F rs Sh j f t lUi .8.5 co ~ - h i ? 3 ThsrcJ S* :Fi: (HP6 ) f i l e s a mp l e LL I v DA! 1 ! ME * st * s rp mavmv 5T K=r snwmsttneennssvsceBnsnss = =" > IGKT2 BPS 2uL 5 On g K.c8 OS/2 0.*96 19 52 > EGKf1 vsionle 010 PPS IC 08/20/96 20 >IGKI2 USTD020 > I Gs< I3 vsrooso 020 PPS 1C 08/20/96 20 v 050 PPS IC 02/20/96 O. T4k 41 > <14 USTO20G 100 PPS IC 08/20/96 22 15 > e g k !5 us r0*2 oo 200 PPS !C 03/20/96 22 46 >IGKS3 U8LKI50 > 1GKS4 L'SLK [ 5 0 U8LKI50 VBLK f 5 0 03/20/96 23 46 08/21/96 00 fl >IGK85 UBLKI5Q UBLKI50 03/21/96 01 38 >IGK86 U8LKI50 J U8LKI50 03/21/96 02 26 >IGK20 00199 25*2933 03/21/96 03 08 > IGK21 U18LK 5 C1 UIBLKIC1 03/21/96 04 00 >IGK22 0 0199 DL 256292? 03/21/96 04 34 >IGK23 002 00 > IG!<24 00201 > tG*2*5 U0201DL 2562925 2562929 2562989 03/21/96 05 2 3 08/22/96 06 > V* 1J. 08/21/96 06 6P > ICK26 00200 2562925 08/21/96 0? 24 > I GK2 ? Ul8LKl02 V1BLKI02 08/21/96 03 06 >IGK2S 'JISLKI03 VIBLK103 08/22/96 08 36 BATCH 12331 12331 J 2331 12331 12331 12531 12331 12 331 12531 12 351 12531 12331 12 331 0. F. NO! ES serr^asr a as*TS w m o.uo 2.0 U 1.00 1.00 i_ 1. UO 1.00 _ 1 . UO 1.00 1.U0 1.00' 16.00' 1.00 400.00 m | \y * 10IJ . 0 u 16.0 0 wo- i . u 40.00 1.00 1.00 W.U Jy 241 DUP050308219 ************* * LANCASTER LABORATORIES INC. RUNLOG FOR HEWLETT PACKARD GC/MS SYSTEM #HP03046 First Shift TLu Second Shift :TL Third Shift SArvv 1 fHP6> FILE SAMPLE LLI# SATE TIME BATCH >ISJT1 BFB 2uL 50ng BFB 09/19/96 06:10 >ISJS1 VSTD050 050 PPB CC 09/19/96 06:34 >ISJB1 VBLKI92 VBLKI92 09/19/96 07:14 12571 >ISJ01 TB909 2578563 09/19/96 07:51 12571 >ISJB2 VBLKI93 VBLKI93 09/19/96 08:44 12631 >ISJ10 BRATB 2583211 09/19/96 10:34 12631 >ISJ11 BRS3D 2583209 09/19/96 11:04 12631 >ISJ12 BRS3DMS 2583209 09/19/96 11:35 12631 >ISJ13 BRS3DMSD 2583209 09/19/96 12:11 12631 >ISJ14 DRA3S 2583210 09/19/96 12:41 12631 >ISJ15 BRS4S 2583208 09/19/96 13:12 12631 >ISJ16 BR4DD 2583207 09/19/96 14:11 12631 >ISJ17 BRA4D 2583206 09/19/96 14:41 12631 >ISJ18 BRA5S 2583205 09/19/96 15:27 12631 >ISJ19 BRA5S 2583205 09/19/96 16:04 12631 >ISJ20 BRA5S 2583205 09/19/96 16:40 12631 >ISJ21 BRA5S 2583205 09/19/96 17:25 12631 >ISJ22 BRA5S 2583205 09/19/96 17:56 12631 D.F. NOTES 0.00 1.00 " 1.00 1.00 " 1.00 1.00 " 1.00 " 1.00 ' 1.00 " 1.00 1.00 " 1.00 ' 1.00 " 1.00 " 1.00 " 1.00 ' 1.00 " 1.00 SJu. 1 AJ * * * * * * * * * * * * * * * * . * DUP050308220 LANCASTER LABORATORIES INC. RUNLOG FOR HEWLETT PACKARD GC/MS SYSTEM #HF03046 (HP6) ** * ______________ First Shift TLi * ** * _____________._______________________ Second Shift * ** * _______ Third shift * ** ** ** ** ** ** ** * ___ _____ * FILE SAMPLE LLI# DATE TIME BATCH D.F. NOTES >ISOTl BFB 2UL 50ng BFB 09/24/96 11:10 >ISOIl VSTD010 010 PPB IC 09/24/96 11:35 >ISOI2 VSTD020 020 PPB IC 09/24/96 12:08 >ISOIl VSTD010 010 PPB IC 09/24/96 11:35 >ISOI2 VSTD020 020 PPB IC 09/24/96 12:08 >ISOI3 VSTD050 050 PPB IC 09/24/96 12:50 >ISOI4 VSTDIOO 100 PPB IC 09/24/96 13:23 >ISOI5 VSTD200 200 PPB IC 09/24/96 13:56 >ISOBl VBLKI95 VBLKI95 09/24/96 14:29 12681 >ISOB2 VBLKI95 VBLKI95 09/24/96 15:04 12631 >ISOB3 VBLKI95 VBLKI95 09/24/96 15:43 12631 >ISO01 BRA5S 2583205 09/24/96 16:23 12631 >IS002 BRA2D 2583823 09/24/96 16:55 12631 >IS003 BRA2S 2583824 09/24/96 17:25 12631 >ISOXl CLEANING BLANK 09/24/96 18:18 12631 >ISOX2 CLEANING BLANK 09/24/96 19:33 12631 0.00 1.00 ' 1.00 1.OOREPk OCESSEDT l.OOREPROCESSEDi 1.00 1.00 ' 1.00 ' 1.00 " uu 1.00 ' 1.00 ' 1.00 " 1.00 " MU 1.00 " t 1.00 ' | * 1.00 " 24 DUP050308221