Document EvyzpJj0geqxoxoeng7rYZ0k0
contract Lab Program Bata Package for
DuPont Env. Remediation Svcs.
IV ORGANICS DATA PACKAGE
Madison - g w Monitoring-1996 Annual Water Samples
ected on 09/17/96 - 09/18/96 . 2583205-2583211, 2583823-2583828
PA Cert. # 36-037 NY Cert. # 10670 NJ Cert. # 77011
Prepared by.
'uCn f4'$L
Quality Assurance Review /D-H-7h
Delivery Date_________If)- I'l-tfbj
Lancaster Laboratories
A Thermo Analytical Laboratory
N36822
Pike, P0 Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681
Lancaster Laboratories
A division of Thermo Analytical Inc.
La Reference List for 806 # f h d o i with a Package Type of IV-O
iim Sample Mummer
2583205 2583806 2583207 2583208 2583209 2583210 2583211 2583823 2583824 2583825 2583826 2583827 2583828
Sample code
BRASS BRA4D BR4DD BRS4S BRS3D BRASS BRASS BRA2D BRA2S BRAIO BRA1S BRAF1 BRAT2
Client Sample Description
FMN-BRA-4S Water Sample FMN-BRA-3D Unspiked Water Sample FMN-BRA-38 Water Sample FMM-BRA-TBLK-1 Water Sample FMN-BRA-2D Water Sample FHN-BRA-28 Water sample FMN-BRA-1D water sample FMN-BRA-lS Water 8ample FHM-BRA-FBLX-1 Water Sample FHN-BRA-TBLX-2 Water Sample
Lancaster uooratones 2425 New Holland Pike PO Box 12425 lanC5Stc,r. PA 17605-2425 717-656-2300 Fax. 717-656-263'
Shipping Address: Lancaster Laboratories 2425 New Holand PikeLancaster, PA 17601
717-656-2300 Fax. 717-656-268'
DUP050307975
TABLE OF CONTENTS
A. Case Narrative-Conformance/Nonconformaiice Suminary....... ....................1
B. chain-of-custody Record....................
4
C. Volatiles Data..................................................................................................................13
1. QC Summary......................
14
2. Sample Data............................
29
3. Standards Data.......... ...................................................................................96
4. Raw QC Data................................................................................................... 198
A
DUP050307976
Case Narrative Conformance/Nonconformance Summary
l
DUP050307977
Lancaster Laboratories
A thermo Analytical Laboratory.
Where quality is a science.
LANCASTER LABORATORIES VOLATILES by GC/MS
LL NUMBERS: SAMPLE CODE:
2583205 2583206 2583207
2583208 2583209 2583209 2583209 2583210 2583211 2583823 2583824 2583825 2583826 2583827 2583828
BRASS BRA4D
BR4DD BRS4S BRS3D BRS3DMS BRS3DMSD DRA3S BRATB BRA2D
BRA2S BRAID BRA1S BRAF1 BRAT2
LABORATORY SUBMITTED QC:
VBLKG24 VBLKI93 VBLKI95
VBLKG24 VBLKE93 VBLKI95
CASE NARRATIVE
CLIENT: DUPONT SDG: FMD01
MATRIX
SOIL
WATER
X X X X X X X X X
X X X X X X
COMMENTS
UNSPIKED MATRIX SPIKE MATRIX SPIKE DUP CLIENT BLANK
CLIENT BLANK CLIENT BLANK
X METHOD BLANK X METHOD BLANK X METHOD BLANK
SAMPLE PREPARATION:
No problems were encountered during the sample preparation for the VOA fraction.
ANALYSIS:
The method used for analysis was EPA CLP OLM03.1 SOW.
No problems were encountered during the analysis of these samples.
QUALITY CONTROL and NONCONFORMANCE SUMMARY: Only client requested compounds are addressed in this narrative. All QC was within specifications.
DATA INTERPRETATION:
No interpretation is necessary for the data submitted.
Lancaster Laboratories 2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681 A subsidiary of Thermo Process Systems Inc., a Thermo Electron company
%
DUP050307978
Lancaster Laboratories
A Thermo Analytical Laboratory
Where quality is a science.
CASE NARRATIVE
Case Narrative Reviewed and Approved by:
/
Wj a
ktfLg.
Date /C s "> C-
ihn F. Morton, M.S., GC/MS Volatiles
Lancaster Laboratories 2425 Mew Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681 A subsidiary of Thermo Process Systems Inc., a Thermo Electron company
t>
DUP050307979
Chain-of-Custody Record
DUP050307980
DU P050307981
DUP050307982
5-157 X3, 10-9W
ANALYZING LAB COPY
DUP0503 07983
5-157 X3, 10-91
an al y zin g l ab c o p y
DUP050307984
AM M V*7IM f2 I A
MSNewHdland WtiiicMter. PA TOOtSSM
Sample Administration Receipt Documentation Log
Client/Project:__________
Date of Receipt:__ i -- /
^&
Time of Receipt:__________ ft
0
Source Code: __ _____
^I
COC Seal: Pre^t / Not Present on cooler
Broken / li^ct
Package: Cl^d / Not Chilled
Unpacker Emp. No.:
----------------
Temperature of Samples
Thermometer ID:
#1
/6 /D 3
Thermometer ID:
#2
Corrected Temo.: B^t^e / Air
e>v *7
W^jle / Dry Ice / ice Packs
Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs
Ice Present?
/N #3
Ice Present? Y / N #4
Thermometer ID:
Thermometer ID:
Corrected Temo.:
Corrected Temp.:
Bottle / Air
Bottle / Air
Wet Ice / Dry Ice / Ice Packs
Wet Ice / Dry Ice / Ice Packs
Ice Present? Y / N
Ice Present? Y / N
Paperwork Discrepancy/LTnpacking Problems:
Sample Administration Chain of Custody
Name
Date
Time
Reason for Transfer
y-nr-w
mZl. f'/A
/ fl f | //
Uppaekmg-- Klace in Storage )or
Entry
t*fOO Remove from Storage^
Place in Storage or Entjy
Entry
j
Rev. 2174 09/09/96
DUP0503 07985
JSNewHolUnd H Uncww.
Sample Administration Receipt Documentation Log
Client/Project: _ Date of Receipt: Time of Receipt: Source Code: __
PfM/fl CO
JEd.
COC Seat: Pr^s^nt / Not Present on cooler Broken / Injj^Ct
Package: Cl^filpd / Not Chilled Unpacker Emp. No.:
Thermometer ID: Corrected Temp.: B<(^ie / Air
#1
j 0 f O'} 1\
Wejtj^e / Cffy Ice / Ice Packs
Ice Present? $) / N
#3 Thermometer ID: Corrected Temp.: Bottle / Air
Wet Ice / Dry Ice / Ice Packs Ice Present? Y` / N
Temperature of Samples
#2
Thermometer ID: Corrected Temp.:
Bottle / Air
Wet Ice / Dry Ice / Ice Packs
tee Present? Y / N #4
Thermometer ID:
Corrected Temp.:
Bottle / Air
Wet ice / Dry Ice / Ice Packs
Ice Present? Y / N
Paperwork Discrepancy/Unpacking Problems:
%
Sample Administration Chain of Custody
1
Name
Date
Time
Reason for Transfer
|
Cml XCaX-.
bnI rrzQxs*t
U> 1 * Ai
A)
i-n-%
1em
Unpackina
1/66 < Place in Storage) or
)soc Remove from Storage ^
Place in Storage or
Entry Entry
. Entry
Rev. 2174 09/09/96
DUP050307986
3425 NewHolland Lancaster PA 17601-SS94
Locked Storage Chain of Custody Original Sample
Client/Project: P)i, PflnT"" F~n\i Fpy** A.irTTi an ^.Vi/a: 2 -
Preservative:
H~C, L,___________
Matrix: IaJ Ll ,'__________
Sample # Range of Entry Group: Pi<T D.f)I!____________
- Of ~P f/'.oA >
_________
SDG: P M P 0 }
Bottle Type: W`0 aPs it La,1'
..
Sample Number(s) Released Received Date of Time of
in Custody
By By Transfer Transfer
Reason for Change of Custody
a vf3aas'-//
Z&320&-U
2c<r-// -2573UOS - ii oJSg'S^os-n
P5054)S -if JSTOos-li
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TL-.W,J
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66
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!<h . y&-* z Vo* Ata-utf's
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Dist., Extr., or Digest Chain
Created (X)
`r/^Kv-
2016 Rev. 09/05/95
ii Page__[_ of
DUP050307987
*25 NewHolland Pika UneasiK,IJ60I-S99*
Locked Storage Chain of Custody Original Sample
Client/Project: Du PfisTf'
UprnpAt/t (iOi.\ St>c\ ,
For~f }V grl/i .%Gs> ___________ _
Preservative:
N Os'JL,___________ Matrix: lOU____________
SDG: FM D Q 1
Sample # Range of. Entry Group:
<35'? 3?33-3 P"__________
Bottle Type: 4# <yJ
Sample Number(s) in Custody
^91% ai-a*
^i
25^597-Z -29
F5b 3sra-3-^J
Released Received Date of Time of By By Transfer Transfer
7a (0-r
SA AtFu~^ 9-f^% yjos
sH`Uo
3'AO'3C. OGlO
Ti^./iy
iLo D"S-lp--3vi
Vfava gif
T Kelly
Ai T Kelly
?>4o
q-lQ-tL oC^S 9'5o-^C, o^oc
340 \Rpt 3t <?'3fc-9fc 0 3l S
Dept 2.1 S7 0-vtnew-
3forru^t.
t7C
y%i/%
f5-oo
Jscpt 2 i / 70 Snr^Hft.
iV-Zo
ofiiZ^c/4
jtemM qz*
Fh
5//
c
0r, tf0
Reason for Change of Custody
S F~
-fVc\w5-f<> + o De-O-f 3. *
^ <;
5 tUV-4 q e yv< Sc K;e v \ 0 CD t x /q -s' 7c-
V-CIvv^ ru Sfolrgyu Vfe- ArtaXtrsiS
Rftucw. to ofc^v^t.
i/u/j
# 7/5 6
Dist., Extr., or Digest Chain
Created (X)
^ Sfr3S>3-9-$-
e?% ~i
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2016 Rev. 09/05/95
------- 2__
Page I of
DUPO50307988
Volatiles Data
13
DUPO50307989
QC Summary
DUP050307990
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: LANCASTER LABS
Contract: ______ .
Lab Code: LANCAS
Case No,: ______ SAS No.: _______.
SDG No.: FMD01
:--------8NE ' ' sNci ` SMC2 " SMC3.. oTfcfiR.. fS?
SAMPLE NO. (TOL)# (BFB)# (DCE)#
OUT
01 ':ViLNS24 02 BRA2D 03 BRA2S 04 BRAID 05 BRA1S 06 BRAF1
07 BRAT2 08
09 10
11
12 13 14 15 16 17 18 19 20 21
22 23 24 25
26 27
28 29 30
100 99
100
102 94 96 97
103 100 104
107 100 100 105
93 92 94 95
90 91
90
0 0 0
0 0 0 0
SMC1 (TOL) Toluene-d8 SMC2 (BFB) = Bromofluorbenzene SMC3 (DCE) = 1,2-Dichloroethane-d4
QC LIMITS (88-110) (86-115)
(76-114)
f Column to be used to flag recovery values
* Values outside of contract required QC limits
D System Monitoring Compound diluted out
page 1 of 1
FORM II VOA-1
OLM03.0
15
DUP050307991
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: LANCASTER LABS
Contract: ______ .
Lab Code: LANCAS
Case No.: _______ SAS No.: ______ .
SDG No.: FMD01
----- gpjj---------- - SMC1 SM<S2" "s mc '3... 0TMER ToT
SAMPLE NO. (TOL)# (BFB># (DCS)#
OUT
01 VBLKI&3 02 BRATB 03 BRS3D 04 BRS3DMS 05 BRS3DMSD 06 DRA3S 07 BRS4S 08 BR4DD 09 BRA4D 10 VBLKI95
11 BRASS 12 13 14 15
16 17
18
19
20
21
22 23 24 25 26 27 28 29
30
101 101
102 100
97 99 102 102 100 104
102
98 99 97 98 98 98 98
102 97
100 99
94 90 94 94 92 94 95 94
94
95
94
0 0 0 0 0 0 0 0
0 0
0
SMC1 SMC2
SMC3
(TOL) = Toluene-d8 (BFB) = Bromofluorobenzene
(DCE) = 1,2-Dichloroethane-d4
QC LIMITS (88-110) (86-115)
(76-114)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D System Monitoring Compound diluted out
page 1 of 1
FORM II VOA-1
OLM03.0
16
DU P050307992
3A WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: LANCASTER LABS
Contract: ______.
Lab Code: LANCAS
Case No.: . . . SAS No.: .
Matrix Spike - EPA Sample No.: BRS3D
s d g No.: _____
COMPOUND
1,1-Dichloroethene Benzene Trichloroethene Toluene Chlorobenzene
"SPISE------ -------- 33EHP0S------
"US------- " 55-
ADDED
CONCENTRATION CONCENTRATION %
l imit s
(ug/L)
(ug/L)
(ug/L)
EEC # REC.
50.00 50.00 50.00 50.00
50.00
0.00 0.00 0.00
0.00 0.00
58.99 57.81 56.61 54.80 52.59
118 116 113
110 105
61-145 76-127
71-120 76-125 75-130
COMPOUND
1,l-Dichloroethene Benzene Trichloroethene Toluene Chlorobenz ene
SPIKE ADDED
(ug/L)
MSD
CONCENTRATION (ug/L)
50.00 50.00 50.00 50.00 50.00
58.74 58.40
57.26 54.44 53.26
MSD %
REC #
117 117 114 109 106
% RPD #
1 1 1 1 1
QC LIEMITS RPD REC.
14 61-145 11 76-127 14 71-120 13 76-125 13 75-130
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: .0 out of
5 outside limits
Spike Recovery: o out of 10 outside limits
COMMENTS:
___________________________________________
FORM III VOA-1
OLM03.0
17
DUP050307993
4A VOLATILE METHOD BLANK SUMMARY
EPA SAMPLE NO.
Lab Name: LANCASTER LABS
Lab code: LANCAS
Case No.: ______
Contract: SAS No.:
VBLKG24 SDG No.:
Lab File ID: >GSPB1
Lab Sample ID: VBLKG24
Date Analyzed: 09/25/96
Time Analyzed: 01:04
GC Column: DB624
ID: 0.53 (mm)
Heated Purge: (Y/N) N
Instrument ID: HP03460
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
Bp F SAMPLE NO.
01 BRA2D 02 BRA2S 03 BRAID 04 BRA1S 05 MRA2S 06 MRA2SMS 07 MRA2SMSD 08 BRAF1 09 BRAT2 10 MRA1S 11 MRA1D 12 MRA2D 13 TB3FM 14 MRA4S 15 MRA3S 16 MRA3D 17 MR3DD 18 MRAFB 19 MRTB4 20 21 22 23 24 25 26 27 28 29 30
COMMENTS:
ESI SAMPLE ID
2583823 2583824 2583825 2583826
2585279 2585279 2585279 2583827 2583828 2585276 2585277 2585278 2585280 2585281 2585282 2585283 2585284 2585285 2585286
LAB FILE ID
>GSP01 >GSP02 >GSP03 >GSP04 >GSP05 >GSP06 >GSP07 >GSP08 >GSP09 >GSP10 >GSP11 >GSP12 >GSP13 >GSP14 >GSP15 >GSP16 >GSP17 >GSP18 >GSP19
page 1 of 1
FORM IV VOA
TIME ANALYZED
01:57 02:30 03:02 03:34 04:05 04:36 05:06 05:39 06:11 06:42 07:13 07:44 08:17 08:50 09:22 09:55 10:27 11:00 11:33
18
QLM03.0
DU P050307994
4A VOLATILE METHOD BLANK SUMMARY
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract
VBLKI93
Lab Code: LANCAS
Case No.: ______ SAS No.: ______ . SDG No.: ___
Lab File ID: >ISJB2
Date Analyzed: 09/19/96
GC column: DB624
ID: 0.53
(mm)
Lab Sample ID: VBLKI93 Time Analyzed: 08:44 Heated Purge: (Y/N) N
Instrument ID: HP03046
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21
22 23 24 25 26 27 28 29 30
COMMENTS:
EPA SAMPLE NO.
BHATB BRS3D BRS3DMS BRS3DMSD DRA3S BRS4S BR4DD BRA4D
ElB SAMPLE ID
2583211 2583209 2583209 2583209 2583210 2583208 2583207 2583206
LAB FILE ID
>ISJ10 >ISJ11 >ISJ12 >ISJ13 >ISJ14 >ISJ15 >ISJ16 >ISJ17
TIME ANALYZED
10:34 11:04 11:35 12:11 12:41 13:12 14:11 14:41
page 1 of 1
FORM IV VOA
OLM03.0
19
A
DUP050307995
iA
4A VOLATILE METHOD BLANK SUMMARY
EPA SAMPLE NO.
Lab Name: LANCASTER LABS
Contract:
VBLKI95
Lab Codes LANCAS
Case No.: ______ SAS No.t
SDG No.
Lab File ID: >ISOB3
Lab Sample ID: VBLKI95
pate Analyzed: 09/24/96
Time Analyzed: 15:43
GC Column: DB624
ID: 0.53 (mm)
Heated Purge: (Y/N) N
Instrument ID: HP03046
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
---------- ggg------------
SAMPLE NO.
SAMPLE ID
FILE ID
TIME. ANALYZED
01 BRA5S
2583205
>ISO01
16:23
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
A 26 27
'
28
29
30
COMMENTS:
page 1 of 1
FORM IV VOA
OLM03.0 20
DU PO50307996
SA " VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK
BROMOFLUOROBENZENE (BFB)
Lab Name: LANCASTER LABS -
Contract: _______.
Lab Code: LANCAS case No.: _______ . SAS No.: _______. SDG No.:
Lab File ID: >GSMT3
BFB Injection Date: 09/24/96
Instrument ID: HP034S0
BFB Injection Time: 01:08
GC Column: DB624
ID: 0.53 (mm)
Heated Purge: (Y/N) N
m/e ION ABUNDANCE CRITERIA
% RELATIVE ABUNDANCE
50 8.0 - 40.0% Of mass 95
75 30.0 - 66.0% of mass 95
95 Base peak, 100% relative abundance
96 5.0 - 9.0% of mass 95 173 Less than 2.0% of mass'" 1*74 174 50.0 - 120.0% of 'mass 95 ........................ 175 4.0 - 9.0% of mass 174
176 93.0 - 101.0% of mass TTZ 177 5.0 - 9.0% of mass 176
26.7 49.0
100.
6.6
0.0 ( 0.0)1 70.7
5.0 ( 7.1)1 69.4 ( 98.2)1
3.9 ( 5.7)2
l-Vaiue is % mass 174 !
2-Value "is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
EPA SAMPLE NO.
LAB SAMPLE ID
ESI
FILE ID
DATE ANALYZED
TIME ANALYZED
01 VSTD010
02 VSTD020
03 VSTD050
04 VSTD100
05 VSTD200
06 VBLKG22
07 FTWAS
08 F8WAS
09 F6WAS
10 DU-P-
11 F8WASDL
12 DU-P-DL
13 3--------
14
5-------------------
15 T------B 16 3--------DL
17 F6WASMSD
18 F6WASMS
19
20
21
22
010 ppb IC 020 ppb IC 050 ppb IC 100 ppb IC 200 ppb IC VBLKG22
2585266 2585227
2585228 2585229 2585227
2585229 2585230 2585231 2585232 2585230 2585228 2585228
>GSMI1 >GSMI2 >GSMI3 >GSMI4 >GSMI5 >GSMB1
>GSM01
>GSMQ2 >GSM03
>GSM04 >GSM05
>GSM06 >GSM09 >GSM10 >GSM11 >GSM12
>GSM13
>GSM14
09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96
09/24/96
09/24/96
09/24/96
09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96
01:40 02:12 02:44 03:17 03:49 04:50
05:33
06:03
06132
07:02 07:37 08:07 09:41 io:i3 10:42
11:21 11:53 12:41
page 1 of 1
FORM V VOA
OLM03.0
21
DUP050307997
5A VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK
BROMOFLUOROBENZENE (BFB)
Lab Name: LANCASTER LABS
Lab Code: LANCAS
Case No.: ______
Contract: ______ . SAS No.: ______.
SDG No.: _______ .
Lab File ID: >GSFT1 Instrument ID: HP03460
BFB Injection Date: 09/24/96 BFB Injection Time: 23:59
GC Column: DB624
ID: 0.53 (mm)
Heated Purge: (Y/N) N
m/e
ION ABUNDANCE CRITERIA
% RELATIVE ABUNDANCE
50 8.0 - 40.0% of mass 95 75 30.0 - 66.0% of mass 95 95 Base peak. 100% relative abundance
96 5.0 - 9.0% of mass 95 173 Less than 2.0% of mass 174 174 50.0 - 120.0% of mass 95
175 4.0 - 9.0% of mass 174
176 93.0 - 101.0% of mass IY4 177 5.0 - 9.0% of mass 176
27.1
50.1
100. 6.9 .4 ( .6)1
70.2 5.0 ( 7.1)1
68.6 ( 97.7)1
4.5 ( 6.6)2
l-value is % mass i>4
2-Value is % mass i7e
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
EPA SAMPLE NO.
La b SAMPLE ID
LAB FILE ID
DATE ANALYZED
TIME ANALYZED
01 VSTD050 02 VBLKG24
03 BRA2D 04 BRA2S
05 BRAID 06 BRA1S
07 MRA2S 08 MRA2SMS 09 MRA2SMSD
10 BRAF1 11 BRAT2 12 MRA1S 13 MRA1D 14 MRA2D
15 TB3FM 16 MRA4S
17 MRA3S 18 MRA3D 19 MR3DD 20 MRAFB 21 MRTB4
22
050 ppb CC VBLKG24 2583823
2583824 2583825 2583826 2585279 2585279 2585279 2583827 2583828 2585276
2585277 2585278
2585280 2585281
2585282 2585283 2585284 2585285 2585286
>GSPS1 >GSPB1 >GSP01 >GSP02
>GSP03 >GSP04 >GSP05 >GSP06 >GSP07 >GSP08 >GSP09 >GSP10 >GSP11
>GSP12 >GSP13 >GSP14
>GSP15 >GSP16 >GSP17 >GSP18 >GSP19
09/25/96 09/25/96 09/25/96 09/25/96
09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96
09/25/96 09/25/96
09/25/96 09/25/96
09/25/96 09/25/96 09/25/96 09/25/96 09/25/96
00:26 01:04 01:57 02:30
03:02 03:34 04:05 04:36 05:06 05:39 06:11
06:42 07:13 07:44 08:17 08:50
09:22 09:55 10:27 11:00 11:33
page 1 of 1
FORM V V0A
OLM03.Q
22
DUP050307998
5A VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK
BROMOFLUOROBENZENE (BFB)
Lab Name: LANCASTER LABS
Contract:
Lab Code: LANCAS
Case No.: ______ SAS No.:
SDG No.:
Lab File ID: >IGKT2
BFB Injection Date: 08/20/96
Instrument ID: HP03046
BFB Injection Time: 19:52
GC Column: DB624
ID: 0.53 (mm)
Heated Purge: (Y/N) N
m/e
ION ABUNDANCE CRITERIA
% RELATIVE ABUNDANCE
50 8.0 - 40.0% Of mass 95 75 30.0 - 66.0% of mass 95 95 Base peak, 100% relative abundance 96 5.0 - 9.0% of mass 95
173 Less than 2.0% of mass 174 174 50.0 - 120.0% Of mass 95
175 4.0 - 9.0% of mass 174 176 93.0 - 101.0% of mass 173 177 5.0 - 9.0% of mass 176
26.4 55.3 100.
7.2
0.0 ( 0.0)1 56.6
4.5 ( 7.9)1 55.5 ( 98.1)1
3.8 ( 6.9)2
l-Value is % mass 174
2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
EPa SAMPLE NO.
EH SAMPLE ID
La b FILE ID
DATE ANALYZED
TIME ANALYZED
01 VSTD010
02 VSTD020 03 VSTD050 04 VSTD100 05 VSTD200
06
07 08
09 10
11 12 13 14 15 16 17
18
19 20
21 22
010 PPB IC
020 PPB IC 050 PPB IC 100 PPB IC
200 PPB IC
5?IGKI1
>IGKI2 >IGKI3
>IGKI4 >IGKI5
08/20/96
08/20/96 08/20/96 08/20/96 08/20/96
20:25
20:59 21:41 22:15 22:46
page 1 of 1
FORM V VOA
OLM03.0
28
DUPO 50307999
5A VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK
BROMOFLUOROBENZENE (BFB)
Lab Name: LANCASTER LABS
Contract: ______ .
Lab Code: LANCAS
Case No.: ______ SAS No.: ______ . SDG No.: _______ .
Lab File ID:, >ISJT1
Instrument ID: HFO3046
GC Column: DB624
ID: 0.53
fmm)
BFB Injection Date: 09/19/96 BFB Injection Time: 06:10 Heated Purge: (Y/N) N
m/e
ION ABUNDANCE CRITERIA
% RELATIVE ABUNDANCE
50 8.0 - 40.0% of mass 95 75 30.0 - 66.0% of mass 95 95 Base peak, 100% relative abundance 96 5.0 - 9.0% of mass 95 173 Less than 2.0% of mass 174 174 50.0 - 120.0% of mass 95 175 4.0 - 9.0% of mass 174 176 93.0 - 101.0% of mass 174 177 5.0 - 9.0% of mass 176
1-Value is %..mass 1?4
26.9 57.9 100.
6.6 0.0 ( 0.0)1 58.0 4.8 ( 8.4)1 56.1 ( 96.8)1 3.9 ( 7.0)2
2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
EPA SAMPLE NO.
LAB SAMPLE ID
es b
:
FILE ID
DATE
TIME
ANALYZED ANALYZED
01 VSTD050 02 VBLKI93 03 BRATB 04 BRS3D 05 BRS3DMS 06 BRS3DMSD
07 DRA3S 08 BRS4S 09 BR4DD 10 BRA4D 11 12 13
14
15
16
17 18
19 20 21 22
050 PPB CC VBLKI93
2583211 2583209
2583209 2583209
2583210 2583208 2583207 2583206
>ISJS1 >ISJB2 >ISJ10 >ISJ11
>ISJ12
>ISJ13
>ISJ14 >ISJ15 >ISJ16 >ISJ17
09/19/96 09/19/96
09/19/96 09/19/96
09/19/96 09/19/96
09/19/96 09/19/96 09/19/96 09/19/96
06:34 08:44 10:34 11:04
11:35 12:11
12:41 13:12 14:11 14:41
page 1 of 1
FORM V VOA
OLM03.0
24
DUP0503 08000
5A
VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK BROMOFLUOROBENZENE (BFB)
Lab Name: LANCASTER LABS
Lab Code: LANCAS
Case No-: ______
Lab File ID: >ISOTl
instrument ID: HP03046
GC Column: DB624
ID: 0.53 (mm)
Contract: ______ . SAS No.: ______ . SDG No.: _______ . BFB Injection Date: 09/24/96 BFB Injection Time: 11:10 . Heated Purge: (Y/N) N
m/e
50 75 95 96 173 174 175 176 177
ION ABUNDANCE CRITERIA
8.0 - 40.0% of mass 95 30.0 - 66.0% of mass 95 Base peak, 100% relative abundance 5.0 - 9.0% of mass 95 Less than 2.0% of mass 174 50.0 - 120.0% of mass 95 4.0 - 9.0% of mass 174 93.0 - 101.0% of mass 174 5.0 - 9.0% of mass 176
1-Value is % mass 174
% RELATIVE ABUNDANCE
21.5 49.6 100.
7.0 1.1 ( 1.8)1 64.2 4.9 ( 7.6)1 62.8 ( 97.8)1 4.2 { 6.7)2
2-vaiue is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
Ip a SAMPLE NO.
es b
SAMPLE ID
:
LAB FILE ID
5EPI ANALYZED
TIME ANALYZED
01 VSTD010 02 VSTD020 03 VSTD050 04 VSTD100
05 VSTD200 06 VBLKI95 07 BRA5S 08
09 10
11
12 13 14 15 16 17 18 19 20 21 22
010 PPB IC 020 PPB IC
050 PPB IC 100 PPB IC 200 PPB IC VBLKI95 2583205
>ISOIl >IS0I2
>IS0I3 >IS0I4
>IS0I5 >ISOB3 >IS001
09/24/96 09/24/96
09/24/96 09/24/96 09/24/96 09/24/96 09/24/96
11:35 12:08
12:50 13:23 13:56 15:43 16:23
page 1 of 1
FORM V VOA
QLM03.0
25
DUP050308001
8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY
Lab Name: LANCASTER LABS
Contract: ______ .
Lab Code: LANCAS
Case No.: _____
SAS No.: ___________ SDG No.: ______.
Lab File ID (Standard): >GSPS1
Date Analyzed: 09/25/96
Instrument ID: HP03460
Time Analyzed: 00:26
GC Column: DB624
ID: 0.53 (mm)
Heated Purge: (Y/N) N
12 HOUR STD UPPER LIMIT LOWER LIMIT
ISl(BGM) AREA #
58132 116264
29066
RT #
9.49 9.99 8.99
IS2(d f E) AREA #
RT #
243476 11.09 486952 11.59
121738 10.59
1S3(CBZ) AREA #
RT #
197202 15.36 394404 15.86
98601 14.86
EPA SAMPLE NO.
01 VBLKG24 02 BRA2D
03 BRA2S 04 BRAID 05 BRA1S 06 MRA2S 07 MRA2SMS 08 MRA2SMSD 09 BRAF1
10 BRAT2 11 MRA1S 12 MRA1D
13 MRA2D 14 TB3FM
15 MRA4S
16 MRA3S 17 MRA3D 18 MR3DD 19 MRAFB 20 MRTB4 21
22
47273
45203
43616 42390
46112 46326 45165 46550 45345
45012
46147
45607 42125 43375-
43050
44476 43668 43617
44189
43139
9.50
9.49
9.46 9.45 9.48 9.49 9.49 9.50 9.46
9.45
9.48 9.48 9.49 9.43
9.45 9.46 9.46 9.46
9.48
9.45
187620
184177
172338 163927 180206 181876 174760 180523 182909
170584 176866
175880 153258
166648
163107
169366 167569 165520
167898
165161
11.10
11.08
11.05 11.05
11.08 11.08 11.09 11.10 11.06
11.05 11.07
11.08
11.07 11.04
11.04 11.05 11.06 11.06 11.07
11.05
153010 148674
136114 132526 145332 149856 141875 143435 143510 136060 144085 142240 124991 133567
133232 137466 137313 134757 134641
132325
15.37 15.37
15.33 15.33 15.35 15.35 15.37 15.37 15.33
15.33 15.35 15.36 15.36 15.31
15.32 15.33 15.34 15.32 15.36
15.32
151 (BCM) = Bromochloromethane
152 (DFB) = 1,4-Difluorobenzene 153 (CBZ) = Chlorobenzene-d5
AREA UPPER LIMIT - +100% of internal standard area
AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = +0.50 minutes of internal standard RT RT LOWER LIMIT = -0.50 minutes of infernal standard RT
# Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits.
page 1 of 1
FORM VIII VOA
OLM03.26
DUP050308002
SA VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY
Lab Name: LANCASTER. LABS
Contract: _.
t .ain code: LANCAS
Case No.: ______ . SAS No.: ___________ SDG No.: _______.
Lab File ID (Standard): >ISJS1
Date Analyzed: 09/19/96
Instrument ID: HP03046
Time Analyzed: 06:34
GC Column: DB624
ID: 0.S3 (mm)
Heated Purge: (Y/N) N
IS1(BCM) AREA #
IS2(DFB)
RT #
AREA #
IS3(CBZ)
RT #
AREA #
RT #
12 HOUR STD UPPER LIMIT
LOWER LIMIT
30709 61418 15355
8.34 8.84
7.84
129120 10.01 258240 10.51
64560 9.51
94592 14.33 189184 14.83
47296 13.83
EPA SAMPLE NO.
01 VBLKI93 02 BRATB 03 BRS3D 04 BRS3DMS 05 BRS3DMSD 06 DRA3S 07 BRS4S 08 BR4DD 09 BRA4D 10 11 12 13 14
15 16
17
18
19
20 21
22
39611 40404 39376
39018
40297
38676 38771 39747 40307
8.35 8.36
8.35 8.36
8.35
8.38 8.36 8.35 8.38
163966 168853
165349 162767
167429
163613 163565 166824 167994
10.02 10.02
10.03
10.02
10.01 10.05
10.04 10.03 10.04
121256 124072 122020 121783
125468 121255
121552 123866 124864
14.33 14.31
14.33
14.32
14.32
14.34 14.33 14.34 14.35
151 (BCM) = Bromochloromethane 152 (DFB) = l,4~Difluorobenzene 153 (CBZ) = Chlorobenzene-d5
AREA UPPER LIMIT = +100% of internal standard area
AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = +0.50 minutes of internal standard RT RT LOWER LIMIT = -0.50 minutes of internal standard RT
# Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits.
page 1 of 1
FORM VIII VOA
OLM03
DUP050308003
8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY
Lab Name: LANCASTER LABS
Contract: ______ .
Lab Code: LAMCAS
Case No.: _____
SAS No.: _________ SDG No.: _______.
Lab Rile ID (Standard): >lSOI3 instrument ID: HPQ3046
Date Analyzed: 09/24/96 Time Analyzed: 12:50
GC Column: DB624
ID: 0.53 (mm)
Heated Purge: (Y/N) N
ISl(BCM) AREA #
" IS2CDFB)..
RT #
AREA #
IS3(CBZ)
RT #
AREA #
RT #
12 HOUR STD UPPER LIMIT LOWER LIMIT
30984
61968 15492
8.17
8.67 7.67
125072 9.84 250144 10.34
62536 9.34
97357 14.15 194714 14.65
48679 13.65
EPA SAMPLE NO.
01 VBLKI95 02 BRA5S 03 04 05 06 07
08 09
10 11 12
13 14 15 16
17 18
19
20 21
22
18842 35115
8.19 8.20
73204 139655
9.85 9.86
55305 14.18 106918 14.18
151 (BCM) "= Bromochloromethane 152 (DFB) == 1,4-Difluorobenzene 153 (CBZ) = Chlorobenzene-dS
AREA UPPER LIMIT = +100% of internal standard area
AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = +0.50 minutes of internal standard RT RT LOWER LIMIT = -0.50 minutes of internal standard RT
/ Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits.
page 1 of 1
FORM VIII VOA
OLMO30S
DUP050308004
Sample Data
DUP050308005
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract:
BRA5S
Lab Code: LANCAS
Case No.: ______ SAS No.:
SDG NO.:
Matrix: (soil/water) WATER
Lab Sample ID: 25S3205
Sample wt/vol: 5.0
(g/mL) ML
Lab Pile ID: >IS001
Level: (low/med) LOW
Date Received: 09/18/96
% Moisture: not dec. _______
Date Analyzed: 09/24/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
1.0
Soil Extract Volume: _______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: fug/L or ug/Kq) UG/L
Q
74-87-3------------------ Chloromethane 75-01-4------------------ Vinyl Chloride 74-83-9----------------- Bromomethane 75-00-3----------------- Ch 1 oroethane 75-35-4-----------------1,1-Dichloroethene
67-64-1------------------ Acetone 75-15-0------------------Carbon Disulfide 75-09-2------------------ Methylene Chloride 75-34-3-----------------1,1-Dichloroethane 540-59-0---------------1,2-Dichloroethene (total) 78-93-3-----------------2 -Butanone 67-66-3------------------ Chloroform 107-06-2----------------1,2-Dichloroethane 71-55-6------------------ 1,1,1-Trichloroethane 56-23-5------------------Carbon Tetrachloride 71-43-2------------------ Benzene 79-01-6------------------ Trichloroethene 78-87-5------------------1,2-Dichloropropane 75-27-4------------------ Bromodichloromethane
10061-01-5-----------cis-l, 3-Dichloropropene 10061-02-6------trans-1,3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane 124-48-1---------------- Dibromochloromethane 75-25-2----------------- Bromof orm 108-10-1------- --------4-Methyl-2-Pentanone 108-88-3---------------Toluene 12 7 -18-4---------------Tetrachloroethene 591-78-6----- ---------2 -Hexanone 108-90-7----------------Chlorobenzene 100-41-4---------------Ethylbenzene 1330-20-7--------------Xylene (total) 100-42-5----------------Styrene 79-34-5----------------- 1,1,2,2-Tetrachloroethane
FORM I VOA
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
OLMO3.0^0
DUP050308006
-m-rot t o m c h r o ma t o g r a m
Data File: >ISQ01::D4
Name: BRA5S
25832U5
Mi sc: ~SJL WL %L 1 + >
Quant Output File: Instrument ID:
#1962631AB &5 *5 $''1SQB3
/'ISO01::D? HPCI3 046
id File: 1A6590::DB
Title: 3/9U SOU Water/'Med Soil ID File for Inst. HP03Q46
Last Calibration: 951122 10:44
Last Qcal Time: 960924 12:50
Operator ID: Quant Time : Injected at:
SJL-176 960924 16:47 960924 16:23
31
DUP050308007
QUANT REPORT
Llperetor ID: SOL-1/6
Uutput Files ~iSU01s sD7
Uata File:
>1SQ0I::U4
Name: BRASS
2583205
mac: ~S0L |WL JSC =! +>
Wuant #1962631AB &5
Revs 5
7 Qu ant Tlme:
Injected at: Dilution Factor:
Instrument ID: `ISQ83
Page 1
VC.U924 it- * A.-
960924 16:23 i . 0U000
HP03046
lu Files IA639B::DB iitie: 3/90 SOW Water/Med Soil Last Calibration: 951122 10:44
ID File
for
Inst. HP03U46 Last Qcal Time:
960924
12:50
Compound
1) 15) i?) 29) 51) 41))
*8ramaehforomethane I,2-Dichloroethane-d4
*154-DiF1uorobenzene *Chlorobenzene-d5
toiuene-d8 4-BromoFluorobenzene
* Compound is IB I'D
R.'l . Q ion
8.20 9.15 9.86 14.10 12.0B 15.90
128.0 65.0
114.0 117.0
98.0 95.0
Area
35115 63490 139655 106918 123922 9B150
*---O Tt C
Un its
50.00 46.76 50.00 50.00 5U . 84 49.53
UG/L UG/L UG/L UG/L UG/L UG/L
9/
91
87
85
y6
81
32
DUP050308008
Lancaster Laboratories Quantitation Report-GC/TIS Volatiles
Lift: SI <5 S 3 2 O 5
SO l--
File: "ISuai Injected: 16:23 09/24/96
Sample: BRASS
2333203
Dilution Factor:
1.0
Initial Uolume/Ut.:
3.0
Standard: "ISOli
Inst. 1^03046
Batch:
I962631AB
Final Volume/Ut.t 5.0
flethod: 7194 Hatrix/level: UL Blank: l'iSUB3
$ Internal Standaras
R.I. (V-RT) Sean Dion
Areal*/-*Area) Cone.
UC Flag tone Units = uq.'L
TX. BramoehIoromethane 17. 1,4-Bifluorobenzene 21. Chisrobfinzene-db
* = RETENTION TIME OUT OF RANGE
8.2041.0324) 550 128
35115( 13)
50.08
9.8561.0178) 692 114
139655( 12)
50.00
14.181.0300) 1064
117
1069181 10)
50.00
* * INTERNAL STANDARD AREA OUT OF RANGE
NC - NOT ABLE TO CALCULATE--NO STANDARD.
Xf Surrogate Standards
R.T. IV-RRT) Scan
Dion
Area
Cone.
ffitee. Q
RHaiesaBaaftaBsacaBaB*a*as>anM(taai
iia>aitaaBMiaatataaaiaaaasaaaKMBaa8BBnaiaaasi8aaaaBnaaasBaaBssaas8XBB&
15. 1,2-Dichloroethane-d4
9.14?(-.0Q1)
631
65
31. Toluene-dfl
12.08C-.0003
683
98
40. 4-Bromofluorobenzene
15.90I-.001) 1212
95
# - RELATIVE RETENTION TIME OUT OF RANGE * - REC OUT OF RANGE
63490
46.76
94
123922
50.84
102
98150
49.53
99
0 SURROGATES DILUTED OUT NC
COULD NOT CALCULATE
Cone.
Quantitaticn
t target Compounds
R. t. (+/-SRT)
Scan Own
Area Cone.A
Conc.B
Blank 0
Limit
3SBaBBBBttBBBBma*B3BBBBBB**B:EBBBmBB*BB*BBBmBB*am3**mBmwBBBBBwBBBBBBSBB:B**BBBB**BBBBBBmBBBBBMB*
Ch Ioromethane
10
Vinyl Chloride Uromomethane Chloroethane 1.1- Qichlorostherie
10
ID 10 10
Acetone Carbon Disulfide
10 ID
Methylene Chloride 1.1- Dichloroethane
10 10
1.2- Dichloroethene (total)
10
2-Butanone
10
Chloroform
10
1.2- Bichloroethane
10
1,1,1-Trichloroathane
10
Car&on letrachloride
10
Benzene
10
Tnchloroethene
10
1.2- Dichloropropane
10
bromodichIoromethane
10
cis-l,3-Dichloropropene
10
trans-1,3-Dichloropropene
10
1.1.2- Trich loroethane
10
sssasss: ssaessssmasxsssassatsttsmssxasBSttKaag essBSseatsasac&sssssssasaesssxsBasss&ssaat&assssscsBeBsiaararcaBisssKs.sssa isasses
ft = RAW CUNC. 6 - CONC. MULTIPLIED BY DILUTION FACTOR E - CONC. OUT OF CAL. RANGE * - RELATIVE RETENTION TIME OUT OF RANGE
Lab Chronicle:
.Ent. by
,,Ver. by
PAGE 1 UF 2
DUP050308009
Lancaster Laboratories Quantitation Report-GC/HS Volatiles'
LLl*: 2 9 O 3 2 O E5
SJL
Fslei AiSUUl injected: 16:23 U9/24/96
Sample: BRA5S
2583285
Dilution Factor:
1.0
initial Uoiume/Ut.!
5.8
Standard: AISUI3
Inst. HP03046
Batch:
1962631A8
Final VeUme/Ut.: 5.8
flethod: 7156 ttatrix/iewel: UL Blank: A1SQB5
t 1argot Compounds
R.T.C+/-RRT)
Scan Qion
Area
Cone.A
Conc.B
Cane. Blank 8
Quantitation Limit
27. Dibromochlororaethane 2B. Brantsform 38. 4'-flethyl-2-Fentanone 32. Toluene 35. ietrachioroathene 34. 2-Hexanone 55. Chlorobenzene 36. Ethylbenzene 58. Xylene (total) 39. Styrene 41. 1,1,2,2-letrachloroethane aaaasaaaaaassaaaaaaaaaaaasaaaa!
A = m COfC. B = DISC. nULf(PLIED BY DILUTION FACTOR
II) IB 1U 10 10
18
10 10 10 10
10 as3E*3ta;xB'SaaiassssBBKaaascBst:
E CUNC. OUT OF UAL. RANGE * = RELATIVE RETENTION TIME OUT OF NANCE
Lab Chronicle:
,,Ent. by
DUPO 50308010
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract:
BRA4D
Lab Code: LANCAS
Case No.: _______ SAS No.:
SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: 2583206
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >ISJ17
Level: (low/med) LOW
Date Received: 09/18/96
% Moisture: not dec. _______
Date Analyzed: 09/19/96
GC column: DB624
ID: 0.53 (mm)
Dilution Factor:
l.o
Soil Extract Volume: ______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3----------------- Ch1oromethane 75-01-4------------------ Vinyl Chloride 74-83-9-----------------Bromomethane 75-00-3------------------ Chloroethane 75-35-4------------------ 1,1-Dichloroethene 67-64-1------------------ Acetone 75-15-0---------------Carbon Disulfide 75-09-2------------------Methylene Chloride 75-34-3-----------------1,1-Dichloroethane 540-59-0----------------lr2-Dichloroethene (total) 78-9 3-3-----------------2-Butanone 67--66--3---------------Chloroform 107-06-2--------------1,2 -Dichloroethane 71-55-6----------------- 1,1,1 -Tr i chloroethane 56-23-5------------------Carbon Tetrachloride 71-43-2------------------Benzene 79-01-6------------------Trichloroethene 78-87-5----------------- 1,2-Dichloropropane 75-27-4-----------------Bromo d i ch loromethane
10061-01-5----------- cis-1,3-Dichloropropene 10061-02-6----------trans-1,3-Dichloropropene 79-00-5------------------1,1,2-Trichloroethane 124-48-1----- ---------- Dibromochloromethane 75-25-2------------------Bromoform 108-10-1---------------4-Methyl-2 -Pentanone 108-88-3---------------- Toluene 127-18-4---------------- Tetrachloroethene 591-78-6----------------2-Hexanone 108-90-7----- ---------- Chlorobenzene 100-41-4----------------Ethylbenzene 1330-20-7--------------Xylene (total) 100-42-5----------------styrene 79-34-5------------------ 1,1,2,2-Tetrachloroethane
FORM I VOA
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
10 V
10 u
----------------------------------------------------------------- --------------------------
_
OLM03.0*>'J
DUP050308011
TdTfiL ION CHROMATOGRAM
Data File: >ISJ17::03
Quant Output File:
Name: BRA4D
2583206
Instrument ID:
Nisc: ~TLN gWL XC =1
*1962631AA &5 *5 $~ISJB2
/*'IS017::07 HPQ3Q46
Id File: IA639Q::DB
Title: 3/-90 SOW Water7Med Soil ID File for Inst. HPD3046
Last. La Iibrat ion: 951122 10:44
Last Qcal Times 960919 06:34
Operator ID: TLN-262 Quant Time : 960919 15:06 Injected at: 960919 14:41
36
DUP050308012
QUANT REPORT
Uperator ID: TLN-262
Output File: '"*ISJ17::D7
Data File:
>1BJ1?::D3
Name: BRA4D
2533206
mac: "TLN JjOWL S4C =1 +>
Quant =11=1962631AA &5
Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
*5 $'"13082
Page 1
96U919 15:U6 960919 14:41
1.UOUUU HPU3Q46
ID File: IA6390::DB
Title: 3290 SOU! Water/Tied Soil ID File for Inst. HP03Q46
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
1) 15 ) 17) 29 ) 51 )' 40 )
^Bromochloromethane 1,2-Dichloroethane-d4
*1,4-Difluorobenzene *Ch16robenzens-d5
To luene-dS 4-Qromofluorobenzene
* Compound is 1STD
R.T. Q ion
8.38 9.33 10.04 14.35 12.25 16.09
128.0 65.0
114. 0 117.0
98.0 95.0
Area
40307 87236 167994 124864 148480 100430
Cone
Units
50.00 46.97 50.00 50.00 50.20 48.60
UG/L US/L UG2L UG7L UG^l UG2L
q
92 90 89 84 97 74
37
DUP050308013
Lancaster. Laboratories Quantitation Report-GC/MS Volatiles
III*: 2583206
Hlei ''1SJ17 Injected! 14:41 89/19/96
Sample: 8RA4D
2583206
Dilution Factor:
1.0
Initial Uoluma/Ut.:
5.0
Standard: AISJS1
Inst. HP03046
Batch:
1962631AA
Final Volume/tlt.: 5.0
Method: >156 Matrix/level: UL Blank: '13^82
t Internal Standards
R.T. (*/-GT) Scan Qion
ftreaU/-)iArea) Cone.
SC Flag Cone Units = ug/L
1. Oroaochloromathane 17. 1.4-Difluorobenzene 29. Chlerobenzana-d5
0 - RETENTION TIKE OUT OF RANGE
8.386(.641?) 570 128
403071 31)
58.UO
10.041.0293) 713 114
1679941 30)
56.08
14.35(.(1267) 1884
117
12B64( 32)
98.08
* - INTERNAL STANDARD AREA OUT OF RANK NC - NOT ABLE TO CALCULATE--NO STANDARD.
S Surrogate Standards
R.T. (+/-RRT) Scan
Qion
Area
Cone.
SRec.
15. l,2-Dichloroatbane-d4
9.334C-.001)
652
65
31. Toluena-dB
12.251.0810)
903
98
40. 4-Bromofluorobenzene
16.09C.0804) 1233
95
# RELATIVE RETENTION TIME OUT OF RANGE * - XREC OUT OF RANGE
87236
46.97
94
148480
50.20
100
100430
48.60
97
D SURROGATES DILUTED OUT NC - COULD NOT CALCULATE
Cone.
Uuantitation
$ Target Compounds
R.T.C+/-KRT)
Seen Qion
Area
Cone.A Cone.if
Blank Q
Limit
x5acea>ssass&BB3!BBaBstEiaaBBSfl98BOSBasssRBnKaBCBSWRnts>anmBaBnstcamMnMBsaaBBiWiBnoasseaaRSi:isas8isss>MSKS
.2 Chloromethane
ID
3. Vinyl Chloride
10
4. Broraomethane
&j Chtoroethane
.6 1.1-DichloroBthene
1U 10 10
1. Acetone
.8 Carbon Disultide
18 lu
9. Methylene Chloride
.11 1.1-Dichloroethane
.12 1.2-Dichloroethene (total)
10
18
10
13. 2-Butanene
18
14. Chloroform
10
16 1.2-Dichloroethane 18. 1,1,1-Triehloroathane
18
10
19. Carbon Tetrachloride
.20 Benzene
.21 Tnchloroethene .22 1.2-Dichloropropane
23. Uromodichloromethane
2a. cis-l,3-Dichloropropene
25. trans-l,3-0ichloropropene
26. l,l)2-Trichloroethane
1U 10
18 10 18
10
10 10
saeaaassssBsase&sasaaasvasessajgtetKatssiasBaaeea&eaesaicattSBssassssssaaBsasssaa&sssesas
ft RfiW C0NC. B - C0NC. MULTIPLIED BY DILUTION FACTOR E C0NC. OUT OF CAL. RANK t RELATIVE RETENTION TIME OUT OF RANGE
Lab Chronicle:
,,Ent. by
.Ver. by
PAGE 1 OF 2
ICO I
DUP050308014
Lancaster Laboratories Quantitation teport-SC/MB Uolatilas
LLi#: 2! "5 3 3 2 O *.
Tl__M
File; A1J17 injected: 14:41 89/19/96
Sanpla! BRS4D Dilution tactor:
2583206 1.1)
Initial Volume/Ut.:
5.0
Standard: A1SJS1
Inst. HPD3Q46
Batch:
1962631fift
Finai yolune/tlt.: 5.0
Rethod: 7156
Hatrix/leval: III Blank: ASSJB2
* larget Compounds
R.T.U/-KRT)
Scan Qion
Area
Cone.ft
Cone.8
Cone. Blank Q
Quantitation Limit
B8usBsBBSBnuHniaaaa8saiaac5smisimBSsaB3iaiss8aatssKnBtaBUUnHS8smnaKKsniBuiSRBiMssamtia3Stsnc8BSB*s*n&
27. Uibromochloromethane
~----- -------------------------------------------------------------------------------- -----------------------
11)
. 28. Bronoform 30. 4-flettiyl-2-Pentanone
32. Toluene
33. letrachloroothene
34. 2-Hexanone
--;------- ;----------------------------------------------------------------------------------------- --------------------------------------------------------------------------- --------------------------------------------- -----------
'------------------- ------------- --------------- ------------------------------- -----------------------------------
----------------------------------- ------------------------------- ------------------------------- ---------------------------
------------------------------ ~---------- --------------------------- ------ -
io 10 10 18 10
35. Chlorobenzene ' 36. Ethylbenzene '
-------------- ------ ---------------- ----------------- --------------------------------------------------------------------- --------------- -------------- ------- ------------ -----------'--------- ---------- i-- -------- *----------
18 '10
38. Xylene Uotell 39. Styrene 41. 1,1,2,2-tetrachloroethane
----------------------- ----------------------------------------------- ------------------------------------------------------------- ----------- --------------------------------------------- ------------- --------------------------------------------------- ------------------------ ;------------------------------------------------------------------------------
18 10 18
ssBsaKss&saBaBBaBBBBBBauBmaBBBBmBaauEaBBsmaaaBSBmsaBBBBaanaBSSBSSBasBBBBBBBamsBBBBBBBBsxBBBmanamBBaasBBBaBsamBBBBaBBmBBaaBaamBBBBBmBm
ft KAO CONC. B = CONC. MULTIPLIED BY DILUTION FACTOR E CUNC. OUT OF CflL. RANGE 4 * RLLftTUJE ROBmuN TIME BUT OF RANGE
Lab Chronicle:
Ent. by,
eft
3
DUP050308015
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Lab Code: LANCAS
Case No.: ____
Contract: SAS No.:
BR4DD SDG NO.:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0
(g/raL) ML
Level: (low/med) LOW
Lab Sample ID: 2583207 Lab Pile ID: >ISJ16 Date Received: 09/18/96
% Moisture: not dec. ______
Date Analyzed: 09/19/96
GC Column: DB624
ID: 0.53
Dilution Factor:
1.0
Soil Extract Volume: ______ (uL)
Soil Aliquot Volume: ______ (UL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3-----------------Chloromethane
75-01-4------------------Vinyl Chloride
74-83-9--------Bromomethane 75-00-3------------------Chloroethane 75-35-4-----------------1/ 1-Dichloroethene
67-64-1------------------ Acetone 75-15-0--------- ---------Carbon Disulfide 75-09-2-----------------Methylene Chloride 75-34-3---------------1,1-Dichloroethane
540-59-0----------------1,2-Dichloroethene (total)
78-93-3----------------- 2-Butanone
67-66-3------------------ Chloroform 107-06-2--------------- 1,2-Dichloroethane 71-55-6------- --------1,1,1-Trichloroethane
56-23-5------------------Carbon Tetrachloride
71-43-2------------------ Benzene 79-01-6------------------ Trichloroethene 78-87-5----------------1,2-Dichloropropane
75-27-4-----------------Bromodichloromethane 10061-01-5-----------cis-1,3-Dichloropropene 10061-02-6--------- -trans-rl, 3-Dichloropropene
79-00-5----------------- 1,1,2-Trichloroethane 124 -48-1------- ----Dibromochloromethane
75-25-2------------------ Bromoform 108-10-1---------------- 4-Methyl-2-Pentanone
108-88-3---------------- Toluene
12 7-18-4--------- -------Tetrachloroethene 591-78-6--------------- 2-Hexanone 108-90-7---------------- Chlorobenzene 100-41-4---------------- Ethylbenzene 1330-20-7--------------Xylene (total) 100-42-5----------------Styrene 79-34-5--------- ---------1,1,2,2-Tetrachloroethane
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VOA
OLM03.0
40
DUP050308016
Data File: >ISJ16::D3
Quant Output File:
Name: BR4DD
25832 07
Instrument ID:
Mi sc: ~TLN @WL KC 1 +> # 1962631AB &5 *5 $'VISJB2
/'ISJ'16::D7 HP03EJ46
Id Files 1A6390::DB
Titles 3/90 SOU Water/Med Soil ID File for Inst. HP03046
Last Calibrations 951122 10:44
Last Deal Times 960919 06:34
Operator IDs TLN-262 Quant Time : 960919 14:35 Injected at: 960919 14:11
41
DUP050308017
QUANT REPORT
Page 1
Uperator ID: TLN-262
Output File: '"'IS316;:D?
Data File:
>1SO16::Q3
Name: BR4D0
2563207
mac: ~TLN WUIL %
*>
Quant #I962631Aft &5
Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
*5 AISJIB2
960919 14:35 960919 14:11
1.00U0U HP03046
ID File: IA6390::OB Title: 3/90 BOW Ulater/Med Boil ID File for Last Calibration: 951122 10:44
Inst. HP03046 Last Qcal Time:
960919 06:34
Compound
1? 15) 17) 29 ) 31 ) 40 )
*Bramochloromethane 1 /2-Di Ohio roe thane-d4
*1,4-Di fluorobentene *Chlorofaenzone-d?
To tuene-d8 4-8romofluorobenzene
* Compound is l&TD
R.T. Q ion
8.35 9.32 10.03 14.34 12.22 16.06
128.0 65.0
114.0 117.0
98.0 95.0
Hrea
39747 86127 166824 123866 149489 104525
Cone
Units
30.00 47.02 50.00 50.00 50.95 50.99
UG/L UG/L UG/L UG/L UG/*'L UG/L
q
92 90 87 84 97 77
42
DUP05030801 8
Lancaster Laboratories Quantitation Raport-GC/ftS Volatiles
LLMM 25832 07
Tl--IN
tiie: *15016 Injected! 14:11 09/19/96
Sample: BR4DD
2583207
Dilution tactor:
1.0
Initial Uolufee/Ot.:
5.0
Standard! *ISJS1
inst. I03046
Batch:
I962631flfl
Final Uialume^Ut.: 5.0
Method: 7156 Matrix/level: WL Blank: *15052
$ Internal Standards
R.T. (+/-RT) Scan Dion
Area(+/-XArea) Lone.
DC Hag Cone Units = ug/L
sBu&e8MCS8sasE8Bsssi8WBBaasimasaasmtaaTCMfuatMiBsiiiummansBiMcwRiuniBcsaBSBswMnans8snB<iBe**sNaaaiBBsx
1. Bromochlororaethane 17. 1,4-Oifluorobenzena 29. Chlorobenzene-dS
* RETENTION TIME OUT OF RAISE
8.5541.8150)
569 128
39?4?( 29)
5B.U0
Id.Q3(.fll32)
713 114
166824( 29)
50.00
14.34(.0122)
1884
117
123B66< 31)
50.0U
* * INTERNAL STANDARD ARBI OUT OF RANGE
NC - NOT ABLE TO CALCULATE--NO STANDARD.
4 Surrogate Standards
R.T. l*/-RRT) Scan Oeo o
Area
Cone.
XRec. 0
15. l,2-f)iehloroethane-d4
9.3181.0018)
652 65
31. Toluene-d8
12.221.0000)
902 98
40. 4-Bromafluorobenzene
16.06(-.008)
1232
95
# * RELATIVE RETENTION TIME OUT Iff RANGE * SREC OUT OF RANGE
86127
47.02
94
149489
50.95
102
104525
50.99
102
D - SURROGATES DILUTED OUT NC COULD NOT CALCULATE
Cone.
Quantitation
$ target Compounds
R.T.(+/-HRT)
Scan Qion
Area Cone.A
Conc.B
Blank Q
Limit
^rr^Tf,^r.tBrTtTrrtttTt.w^y>ta,gB:T1rfff.Mi!!.Miea^Mmai-acgaiegaigMtKggaatMiMamaKtKaiaBiauaameaMggaaaiititBsmoiKwBBttat8
2. Chloroaethane 3. Uinyl Chloride
--------------------------------------- ------------------------- *------------------------------------------------------------------------------- -------------- ------------------------------ -------------------------------------
10 10
4. tiromofflethane
------------------------<-----------------------------------------------------------------------------------------------------
18
5. Chloroethane 6. 1,1-Dtehloroethene
--------------------------------- ----------------------------- _-------------------------------------------- ---------------
10
-------- -1-TM------- ---------- ------- -------- ------- -------------- ---------------------------10
7. Acetone
3. Carbon Uisuifide
9. Methylene Chloride
11. l.l-Dichloroethene
-------------------------------------------------- -------- -------- --------- ---------- -------------------------------
18
12. 1,2-Dichloroethene (total) ---------------------------------------------------------- :------------------------------------------------------------------
10
13. 2-Butanone
------------------------------------ *------------------------------------ --------------------------------------------------
10
14. Chloroform
------------------------------------------------------------------- ---- ------------------------------------------------
10
16. 1,2-Dichtoroethane
15. 1,1,1-Tr ich toroethane
19. Carbon tetrachloride
20. Benzene
------------------------------------------------ -------------------------------------------------------------------- ---
10
21. Irichloroethene
22. 1.2-Dichlorcpropane
23. Bromodicnloromathane
24. cis-l,3-Dichloropropene
------------------------------------------------------------------------------------------------------------------------------------
10
25. trans-l,3-Dichioropropene
----------------------------------------------------------------------------------------------------------------- 1-----------
1(1
26. 1,1,2-Trichloroethane
sa=saasaBsesas8SBaasrttCssessaBS3B&ttSBeBSSKSBBa8BBttssssaaBeS8S3msaaKVSessSKOB3cttBBCSas8%esassssSBSSBSSsaDBBa_sseBSasxass.ss:s;3.18D8ESSsms
A - RAW CQIC. B - C0NC. MULTIPLIED BY DILUTION FACTOR E CQNC. OUT OF CAL. RANGE * RELATIUE RETENTION TIME OUT OF RANGE
Lab Chronicle: ;Ent. by.
------------------:------------------------------------------------------------------------------:----------------------------------------------------------------------------------------------:-------------------------------------------------------------------------------------------------------------------------------------------------
PftEE 1 OF 2
DUP050308019
Lancaster laboratories Quantitation Report-GC/flS Uolatiles
LLl#: 2^032 07
Tl__N
Files '"ISO16 Injected: 14*.II 09/19/94
Sample: BR40B
2583207
Dilution Factor:
1.0
Initial Uolune/Ut.:
5.0
Standard: "ISJSl
inst. HP03846
Batch:
IH2631AA
Final Dolune/Ut.: 5.0
Method: 7156 Matrix/lavel: VIL Blank: *15082
$ Target Compounds
R.T.(*/-RRT)
Scan Qiort
Area
aaaica*6s***:am*misaiem***J*aa*****a*a***a********f*****i
27. Qibromach loronethane
------ -------------------- -------------- ------------ ---------
38. 4-ttethyl-2-Pentanone 32. Toluene 33., letrachloroethane 34. 2-Hexanene 35. Chlorobenzene 36. Ethylbenzene
38. Xylene (total) 39. Styrene 41. 1,1,2,2-Tetrachloroethane
--------------------------------------------------------------------------- ----------------------- ------------------------------- --------- ----------------- ----------------------------------------. ------------ --------- ---------------------------;------------------------------------- ---------- --------
-------------------------------- -------------------------------.------------------------ ---------------------------------------- -------------------- --------------------- --------------------
Cone.A
lone.8
Cone. Blank Q
Quantitation Limit
10
10 ID 10
la
10
10
18
10 10 10
A = RAD OJfC. B - tOC. MULTIPLIED BY DILUTION FACTOR E = CISC. OUT OF CAL. RANGE * = RELATIVE RE1ENT1UN TIME OUT OF RANGE
Lab Chronicle:
,,nt. by
44
DUP050308020
' 1A . VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract: ______
BRS4S
Lab Code: LANCAS
Case No.: ______ . SAS No.: _____ _
SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: 2583208
Sample wt/vol: 5.0 (g/mL) ML
Lab File ID: >ISJ15
Level: (low/med) LOW
Date Received: 09/18/96
% Moisture: not dec.
..
Date Analyzed: 09/19/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
1.0
Soil Extract volume:
. ' (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) tXG/L
Q
74-87-3----------------- Chloromethane 75-01-4------------------Vinyl Chloride 74-83-9-----------------Bromomethane 75-00-3------------------Chloroethane 75-35-4--------- -------- 1,1-Dichloroethene 67-64-1-----------------Acetone 75-15-0------------------carbon Disulfide 75--09--2-------------- Methylene Chloride 75-34-3------------------1, l-Dichloroethane 540-59-0----- ----------1,2-Dichloroethene (total) 78-93-3---------------2-Butanone 67-66-3------------------ Chloroform 107-06-2---------------1,2-Dichloroethane 71-55-6------------------1,1,1-Trichloroethane 56-23-5----------------Carbon Tetrachloride 71-43-2------------------Benzene 79-01-6-----------------Tr ichloroethene 78-87-5------------------1,2-Dichloropropane 75-27-4------------------Bromodichloromethane 10061-01-5----------cis-1,3-Dichloropropene 10061-02-6-----------trans-1,3-Dichloropropene 79-00-5------------------1,1,2-Trichloroethane 124-48-1-- ----- --Dibromochloromethane 75-25-2----------------- Bromof orm 108-10-1----------------4-Methyl-2-Fentanone 108-88-3----------------Toluene 127-18-4----------------Tetrachloroethene 591-78-6------ ---------2-Hexanone 108-90-7--------------Chlorobenzene 100-41-4---------------- Ethylbenzene
1330-20-7------------Xylene (total)
100-42-5--------------- Styrene
79-34-5-------------- ir 1 2,2-Tetrachloroethane
FORM I VOA
10 u 10 u
10 D
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 tr 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 D 10 u 10 u 10 u 10 u 10 u 10 u
OLM03.o45
DUP050308021
Data File: >18315::D3
Names BR84S
2583208
Mi sc: ~TLN gWL HC =1 +>
Quant Output File: Instrument IDs
#I962631AA &5 *5 $AISJB2
''IS315::D7 HF'03046
Id Fj les IA639D::DB
Titles 3/90 SQW Water/Med Soil ID File for Inst. HPO3046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLN-262 Quant [irae : 960919 13:36 Injected at: 960919 13:12
46
DUP050308022
QUPNT REPORT
Page 1
tip erstor ID: TLN-262
Quant
Output File! 'MSJlSi: : D7
Data Fites
>1S315:s 03
Name: BRS4S
25832OS
til sc: "TLN .{WL; *C =1 ** ,#1962631AA &9
Revs 7
Quant Time
Injected at
Dilution Factor
Instrument ID
*5 ' ISJB2
960919 13:36
960919 13:12
1.00UGU
HP03046
ID .Files 1A639Q::DB .
Title: 3790 SOW Water''fled Soil ID S- i le for Inst. HP03046
Last Calibration: 951122 10:44
Last deal Time
960919 06:34
Compound
1) 15) 17) 29 ) 31) 41) J
*8romocti loromethane 1,2-Dichloroeth8ne-d4
*1,4-Difluorobenzene *Chlorobenzene-dS
To 1uene-d8 4-Sromofluorobenzene
* Compound is ISTD
R.T. Q ion
8.36 9.32 10.04 14.33 12.23 16.07
128.0 65.0
114. 0 117.0
98.0 95.0
ftrea
38771 84719 163565 121552 146327 99086
Cone
Units
50.00 47.42 50.00 50.00 50.82 49.25
UG7L UG7L UG7L UG/L UG7L UG/'L
q
9a 89 87 85 96 75
47
DUP050308023
Lancaster Laboratories Quantitation Report-GC/MS Volatiles
LLM: 2583200
TL.N
File: "IS315 injected: 13:12 09/19/96
Sample: BRS4S
2583208
Dilution Factor:
1.0
Initial Vniurae/Ut.:
5.8
Standard: ''TSJS1
Inst. HP83846
Batch:
I962d31ftfl
Final Uolume/Ut.: 5.0
Method: 7156 Natrix/level: UL Blank; AlSJd2
* Internal Standards
R.T. (*/-RT) Scan Uion ftrea(*/-SArea) Cone.
QC Flag Lone Units = ug/L
issBessaas*eBBBaBBSs*BBBBBBBBBaBaaBBBS*BBsBBBaBBBBmBBBBBaBBmBmBBBBmBmBBBBBBBBm*BBBmBBB**aBmaBBBBBmi>airs=mB*B==BB=BBm**:
1. Bromochloromsthane 17. 1,4-Difluorobenzane 29 . Chlorobenzene-dS
# RETENTION TltlE OUT DF RANGE
8.365(.0262) 566 128
38771( 26)
50,88
10.84(.O246) 718 114
163565( 27)
58.88
14.33(.81968) 1079
11?
121552( 29)
50.00
* INTERNAL STANDARD AREA OUT OF RANGE
NC NOT ABLE TO CALCULATE--!*) STANDARD.
Surrogate Standards
R.7. (V-RRO Scan
Qian
SSSSSSBSISSS
15. 1.2-Uvchloroethane-d4
9.318C-.808)
64B
65
31. Toluane-dS
12.23(.0006)
898
98
48. 4-Bromofluorobenzene
16,0?(.B807) 1228
95
* = RELATIVE. RETENTION TIME OUT OF RANGE * = *REC OUT OF RANGE
Area
Cone.
XRec. Q
laiaBisiisxstwKCissismsauiisxi!
84719
47.42
95
146327
58.82
102
99886
49.25
98
D SURROGATES DILUTED OUT NC COULD NOT CALCULATE
Cone.
Quantitation
$ target Compounds
R.T.U-/-KRD
Scan Qion
Area
Conc.A
Lonc.B
Blank 0
Limit
BBBBSBBBSBBSSBBBKSBBBSBBBSSBBSBSBBBBBBBBBBBBBBBBBBBBSBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBaBBBBBBBBBBBBBSBBBBBBBBBBBBBBBttSSBBBBSBBBBBBBBB
2. Chloromethane 3. Vinyl Chloride 4. Bromoaethane 5. Cbloroethane 6. 1,1-Dichloroethene 7. Acetone 8. Carbon Disulfide 5. ttethylane Chloride 11. l.l-D:chloroethane 12. 1,2-Dichloroethane (total) 13. 2-Butanona 14. Chloroform 16. 1,2-Dichloroethane 18, 1,1,1-Tnchloroe thane 1?. Carbon Tetrachloride 2U. Benzene
18
18
18
10
18
10
18
18
18
18 18 10 18 10
18
18
21. Irichloroethene 22. 1,2-Dichloropropane 23. Broir.odicnloromethane
24. cis-l,3-Dichloropropene 23. trans-l,3-Dichloropropene 26, 1,1,2-Trichloroethane ssssssasrsssttsssassstsssssss&sassatBStBxeteMfissetsseassatrsstsssesssttSBatBatssflKtssss
18
10
18
10
18
10
sastssssscssscsssessssBSsa
A = RAW CONC. B = CONC. MULTIPLIED BY DILUTION FACTOR E * EMC. OUT OF CAL. RANGE * - RELATIVE RETENTION TIME OUT OF RANGE
Lab Chronicle:
_Ent. by.
Pag e i o f 2
_Ver. by --^ g....
DUP050308024
Lancaster Laboratories Quantitation Report-GC/MS Uolatiles
Lilts St E? S 3 22 O S
T l--i'-'l
:Hlie: "'1SJ15 Injected: 13:12 89/19/96
Sanple: BRS4S
2583208
Dilution Factor:
1.0
lmttai DdltlraB^Ut.s
5.0
Standard: A1SJS1
Inst. HPD3046
Batch:
I962631flfl
Final Uoluaa/Ut.: 5.8
Method: 7156 Matrix/level: Blank: A1S382
Cone.
Quantitation
# target Compounds
R.T.H/-RRTJ
Sean Qian
Area
Conc.fi
Lone.8
Blank Q
Limit
39sastnanaiasiERSralBi&^aatM8XB:BSKS&asaBSBteCBasamtMlBas3imHSlinBB*KsKlBKBM*MKSliVsaiatKKMgMttSSttBaHKnasisaiKMalieesssv
27. Dibromochloromethane
10
28. Bramaform
18
38. 4-ftethyl-2-Pentanone
10
32. Toluene 33. tetrachloroethene
18
1
34. 2-Hexanone 35. Chlorobenzene 36. Ethylbenzene
ID
10 10
38. Xylene (total)
10
39. Styrene
10
41. 1,1,2.2-letrachloroethane
10
asseeesBB8msssa8BesssBBsccaBseisssmaBtianmats>ei*sHMass88ini8aiBMtanMumBnBBraaBBBasn8scsBsases3BsiBS8{iBeMe*
fl RAW CGNC. 8 = LU1C. MULTIPLIED 8 DILUTION PACTUR E * CUNC. OUT UF CfiL. RANGE # = RELflTlDE HETEMT1UN TIME UUI UF RANGE
Lab Chronicle:
.Ent. by
Analyst; Auditor;
A *r
JDates
ll~t)ate:
.. ?/?!%
Uer. by
PAGE 2 Iff 2
40
DUP050308025
. . 1A ^ VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE MO
Lab Name: LANCASTER LABS
Contract:
1
Lab Code: LANCAS
Case No.:___
SAS No.:
BRS3D SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: 2583209
Sample wt/vol: 5.0
(g/mL) ml
Lab File ID: >ISJll
Level: (low/med) LOW
Date Received: 09/18/96
% Moisture: not dec. _
Date Analyzed: 09/19/96
GC Column: DB624
ID: 0.53
Dilution Factor:
1.0
soil Extract velum? ______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) 0g /l
q
74-87-3------------------chloromethane
10 u
75-01-4------------------Vinyl Chloride
10 u
74--83--9-------- --Bromomethane
10 u
75-00-3-----------------Chloroethane
10 u
75-35-4---------------- -1,1-Dichloroetheme
10 u
67-64-1------------------ Acetone
10 u
75-15-0------------------ Carbon Disulfide
10 u
75-09-2-------- --Methylene Chloride
10 u
75-34-3----------------1,1-Dichloroethane
10 u
A
540-59-0----------------1,2-Dichloroethene (total)
10 u
78-93-3---------------2-Butanone
10 u
67-66-3-----------Chloroform
10 u
107-06-2---------------1,2-Dichloroethane
10 u
71-55-6-----------------1,1, l-Trichloroethane
10 u
56-23-5-- ----- ----Carbon Tetrachloride
10 u
71-43-2------------------Benzene
10 u
79-01-6---------------- -Trichloroethene
10 u
78-87-5------------------1,2-Dichloropropane
10 u
75-27-4-------------Bromodichloromethane
10 u
10061-01-5----------- cis-1,3-Dichloropropene
10 u
10061-02--6----------- trans-1,3-Dichloropropene
10 u
79-00-5----------- ------1,1,2-Trich1oroethane
10 u
124-48-1--------------- Dibromochloromethane
10 u
75-25-2------------------Bromoform
10 u
108-10-1--------------- 4 -Methyl-2 -Pentanone
10 u
108-88-3----------------Toluene
10 u
127-18-4----------------Tetrachloroethene
10 u
591-78-6----------- --2-Hexanone
10 u
108-90-7----------------Chlorobenzene
10 u
100-41-4---------------Ethylbenz ene
10 u
1330-20-7--------------Xylene (total)
10 u
A 100-42-5----------------Styrene 79-34-5------------ 1,1,2,2 -Tetrachloroethane
10 u 10 u
FORM I VOA
50OLM03.0
DUP050308026
TOTOL ION CMROMCTOSRClII
Data Filet >ISJ11::D3
Name: BRS3D
2583209
Misc: ~TLN @WL %C =1 +>
Quant Output Files
Instrument ID:
#I962631AA
*5 *'"ISJB2
^IS311::D7 HP03046
Id file: 1A6390::DB
Title: 3/90 SOUi Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLM-262 Quant lime : 960919 11:29 Injected at: 960919 11:04
5i
DUP050308027
QUANT REPORT
Uperator ID: TLN-262
Output Fi le; ''"ISJll: :D7
Data File!
>iSJll:sD3
Name: E3RS3D
2583209
mac: ~TLN (jlWL. KC =1 +>
Uuant #1962631AA &5
Ke u>: 7
Qu ant Ti me
Injected at
Dilution Factor
Instrument ID
*5 $'N1S3B2
Page 1
y609iv ii:2y
960919 11:04
1.ou uoo
HP03046
ID File: IA6390:::DB Title; 3790 BOW Water/fled Soil ID File Last Calibration: 951122 10:44
For
Inst. Last
HPC3046 Qcal Time:
960919
06:34
Compound
1) 15 ) 17) 29 > 31 ) 40 )
Bromoch16 romethane 1,2-Dichloroethane-d4
*1,4-Dif1uorobenzene *Chlorobenzene-d5
'l o iuene-dB 4-Bromo Fluorobenzene
* Compound is tSTD
R.T. Q ion
8.3? 9.30 10.03 14.33 12.22 16.06
126.0 65.0
114.0 117.0
98.0 95.0
Area
39376 85646 165349 122020 147990 97619
Cone
Units
5U.- 00 47.20 50.00 50.00 51.20 48.34
Uc-'L uc/c UG/L UG7L UW7|_ UG7L
A
9j90 89 84 97 76
5S
DUP050308028
Lancaster Laboratories Quantitation Report-SC/ftS Volatiles
LL.I4: 25832 O V
TI_M
hie! "1SJ11 injected! 11:84 09/19/96
Cample: BRS5D
25B320?
Dilution factor:
1.0
Initial Volume/ldt.:
$.0
Standard: AISJS1
Inst. HP03046
Batch:
1962631AA
Final Volume/Ut.: 5.0
Bethod: 7156 ftatrix/level: UL Blank: AlSJli2
V internal Standards SS8)
1. JBrosochloromethane 17. 1,4-Uifiuorobenzene 29. Chlorobenzene-d5
- RETENTION TIME OUT OF RANGE
R.T. ( ART) Sean Qion
Area(+/-*ftrea) Cone.
UC Flag Lone Units = ug/c
8.35U.8124) 566 128
39576( 28)
50.08
18.O5C.0117) 718 114
165349( 28)
50.00
14J3C.8817) 1088
117
122028C 29)
58.09
* - INTERNAL STANDS AREA OUT OF RANGE
NC * NOT ABLE TO CALCULATE---NO STANDARD.
* Surrogate Standards
R.T. CV-RRT) Scan
(lion
Area
Cone.
XRee. It
s8sassQSccasssMBas*iisesBsttBss8S3assaeacuMSicscHKMua8*HsassntBMaBtiiBMn8aa8stnw8>aiUHUsBMasra8as8
15. l,2-Uichloroethane-d4
9.394C-.9U0)
648
65
51. Toiuene-dB
12.22C.8886)
89?
98
48. 4-Qrowjfluorobenzane
16.06C.0906) 1229
95
4 * RELA'I WE RETENTION TIME OUT OF RANGE * - *REC OUT OF RANGE
85648
47.20
94
147990
51.28
182
97619
48.34
9?
D - SURROGATES DILUTED OUT NC COULO NOT CALCULATE
Cone.
Quantitation
target Compounds
R.1.U/-RRTJ
Scan Cion
Area
Cone.A
Conc.b
Blank
Limit
tsaaaniinsnauaiRinnininnainnimniBnnnnnnnminmnnuniBntunninnKonin
2. Ubloromethane 3. Vinyl Chloride 4. Bromomethane 5. Chioroethane 6. 1,1-Dichioroethane 7. Acatone S. Carbon Disulfide 5. Methylene Chloride 11. l.-l-Biciiloroetbane 12. 1,2-Dichloroethene ttotal) 15. 2-Butanone 14. Chloroform 16. 1,2-Oichloroethane 10. 1,1,1-Triehloroethane IV. Carbon ietrachlonde 21). Benzene 21. Snchloroethene 12. 1,2-Dichloropropane 23. arotnodichloromethane 24. cis-l,3-Diehloropropene 25. trans-l,5-Dichtoropropene
18 10 111 10 18 18 18
18 10 18 10
10 1U
10 iu
10 10 18 18 18 18
26 1,1,2-Trich to roe thane
--------------------------------------------------------------- ------------------------------------------------------------
18
sssaMassass9SS8e9Saeefts3s^Sess8aSSS9ssttBSSga8S1B9SSSeaSSSS3QS^BseSaS~eM(!|SeSBttSSSBSXSSSBsasCSS:ra3ne3as98XSeSSSSaSesssBseS8S.asaas
A = RAW CUNC. B - COUC. MULTIPLIED BY DILUTION FACTOR E - CONE. OUT OF CAL. RANGE * = RELATIVE RETENTION TIME OUT OF RANGE
Lab Chronicle:
JEnt. by
PASt 1 UF 2
Ver. by _________
K
%}
a
V
DUP050308029
Lancaster Laboratories Quantitation Report-GC/fB Volatiles
LLl$: 2585209
TLN
Hie: A1SJ11 Injected: 11:04 0949/96
liampie: BRS3D
2583269
Dilution Factor:
1.0
initial Uoluie/Ut.:
5.8
Standard:
Inst. HP03046
Batch:
194263188
Final Volune/Ut.: 5.0
Method: 7156 flatrix/level: Blank: AISJti2
target Compounds
R.1.(*/-RK0
Scan Qion
Cone.
Quantitation
Area Lone.A Conc.B Blank
Limit
MraBsaxascmaBssKattsesttnKSBeetKriBttBafivsMstfcsinBnBs
27. DibroaiochlsrOBiethane
------------ ---------------------------- ----------------------
3tt. 4-nethj)l-2-Pentanone
------------------------------ :------- ------------------------------
32. loluene
TM------------------- ------------------------------
33. letrachloroethene
--------------------------------------------- .---------- -------
34. 2-Haxanona
------------------------------------------ ----------------------
35. Chlorobenzene
------------------------------ --------------------------------------
36. Ethylbenzene
------------------------------- ------------------------------------
38. Xylene (total)
------------------------------------ --------------- ----------------
39.. Styrene
------------------------------------------
41. 1.1.2,2-Set rachloroethane
-------------------- :--------- *---------------------------------------------------------------------;--------
Baaaai3sstsBa8:cc8aBBseBaaaa23s;8B8BBBaB38ss*n8SSBnr3uat8BaBBit8iB8BBnBBn8*BBesnnsBSsoi**8CtMai
1U 111
16
la
10
lit
10
111 10
11)
A t LOtC. B CDHL. MULT IfLIS) BY DlLtltlON FACTOR E * LUC. BUT OF CfiL. SftfffiE * * RELATIVE HElLMTlUN UflE UUf OF RANGE
Lab Chronicle:
_Ent. by
Analyst: Auditor:
iAO-Ctt'&
_Date:
^^-Date:
ijjlfcik
_Ver. by
PAGE 2 OF 2
54
DUP050308030
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
SPA SAMPLE HO
Lab Names LANCASTER LABS
Lab Code: LANCAS
Case No.: ______
Contract: ______ . SAS No.: ______ .
DRA3S SDG No. :
Matrix: (soil/water) WATER
Lab Sample ID: 2583210
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >ISJ14
Level: (low/med) LOW
Date Received: 09/18/96
% Moisture: not dec. .
Date Analyzed: 09/19/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
1.0
Soil Extract Volume: ______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3------------------ Chloromethane
75-01-4------------------Vinyl Chloride 74-83-9------------- --Bromomethane 75-00-3------------------chloroethane 75-3 5-4 --------------1, l-Dichloroethene
67-64-1------------------Acetone 75-15-0----- -------------Carbon Disulfide 75-09-2------------------Methylene chloride
75-34-3------------------1,1-Dichloroethane 540-59-0----------------1,2-Dichloroethene (total)
78-93-3------------------2-Butanone 67-66-3------------------chloroform 107-06-2--------------1,2-Dichloroethane
71-55-6----- ------------1,1,1-Trichloroethane
56-23-5------------------carbon Tetrachloride
71-43-2-------- --------- Benzene 79-01-6------------------Trichloroethene 78-87-5------------------ 1,2-Dichloropropane
75-27-4-----------------Bromodichloromethane
10061-01-5------------cis-1,3-Dichloropropene
10061-02-6----------- trans-l, 3-Dichloropropene 79-00-5-----------------1,1,2-Trichloroethane
124-48-1----- --------- -D ibromochloromethane
75-25-2------------------ Bromoform 108-10--1---------------4-Methyl-2-Pentanone
108-88-3------------- Toluene 127-18-4----------------Tetrachloroethene 591-78-6----------------2-Hexanone
108-90-7----------------Chlorobenzene 100-41-4----------------Ethylbenzene 1330-20-7--------------xylene (total)
100-42-5----------------Styrene 79-34-5----------------1,1,2,2-Tetrachloroethane
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VOA
OLMG3. Cjjj g
DUP050308031
Data File! >ISJ14::D3
Quant Outpuf Fi1e: 'MSJ14::D?
Names DRR3S
2583210
Instrument IDs HPG3046
flisc: ~TLN gML C =1 +> #I962631AA &3 *5 $'"1S3B2
Id F.i le s 1A6390: :DB
Title: 3^90 SOW Uater/'Med Soil ID File for Inst. HPG3046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLN-262 Quant lime : 960919 13:06 Injected at: 960919 12:41
56
DUP050308032
QUANT REPORT
Page 1
Operator IDs TLN-262
Output File: rtISJ14ssD7
Data File!
>1S314:-D3
Nfime ! 0RA3S
2583210
(i;isc: ~TLN (jjfWL.. %C "1 + >
Quant #1$>6263lAA &5
Rev! 7
Quant Time!
in jected at:
Dilution Factor:
Instrument ID:
*5 $-'IS3B2
96U9I9 13 : Ltd 960919 12:41
1.0 0 U 0 0
HP03G46
ID File: IA6390: iBlS: Title ! 5790 EOU) Water/Fled Soil Last Calibration: 951122 10:44
ID File
for
Inst. Last
HP03046 Qcal Tima:
960919
06:34
Compound
1) 15) 17) 29) 31) 40)
^Bromoch iorometbane 1,2-Dichloroethane-d4
*1;4-Difluorobenzene *Chlorofaenzene-d?
Toluene-d8 4-Bromofluorobenzene
* Compound is (STD
R.T. Q ion
Area
8.38 9.33 10.05 14.34 12.24 16.07
128.0 65.0
114. 0 117. 0
98.0 95.0
38676 83628 163613 , 121255 142624 97919
Corec
Units
5 0.00 46.92 50.00 50.00 49.66 48.79
UG/L UG/L UG/L UG/L UG/L UG/L
q
94
8B 87 85
9tl
77
57
DUP050308033
Lancaster Laboratories Buantitatien Report-SC/MS Volatiles
LLt 2583210
TL.N
files A1SJ14 Injected: 12:41 09/12/26
Sample: DRA3S
2583210
Dilution Factor:
1.0
Initial Volune/Wt.f
5.0
Standard: "ISDSl
Inst. HP0J046
Batch:
1962631m
Final Volume/Ut.: 5.0
Method: 7126 tlatrix/level: UL Blank: "ISJua
i Internal Standards
R.T. C*/-RT) Scan Dion
fireaCV-XArea) Cone.
liC Flag Cone Units = ug/L
sasHsmBiraasa3x*a38nEsBi&8:8XBm*Baist9BrtttaBKKaMLBrtaNBaDBmBassataKMSinsanBaBBBmBBMBIBRBWMMBSmiBBBIB8SBIBZ88aBBBBB88BBBBBa*BB8BaS*BnaB8a*
1. Bromochloramethane
17. 1,4-Difluorobenzene 2y. Chiorobenzene-d5
# RETENTION TIME OUT OF RANGE
8.3761.8376) 560 128
38676C 26)
58.00
10.B5t.03ai) 704 114
1636131 27)
5O.0O
14.34C.0184) 1073
117
121255C 28)
50.00
* * INTERNW. STANDARD AREA OUT OF RANGE NC NOT ABLE TO CALCULATE-NO STANDARD.
i Surrogate Standards
R.T. <*/-RRO Scan
9 ion
Area
Cone.
SKee. U
15. I.2-Dichloroethane-d4
9.330C-.080)
642
65
31. Toluena-dS
12.24C.0OD7)
892
98
40. 4-Braiwfluorobenzene
16.07I-.008) 1221
95
* RELATIVE RETENTION TIME OUT OF RANGE * *REC OUT OF RANEE
83628
46.92
142624
49.66
97919
48.79
0 - SURROGATES DILUTED OUT
94 99 98
1C - COULD NOT CALCULATE
Cone.
Quantitation
n
$ Target Compounds
R.T.C+/-RRT)
Scan Oion
3sDsssea*B83*s8saac8aacsrvs8ttiisa8sssss9sssssB8iBa8tSBn8SHt!
Area
Cone, ft
8888B8B1
Cone,8
Blank Q
Limit
ia*SB8mssaBi
2. Chloromethane 3. Vinyl Chloride 4. Bromomethane 5. Chlsroethane
10 is 18 10
6. 1.1-Uichloroethene 7. Acetone
18
10
8. Carbon OisulFide 9. Methylene Chloride
18
10
11. 1,1-Oichleroethane
18
12. 1,2-Dichloroethene (total)
A 13. 2-8utanone
14. Chloroform'
10 18 10
16. 1.2-Qichioroethane
18
18. 1,1,1-Trichloroethana
10
19. Carbon Tetrachloride 20. Benzene
10
ID
21. Triehlaroethene
18
22. 1,2-Biehloropropane 23. Bromodichloromethane
10 lu
24. cis-l,3-Dichloropropene 25. trans-1.3-Uichloropropene
10
10
26. 1,1,2-Trichloroethane
10
ft * RAW core. B * CISC. MULTIPLIED B1 DILUTION FACTOR E - CQNC. OUT OF CAL. RANGE i - RELATIVE RETENTION TIME OUT OF RANGE
Lab Chronicle:
Ent. by.
PACE 1 OK 2
*' --os-
DUP050308034
Lancaster Laboratories Quantitation Report-GC/WS Volatiles
Lilts 25&32 1Q
TLN
File: "(SJ14 injected: 12:41 09/19/96
Sample: DRAJS
25B3210
Dilution hector:
1.0
initial Volims/Ut.:
5.0
Standard: A1SL)S3,
Inst. HPA3046
Batch;
mi&Jlfifi
Final Uoiune/Ut.: 5.11
Method: 7156 Matrix/level: UL Blank; AISJB2
Cone.
Quantitation
# Target Compounds
R.T.(v-RRT)
Sean Qion
Area
Cone,A
Lone.8
Blank Q
Limit
aBtaaa*a*BO***c**mtt******|t***J****t**a*****aMa3a(****dia*KJtatti*****a*MttuaB*a*Mm******a***x3ca=
27. OibromochloromethaOB
----- ----------- ------------------------------------------------------- ------
18
28. Bromoform JO. 4-Plethy1-2-PentanonB
----------------- -------------------------------- ------------- -- ---------------------- ~------ ----------------------- ------------- ------------------------------------------ *-------------------- ---------`--t ------- ----------- --
10 111
32. Toluene
,
------------------- ----------- --------------------------- ------------------ --
10
ii. Tetrachloroethene
------~~-------- -- ------------------- -------------- -
"IB
34. 2-feKdnone
----------------------- ---------------------- --------------*------------------------------ ---18
35. Chlorobenzene
-- --------- -----------*-
1
36. Ethylbenzene
.. ------------ ------------ ----------- --------------------------- ------------ ----------------
IB
38, Xylene (total)
---------------- -- ---------------------- ------------ ------------ ---.------------------ ,-- ----------------- --
iu
39. Styrene
-- ---------------------- -- ---------------------------- ------------------------------ --------------
10
41. 1,1,2,2-Tet rach loroet hane
------------------------------------- ------ ------ ----------------------- ------------------------------
1U
3tsisa3aea3acsBasaitaaa8ota:saasBsetBSBMBUisaKiuaiiKSMaxiimiiMBmnt!UBSMBaaatffsmnBmsaaMssraaattaattta8mBma*sa*B8mBxaisttx
ft = RfiU CONC. 8 * COMC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT IF CAL. RANK * - RELATIVE RETENTION TIME OUT OF RANGE
PAGE 2 OF 2
oJ^'.
)D
DUP050308035
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract: ______.
BRATB
Lab Code: LANCAS
Case No.: ______ SAS No.: ______. SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: 2583211
Sample wt/vol: 5.0
(9/mi) ml
Lab Pile ID: >ISJ10
Level: (iow/ffied) LOW
Date Received: 09/18/96
% Moisture: not dec. '
Date Analyzed: 09/19/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
1.0
Soil Extract Volume: ______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3---------------- Chloromethane 75-01-4------------------Vinyl Chloride 74-83-9------- -----------Bromomethane 75-00-3--------- --------Chloroethane 75-35-4------------------1,1-Dichloroethene 67-64-1------------------Acetone 75-15-0------------------carbon Disulfide 75-09-2------------------Methylene Chloride 75-34-3-----------------1,1-Dichloroethane 540-59-0----------1---- 1,2-Dichloroethene (total) 78-93-3----------------- 2-Butanone 67-66-3--------- ---------Chloroform 107-06-2----------------1,2-Dichloroethane 71-55-6-----------------1,1,1-Trichloroethane 56-23-5--------- --------Carbon Tetrachloride 71-43-2-----------------Benzene 79-01-6------------------Trichloroethene 78-87-5-----------------1,2 -Dichloropropane 75-27-4-----------------Bromodichloromethane 10061-01-5------------cis-1,3-Dichloropropene 10061-02-6--------trans-1,3-Dichloropropene 79-00-5------------------1,1,2 -Trichloroethane 12 4 -48-1---------------Dibromochloromethane 75-25-2----------------- Bromof orm 108-10-1-------------- -4-Methyl-2-Pentanone 108-88-3----------------Toluene 12 7-18-4----------------Tetrachloroethene 591-78-6----------------2 -Hexanone 108-90-7---------------Chlorobenzene 100-41-4----------------Ethylbenzene 1330-20-7--------------Xylene (total) 100-42-5---------------- Styrene 79-34-5------------------1,1,2,2-Tetrachloroethane
FORM I VOA
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
5OLM03.0
DUP050308036
Data File: >IS310::D3
Name: BRFitB
2983211
Hisc: "TLN gUL %C = 1 + >
Quant Output File*. Instrument 10:
#I962631AA 6.5 *5 $AISJB2
'"IS.KIO: :D? HP03Q46
id File: 1A6390::DB
Title' J/'yp SOW Water/Tled Soil ID File for Inst. HPG3046
Last Calibration: 951122 10:44
Last Deal Time: 960919 Q6.*34
Operator 10: TLN--262 Quant Time : 960919 11:06 Injected at: 960919 10:34
60
DUP050308037
QUANT REPORT
Page 1
Qnerator IDs ILN-262
Output File: '''ISJ1Q s :D7
Data File:
>iSJ10::D3
Names SRATB
2583211
Hi sc: ~TLN WL C =1 +>
Quant #1962631Aft &5
kew: *5
7 Quant Time: In j ected at:
Di lution Factor: Inst rument ID:
1SJ82
>'6 0viy il s U6 960919 10:34
1 . U U !J U u ' HP03046
ID- Files IA63^D;s -:DB' Titles 3-"90 S(ilQ Water/Necl Soil Last Calibration: 951122 10:44
ID File
for
Inst . Last
HP03U46 Qcal Times
960919
06:34
Compound
1) 13) 1?) 29) 31) *0)
*0romochior6methane 1 J,2-Dicftioroethane-d4
*1,4-Difluorobenzene *Lhlorobenzene-d5
Taiuene-d8 4-Bramofluorobenzene
* Compound is iSTD
R.T. Q ion
8.36 9.30 10.02 14.31 12.22 16.03
128.0 65.0
114. 0 117.0
98.0 95.0
Area
404U4 84059 168853 124072 147845 101420
Lone
Units
3U . 00 45.15 90. U0 50.00 50.31
49.39
UG/L UE/L UG/L UG7L UG-'L UG2L
q
92 91 88 84 y i> 78
61
DUP050308038
Lancaster Laboratories Quantitation Rfcport-GC/MS Uelatilas
LLI*: 2 S? O 3 2 X X
TUN
File; "lbilU Injected: lit:>4 uy/19/96
Sample: BRATS
2983211
Dilution Factor:
1.8
initial Uolusie/Ut.:
9.0
Standard: AiSJSl
Inst. HP03Q46
Batch:
1962631AS
Final Uolune/Wt.: 9.0
Method: 7196 Hatnx/level: WL Blank: AlSJU
# internal Standards
R.T. t*/-RT) Sean Dion AreatV-XArea) Cone.
UC Flag Cone Units * ug/L
^ffq|ffiyi'mi!ffTrB]B8Ti'^wp'W^|i'gq:agBMe=ffaMe!MeBaiBlilBaiiBgaBBaBBBBBBBBBB8iBaBBBBaBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB**MaineiaasKessvastssatgsiasawBsssa
1. Brotsoehioromethane 17, 1.4-Difluorobenzene 29, Chlorobenzene-dt*
* - RETENTION TIME DOT OF RANGE
8.3611.0224) 970 126
48404( 32)
98.80
10.02t.0093) 713 114
1688931 31)
90.00
14.31t-.014) 1082 117
124872( 31)
90.00
* - INTERNAL STANDARD AREA OUT OF RANGE NC K NOT ABLE TO CALCULATE--NO STANDARD.
4 Surrogate Standards
R.T. t+/-RRi) Scan Dion
Area
Cone.
sftec. 6
se:am>uc.U3sioa!S>imnn>ema><niaitEnnnniminnnnnn>n>nn>nnn>nnn<ni>aaisnunxnaii
19. l,2-B!ehloroethBrte-d4
9.3O2<-.002> 691
69
>1. loiuene-dti
12.22t.0013) 902
98
48. 4-BrqKpHuorobenzene
16.U3t-.00il) 1230
99
* RELAIIUE RETENTION TIME GUT BF RANGE * - KREC OUT OF RANGE
84099
49.19
vu
147849
90.31
101
1&1420
49.39
9V
0 SURROGATES DILUTED CUT NC COULD NOT CALCULATE
$ target Compounds
R.T.(*/-RRT) Scan Qion
Cone,
Uuantitation
Area Conc.A Conc.B Blank (I
Limit
2. Chloromethane 3. Utnyl Chloride 4. Bronomsthane b. Chioroethane 6. 1,1-Dichtoroethena 7. Acetone 8. Carbon Disulfide 9. Methylene Chloride 11. 1,1-Uichloroethane 12. 1,2-Uichloroethene Itotal) 13. 2-8utanone 14. Ch lorotons 16. 1,2-Uichloroethane IB. 1,1.1-Trichtoroethane 19. Carbon tetrachloride 20. Benzene 21. frichloroethene 22. 1,2-Dichloroprapane 23. Bromadichtaromethane 24. cts-l?3-Dichloropropene
2b. trans-l,i-Cuchloropropene 26. 1,1,2-lrichlorosthane 3BsBBssB8BSBsasBssBssss8BBSBBass&SBSasassBassaKB8BaBBSssBa888BassBBBBBBttB8aBesB8BBBBBBBSt8asssBBasssaaB:BSBSsms:
lit
10 1U
18 10 10 18
10
10 10 18
18
18 10 10 10 18 10 10 10 18 10
A = RAW C01C. B CQNC. MULTIPLIED BY DILUTION FACTOR E CONC. OUT OF CAL. RANGE # = RELAT1UE RETENTION TIME OUT OF RANGE
Lab Lhronicie:
tnt. by
_0er. by
PAGE 1 OF 2
DUP050308039
Lancaster Laboratories Quantitation Report-GL/tlS Uolatilea
LL1*: 2 3 3 2 X X
TLN
File: AlSJllf injected! 10i34 09/19/96
taample: CttftTB
2583211
Dilution factor!
1.1)
inttial (to lume/Ut.:
5.0
Standard: A1SJS1
Inst. HP83046
Batch:
1962631AA
Final Uolum/Ut.: 5.0
Metnod: )l% ttatrix/leveli UL Blank! A1SJB
: Target Compounds
R.M*/*RRi> Scan Sion
Area
Lone. A
Uonc.t)
Cone. Blank U
Quantitation
Limit BBBBIMKt
22. Uibrorcochtoromsthane
10
28. Bromoform
10
30. 4-fletftyl-2-F'entanone
1U
32. toluene
ID
33. (etrachloroethena
10
34. 2-Hexanone
10
35. Chlorobenzene
10
36. Cthylbanzena
10
38. Xylene (total)
1U
39. Styrene
10
41. 1.1,2,2-1et r achloroetbane
10
aaaaaeaass*SBa*e*as**aBsa**c***MM**aa*axs*aBMBBmBM*BnBM*aa*aa*a***asa*a*attaBaa*saaaa
ft = RftU tunc. B * UUfC. nuLflftLSBi BY DILUTION tftCTOR E = CUNC. UUl UF COL. RtoiLE * = RELATIUE RtltNTIUN "11ME UUl OF RAN1
Lab Chronicle!
JEnt. by
Analyst Auditor
n
..ob. *44-
Dates
_^2_Date! j/lflfL
tier. by
PA0E 2 OF 2
A <*
06
DUP050308040
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract:
BRA2D
Lab Code: LANCAS
Case No.: ______ SAS No.:
SDG No.:
Matrix: {soil/water) WATER
Lab Sample ID: 2583823
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >GSP01
Level:
(lqw/med) LOW
Date Received: 09/19/96
% Moisture: not dec. _______
Date Analyzed: 09/25/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
1.0
Soil Extract Volume: _______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ucr/L or ug/Kgr) UG/L
o
74-87-3------------------ Chioromethane 75-01-4------------------- Vinyl Chloride 74-83-9------------------ Bromomethane 75-00-3 ---- -------- Chloroethane 7 5-35-4------------------1, l-Dichloroethene 67-64-1---------- -------- Acetone 75-15-0------------------- Carbon Disulfide 75-09-2------------------- Methylene Chloride 75-34-3------------------- 1, l-Dichloroethane 540-59-0----------------- 1,2-Dichloroethene (total) 78-93-3------------------- 2-Butanone 67-66-3------------------- Chloroform 107-06-2---------------- 1,2-Dichloroethane 71-55-6------------------ 1,1/ 1-Trichloroethane
56-23-5------------------- Carbon Tetrachloride
71-43-2------------------- Benzene 79-01-6------------------ Trichloroethene 78-87-5------------------ 1,2 -Dichloropropane
75-27-4--------------------Bromodichloromethane 10061-01-5----------- cis-1,3-Dichloropropene 10061-02-6------------trans-l, 3-Dichloropropene 79-00-5-----------------1,1,2-Trichloroethane 124-48-1----------------- Dibromochloromethane
75-25-2------ -----Bromoform 10 8 -10-1-------- -------- 4 -Methyl-2 -Pentanone 108-88-3----------------- Toluene 127-18-4----------------- Tetrachloroethene 591-78-6----------------- 2-Hexanone
108-90-7----------------- Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-42-5----------------- Styrene 79-34-5------------------- 1,1,2,2-Tetrachloroethane
10 u 10 u 10 u 10 u 10 u 10 u 10 u
3J
10 u 10 u 10 u 10 u 10 u 10 u
10 D
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VOA
4OLM03.06
DUP050308041
THTiftL i-: flRR0MTftf*R$'^ "
. 4.00
3iiU0yiH.
'Tie
5$3*c
S&OOOO-J
: :J . i*/
40000-]
' 4: 2CS0(k M
I. rjpOOO"
onrtrirL
40000-
1
.i
V
s J2.
I
t 0E2i
4-
io ?
. J.
A.Jt
i.=
PUL 120 0
*> :T
I0
f! !L
16 16
30
Do. la Fite: > GSF!) 1 : : 04
Quant Output File: /'GSFfll : : FM
Name : BSR2D
2583823
Instrument ID: HP0346Q
Mias : ~SHM gW:,, %C *>
#098268IftA S^GSPBl &5 *5 =1
Id Fi le : Ifi'4390 : : DB
Title : 3/9H Water/Med Soil ID File for Inst. HK"346s.:
Last Calibration: 951207 01:53
Last ycal Time: 360925 0i::26
Operator II:: SftM-983 Quant Time : 960925 02:22 Injected at: 9BM92-5 01:57
65
DUP050308042
Cy. ; ,nU IlH*' FUal<'U' fVJ- ":'
f'aj- -
Operator ID : SAM'963
Output File : ''GSP01: : FM
Data File:
> GeHO1: :
Haros : Bf;-'2D
25838 Id d
Hist 1 -'SftM UL %C +>
yuant Rev: #(2962681ftA S^GSPBl
? ytiant Tawe ; 1 ejected at
Dilution Factor:
Instr unient ID: &5 *5 .. =1
Ht<>-925 U: 2 9k .132S< ! I : b' '
i . ' :::. u 0 H- -:4t.:
ID File: IP 390::DB . Title 3/90 'UaterVMed Soil ID File Last. Ca l i far at icri: 351 20? 01:59
for
Inst.. HPOS'-'SO Last. Qcsi
Tarr.e:
9hH325
U0:26
(lompoand
1) 9; 15} 1?! 29 > 31 > 10)
*Bromochlororoethane Me thylene CbIo ride 1 J>2-Dichloroethane-d4
*1,4-Difluor obenzene *Ch 1 o r o be.ns e ne - d5
Toiuene-d8 4-Bromofluorobenzene
* Compound as ISTD
R.T. Q ion
3.49 S . 85 10.40 11 . 08 15.37 13.26 1? . 09
128.0 84.0 65.0
114.0 11?. 0
98 . o 95.0
fires
d Li S 342? S'? bn 6 184:17? 148674 1913159 125190
Cone
Units
5 0.0 0
3.19 4b . 06 5 00 5U . 00 4? 47 4 9.82
ug, L uq ' L.
uq/L u.g/'L _* ' i_j ug/L l j g Ej .
c
M ,,' 99 3 OV 99 S3
66
DUP050308043
{grRgNi? feTRBffSRD S.FECTRLm
rru >i5r0**3n a He'fhyi--^ n- * Chior-i (JOT 49 84
Srsn 403|
HI 1 i'i . |
10000-j
rI r4WuJ|Li
n
8b` L
Trnrrr J DO
rrrr 150ri-yt.'i r'T*'-0rr0r
_J
Sftt1Pi_E SPFCTPLIrt <BfiCt=8R0>JMn SiJBTRSOTFD
p l ie ; i!M?5'P01 BSH2U
2b&383
&c k fib 794.
SUB
49
/ Si
Scan 40 6 . mitt.
j-100
SQiP
L
1&
SO
1, 100
150
SAMPLE SPECfSUM (UHSLTERED>
ffi l b yespdi Bm&o
583823
[Spl fib 794.
49
i{
84
50ihj
jJ
50
100
150
ecr
, . nL
' eoo
Scats 420 6.85 min.
100
07
"r*,rrt 200
Fils .'^SSPOi 4-r * 7--41? 7
80 Cn
40(4 rJt.
v*""\
/ / -j-x-,-; ~n-r-
7.0
Fills N3SPQ1 SS.7-S1." am
2o 4 F \
J/
V..
0-^*4=4r
6.8 '
7.0
Fiis >6SPG1 83.7-84.7 an
4004j //*\\
1/ O-Hfri.u
6.8
\ ,T?-
7 .0
File >SSPvi 85.7-66.7 an
D.-r.a File: >GSFU1 i s D4
Quant Output File: ''GKFOl : : FM
Name: BRP2D
2583823
Instrument ID: HPU34S0
Mi sc : ~SHM @Wi. %C + >
#CH626Blftfl S^GSPBl 65 *5 =1
Quant Time: 960925 02:22
Quant ID Pile: IM39U : DB
In igcted at: 9SU925 01:57
Last Calibration: 95 1207' 1:1:59
Bast Qcal Time; 960925 00:26
Compound No
:
Compound Name :
Scan Number
:
Retention Time:
Quant Ion
:
Area
:
Concentration :
o-walue
:
9 Methylene Chloride 420
S.S5 rnm. 84.0
3427 3.13 ug/L 32
67
DUP050308044
Lancaster Laharatones Quantitation Report-GIL'ME Ooistiles
LL1I;
'!!-:
File! AGSP0I Injected: 01:57 (19/25/96 Sample: BRH2D " 2593823
Dilution Factor' Initial Uoiume/Bt.:
1.0 5.0
Standard: AGSPS1
Inst. 89(13460
Batch;
G962681AA
Final Dclune/Ut.: 5.B
Method; 7156
Katri5./leuEl: Ii.
Blank. -'GSl'Bl
1 Internal Standards
R.T. <*/-RT) Scan Qion
Areal+/-$ftrea) Cone.
ESS
-s----;.-s;---,-----Btssr 53assistetss-cas ================= ======== ======= ================== =========:
Flag Con: Units = ug/
1. BromcchioroTfiethane 17. 1,4-fiiflucrebenzene 29. Chlorobenzene-d5
9.48B(-.B01) 11.08S-.005) 15.37C.0072)
647 7B4 1152
128 114 117
45203(-22) 1841771-241 14BG74C-25)
50.00 5U.80 50.00
1 RETENTION TIME OUT OF RANGE
* INTERNAL STANDARD AREA OUT OF RANGE
NC - NO? ABLE TO CALCULATE--NO STANDARD.
I Surrogate Standards
R.T. (+/-RRT) Scan
ftion
Area
Cone.
tEec. Q
15. l,2-Dichloroethane-d4
10.40.000)
725
65
3). Toluene-dB
13.261-.000)
971
88
40. 4-Bromofluorobenzene
I7.83C-.000) 1380
85
I = RELATIVE RETENTION TIME OUT OF RANGE * = TREC OUT OF RANGE
67856
46.06
92
15B159
49.4?
99
125140
49.82
100
D = SURROGATES DILUTED OUT NC = COULD NOT CALCULATE
Target Compounds
R.T.H/-RKT)
Scan Qion
Area Cone.A
Conc.B
Cone. Blank Q
Quantitation Limit
2. Chloronsethane 3. Omul Chloride 4. Bromotnethane 5. Chloroethane 6. 1,1-Dichloroethene ?. Acetone B. Carbon Disulfide S. Methylene Chloride 11. 1,1-Uichloroethane 12. l//-Diehlnroethene (total) 13. 2-Butanune 14. Chloroform 16. 1,'2-Dichloraethane 18. 1,1,1-Tnchloroethane 19. Carbon Tetrachloride 20. Benzene 21. Trichloroethene 22. 1,2-Dichloropropane 23,. Bromcdichlaromethane 24. cis-l,3-Dichloroprapene
25. trans-l,3-Dichloropropene 26. l.lj2-Trichloroethane
-------------------------------------------------------------------------- :----------------------- ------------------------------------------------------------------------------------------------------------------------------------------------- --
------------------------------------------------- 4--------------------------------------------------------------------------
6.851 .0001 420 84 3427 3.188
3J
-----------------------------------------------------------------------------------------------------------------------------
----------------------------------------------------------------------------------------------------------------'-------------------------------------------------------------------------------------------------------------------------- .------------
-------------------------------------------------------------------------------------------- ------------------------------------------------------------------------------------------------------------------------------------------------------------
10 111 10 1U 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
10 10
A = RAW CQNC. B = CONC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CAL. RANGE I = RELATiUE RETENTION TIKE OUT OI RANGE
Lab Chronicle:
tnt. bp
PAGE 1 OF 2
Uer, by _______
68
DUP050308045
':' Lancaster Laboratories . Quantitation Eaport-GC/MS ttoiatiiss
LLiff: Si '~zn &
% r-n
FiLe: "GSPOl Injected:01:57 <W:25/9&
Sample: BSA2D
2583S23
Dilution Factor;
1,0
Initial I'olume/liSt.:
5,0
Standard: "GSPS1 Inst. HP03460
Batch;
G9S2681ftft
Final Uolume/Ut ; 5.0
Method: 7156 Matrix,-level: SL Blank: -'GSPBl
1 Target Compaunas
8 ? f-.-Sk'.'J
Scan Qion
Area
Conc.fi
Ccnc.B
Cent. Blank Q
Quantitation Limit
27, Dibromochlorofflethane 2fi Bromotoriri 30 `S-Methyl-2-Fentanone 3V. Toluene 33, Tetrachloroelhene 34, 2-Hexannne
,.
35, Chlorobenzene 3K. Ethylbenzene 38. Xylene (total) ,3M, Styrene 41, 1,1,2,2-Tetrachloroethane
tssrestsesttsaasrasassareiesaataas
ft = Ml CONC. 8 = CONC. MULTIPLIED BY DILUTION FfiCTOE E = CONC. OUT OE CAL. RANGE
10 10 10
Ilf
10 10 10 10 10 10 10
i = EELfiTlUE RETENTION TIME OUT OF EHNGE
Lab Chronicle; _______________
' __________________________ Ent,. by
65
DUP050308046
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract
BRA2S
Lab Code: LANCAS
Case No.: _______ SAS No. : _______ . SDG NO.: _______ .
Matrix: (soil/water) WATER
Lab Sample ID: 2583824
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >GSP02
Level: (low/med) LOW
Date Received: 09/19/96
% Moisture: not dec. _______
Date Analyzed: 09/25/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
l.o
Soil Extract Volume: _______ (uL)
Soil Aliquot Volume: _______ <uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3------ ---------- Chloromethane 75-01-4------------------- Vinyl Chloride 74-83 -9------------------ Bromomethane 75-00-3------------------- Chloroethane 75-35-4------------------- 1,1-Dichloroethene 67-64-1------------------- Acetone 75-15-0------------------- Carbon Disulfide 75-09-2------------------- Methylene chloride 75-34-3------------------ 1,1-Dichloroethane 540-59-0----------------1,2-Dichloroethene (total) 78-93-3------------------- 2-Butanone 67-66-3--------------- -Chloroform 107-06-2----------------- 1,2-Dichloroethane 71-55-6------------------- 1,1,1-Trichloroethane 56-23-5------------------- Carbon Tetrachloride 71-4 3-2---------- -------- Benzene 7 9-01-6------------------ Trichloroethane 78-87-5------------------- 1,2-Dichloropropane 75-27-4------ ------ --Bromodichloromethane 10061-01-5---------- -cis-l,3-Dichloropropene 10061-02-6-------------trans-1,3-Dichloropropene 79-00-5------------------ 1,1,2-Trichloroethane 124-48 -1----------------Dibromochloromethane 75-25-2------------------- Bromoform 108-10-1-------- --~4-Methyl-2-Pentanone 108-88-3----------------- Toluene 127-18-4----------------- Tetrachloroethene 591-78-6---------------- 2 -Hexanone 108-90-7------------ --Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-42-5----------------- Styrene 79-34-5------------------ 1,1,2,2-Tetrachloroethane
FORM I VOA
10 U
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
OLM03.C)7 0
DUP050308047
TON
>fc>? Vc
r
80000n
40OQO-j
320000-j 2C2:0C'C4
I
18000CH
4
160000^
140000-j
ISQOCHH
1000004 4
80000-j
Si'C'OC"FI
4QQQ0j
20000-j j
Cm=
I400
.___ ___i.
gJep?"
gflftSSgc
TIC
SCO
V$CTT ftUL 1200
a
jj
=gC 5
T<Tc65= 3
mok
iI
I
iT
jc
S j! <Mi
m!
ii n a
1--1rC~' 1--iFf r
14
--r~ if.
If
2t0
Dr. t. a F=.Le: >GSF02 : : D4
Quant Output File: ''GSFU2 ! : FM
Name: BRA2S
2583824
Instrument ID: HPQ346G
Mi sc : ~SH @JilL %C + >
#G9H2681fift S^GSPBl &b *5 =1
Id File: IH4390::DB Title: 3/Sli Uater/Med Soil ID File Last Calibration: 95120? 01:59
tor Inst. HPH34fc>l! Last yeal Time:
860925
00:26
Operator ID: Quant Time : Injected at:
SPlM-BBB 960925 02:55 960925 02:30
71
DUP050308048
Ooerator ID: SAM-9H3
Out pu t f'l ie : ''GSHU2 ; : FM
Do * a File:
> CS H i] 2 : : D4
Newift : BRH2S
25838V4
M 1 S C ' ~SPM &JL 'SC +>
yuant #0962681 HP
Hev:
7 ont Time : Injected at:
Dilution Factor: Instrument ID:
&5 *5 =1
i.i j- p O ? er, n ? s u
St- i!S2w :j 2 : 3 U i . o 0;; o o
Hi- -346
ir, Fi Is : JP439U : : DH Title : 3790 tdater^'Med Soil ID File Last Calibration: 951207 01 : 59
For
Inst . HP0346 0 . Last. Qcal Time.:
961ISV5
0 0 : 2 r-
Compound
1> lb i 17) 9W \
31) 4H )
*BroTnoc hloromet hane 1 .2.-Die hior oet hane-d4
*1 ,4-DiflQDrobenseris *Cb 1 orc benzene-d5
To 1uene-d8 4 Kromofluorobensene
* Compound is 1 STD
R . T . Q ion
9.46 10.37 11 . 05 IS .33
13.24 17.05
128.0 65.0
114.0 117.0
98.0 95-0
Area
43616 66262 172338 136114 144153 119975
Cone
lira t s
5 0.0 0 46.75 50.00 5i: . 0 0 49.88 5 V . 17
ag.*'L ug/L ug/L ug.-'L
ug7L
ug.-''L
q
yu a ri 95 92 98 84
t-J
DUP050308049
Lancaster Laboratories Quantitation Report-GC/MS Volatiles
LLH:
File: AGSP02 Injected: 82:30 19/25/96
Sample: BKA2S
2583B24
Dilation Factor:
1.8
Initial Qoiame/lilt.:
.5.0
Standard: AGSFS1
Inst. HP034S8
Batch:
G962681HA
Final Uolume/lOt.: 5.0
Method '/156 Matrix/levei: Blank: %`bi'Bi
S internal Standards
R.T. (+/-RT3 Scan Qian
Areal+z-tArsa) Cone.
QC Hag. Cone Unit;. = an 'L
ssssB%ss3Sssss3Ss&3asaails=ssBS8ssssssBSSSS=sss$3asss99Sss8SS:a9seseeas8sesB*HasssBaBcssac9BBsasa&aa&esessssBssssssBaeaa9a&ssssss = :;
1. Bromochloromethane 17. 1,4-Difluorobensene
9.465I-.0253 646 12S 11.05(-.04B) 782 .114
43S16C-25) 172338C-23)
50.00 50.00
29. Chlorobenzene-d5 8 = RETENTION TINE OUT OF RANGE
15.33t--. 029 > 1150
11?
13S114C-31)
50.130
* = INTERNAL STANDARD AREA OUT OK RANGE
NO = NOT ABLE TO CALCULATE--NO STANDARD.
f Surrogate Standards
R.T. (+/-RSTS Scan
Qion
Area
Cone.
%Rec.
15. l,2-Dichloroethane-d4
10.37(.OUOOi
724
65
33. Toluene-dB
13.241.00823
970
96
40. 4-BroTiiofluorohenzene
17.05(-.0903 1298
95
8 * BELATIUE RETENTION TIME OUT OF RANGE * = iC OUT OF RANGE
66262
46.75
94
144153
4S.B8
100
119975
52.17
IU4
D = SURROGATES DILUTED OUT NO = COULD NOT CALCULATE
8 Target Compounds
R.T.(+/-RRT3
Scan Qion
Area
Cone,A
Conc.B
Cone. Blank Q
Quantitation Limit
2. Chloromethane 3. Oinyl Chloride 4. Bromomethane 5. Chloroethane 6. 1,1-Dichloroethene 7. Acetone 8. Carbon Disulfide 8. Methylene Chloride 11. 1,1-Dicbloroethane 12. 1,2-Dichloroethene (total) 13. 2-Butanone 14. Chloroform 16, 1,2-Dichloroethane 16. Ijl.l-Tricbloroethane 15. Carbon Tetrachloride 20. Benzene 21. Trichloroethene 22. 1j2-0ichioropropane 23. Bromschchioronethane 24. cis-l,3-Dichlorapropene 25. trans-l,3-Dichioropropene 26. 1,1,2-Tnchloroethane
------------------------------- :--------------------------------------------------------------------------------------------
---------------------------------------------------------------------------------------------------- ;-----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------.------------------------------------ --------------------------------------------------------------------------------------------------------------------.-----------------------------------------------------------------------------------------------------------------------------
----------------------------------------------------------------------------------------------------------------------------- . ------------------------------------------------------------------------------------------------------------------------------------
1(3 10 10 10
10
10 10
A RAN CCC. B = CONC. MULTIPLIED BY DILUTION FACTOR E CUNC. OUT OF CAL. RANGE 8 = RELATIVE RETENTION TIME CUT OF RANGE
Lab Chronicle: _____________________________________________________________________________________
Ent, bu
PAGE 1 OF 2
Uer. by _____ r4f-Z;S
DUPO 50308050
Lancaster Laboratories Quantitation Repori-GC/llS Udatiies
LLli; *JcJ* ^ *~Tj
fcS IrJ!
1M
File: -GSP02 Injected: 02:36 G3/25.'S6
Sample: 8Rfl2S
2583823
Dilation Factor:
1.0
Initial (lolmfe/Ut.:
5.0
Standard: ''GSPS1
Inst. HP03460
Batch:
($6268IftA
Final Uoiume4Jt.: 5.0
Target Compounds
R.T.lv-RR?)
Scan Qion
Area
Method: 7158 Matrix/leoei: (it. Blank: "GSPB1
Cone.ft
Cone.B
Cone. Blank Q
Quantitation Limit
27. Dibrcmochloromethane 28. Bramoi-onts 30.. 4-Methyl-2-Pentanone 32. Toluene . 33. Tetrachlornethene 34. 2-Hexanone 35. Chlorobenzene 36. Ethylbenzene 38. Xylene (total) 39.. Styrene 41. 1,1,2,2-Tetrachloroethane
--------------------------- --------------------------------------------------------------------------------------------- -- -----------------------------------;------------------ ;---------------------------------- ----------------------------------------------------------------- ;--------------- 1------------------------------ --------------------------------------------------------------------------------- 1--------------------------------------------------------------------
----------*--------------------------------------------------------------------------------------------- -------------------------------------------- ;------------------------------------------ ----------------------------------------------------------------------------------------------------------------------------------------------- -------------- :------------
-----------------------------------------------------------------------------------------------------------------------------
10 10 16 10 16 10 16 1(1 10 10 18
ft = HAli CONC. B = CONC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CflL. RANGE i KELflTSUE RETENTION TIME OUT OF RANGE
Lab Chronicle:
Ent. by
DUP050308051
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract
BRAID
Lab Code: LANCAS
Case No.: _______ SAS No.: _______ . SDG No.: _______ .
Matrix: (soil/water) WATER
Lab Sample ID: 2583S25
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >GSP03
Level:
(low/med) LOW
Date Received: 09/19/96
% Moisture: not dec. _______
GC Column: DB624
ID: 0.53
(mm)
Date Analyzed: 09/25/96
Dilution Factor:
l.o
Soil Extract Volume: _______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3------- --------- Chloromethane
75-01-4------------------- Vinyl Chloride 74-83-9---------- -------- Bromomethane 75-00-3------------------ ch1oroethane
75-35-4------------------ 1,1-Dichloroethene 67-64-1------------------- Acetone 75-15-0------------------- Carbon Disulfide 75-09-2---------- -------- Methylene chloride 75-34-3------------------- 1,1-Dichloroethane
540-59-0------ 1,2-Dichloroethene (total) 78-93-3---------- ---------2-Butanone 67-66-3------------------- Chloroform 107-06-2-------- ---------1,2 -Dichloroethane 71-55-6---------- -------- 1,1,1-Trichloroethane 56-23-5------ -------------Carbon Tetrachloride 71-43-2---------- ------ Benzene
79-01-6------------------- Trichloroethene 78-87-5---------- ---------1,2 -Dichloropropane
7 5-27-4---------------- Bromodichloromethane 10061-01-5-- ------ cis-1,3-Dichloropropene 10061-02-6------------trans-l,3-Dichloropropene 79-00-5------------------ 1,1,2 -Trichloroethane 124-48-1----------------- Dibromochloromethane 75-25-2------------------- Bromoform 108-10-1--------------- 4 -Methyl-2-Pentanone 108-88-3------------ --Toluene 127-18-4--------- -Tetrachloroethene 591-78-6-----------------2-Hexanone
108-90-7----------------- Chlorobenzene
100-41-4----------------- Ethylbenzene
1330-20-7-------------- Xylene (total) 100-42-5----------------- Styrene
79-34-5------------------ 1,1,2,2-Tetrachloroethane
10 U
10 u 10 u 10 u 10 u 10 u 10 u
3J
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
10 tr
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VOA
OLM03. 0 _
DUP050308052
Data File. X3SF03: : D*;
yuan! Output File! AGHHQ3 : ; I'M
Name: RRH1D
2582825
' Instrument ID: HP034K0
Mi sc : ~SdM @(Jl. %0 +>
#CaK2681fM-: $~<3SPB1 S.5 *5 =1
Id E'; Is' IM39Q : ' DB Title : 3/yil Uat.er/'Mp.d So: i ID File Last Calibration: 951207 0.1:59
for Inr.t . HPU348!) Last Qeal Time: H8U925
UU: 26
Operator ID: Q'lnnt Time : Injected at:
SfTS=9S3 Sfci 11925 03:27 98HS25 03:0V.
76
DUP050308053
QMMNT PLFORT
f1
/i'!p:eratnr ID:: SWM=483
Quant
Output ,F) ie : ''GAP 17 3 : : FM
Data Ftlia
> LIS P 0 3 ! L>9
:: 2;5H282S/
' -SAM @UL %C +;
*G9S26S1AA
Rev!
7- ycant T-'t w Inje.a+.ed a- '
Dilution Factor' Instrument IS!,' '
&5 *5 = 1
9S;t923
; 1 '
3 >','4'.7 U : !iy
1 . 1.1 n *.p ,i ij
Hu' '' 46 =
iy Ft !.; . IA A 3 9 C ! ! DH
Title : 3790 fOater/Hed Soil ID File for Inst ; HP 03 96 0
Lost Ca 11 briatapn ; &5:T2 Bp 01! 59
Last Qcai T iw: 9 1I9 2 3 0 0 : 76
Compound
: i) :S>
i s :> 17 > 29 ) 31 ) -til >
*Br omcchlor OTethar=e MctHplene Chloride . 1 .. 2- Dichiorciet hane-- d4
*1 . 4-Di f liiorohensiftne *Chlorobenzene-d5
Tc. Iuerft-d8 4-Sromofluorobensnne
* Comprand is 1ST!)
R.T. Q ion
9.45 6.82 10.37 11 . Q5 15.33 13.24 17. 05
12S . 0 .89.0 65.0 114.0 117.0 98.0 95.0
ftrea
423 9 0 331 a
65314 163927 132326 144071 1J 9970
Cone
0 n its
5U . do 3 . 26
Q? - 42 *"< 1 i ou 3 U . CL! b `.1 . 2 U t*. 36
t i-j L>
UQ.'L ug/L uqv'I,
u*3 .''L uq-.'-'L i.in .-'L
l**1 "*!
94 99 99 91 H\ ' 34
11
DUP050308054
Hrn.UHKw ;rr t,'L
- i ii.g VirH'^0%? '
j t4fc- .4.5* >?:? *
"'ien^ cr*. x cv-1
.: CuC
i<r pin 4>j.* i . *1- JV I i`t *
,iOp;OC^
'. k t
: ? . :; 4 :
T tTif--JjUii
M.
ew
j-iccj i\
?00
^ariF.i. e fF-.TFiirl (RfSr.KGRC'iftin SCBTFa.'.Trp ,
C i-jV-e*
: iiRwuyOk
o$y
I
)ri Rfc> ..
SUB
Tc-
Jd nir*
!
'"it C" i <JWV1 H.
ti-jcu-i!
.y !
SOS f 1
L
^04-
i
5c:
i 00
iBC-
goo
SflfWtE SPFVTRMF .UNSI.TEREOT
iFiia ::&s.03;:sftKiD
"582825
I Dp * fib oi?0._
Scan 414
6.30 in i ii . ]
| ^|
[- IC'Oj
tI
SOT !
j
!
i
40 4
ru-
i File >SSPSS
,! i 8`T
I/
! o-i^.4-,,,..,. !e
l -- ___
Kile 1SSD&S
-84 .T
! 40C-,
/
}^
6.8'
j..,---^. File >6SP0S S5.F--36."
!
i !
4.V.0.-v} ^rj'
!
i
V. C! =
an!
Data File: ' G5F0':5 : ; DC
Quant Output File: ''GAFtiS ' : Fit
Mime : BRAID
2582B25
Instrument ID: HPU3c60
Misc : ~Sf-m (3Di:.. %C *)
#t39626lHA $-sGSPBl &6 *5 =1
Quant Time: 960925 03:2?
Quant ID Fi le: 1DM390: : DB
Injected at: 9611925 03:02
Last Calibration: 95120? 01:59
Last Qcal Time; 9611925 DU: 26
Compound No Compound Name1., scan Numiner Retention Time Quant Jon
Area
Concent.r at i nn
o-uaJ ue
<3
Met'hii j ene Chloride
4! 1 C ' fc . 92 mm .
8 -'! . 0
3310
3.28 ug/L
78
DUP050308055
. l.ancasfRr tahinratoriBR Sjnanf statinn Rp.nnrt-Rn/IIK Uniat Up."
!! 14! ?* > "9 FI 1?
^ r-r
Filft! AfSPIIi In jfintp.d: 81:8? 119/99/94
Ra.-nr.lRl RRam IhluHnn Factnrl
9501095 l.fl
Initial Un liina/ldt.!
5.11
Standard: /'SKPS1
Inst. HPK14f.ll
Hatch!
B94?481fV)
Fins! UnhimR/tlt.: 5.11
tlathnd! 7154 flat riv/laua!! Rlar.1;: "fiSPRI
Internal Standards
R.T, I+/-RT5 Scan t}trm
flreat +/-8flren t Rnr.r..
==========s:===:===ts===:s:s=t::=:=::5J=:=ssssasssssaessssxssat#wn===sss ======= SSSSSSSSSS5SS9S69S========;
!?: Fta.j I'nnr. Units = ii,-/i
1. Hrnmnr.hlcrrasBthane 1/. 1 ,4-Hi f hinrnhanrp.nfi
9.4541-.H14) 11.1151-.I1T9)
m\ 198 777 il4
4919111-97) 141997!-Ill
58.1111 58.811
99. IThlnrnhttn7Rnfi-rf5
t = k f t f h i k in t mf n':s rs r mk f '
15.TK-.fl98) 1145
117
11959ft(-y5)
58.111!
* = IMFHNfi! STANIK ARRA SUIT HI RW
NT. = HITT AHIF TJI i:a: SIISI ftTI--KIT STAWitfW.
$ FtiirrnqatR Standards
R.l. H/-RRT) Scan
fjinn
firea
F.nnc.
SRar.
a
I*;. 1 j?-flir.hlnrnRthanfi-ri4
18.171.81114)
719
45
1'.. Tnit:p.na-riH
11.94! .11089)
9*5
90
411, 4-Rrnmnf InornhenTBUR
17.1151-.811111 1991
95
t SFlfiltur RFrFSTtfiN I!(l IS IT II RAN * = r: ran nr
45114 144871
47.4? S') *^*|
95 1!!'/
119478
51.14
1117
n = stewKRTKSi rnimm ran w: = misi) uni it a ii't s a ii-
1arnaf Cnropnunrts
R. 1.1 t7-SRl1
Scan flsr.n
flraa
Cnr.r .3
I.ann.R
f.nnr.. Hlar.k
I1. (ThlnrniiiRfhanR
----------------------------------------------- -----------------------
1. Utny! rhlnriria
-----------------------------------------------------------------------
4. Brnninmethanfi 8. nhinrnalhana
---------------------------------------------------------------------------------------------------------------------------------------------
4. 1 .t-Oirhlhrnp.thanR 7. ftr.atnr,R
--------------------------------------------------------------------------------------------------------------------------------------------------
5. narhnr. Disul f i rtn
-----------------------------------------------------------------------
9. tV.thylar.R lli-.lnriria 11. 1,1-nichlornethane
4.891 .am I 414 B4 1118
i. VP. f
IV. 1
-hlr.r.-p.rhRnF. (t,stall
1?. ?~Rntannne
14. f>.lnrnf.-.nri
If,. 1 ;9-!)ir.H Inrnp.fhana IB. 1 ,1,1-Tr >r.h inrnp.thana
19. Carbnn 1atrar.hlnrtdB
V:i. Ranrana.
91. Trichlnmathfine
99. 1 .V-Dirh lr.rnnrnr.ana
?i. Flrninriir.hlnrnmp.thanp. V4. r.is-l .l-lhr.hlftrnr.rnnRnR
A 95. trsns-1 jT-Oir.hlnrnnrnpp.np.
94. 1 .I .'V-TrichlnrnfifhanR
A fi = lift!.' CT!!:. F: = IT1S2:. WiTlH U tl f!Y D!I !t", HIM FftiiTlIk' f = !lf!:. I!!!T 13 ['.ft! . KftNFi!
RSTftityr wiFHiinn t ih f rs::: ra- r j ^k f
!ah nirnnictr.! ______________________________________________________________________________
FfiKh i nr' v
_______________________F-,t. hy
ifep. t.
*icc.-
DUP050308056
! ar.r.sstF.r tahfiratr.rip.f, Eltiar.t ifatinn ftannrt-KK/Ttii Ur.lafilea
I! li! ? ci- I--I "-5 !--I T'
P"!
S-Ilp.: A(SPR5 tnjRr.ffiri: DHfi? )//
Sample: RBfil.!)
WHjfiVh
fti lijtian Factnr!
1,0
Initial Ur,!ii7iia/U(.!
5.JI
Standard: AKSPSl
Inst.
Hatch!
GYiWfiSIAft
F:fls! Uhliime/fit.: <i.!!
nsthe.a I ?1W, Rsfrix/lflue!: IT Blank: ''RSPR1
Vi Tsrqet Caratimintis
S.J.f/-BRT)
Scan Qinn
ftr'iw
flnnc.ft
f.nnc.B
Dins. Blank g
latent 1 tat inr. l imit
7'K Rihrnmr.r.hlnrnmR thane ?l`.. Rrnsnfnrn III. 4-flp.thjit^?-PentannnB
v:. I.'.tuene
'V. Ifttrar.hlnrnp.thBnfi T-. V-Hr.vannnfi
-* * ----------- ------------------- ----------------------------------------------------------------------------------------------------------- -------`--------------------------------------------------------- ------------------------------------------- --- ----------------------- ---- -------------------------- ---------------------------------------------- ----------------------------------- ---------------------------------- ---r---------------------------------- -------------------- ----------------------------------------- -------------------------------------------------------------------------------*------ ------------------------------------------------------------------------------------------------------ -----------------
111 111 HI HI HI If!
V.. P thiiShenrane IS. Xylene. ttnta 1) IV. Styrene 41. 1,1,? j?-Tetrar.hlnrnBthana
-- ---- ------ -------- --------- ------- ------- -------- -------- --------- ----------- ------ --- ------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------ -------------------------- -----------------------------------------------------
11! Hi HI 111
ft K'Au ratr.. r raw:. ran t ip i if d r y mi iit iiim f firms f = rjiw:. mu iif :at. r p w 4 = n f ir t h if r f t f n t iu n t ih f mu if raw
I ah Chrar.iria:
fins Iys 11
fiiirittnM
r jL__.
Dntfil
riatR! PfiKF ? Rf ?
_Fnt. hy Uar. hy
80
DUP050308057
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract
BRA1S
Lab Code: LANCAS
Case No.: ______
SAS No.
. SDG No.: ____________ .
Matrix: (soil/water) WATER
Lab Sample ID: 2583826
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >GSP04
Level:
(low/med) LOW
Date Received: 09/19/96
% Moisture: not dec.
'
Date Analyzed: 09/25/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
l.o
Soil Extract Volume: _______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3------------------- Chloromethane 75-01-4---------- ---------Vinyl Chloride
74-83 -9--------- --------- Bromomethane 75-00-3-------- -----Chloroethane 75-35-4------------------- 1,1-Dichloroethene
67-64-1------------------- Acetone 75-15-0---------- ---------Carbon Disulfide 75-09-2------------------- Methylene Chloride 75-34-3------------------- 1,1-Diehloroethane 540-59-0---------------- 1,2-Dichloroethene (total) 78-93-3------------------ 2-Butanone
67-66-3------------------- Chloroform 107-06-2----------------- 1,2-Dichloroethane 71-55-6----------------1,1,1-Trichioroethane
56-23-5------------------- Carbon Tetrachloride 71-43-2------------------- Benzene 79-01-6----------------- -Trichloroethene 7 8-87 -5-------------1,2 -Dichloropropane 75-27-4------------------- Bromodichloromethane 10061-01-5-------------cis-1,3-Dichloropropene 10061-02-6-------------trans-1,3-Dichloropropene
79-00-5------------------ 1. l, 2-Trichloroethane 124-48-1----------------Dxbromochloromethane 75-25-2------------------- Bromoform
108-10-1----------------- 4 -Methyl-2 -Pentanone 108-88-3-------------- Toluene
12 7-18-4-------------- -- Tetrachloroethene 5 91-7 8-6-----------------2 -Hexanone 108-90-7----------------- Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-42-5---------------Styrene 79-34-5-------- ---------- 1,1,2,2-Tetrachloroethane
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VOA
GLM03. o81
DUP050308058
ITiTai. JTlN nHPntiSTjlRRBM
ft ; i s >g*.eriu 35.0-3f'O .P arau. BRi-lfe TIC
400'
GOO
,-uyyC^-
Z&QQQQ-
34900.5-
EiOOOO
S 0-0 0004
isoooo-i
-
c~
11
r.
ri
i
rU
14Q90gj
i:ooa0"|
l'JUUOOii
j S0030-1|
i OOOQO-j
4GOOC4 I
GQOQC-j
-I <H =
S %
TO K
C*iO
1f
JK "rf-
os l `
e23 o
en
\ 1?
\ iV i Vi............ -............Il j l ..f!]l..... ... i
10 14
.1 BUL r",C- +
1200 ..,<.. i........ ...--;..... .
% cE ? 't
i
I i!l in l. . ]'S._ _
X*
*_
Data File: XJSFG4 : : D4
Quant Output File; ''GSP04: : FM
Name: BRP1S
2583826
Instrument ID: HP0346Q
Misc : ~SMM @Ud. %C +>
#G9fi2881AP S^GSPBl &5 *5 =1
Id File : IA43S0 : : DB
Title: 3/30 bJater/Med Soil ID File for Inst. HF0346U
Last Calibration: 951207 01:59
Last Qcal Time: 3611325 OU : 26
Op.-rat or ID: SAM983 Quant Time : 960925 03:59 Injected at: 960925 03:34
U hi DUP050308059
O'DPNT REPORT
Pago
Operator IB: SPtM-98'3
Quant Rev: 7
ijuant Tsrne : 9b 092 r r. - - c Ci
Output File: 's 6960 4: ' FM
Injected at: 91-': ^ 2 5 i's r- : 3
Data File:
> Gf.P04 : ;D4
Dilution Factor:
1 . i.l: riQU
Name': BKA1S
2583826,
Instrument ID: Hu !34 ir* *
1 fiisc : ~SFtH (3UL %C =)
#G962S8 Iftfi S"'GSFB1 as *5 -1
ID tilfc: IPd 39 0 : : DB
Title- 3---9 0 b.later.-''Med Soil ID File for Inst . HP03460
Loot C& libra tion: 991307 01 : 59
Last Qc.i 1 Time: 9fc 0925 U !.! -J to
Compound
1) lb :> 17) ", LJ I
31 ) 4!! )
tBromoc hi orouie thane 1,2-Bichloroethane-d4
*1,4-Difluarabensene
*Chiorobenzene-dS Toluene-dS 4- tfromof iuorobenzene
* Compound is. ISTD
R -T. Q i on
3.48 1 U - 39 11.08 lb .35 13 .24 17.07
128 . t) 65.0
114.0 117.0
38.0 35.0
rtrea
46112 67358 130206 1.493 32 149636 123157
Cone
Units . q
50 . 00 44 - 95 5 0 . 00 50 . 00 47 . 19 cr 16
ug/L UQ ug.-'"L uq-'L US'/L ug-'l.
81 uw1.:i1
32
9 *! 88 89
A
DUP050308060
Lancaster Laboratories Quantitation Report-GC/NS Uoiatiies
: -4 r
Fiie: AGSPiJ4 Injected1 63:34 09/25/96
Sample: BRH1S
2583826
Dilution Factor:
1.8
Initial Ut>Unae/Qt..'
5.0
Standard. AGSPS1
Inst. 8903460
Batch;
G9S2681AA
Final Uolurac/yt.i 5.0
Met.hoS' 71.56 Matrix/levs 1; 131. Blank AGSPB1
t Internal Standards
E.T. ?*/-8T> Scan ftioti
Areal+/-%Areai Cone.
QC Fiat Cone Units og/L
1. Bromochloromethane 17. 1;4-Difluorobenzene
29. Chlorcbenzene-dS * = RETENTION TIME OUT OF RANGE
9.482(-.U80! 642 128
46112(-21)
50.00
u. oat-, ons 779 114
18828B(-26)
58.00
15.35l-.0125 1146
117
145332(-26)
50.00
* = INTERNAL STANDARD AREA OUT OF RANGE
NC = .N0T ABLE TO CALCULATE--NO STANDARD.
* Surrogate Standards
P.T. 1+/-RET) Scan
Qion
Area
Cone.
%8ec.
15. l,2-Dichloroethane-d4
10.39t-.B88)
720
65
31. ToJuene-dB
13.24t-.0O8)
965
9B
40. 4-Broiaofluorobenzene
17.07(-.000) 1234
95
{ > RKIATIUE RETENTION TIME OUT OF RANGE * = IREC OUT OF RANGE
67358
44.95
90 '
145636
47.19
94
123157
50.16
106
D = SURROGATES DILUTED CUT HO = COULD NOT CALCULATE
i Target Compounds
R.T.I+/-8RT)
Scan Qitm
Area
Cone.A
Conc.B
Cone. Blank Q
Quantitation Limit
2. Chlorcmethane 3. Uinpi Chloride 4. Bromomethane 5. ChJoroethsne 6. 1,1-Dichioroethene 7. Acetone 8. Carbon Disulfide 9. Hcihyiene Chloride 11. 1.1-Biehloroethane IT. l;2-D`.chloroethene (total! 13. 2-Butanone 14. Chloroform 16, l;.2-Dichioroethane 15. 1,1;l-TrichloroEthane 19. Carhon Tetrachloride 20. Benzene 21. Tnchloroethene 22. 1,2-Dichloroprapane 23. Bromodichlororaethane 24. oi3-l,3-Dichloropropene 25. trans-1.3-Dichloropropene 2E. 1.1,2-Trichloroethane
-------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------'----------------------------------------------------------------------- ---------------------------------------------------------------------------------------------------- --------------------------------------------------------------------------------------------------------------------------------------------------- ---------- .------------------------------- '---------------------------------------------------------------------- ------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------...........--........... -....................................................-------------
------------------------------------------------------------------------------------------------------------------------------- --------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
ID
10
Hi
ID
lit
18 10 10 10 10 10 10
is
10 to 10 10 10 10
t*. n>.
10
Hi
A * RA!i! CONC. E - CCNC. MULTIPLIED BV DILUTION FACTOR E - C*JNC. OUT OF CAL. RANGE - SELAT'.UE RETENTION TIME OUT OF RANGE
Lab Chronicle:
Ent. bp
--- -------------------------------------------------------------------------___>r bp ^4 PAGE 1 OF 2 -
DUP050308061
Lancaster Laboratories Quantitation Repert-GC/HS Volatiles
U*I:
t=> s 3 i B
tH7. ;"-a
; File: 7GSPSI4 Injected: 03:34 0.9/25/96
Sample: . BHflIS
2583828
Dilation factor:
1.0
; Initial UoluW/tlt.: ; -5.0
Standard: nGSPSl
Inst.HH03460
Batch:
G962681fifi
. Final Ublume/Gt..: 5.0
Method 7156 Hatrix/leuei: U: Blank' ''GBPEi
t. Target Compounds
B,T.(+/-8RT)
Sean Qibn
Area
Conc.fi
Conc.B
Cone Blank
Quantitation Limit
27. Dibromochloromethane 28. Bromotarm 30. 4-Methyl-2-Pentanofie 32. Toluene 33. Tetrachloroethene ;34. 2-Hetansne 35. Chlorobenzene 36. Ethylbenzene 38. Xylene (total) 39. Sturens 41. 1,1,2,2-Tetraehioroethane
------------------------------ *------------------------------ ---------<-------------;--------------------------------------------------------------------------------------------------------------------------------------------------------------------- -------------------- -------------------- ----------------------------------------------- -------------------
to lc U!
---------------------------------------------------------------------'---------------------------------------------- ------;---------- ;--------------------------------------------------------------------------------------------------------------------------------------------------------------------------- *--------------------------------------------------------
lit 10 10
----------------------- 7----------------------------------------------------------------------------------------------------------------------------------------- ;-----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
10 10
10
fi = ftfiU CONG. 8 = OONC. MULTIPLIED BY DILUTION FACTOR E CONC. OUT OF CfiL. RANGE S SELATIUE RETENTION TIME OUT OF RANGE
Lab Chrom-cie_Ent. by
85
DUP050308062
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
SPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract: ______ .
BRAF1
Lab Code: LANCAS
Case No.: _______ SAS No.: ______ .
SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: 2583827
Sample wt/vol: 5.0
(g/fflL) ML
Lab File ID: >GSP08
Level: (low/med) LOW
Date Received: 09/19/96
% Moisture: not dec. _______
Date Analyzed: 09/25/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
1.0
Soil Extract Volume: _______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3------------------ Chloromethane 75-01-4-------- ---------Vinyl Chloride 74-83-9------------------- Bromomethane 75-00-3-----------------Chloroethane 75-35-4-- -------------- 1, l-Dichloroethene 67-64-1---------- ---------Acetone 75-15-0------------------- Carbon Disulfide 75-09-2------------------- Methylene Chloride 75-34-3-----------1, l-Dichloroethane 540-59-0------ -------- -I,2-Dichloroethene (total) 78-93-3---------- ---------2-Butanone 67-66-3------------------- Chloroform 107-06-2----------------- 1,2-Diehl oroethane 71-55-6------ -------------1, l, l-Trichloroethane 56-23-5------------------- Carbon Tetrachloride 71-43-2------------------- Benzene 79-01-6------------------- Trichloroethene 78-87-5------------------ 1,2-Dichloropropane 75-27-4----------------Bromodichloromethane 10061-01-5------------ cis-l,3-Dichloropropene 100 61-02-6----------- trans-1,3 -Dichloropropene 79-00-5------------------ 1,1,2-Trichloroethane 124-48-1----------------- Dibromochloromethane 75-25-2------------------- Bromoform 108-10-1----------------4 -Methy1-2 -Pentanone 108-88-3------ ---------- Toluene 127-18 -4---------------- Tetrachloroethene 591-78-6----------------- 2-Hexanone 108-90-7----------------- Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-4 2-5----------------styrene 79-34-5------------- 1,1,2,2-Tetrachloroethane
FORM I VOA
10 U
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 c 10 u 10 c 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
OLM03.08^ &^
DUP050308063
TflT&t frftM r.HKftMCTrtftgfitt
[c i i o
3? C51-`SC'C*. t1
( *.-.O<-. ^W.~tU^-. Vr. il
400
..-.I....
S^OGOO-
s^o^aorl
22OB00-
Sfn/QOO-
1O0CW
i AOOQfW " ; ' !
I-iOOOOi' : . -1
1S3Q0CH lOiJOOO-i
coooc
I 40000-11I
COOOO-J
oi
*N.
B&ar-,
pns^?7
TIC
! ... 801 0 ... I
~san aty,_ sr L00
fPcr
& Cfc o!
fc: K
t
ii i a t .:":ici......i..... i
I
Data File: >GSFQ8 : : D4
Quant Output File: 'vGSi-'U8: : FH
Nome : B^HFl
2583827
Instrument ID: HPU'.-MISO
Mi sc: ~SMM @UL %C *>
#0882 88:1 MO $~GSPS1 &5 *5 =1
Id File : IfVi39 0 : : D8 Title: 3/9 1J Uater/MeC Sell ID File Last Calibration: 9512 07 01:59
for Inst. H-03490 Last !:cal Time:
980925
U ll : 26
Operator ID : SMM=9t: i Quant Ti me : 980925 OS : 0 I n j p. c t e d at : 980928 05 :3
87
DUP050308064
QiJHNT SEF'OET
Pc. c---
Uperator ID : SAM"983
Output File : ''GSS-'OS : ; Fm
Data File:
>CSF08.:;D4
Name: BPMFl
288382/
Misc! ~S0H (at)L %c
yuant fteu; #G9K28818 S-NSSHBl
7 yuant `ID me : Injected at ;
Dilation Factor: Instrument ID:
&5 *5 =1
33113 25 lib ; U3 g K:: 3 2 s f15 3 9
1 . U ! i i! U i.' H`-:!34F1i
ID File: IN 4338 :D DE Ta 11 e : 3/90 Ulster/Had Soil ID File L uo t, Cc. 11 fa r atiorri 9512 02 01 ; 59
tor
Inst . HP03460 Last Qc-al Time :
9 feU 925
0 0: 2 6
Compound
15 15 )
17)
29 ) 31 ) 4!J ;
*Brq-roochlorometfaane
1,2-Dichloroethane-d4 *114-Dx Fluorobenzene *Cfelorobensene-dS
Toluene d8 4-Bromotluorobenzene
* Conpounc! is. I STD
R.T. Q ion
8 46 128.0 10.37 65.0 11 . 06 114.0 15.33 117.0 13.23 98.0 12.05. 95 0
Hr ea
453 95 6728IJ 18 2 H ll 9 193510 146/07 121223
Cone
U Vi j. *t. s
50 . 00 4b .66 5 0.00 5:: . 0U 48.14 5 0.0 U
ug/L uo/L uo .-'L ug/L ug-'L ug/L.
q
'dli' qQ
92 9 98 86
88
DUPO 50308065
Lancaster Laboratories Quantitation Report-GC'ES Uoiatile:
Lit:
a r-
File: ''GSHUS Injected: 05:33 09/25/96
Sample; MFi
258382?
Dilation Factor:
1.8-
Initial Uoluwe/Ut.:
5.0
Standard: AGSPSi
Inst. HP034&U
Batch:
G962681RA
Final Uotune/(Jt.: 5.0
Method: ?'b Matrix/leoel: 6); Blank: AGSHB1
t Internal Standards
8.T. (+/-RT) Scan Qion ftreal+/-$Area) Gone.
ijC Flag Cone Units = cg/l
1. Bromochloromethane 17. 1,4-Difluorobenzene 29. Chlorobenzene-d5
f - RETENTION TIME OUT Of 8RNSE
S.46U-.U29) S42 128
45345C-22)
50.00
11.06(-.S33) 77S 114
182909(-25)
50.00
15.33(-.fl33) 1146
117
1435101-27)
50.00
* - INTERNAL STANDARD RHER OUT OF RANGE NC = NOT ABLE TO CALCULATE--NO STANDARD.
# Surrogate Standards
R.T. (V-R8?) Scan
Qion
Rrea
Cone.
tRec. y
aaBSs&3SBBBSSS9a:sssss=ss=BssB5S&r:
15. l,2-Dichloroeihane-d4
10.371.00(10)
?20
65
31. Talaene-dH
13.23 (.00111)
966
98
40. 4-Bromofluorobenzene
17.USt-.DOO) 1294
95
? = EELRTIUE RETENTION TIME OUT OF RANGE * tREC OUT OF RRNSE
67280
45.86
91
146707
48.14
86
121229
50.00
100
D = SURROGATES DILUTED OUT NC = COULD NOT CftLCULHTE
Target Compounds
R,T.t+/-RKT)
Scan Qion
Rrea
Cone.fl
Cone.B
Cone. Blank 0
Quantitation
limit
2. Chloromethane 3. Uirtyl. Chloride 4. Bromomethane 5. Chioreethane 6. 1,1-Dichloroethene 7. Acetone 8. Carbon Disulfide 9. Methylene Chloride 11. 1,1-bichloreethane
12. 1 ;2-Di.chloroethene (total i 13. 2-Butanone 14. Chloroform 16, 1 ;5-Dichloroethane IK. 1,1,1-Trichloraethane 19. Carbon Tetrachloride 20. Benzene 21. Trichioroethene 22. l;2-Diehiorr.propane 23. Sromcdiehioromethane 24. ets-1,3-Dichiorapropene 25. trans-l,3-Dichloropropene 26. i;i,2-Tri.chLoroethans
10 10 10 18 10 10
16
10
10 10
10 10
10 10
10
10 10 10 10 10
10
10
fl = 8RU COKC. B = case. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CfiL. RANGE
RELflTJUE RETENTION TIME OUT OF RANGE
Lab Chronicle:
______________________________________________________________Ent. by _____
----------------------------------------------------------------------------------------------Uer. by PRGE 1 OF 2
DUP050308066
Lancaster Laboratories Quantitation Report-GC/H9 Volatiles
U.U L? If) & 3 fc-:
t-:s -4 t
File: ''SSPlffi Injected: (15:39 09/25/98
Sample: BRAF1
2583827
Dilution Factor:
1.8
initial Volume/tlt.:
5.8
Standard: WSl
Inst. HFU34S0
Batch:
G3626S1HA
final Uclrnne/Ut.: 5.0
I Target Compounds
77, Bibromochloromethane ?K. Bromororm 36. 4-Methyl-2-Perrtanone 32. Toluene 33. Tetrachloroethene 34. 2-Hexanone 35. Chlorobenzene 36. Ethylbeiaene 38. Xylene !total) 39. Styrene 41. 1,1,2,2-Tetrachloroethane
R.T.I+/-RBT)
Scan (Jion
Area
Method: 7158 Matrix/leuel: 8.. Blank: '"GSKBi
Cone. A
Cone.B
Cone. Blank Q
Quant itat ion
Li it =^=
:0 u 10
Il
ls
lii 10 ID 10
10 10
H . RHlii cone. & CONC. MULTIPLIES! BY DILUTION FACTOR E = CONC. OUT OF CAL. RANGE = RELATIVE RETENTION TIME OUT OF RANGE
Lab Chronicle:
_Ent. by
Ver . by
Anaiust:
-2ZZv
_Date:
Auditor:
_________________ _________________________ Date: ............ .............................. PAGE 2 OF 2
90
DUP050308067
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract: _______.
BRAT2
Lab Code: LANCAS
Case No.: ______
SAS No.:
SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: 2583828
Sample wt/vol: 5..0
(g/mL) ML
Lab File ID: >GSP09
Level:
(low/med) LOW
Date Received: 09/19/96
% Moisture: not dec. _______
Date Analyzed: 09/25/96
GC Column: DB624
ID: 0.53 (mm}
Dilution Factor:
1.o
Soil Extract Volume: _______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3------------------- Chloromethane 75-01-4------------------- Vinyl Chloride 74-83-9------------------ Bromomethane 75-00-3-- ----------- Chloroethane 75-35-4------------------- 1,1-Dichloroethene 67-64-1------------------- Acetone 75-15-0------------------- Carbon Disulfide 75-09-2------------------- Methylene Chloride 75-34-3------------------- 1,1-Dichloroethane 540-59-0----------------1,2-Dichloroethene (total) 78-93-3------------------- 2-Butanone 67-66-3------------------Chloroform 107-06-2----------------- 1,2-Dichloroethane 71-55-6----------- --1,1,1-Trichloroethane
56-23-5------*------------ Carbon Tetrachloride 71-43-2------------------- Benzene
79-01-6------------------- Trichloroethene 78-87-5------------------ 1,2-Dichloropropane 75-27-4------------------ Bromodichloromethane 10061-01-5-------------cis-1,3-Dichloropropene 10061-02-6-------------trans-1,3-Dichloropropene 79-00-5------------------ 1,1,2-Trichloroethane 12 4-48-1----------------- Dibromochloromethane 75-25-2------------------- Bromoform 108-10-1-------- ---------4-Methyl-2-Pentanone 108-88-3----------------- Toluene ' 12 7-18-4-----------------Tetrachloroethene 591-78 -6----------------2 -Hexanone 108-90-7----------------- Chlorobenzene 100-41-4----------------- Ethylbenzene 1330-20-7---------------Xylene (total) 100-42-5----------------- Styrene
79-34-5------------------- 1,1,2,2-Tetrachloroethane
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VOA
OLM03. o9i
A
DUP050308068
rriTq \ in?* nwRiTMBTnfi**s"
40 s'
! SfetfOCOi ; --40000-]
IH
! C0QCv-j
Ii
l*0000-j
it-uoucH
I4GG00-1
12Q0Q0\ j.
X O 0 000~
tl{ b'JOOOi 40000i :o c c *;h
f fV
Tic
3 I
4
*NI _
n11 j,
pul
l?oo
iU
l. iT i*
Usxa Fiie ; >CBFOS : : D")
yuant Output File; '"GS5FUS : : FM
Name : BRRT2
2583828
Instrument ID; HP03';1S0
Muc: ~SRM (cil.Jl, %V +>
'IGHS2B81HH S''GHFHi
*5 =1
Id File ; IW-i9 0 : : UB Tit le : 3-"SI l Water .'Med Soil ID File Last Calibration: 951207 01:59
for Inst, Hf 1346 0 Past ycal Time:
ybl!S25
0 0:26
Operator IP: SMM-98*
Quant Time : 960925 06:36 Injected at: 960925 06:11
9 /j
DUP050308069
""iv*
yi!.4NT RKKORT
Operator ID` SttM-983
Output File: ''GSP09 : : Fh
Data File :
>CSf09 : : U4
Name ; BKHT2
2bK382W
Mi sc i ' SAM (3UL %C +>
yuant Rev: ftG96268IHA S'-GSFBl
y iguant `Lme : 1 r.jer, ted at :
D11 u t ion Factor Ins trament II'1'
&5 *5 = 1
Ft: ,- :'5 08-36 9- Or. 2 5 l.ifcl : L i
i ; = ! l 1. H- 0346-.
ID File : If' 4 3 9 U : : DB Title: 3/90 tiater/Med Soil ID File Last Calibration: 35120!/ 01:59
For
Inst. HPO 3'16 0 Las t ftcal
Time :
98 0929
0 0 :26
Compound
1) 15 ) 17) O U %
31 ) <31! I
*br otnoohlor omet hane 1 /i-DichlorGethane~d4
*1}4-Difluorobensene *C:.ior o benzene ~d5
Toiuene-dB 4- dr OTr.o r iuor obenzene
* Compound is- I STD
R.T. Q ion
S . 45 128.0 1 L! . 36 .65.0 11 . 05 114.0 lb . 33 117.0 13.22. 38.0 17.05 95.0
fH 65 3
45 ! i ! 2 65688 170584 136116 0 13ybbl 12U231
( y'.i nc
i.inrts
50 . 00 . 31
5U . 00 5o.au ' > ci . O 0 52.311
un.'L uq ag/L u g 1., <L: Ij j_i ag/u
q
8 8 9 y ."r .H
9
DUP050308070
Lancaster Laboratories Quantitation Report-GC/HS Oolatiies
LLit; li? rn fc-:e; v; s h
Fite' '`GSRllS Injected: OS; 11 03/25/36 Sample: BKAT2 " 2583328
Dilation Factor: Initial Ur. lune/OR.:
1.0 5.0
Standard: /'GSFS1
Inst. 8603480
Batch:
G962681HA
Final Onlonse/IOt.: 5.0
Method: 711& Matrix/level: Blank: "GSHBl
8 Internal Standards
R.T. t+/-RT! Scan Qion
Areas*/-flrea) Cone.
yC Frag Cone Units * u -j -'l
1. Bromochioromethane 1?. 1.4-DifIuorobenzene 28. ChLoroberzene-dS
S = RETENTION TIME OUT OF RANGE
9.453t-.037) 645 128
45012(-23!
50.00
11.05!-.040) 782 114
l?0584t-3D)
50.00
15.33t-.029) 1150 117
136O60(-31)
50.00
* = INTERNAL STHNDHRD AREA OUT OE RANGE
NC = NOT ABLE TO CALCUl ATE-h :.' STANDARD
i Surrogate Standards
R.T. (+/-RRT) Scan
Qian
Area
Cone.
tRec. Q
15. l/2-Bichioroethane-d4
ia.3St.oao2)
723
65
31. Taluene-dB
13.22l-.081)
963
96
48. 4-BroraofIuorobenzene
17.tlSL-.a08) 1298
95
i - RKLATIOE RETENTION TINE Ol!T OF RANGE * = %REC OUT OF RANGE
65688
44.91
90
139551
48.30
97
120231
52.30
105
D = SURROGATES DILUTED OUT NO = COULD NOT CALCULATE
t Target Compounds
R.T.(*/-RRT)
2. Chloromethane 3. Oir.yl Chloride 4. Bramomethane 5. Chioroethane 6. 1jl-Dichloroeinene 7. Acetone 8. Carbon Disulfide 9. Methylene Chloride U. 1,1-Sichloroethane 12. l}2-Dichloroethene (totalJ
13. 2-Butanone 14. Chloroform 16. 1,2-Dichloroethane 18. 1^,1-Tnchloroethane 18. Carbon Tetrachloride OIL BenzEne 21. Trichloroethene 22. 1,2-L'ichioropropane 73. Bromod ichloroaethane 24. cis-1jS-Dichicropropene 25 trans-1,3-Dzchloroprcpene ?E. 1 ,2-Trich.Ioroethane
------------------------------------------ ---------- ------ ------------------- --
Scan Qion
Area
Co.nc.fl
Conc.O
Cone. Biank Q
Quantitation Limit
10 10
10
10
10 It 10 10 10 10 10 10 10 10 10 IS 10 10 10
lti
10 10
P. = RAF! CON". t - CONC. MULTIPLIED BY DILUTION FACTOR E = OONC. OUT OF CAL. RANGE I = RELATIUE RETENTION TIME OUT Of RANGE
Lab Chronicle:Ent. by
_______________________________ _________________________________________________________________Cer. by 0 A RAGE i OE 2
DUP050308071
Lancaster Laboratories Quantitation Report-GC/MS Uctaiiie:
! =: fi *!_
File: "6SKS9 Injected: 86:11 83/25-'96 Sample- BHAT2 " 258382k
Dilution Factor: Initial Uclame/Ot.:
1,8 5.8
Standard: "SSPSl
Inst. HHII34B0
Batch;
G962S81RR
Final Uciune/Ut.: 5.0
Method. ?'.56
Matrix.-'lew! C; Blank- "GSKS1
t Target Compounds
R.T.t*/-KR?l
Scan- Qion
ftrea
Cone.ft
Cone.B
Cone. Blank
anti tat; or.
Lioiiit
27. Dibromochlcransethane 28. Bromoform 30. 4-Methyl-2-Pentanone 32. Tnitiene 33. Tetrachloroethene 34. 2-Bexanone 35. Chlorobenzene 38. Ethylbenzene 38. Xylene I totalJ 38. Styrene 81. 1 ,l,2j2-Tetrachloroethane
---------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------:------------------------------------------------------------------ 1------------------------------------------------------------------------------------ 1------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------ -----------------
....................
ll:
.......................... .............
18
----------------------------------------- ly
............ ......................................
It!
---------------------------------------------- .y
ft - m CONC. B COSC. MULTIPLIED BY DILUTION FACTOR E CONC. OUT OF CftL. BHNSE Lab Chronicle:
RELftTiOE RCTar-lON TIME OUT OF BUNGE tnt. by
95 DUP050308072
Standards Data
9(
DUP050308073
6A VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: LANCASTER LABS
Contract: ______ .
Lab Code: LANCAS Case No.: ________ . SAS No. _______ . SDG No.: _______
Instrument ID; HP03460
Calibration Date(s): 09/24/96
09/24/96
Heated Purge; (Y/N) N
Calibration Times: 0140
0349
GC Column: DB624
LAB "FIEimn--------------
RRF 50= >GSMI3
ID: 0.53 (mm)
RRF 10= >GSMI1 RRF100= >GSMI4
RRF 20= >GSMI2 RRF200= >GSMI5
COMPOUND
RRF 10 RRF 20 RRF 50 RRF100 RRF200
--f--
SKF RSD
Dichlorodifluoromethane
2.648
Chloromethane Vinyl Chloride
1.601 9if 1.512
Bromomethane
if 1.025
Chloroethane
.863
Trichlorofluoromethane
1.392
Furfuran
1.549
Ethyl Ether
.905
Acrolein 1,1-Dichloroethene
.158 9t 1.082
Freon 113
2.244
Acetone
.418
Methyl Iodide
3.589
Carbon Disulfide
3.350
Allyl Chloride
2.237
Methylene Chloride
2.082
t-Butyl Alcohol
.088
Acrylonitrile
.243
Methyl t-Butyl Ether
2.842
1,2-Dichloroethene (total) 1.353
n-Hexane 1,1-Dichloroethane 1-Propanol
1.533 ifc 2.773
.002
2-Butanone
.411
Propionitrile
.089
Ethyl Acetate
1.490
Methacrylonitrile
.318
Tetrahydrofuran Chloroform Cyclohexane
.312 if 2.967
2.012
1,2-Dichloroethane
* 1.971
Vinyl Acetate
.055
1,1,l-Trichloroethane
* .490
J
2.285 1.179 1.143
.904 .680 1.274 1.252 .764
.132 .944 1.831
.285 3.601 2.630 1.654 1.489
.074 .191 2.396 1.167
.992
2.211
.003 .314 .070
1.110
.266
.232 2.525
1.359 1.716
.051 .450
2.196 1.095 1.091
.755 .593 1.215 1.179 .697
.118 .914 1.813 .248 3.594 2.564 1.571
1.210
.065 .182
2.241 1.125 1.117 2.142
.003 .300 .066 .996 .236 .193
2.485 1.401
1.614 .046 .448
2.221
1.033 1.039
.711 .558 1.258
1.218 .716 .132 .876
1.822
.253 3.579 2.607 1.689
1.112
.066 .194
2.372 1.106 1.162 2.068
.003 .301 .069 1.055 .255
.220
2.385 1.444
1.562 .049 .451
2.221
1.061 1.083
.662 .387 1.176 1.233
.734 .143 .885 1.725 .254 3.663 2.685 1.761 1.151
.074
.211
2.406 1.144
1.082 2.130
.004 .326 .076 1.179 .271 .234
2.396 1.431
1.534 .052 .444
2.314 1.194 1.173
.811 .617 1.263 1.286 .763 .137 .940 1.887 .292 3.605 2.767 1.782 1.409
.073 .204
2.452 1.179 1.177 2.265
.003 .330 .074 1.166 .269 .238
2.552
1.529
1.679 .050 .456
All other compounds in OLMOl.8 must meet a minimum RRF of o.oio.
8.2
19.6 16.4* 18.5* 28.5
6.5 11.6 10.9
10.8
8.9*
10-.8
24.8 .9
11.9 14.8 28.7
12.3 11.7
9.3 8.5
17.7 12.7* 20.4 14.0
12.2
16.6 11.3 18.7
9.4* 17.8
10.5* 6.4 | 4.1*
1
page 1 of 3
FORM VI VOA
OLM03.0
97
DUP050308074
6A VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: LANCASTER LABS
Contract: _______ .
Lab Code: LANCAS
Case No.: '. SAS No. _______ . SDG No.: _______
Instrument ID: HP03460
Calibration Date(s): 09/24/96
09/24/96
Heated Purge: (Y/N) N
Calibration Times:
0140
0349
GC Column: DB624
ID: 0.53 (mm)
LAB FILE ID: RRF 50= >GSMI3
Rr F 10= >GSMIl ERF100= >GSMI4
Er f 2o= >g s mI2-------RRF200= >GSMI5
COMPOUND
RRF 10 RRF 20 RRF 50 RRF100 RRF200
--s-- KKF RSD
Carbon Tetrachloride
1 t .501
Isobutyl Alcohol Benzene
1 .008 * .861
n-Heptane
.227
n-Butanol Trichloroethene
.006 k .409
l? 2-Dichloropropane
.429
Dibromomethane
.324
1,4-Dioxane
.003
n-Propyl Acetate Bromodichloromethane
.547 4k .731
2-Nitropropane
.092
2-Chloroethyl Vinyl Ether
.197
cis-l,3-Dichloropropene
* .594
trans-1,3-Dichloropropene * .507
1,1,2-Trichloroethane
* .366
Dibromochloromethane
* .689
Bromoform
* .609
trans-1,4-Dichloro~2-Butene .123
4-Methyl-2-Pentanone Toluene
.418 * 1.151
Ethyl Methacrylate
.444
Tetrachloroethene
.529
2-Hexanone
.255
1,2-Dibromoethane Chlorobenzene
.631 b 1.001
1,1,1,2-Tetrachloroethane
.433
Ethylbenzene Xylene (total)
j .398 k .502
Isoamyl Acetate Styrene
.426 ib .883
Cumene
1.280
Cyclohexanone
.012
.459 .007
.721
.157 .005
.389 .351
.290 .003 .461 . 656 .081 .175 .522 .444 .319 .672 .608 .115
.324 .999 .416 .488 .209 .609 .918 .412 .350 .430 .370 .780 1.068 .011
.467
.006 .701
.201 .005
.380 .331
.275 .002 .428 .652 .065 .172 .511 .435 .305 .663 .606 .104
.296 .976 .402 .511 .201
.574 .889 .405 .351 .434 .345 .797 1.144 .010
.455 .006
.688 .201 .005 .379
.319 .333 .002 .442 .641 .081 .180 .515 .448 .299 .646 .593 .104
.335 1.043
.492 .528 .222
.629 .883 .531 .349 .436 .367 .798 1.231 .010
.445 .006
.685 .177 .005
.373 .323 .311 .002 .465 .624 .085
.191 .509 .436 .294 .628 .606 .100
.362 1.075
.512 .503 .251
.660 .901
.507 .338 .408 .389 .756 1.197 .011
.465 .006
.731 .193 .005
.386 .350
.307 .003 .469 .661 . 083r .183 .530 .454 .317 .660
.604 .109
.347 1.049
.453
.512 .228
.621 .918 .457 .357 .442 .380 .803 1.184 .011
4.6 14.2
10.1 13.9
12.0
3.6' 12.9
7.8 15.8
9.9 6.3' -12.0 5.9 6.86.6 9.2 3.6'
1.1' 8.8
13.4 6.5
10.5
3.4' 10.8
5.1 5.2' 12.5 6.5' 8.0' 8.0 6.0' 6.9
7.9
..tyi All other compounds in OLMOl.8 must meet a minimum RRF of 0.010.
page 2 of 3
FORM VI V0A
OLM03.0
98
DUP050308075
6A VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: LANCASTER LABS
Contract: _______ .
Lab Code: LANCAS
Case No.: '. SAS No. _____ SDG No.: _______________
Instrument ID: HP03460
Calibration Date(s): 09/24/96
09/24/96
Heated Purge: (Y/N) N
Calibration Times:
0140
0349
GC column: DB624
ID: 0.53 (mm)
LAB FIOTHd ! RRP 50= >GSMI3
RRF 10= >GSMll RRP100= >GSMI4
Rr E 20= >GSMI2 RRF200- >GSMI5
COMPOUND
RRF 10 RRF 20 RRF 50 RRF100 RRF200
--r~ KKF RSD
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane 2-Chlorotoluene Pentachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl Chloride 1,2-Dichlorobenzene 1,2-Dibromo-3-Chloropropane
.728 .164 .366 .390 .891
.992 .754 .879 .148
.642
.149 .319 .372 .780 .900 .719 .789 .148
.598 .137 .335 .374 .841 .925 .669 .795 .124
.621
.145 .357
.485 .904
.990 .728 .870 .136
.651 .143
.349 .484 .897 .980 .751 .892 .150
.648 .148
.345 .421 .863 .958 .724 .845 .141
1,2-Dichloroethane-d4
1.472 1.584 1.494 1.470 1.500 1.504
Toluene-d8
.971 1.104 1.059 1.110 1.116 1.072
4-Bromofluorobenzene
* .766
.899 .856 .873 .817 .842
I
,r Compounds with required minimum RRF and maximum %RSD values.
All other compounds in OLM01.8 must meet a minimum RRF of 0.010.
7. 6 7. 0 5. 4 13. 9 6. 1 4. 4 4. 8 5. 8 7. 9
3. 1 5. 7 6. 2
page 3 of 3
FORM VI V0A
OLM03.0
99
DUP050308076
TOTAL ION CHROMATOGRAM
File >6Snil 35.0-300.o'amu. VStOOlO TIC
400
rI
800
80000-
260000-
010 ppb IC"SAn 7.C OWL *1 +OCEC
1200 1
1600
.x--i,,.. -E-..i__i.
i t'r 20 22
Data File: >GSMI1::D5
Quant Output File: AGSMI1::FM
Name: VSTD010 010 ppb IC
Instrument ID: HP03460
Misc: -SAM %C @WL =1 +DCE05Y-W
Id File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960910 21:25
Operator ID: SAM-983 Quant Time : 960924 02:06 Injected at: 960924 01:40
100
DUP050308077
Operator ID: SAM-983 Output File: ~GSMI1::FM Data File: >GSMI1::D5
Name: VSTD010 010 ppb- ic Misc: -SAM %C @WL =1 +DCE05Y-W
QUANT REPORT
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Page 1
960924 02:06 960924 01:40
1.00000 HP03460
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst HP03460
Last Calibration: 951207 01:59
Last Qcal Time 960910 21:25
Compound
1) 2)
3) 4) 5) 6) 7)
8) 9) 10) 11)
12) 13) 14) 15) 16) 17)
18) 19) 20) 21)
22) 23)
24) 25)
26) 27)
28) 2 9) 30) 31) 32) 33) 34) 35) 36)
37) 3 8)
39) 40)
*Bromochloromethane Dichlorodifluoromethane
Chloromethane Vinyl Chloride Bromomethane chloroethane Trichlorofluoromethane
Furfuran Ethyl Ether Acrolein 1,1-Dichloroethene
Freon 113 Acetone Methyl Iodide Carbon Disulfide Allyl Chloride Methylene Chloride
t-Butyl Alcohol Acrylonitrile Methyl t-Butyl Ether trans-l,2-Dichloroethene
n-Hexane l,l-Dichloroethane
1-Propanol cis-l,2-Dichloroethene
2-Butanone Propionitrile
Ethyl Acetate Methacrylonitrile Tetrahydrofuran Chloroform Cyclohexane l,2-Dichloroethane-d4 1,2-Dichloroethane *1,4-Difluorobenzene Vinyl Acetate
1,1#1-Trichloroethane Carbon Tetrachloride
Isobuty1 Alcoho1 Benzene
R.T. Q ion
9.48 128.0 3.06 85.0 3.28 50.0 3.52 62.0 4.07 94.0 4.29 64.0 4.84 101.0 5.50 68.0 5.43 59.0 5.68 56.0 5.86 96.0 5.94 101.0 5.99 43.0 6.14 142.0 6.27 76.0 6.60 41.0
6.83 84.0 7.16 59.0 7.30 53.0 7.39 73.0 7.37 96.0 7.88 57.0 8.11 63.0 8.38 59.0 9.10 96.0
9.12 43.0
9.20 54.0 9.25 43.0 9.45 67.0 9.57 42.0 9.62 83.0 10.01 56.0 10.39 65.0 10.51 62.0 11.07 114.0 8.24 86.0 9.90 97.0
10.17 117.0 10.39 41.0 10.49 78.0
Area
Cone
Units
52918
50.00 ug/L
28026
10.66 ug/L
16944
12.84 ug/L
16000
12.07 ug/L
10850
12.55 ug/L
9189
12.60 ug/L
14733
7.94 ug/L
16392
12.08 ug/L
9581
13.16 ug/L
8348
52.99 ug/L
11451
11.30 ug/L
47499
17.37 ug/L
4427
16.30 ug/L
37980
6.76 ug/L
35457
10.60 ug/L
23674
15.73 ug/L
22036
17.47 ug/L
4644M. 258E-37 ug/L
12843
57.71 ug/L
30083
12.45 ug/L
13839
11.46 ug/L
16223
13.58 ug/L
29349
12.04 ug/L
262
90.12 ug/L
14795
12.25 ug/L
4349
11.85 ug/L
4693M. 261E-37 ug/L
15774
16.83 ug/L
8414M. 467E-37 ug/L
3307
17.05 ug/L
31404
11.31 ug/L
21291
14.28 ug/L
15579
9.32 ug/L
20860
11.78 ug/L
220675
50.00 ug/L
2408
11.19 ug/L
21605
10.87 ug/L
22107
10.33 ug/L
4409 228.08 ug/L
37984
12.82 ug/L
q
59 98 96 99 86 91 95 78 70 86 91 97 90 69 100 82 87
93 95 89 94 95 100 93 90
96
88 94 88 98 82 93 93 87 95 99 91
101
DUP050308078
QUANT REPORT
Page 2
Operator ID: SAM-983 Output File: ~GSMI1::FM
Data File: >GSMI1::D5 Name: VSTD010 010 ppb IC Misc: -SAM %C @WL =1 +DCE05Y-W
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
instrument ID:
960924 02:06 960924 01:40
1.00000 HP0346D
ID File: IA439Q::DB
Title: 3/90 Water/Med Soil ID File for Inst HP03460
Last Calibration: 951207 01:59
Last Qcal Time 960910 21:25
Compound
41) n-Heptane 42} n-Butanol 43) Trichloroethene 44) l{2-Dichloropropane 4 5) Dibromomethane 46) 1,4-Dioxane 47) n-Propyl Acetate 48) Bromodichloromethane 49) 2-Nitropropane 50) 2-chloroethyl Vinyl Ether 51) cis-l,3-Dichloropropene 52) trans-1,3-Dichloropropene 53) 1,1,2-Trichloroethane 54) Dibromochloromethane
55) Bromoform 56) trans-1,4-Dichloro-2-Butene 57) *Chlorobenzene-d5 58} 4-Methyl-2-Pentanone
59) Toluene-d8 60} Toluene 61) Ethyl Methacrylate 62) Tetrachloroethene 63) 2-Hexanone 64) 1,2-Dibromoethane 65} Chlorobenzene 66) 1,1,1,2-Tetrachloroethane 67} Ethylbenzene 68) m+p-Xylene 69) Isoarayl Acetate 70) o-Xylene 71) Styrene 72) Cumene 7 3) Cyclohexanone 74) 4-Bromofluorobenzene 75) 1,1,2,2-Tetrachloroethane 76) l,2,3-Trichloropropane
77) 2-Chlorotoluene 78) Pentachloroethane 79) l,3-Dichlorobenzene 80) 1,4-Dichlorobenzene 81) Benzyl Chloride
R.T. Q ion
10.91 71.0 11.39 56.0 11.48 130.0 11.79 63.0 11.98 93.0 11.99 88.0 12.06 43.0 12.21 83.0 12.53 41.0 12.64 63.0 12.85 75.0 13.66 75.0 13.93 97.0 14.51 129.0 16.60 173.0 17.35 53.0 15.35 117.0 13.06 43.0 13.25 98.0 13.34 91.0 13.79 69.0 14.16 164.0
14.28 43.0
14.69 107.0 15.40 112.0 15.51 131.0 15.55 106.0 15.71 106.0 15.80 70.0 16.31 106.0 16.32 104.0 16.84 105.0 16.97 55.0 17.08 95.0 17.26 83.0 17.33 110.0 17.59 126.0 18.23 167.0 18.70 146.0 18.83 146.0 19.03 91.0
Area
Cone
Units
10021
11.22 ug/L
3444 217.99 ug/L
18046
10.97 ug/L
18914
12.31 ug/L
14295
8.86 ug/L
1745 181.59 ug/L
24161
14.20 ug/L
32283
10.53 ug/L
8088
25.15 ug/L
8699
10.58 ug/L
26234
12.30 ug/L
23297
12.80 ug/L
16149
11.60 ug/L
30392
10.15 ug/L
26896
9.60 ug/L
13625M. 18IE--37 ug/L
179841
50.00 ug/L
15035
13.97 ug/L
34909
9.06 ug/L
41383
11.87 ug/L
15983
9.40 ug/L
19023
10.85 ug/L
9185
12.91 ug/L
22691
8.81 ug/L
35995
10.95 ug/L
15561
6.37 ug/L
14316
11.64 ug/L
37084
25.25 ug/L
15324
11.85 ug/L
18051
12.29 ug/L
31749
10.97 ug/L
46040
9.97 ug/L
5261 174.28 ug/L
27567
8.91 ug/L
26179
13.10 ug/L
5901
9.51 ug/L
13172
10.34 ug/L
14011
6.24 ug/L
32049
7.99 ug/L
35679
8.16 ug/L
27112
9.77 ug/L
q
81 92 88 79 79 83 95 94 94 86 89 92 95 99 97
93 88 97 92 69 92 98 92 90 89 99 96 93 96 88 93 89 97 96 60 94 86 94 92 90
10 3
DUP050308079
Operator ID: SAM-983 Output Pile: " GSMI1: :FM Data File: >GSMI1::D5
Name: VSTD010 010 ppb IC Misc: -SAM %C @WL =1 +DCE05Y-W
QUANT REPORT
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
Instrument ID
Page 3
960924 02:06 960924 01:40
1.00000 HP03460
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last calibration: 951207 01:59
Last Qcal Time: 960910 21:25
Compound
82) 1,2-Dichlorobenzene 83) l,2-Dibromo-3-Chloropropane
* Compound is ISTD
R.T. Q ion
19.40 146.0 20.61 157.0
Area
31600 5306
Cone
Units
8.37 ug/L 9.84 ug/L
q
Z 8'
10:
DUP050308080
Compound No: 18
Compound Name: t-Butyl Alcohol
Scan Number: 442
Retention Times 7.16 min
Quant ion: 59.0
Area:
4644M
Concentration:
.00 ug/L
q-value: 0
This report was produced by QAREA at:
4:40 AM TUE., 24
SEPT, 1996
104
DUP050308081
Data File: >GSMI1 Name: VSTD010 010 ppb IC Misc: -SAM %C @WL =1 +DCEOSY-W
Quant Time: 960924 02:06 Injected at: 960924 01:40
Compound No: 27
Compound Name: Fropionitrile
Scan Number: 618
Retention Time: 9.20 min
Quant Ion: 54.0
Area:
4693M
Concentration:
.00 ug/L
q-value: 0
Quant Output File: *GSMI1 Instrument ID: HP03460
Quant ID File: IA4390 . Last Calibration: 951207 01:59
This report was produced by QAREA at: 4:41 AM TOE., 24 SEPT, 1996
105
DU P 05030 8082
Data File: >GSMI1
Name: VSTDQ10 010 ppb XC Misc: -SAM %C @WL =1 +DCEQ5Y-W Quant Time: 960924 02:06 Injected at: 960924 01:40
Quant output File: 'GSMIi Instrument ID: HP03460
Quant ID File: IA4390 Last Calibration: 951207 01:59
Compound No: 29
Compound Name: Methacrylonitrile
Scan Number: 639
Retention Time: 9.45 min
Quant Ion: 67.0
Area:
8414M
Concentration:
.00 ug/L
q-value: 0
This report was produced by QAREA at: 4:42 AM TUE., 24 SEPT, 1996
106
DUP050308083
Data File: >GSMI1
Quant Output File: *GSMI1
Name: VSTD010 010 ppb IC
Instrument ID: HP034 60
Misc: -SAM %C @WL =1 +DCEOSY-W
Quant Time: 960924 02:06
Quant ID File: IA4390
Injected at: 960924 01:40 A
Last Calibration: 951207 01:59
Compound No: 56
Compound Name: trans-1,4-Dichloro-2-Butene
Scan Number: 1316
Retention Time: 17.35 min
Quant Ion: 53.0
Area:
13625M
Concentration:
.00 ug/L
g-value: 0
This report was produced by QAREA at: 4:43 AM TUB., 24 SEPT, 1996
7
DUP050308084
TOTAL ION CHROMATOGRAM File >6St1I2 36.0-300.0 amu. VSTDQ2Q
TIC < I i < 40I 0 1__!_I--I---1--1--801--0X
80000-
020 ppb IC~SRI1 J5C 0WL -1 +DCEC
1200
1 - 1 1 1
, 1600
-i -t-I-, i i
240000220000-
Data File: >GSMI2::D5
Quant Output File: A-GSMI2::FM
Name: VSTD020 020 ppb IC
Instrument ID: HP03460
Misc: -SAM %C @WL =1 +DCE05V-W
Id File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
operator ID: SAM-983 Quant Time : 960924 03:07 Injected at: 960924 02:12
108
DUP050308085
QUANT REPORT
Page 1
Operator ID: SAM-983 Output Pile: ~GSMI2;:FM Data File: >GSMI2::D5
Name: VSTD020 020 ppb IC Misc: -SAM %C @WL =1 +DCE05Y-W
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960924 03:07 960924 02:12
1.00000
HP03460
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Compound
1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Furfuran 9) Ethyl Ether 10) Acrolein 11) 1,l-Dichloroethene 12) Freon 113 13) Acetone 14) Methyl Iodide 15) Carbon Disulfide 16) Allyl Chloride 17) Methylene Chloride 18) t-Butyl Alcohol 19) Acrylonitrile 20) Methyl t-Butyl Ether 21) trans-lf 2-Dichloroethene 22) n-Hexane 23) 1,l-Dichloroethane
24) 1-Propanol 25) cis-l,2-Dichloroethene 26) 2-Butanone 27) Propionitrile 28) Ethyl Acetate 29) Methacry1onitri1e 30) Tetrahydrofuran 31) Chloroform 32) Cyclohexane 33) 1,2-Dichloroethane-d4 34) 1,2-Dichloroethane 35) *1,4-Difluorobenzene 36) Vinyl Acetate 37) 1,1,1-Trichloroethane
38) Carbon Tetrachloride
39) Isobutyl Alcohol
40) Benzene
R.T. Q ion
9.50 128.0 3.08 85.0 3.31 50.0 3.56 62.0 4.10 94.0 4.31 64.0 4.86 101.0 5.52 68.0
. 5.45 59.0 5.70 56.0 5.90 96.0 5.97 101.0 6.02 43.0 6.18 142.0 6.32 76.0 6.63 41.D 6.86 84.0 7.15 59.0 7.32 53.0 7.41 73.0 7.39 96.0 7.91 57.0 8.13 63.0
8.39 59.0 9.12 96.0 9.15 43.0 9.23 54.0 9.26 43.0 9.47 67.0 9.58 42.0 9.64 83.0 10.02 56.0 10.41 65.0 10.52 62.0 11.08 114.0 8.24 86.0 9.93 97.0 10.19 117.0 10.40 41.0 10.51 78.0
Area
Cone
Units
56711
51841 26736 25924 20500 15420 28904 28402 17329 14919 21421 83090
6455 81690 59650 37520 33783
8369 21710 54346
25729 22506
50154
867
27229 7117 7960
25189 15067
5263 57277 30837 35934 38921
226246 4644
40733 41524
7662 65209
50.00 ug/L
18.40 ug/L 18.90 ug/L 18.24 ug/L 22.13 ug/L 19.73 ug/L 14.54 ug/L
19.52 ug/L
22.21 ug/L
88.36 ug/L 19.73 ug/L 28.36 ug/L 22.18 ug/L 13.57 ug/L 16.64 ug/L 23.27 ug/L 24.99 ug/L . 434E-37 ug/L 91.03 ug/L
20.99 ug/L 19.89 ug/L 17.58 ug/L
19.20 ug/L
278.26. ug/L
21.05 ug/L
18.09 ug/L .412E-37 ug/L
25.07 ug/L .781E-37 ug/L
25.31 ug/L 19.25 ug/L 19.30 ug/L 20.07 ug/L 20.51 ug/L 50.00 ug/L 21.05 ug/L 19.99 ug/L 18.92 ug/L 386.59 ug/L 21.46 ug/L
q
72 96 99 96 85 91 97 84 71 97 93 94 86 66 100 88 91 96 91 98 92 95 96 100 98 86 88 98 85 93 96 89 98 85 93 94 91 97 88 94
ios
DUP050308086
Operator ID: SAM-983 Output File: AGSMI2::FM
Data File: >GSMI2::D5 Name: VSTD020 020 ppb IC . Misc: -SAM %C WL =1 +DCE05Y-W
QUANT REPORT
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Page 2
960924 03:07 960924 02:12
1.00000 HP03460
ID File: IA4390::DB
,
^.
Title: 3/90 Water/Med Soil ID File for Inst HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Compound
41) 42) 43) 44) 45) 46)
47) 48)
49) 50) 51) 5 2) 53) 54)
55) 56)
57) 58) 59) 60) 61) 62)
63) 64)
65) 66)
6 7) 68) 69) 70) 71) 72) 73) 74) 75) 76) 77)
78) 79) 80) 81)
n-Heptane n-Butanol Trlchloroethene 1,2-Dichloropropane Dlbromomethane 1,4-Dioxane
n-Propyl Acetate Bromodichloromethane
2-Nitropropane 2-Chloroethyl Vinyl Ether cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane
Bromoform trans-1,4-Dichloro-2-Butene
*Chlorobenzene-d5 4-Methyl-2-Pentanone Toluene-d8 Toluene Ethyl Methacrylate Tetrachloroethene
2-Hexanone 1,2-Dibromoethane
chlorobenzene 1,1,1,2-Tetrachloroethane
Ethylbenzene m+p-Xylene Isoamyl Acetate o-Xylene Styrene Cumene Cyclohexanone 4-Bromofluorbenzene 1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane 2-Chlorotoluene
Pentachloroethane. 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl Chloride
R.T. Q ion
10.93 71.0 11.40 56.0 11.49 130.0 11.81 63.0 11.99 93.0 12.01 88.0 12.06 43.0 12.23 83.0 12.53 41.0 12.65 63.0 12.87 75.0 13.66 75.0 13.93 97.0 14.53 129.0 16.60 173.0 17.35 53.0 15.37 117.0 13.08 43.0 13.27 98.0 13.36 91.0 13.79 69.0 14.18 164.0
14.28 43.0
14.69 107.0
15.41 112.0 15.52 131.0 15.55 106.0
15.73 106.0 15.81 70.0 16.31 106.0 16.32 104.0 16.85 105.0 16.98 55.0 17.03 95.0 17.27 83.0 17.34 110.0 17.60 126.0 18.24 167.0 18.71 146.0 18.84 146.0
19.03 91.0
Area
Cone
Units
14204
5720 35191 31762 26251
3039 41763 59359 14655 15830 47226 41828 28900 60837
55067 25982 181413 23490 80133 72475 30180 35400
15134 44210
66605
29903 25387
64381 26865 31233 56631 77503 10121 65244 46622 10835 23137 26984 56635 65291
52205
15.51 ug/L 3 53 X4 ug/L
20.87 ug/L 20.17 ug/L 15.87 ug/L 308.46 ug/L 23.94 ug/L
18.89 ug/L 44.45 ug/L 18.77 ug/L 21.60 ug/L 22.42 ug/L
20.24 ug/L 19.83 ug/L 19.18 ug/L . 337E-37 ug/L 50.00 ug/L 21.64 ug/L 20.63 uq/L 20.62 ug/L 17.60 ug/L 20.01 ug/L
21.09 ug/L
17.02 ug/L
20.08 ug/L
12.13 ug/L 20.47 ug/L
43.46 ug/L 20.59 ug/L 21.08 ug/L 19.39 ug/L 16.64 ug/L 332.36 ug/L 20.91 ug/L 23.12 ug/L 17.31 ug/L
18.01 ug/L 11.91 ug/L 14.00 ug/L
14.79 ug/L
18.64 ug/L
q
79 98 92 78 85 68 94 94 97 90 89 93 96 98 96 86 89 90 97 99 71 90
99 90
91
88
95 97 93 94 89 96 87 91 93 61 97 80 97
96 92
110
DUP050308087
Operator ID: SAM-983 Output File: AGSMI2::FM
Data File: >GSMI2::D5
Name: VSTD020 020 ppb IC Misc: -SAM %C @WL -1 +DCE05Y-W
QUANT REPORT
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Page 3
960924 03:07 960924 02:12
1.00000 HP03460
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Compound
82) 1,2-Dichlorobenzene 83) 1,2-Dibromo-3-Chloropropane
* Compound is ISTD
R.T. Q ion
19.41 146.0 20.62 157.0
Area
57283 10755
Cone
Units
15.04 ug/L 19.78 ug/L
q
91 92
A fttt 1,, .1 ,
111
DUP050308088
Data Files >GSMI3::D5
.. Quant Output Files AGSMI3s:FM
Names VSTD050 050 ppb IC
Instrument ID: HP03460
Misc: -SAM %C @WL =1 +DCE05Y-W
Id File: IA4390::DB
Titles 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Operator ID: SAM-983 Quant Time : 960924 03:11 Injected at: 960924 02:44
1 t-J
DUP050308089
QUANT REPORT
Page 1
Operator ID: SAM-983 output File: -GSMI3::FM
Data File: >GSMI3::D5
Name: VSTD050 050 ppb'IC Misc: -SAM %C @WL =1 +DCE05Y-W
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960924 03:11 960924 02:44
1.00000 HP03460
ID File: IA4390::DB
Title: 3/90 Mater/Med Soil ID File for Inst HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Compound
1) 2)
3)
4) 5} 6) 7) 8) 9)
10)
11} 12) 13)
14) 15)
16) 17) 18) 19) 20) 21) 22) 23) 24)
25)
26)
27)
28)
29) 30)
31) 32) 33) 34) 35) 36)
37)
38) 39) 40)
*Bromochloromethane Dichlorodifluoromethane
Chloromethane
Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane
Furfuran Ethyl Ether Acrolein 1,l-Dichloroethene
Freon 113 Acetone
Methyl Iodide Carbon Disulfide Allyl Chloride Methylene Chloride t-Butyl Alcohol Acrylonitrile Methyl t-Butyl Ether trans-1,2-Dichloroethene
n-Hexane 1,1-Dichloroethane
1-Propanol cis-1,2-Dichloroethene
2-Butanone
Propionitrile Ethyl Acetate Methacrylonitrile Tetrahydrofuran Chloroform Cyclohexane 1,2-Dichloroethane-d4 1,2-Dichloroethane *1,4-Difluorobenzene Vinyl Acetate l,l,l-Trichloroethane Carbon Tetrachloride Isobutyl Alcohol Benzene
R.T. Q ion
9.51 128.0 3.08 85.0 3.32 50.0
3.57 62.0 4.10 94.0 4.30 64.0 4.85 101.0 5.52 68.0 5.46 59.0 5.71 56.0 5.91 96.0 5.98 101.0 6.03 43.0 6.17 142.0 6.30 76.0 6.63 41.0 6.86 84.0 7.17 59.0 7.32 53.0 7.41 73.0 7.39 96.0 7.90 57.0 8.15 63.0 8.41 59.0 9.13 96.0
9.15 43.0 9.23 54.0 9.27 43.0 9.48 67.0 9.59 42.0 9.65 83.0 10.04 56.0 10.41 65.0 10.54 62.0 11.10 114.0 8.25 86.0 9.93 97.0 10.20 117.0 10.41 41.0. 10.51 78.0
Area
Cone
Units
59428
50.00 ug/L
130520
44.20 ug/L
65049
43.89 ug/L
64809
43.52 ug/L
44863
46.21 ug/L
35257
43.06 ug/L
72182
34.64 ug/L
70070
45.97 ug/L
41415
50.65 ug/L
35166 198.76 ug/L
54338
47.75 ug/L
215468
70.18 ug/L
14747
48.36 ug/L
213591
33.86 ug/L
152367
40.57 ug/L
93332
55.24 ug/L
71932
50.78 ug/L
19336 .956E-37 ug/L
54084 216.40 ug/L
133186
49.08 ug/L
64345
47.46 ug/L
66367
49.47 ug/L
127274
46.50 ug/L
2420 741.19 ug/L
69283
51.10 ug/L
17844
43.28 ug/L
19479 .963E-37 ug/L
59199
56.23 ug/L
35022 .173E-36 ug/L
11475
52.67 ug/L
147690
47.36 ug/L
83268
49.73 ug/L
88787
47.32 ug/L
95905
48.23 ug/L
237050
50.00 ug/L
10921
47.24 ug/L
106122
49.70 ug/L
110632
48 11 ug/L
17447 840.18 ug/L
166155
52.19 ug/L
5
72 95 98 96 92 93 97 80 77 94 96 95 98 68 100 87 95 98 96 97 93 91 96 100 96
89 94 97 83 82 97 94 98 89 92 92 87 98 85 92
ns
DUP050308090
QUANT REPORT
Page 2
Operator ID: SAM-983 Output File: AGSMI3::FM
Data File: >GSMI3::D5
Name: VSTD050 050 ppb IC ' Misc: -SAM %C 0WL=1 +DCE05Y-W
Quant Rev
7 Quant Time: Injected at:
Dilution Factor: Instrument ID:
960924 03:11 960924 02:44
1.00000 HP03460
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Compound
41) 42) 43) 44)
45) 46) 47) 48) 49) 50) 51} 52)
53) 54)
55) 56)
57) 58) 59) 60) 61) 62) 63)
64)
65) 66) 67)
68) 69) 70) 71) 72) 73) 74)
75) 76)
77)
78) 79)
80) 81)
n-Heptane
n-Butanol Trichloroethene 1,2-Dichloropropane
Dlbromomethane 1,4-Dioxane
n-Propyl Acetate Bromodichloromethane 2-Nitropropane 2-Chloroethy1 Vinyl Ether cis-1,3-Dichloropropene
trans-l,3-Dichloropropene
1,1,2-Trichloroethane Dibromochloromethane
Bromoform trans-1,4-Dichloro-2-Butene
*Chlorobenzene-d5 4-Methyl-2-Pentanone Toluene-d8 Toluene Ethyl Methacrylate Tetrachloroethene
2-Hexanone 1,2-Dibromoethane
Chlorobenzene 1,1,1,2-Tetrachloroethane Ethylbenzene m-f-p-Xylene Isoamyl Acetate o-Xylene Styrene Cumene Cyclohexanone 4-Bromofluorobenzene 1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
2-Chlorotoluene Pentachloroethane 1,3-Dichlorobenzene
1,4-Dichlorobenzene Benzyl Chloride
R.T. Q ion
10.93 71.0 11.41 56.0 li.50 130.0 11.82 63.0 12.00 93.0 12.02 88.0 12.08 43.0 12.23 83.0 12.53 41.0 12.65 63.0 12.87 75.0 13.67 75.0
13.94 97.0 14.52 129.0 16.61 173.0 17.36 53.0 15.37 117.0 13.08 43.0 13.27 98.0 13.36 91.0 13.80 69.0 14.17 164.0 14.29 43.0 14.70 107.0 15.42 112.0 15.52 131.0 15.56 106.0 15.73 106.0 15.82 70.0 16.32 106.0 16.33 104.0 16.86 105.0 16.98 55.0 17.08 95.0 17.28 83.0 17.35 110.0 17.61 126.0 18.25 167.0 18.72 146.0 18.85 146.0 19.03 91.0
Area
Cone
Units
47761 14619
90007 78403 65242
7061
101420 154465
30911 40674 121185 107426 72261 157229
143542 61643
189164 55945
200295 184698
76031 96665
38037 108514
168208 76642 66308
173276 65310 82119
150679 216358
22630
161949 113203
25857
63415 70764 159001 175048 126470
49.77 ug/L
861.41 ug/L 50.96 ug/L
47.52 ug/L
37.64 ug/L 684.03 ug/L
55.50 ug/L 46.91 ug/L 89.48 ug/L 46.04 ug/L 52.89 ug/L
54.96 ug/L
48.30 ug/L 48.91 ug/L 47.71 ug/L . 764E-37 ug/L
50.00 ug/L 49.42 ug/L 49.45 ug/L 50.39 ug/L 42.51 ug/L 52.39 ug/L
50.84 ug/L
40.07 ug/L
48.64 ug/L 29.83 ug/L 51.27 ug/L 112.17 ug/L 48.00 ug/L 53.16 ug/L 49.48 ug/L 44.55 ug/L 712.70 ug/L 49.77 ug/L
53.84 ug/L 39.62 ug/L 47.34 ug/L 29.95 ug/L 37.70 ug/L 38.04 ug/L 43.31 ug/L
g
82 98 93 80 85 75 95 95 98 90 88 93 94 95 98 87 92 90 97 92 72 88
96 93
95 91 98 93 89 93 90 94 93 92 93 61 99 81 95 95 93
114
DUP050308091
Operator ID: SAM-983 Output File: ~GSMI3::FM Data File: >GSMI3::D5 Name: VSTDOSO 050 ppb IC Misc: -SAM %C @WL =1 +DCEOSY-W
QUANT REPORT
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Page 3
960924 03:11 960924 02:44
1.00000 HP03460
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01*40
Compound
82) 1,2-Dichlorobenzene 83) 1,2-Dibromo-3-Chloropropane
* Compound is ISTD
R.T. Q ion
19.41 146.0 20.62 157.0
Area
150309 23367
cone
Units
37.86 ug/L 41.22 ug/L
q
g" si
115
DUP050308092
TOTAL ION CHROMATOGRAM
Data File: >GSMI4::D5
Quant Output File: AGSMI4::FM
Name: VSTD10Q 100 ppb IC
Instrument ID: HP03460
Misc: -SAM %C @WL =1 +DCE05Y-W
Id File: IA4390::DB
Title: 3^90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Operator ID: SAM-983 Quant Time : 960924 03:44 Injected at: 960924 03:17
A - v ,,g
116
DUP050308093
Operator ID: SAM-983 Output File: `"'GSMI4:: FM
Data File: >GSMI4::D5. Name: VSTD100 100 ppb IC . Misc: -SAM %C WL 1 +DCEQ5V-W
QUANT REPORT
Quant Rev: 7
Quant Tine
Injected at
Dilution Factor
Instrument ID
Page 1
960924 03:44 960924 03:17
1.00000 HP03460 .
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time 960924 01:40
Compound
1) 2)
*Broraochloromethane Dichlorodifluoromethane
3) Chloromethane 4} Vinyl Chloride 5) Broxnomethane
6) Chloroethane 7} Trichlorofluoromethane
8} Furfuran
9) Ethyl Ether
101 Acrolein
11) 1,l-Dichloroethene 12) Freon 113
13) Acetone
14) Methyl iodide
15) Carbon Disulfide
16) Allyl Chloride
17) Methylene Chloride
18) t-Butyl Alcohol
19) Acrylonitrile
20) Methyl t-Butyl Ether
21) trans-l,2-Dichloroethene
22) n-Hexane
23) 1,l-Dichloroethane
24) l-Propanol
25) cis-1,2-Dichloroethene
26) 2-Butanone
27) Propionitrile
28) Ethyl Acetate
29) Methacrylonitrile
30) Tetrahydrofuran
31) Chloroform
32) Cyclohexane
33) 1,2-Dichloroethane-d4
34) 1,2-Dichloroethane
35) *1,4-Difluorobenzene
36) Vinyl Acetate
37) 1,1,l-Trichloroethane
38) Carbon Tetrachloride
39) Isobutyl Alcohol
40) Benzene
R.T. Q ion
9.50 123.0 3.07 85.0 3.33 50.0 3.59 62.0 4.10 94.0 4.30 64.0 4.83 101.0 5.52 68.0 5.46 59.0 5.70 56.0 5.90 96.0 5.97 101.0 6.02 43.0 6.18 142.0 6.31 76.0 6.63 41.0 6.87 84.0 7.18 59.0 7.32 53.0 7.41 73.0 7.39 96.0 7.90 57.0 8.14 63.0 8.41 59.0
9.13 96.0 9.15 43.0 9.22 54.0 9.27 43.0 9.48 67.0 9.59 42.0 9.66 83.0 10.03 56.0 10.41 65.0 10.53 62.0 11.09 114.0 8.26 86.0 9.92 97.0 10.19 117.0 10.41 41.0 10.52 78.0
Area
Cone
Units
60383 268177 124772 125423
85865 67410 151881
147079 86525 79941
105786 439989
30581 432186 314806 203927 134343
40109 117073 286435 127714 140364
249788 5048
139380 36401 41835
127448 77088 26542
288086 174365 177477 188644 240039
23355 216382 218497
34885 330285
50.00 ug/L 89.37 ug/L 82.85 ug/L 82.89 ug/L
87.04 ug/L
81.02 ug/L
71.73 ug/L
94.96 ug/L 104.15 ug/L 444.68 ug/L
91.49 ug/L 141.04 ug/L
98.69 ug/L 67.44 ug/L 82.50 ug/L 118.78 ug/L 93.34 ug/L .195E-36 ug/L 461.03 ug/L 103.88 ug/L 92.71 ug/L
102.97 ug/L
89.81 ug/L
1521.63 ug/L
101.18 ug/L 86.89 ug/L
.204E-36 ug/L 119.15 ug/L
.375E-36 ug/L 119.89 ug/L 90.92 ug/L 102.49 ug/L 93.08 ug/L 93.36 ug/L
50.00 ug/L 99.77 ug/L 100.08 ug/L 93.84 ug/L 1659.01 ug/L
102.46 ug/L
g
77 98 97 98 96 94
99 81 78 93 93 94 97 71 100 86 93 93 94 92 92 93 96
100 96 90 90 98 82 86 95 96 97 86 93 92 92 97 89 92
117
DU P050308094
QUANT REPORT
Page 2
Operator ID: SAM-983 Output File: ~GSMI4::FM
Data File: >GSMI4::D5` Name: VSTD100 100 PPb 1C ' Misc: -SAM %C 0WL *1 +DCE05Y-W
Quant Rev
7 Quant Time:
Injected at:
Dilution Factor: Instrument ID:
960924 03:44
960924 03:17 1.00000
HP03460
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst HPQ3460
Last calibration: 9S1207 01:59
Last Qcal Time: 960924 01:40
Compound
41) 42) 43) 44)
45) 46) 47) 48)
49)
50) 51)
52) 53) 54)
55) 56) 57) 58)
59) 60)
61) 6 2)
63) 64)
65) 66)
67) 68) 69}
70} 71} 72) 7 3} 74) 75) 76)
77) 78) 79) 80)
81)
n-Heptane n-Butanol Tr i chi oroetitiene 1,2-Dichloropropane
Dibromomethane 1,4-Dioxane n-Propyl Acetate Bromodichloromethane
2-Nitropropane
2-Chloroethyl Vinyl Ether cis-l,3-Dicnloropropene
trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane
Bromoform trans-1,4-D:tchloro-2 -Butene *Chlorobenzene-d5 4-Methyl-2-Pentanone
Toluene-d8 Toluene
Ethyl Methacrylate Tetrachloroethene
2-Hexanone 1,2-Dibromoethane
Chlorobenzene 1,1,1,2-Tetrachloroethane
EthyIbenzene m+p-Xylene Isoamyl Acetate
o-Xylene Styrene Cumene Cyclohexanone 4-Bromofluorobenzene 1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane
2-Chlorotoluene Pentachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene
Benzyl Chloride
R.T. Q ion
10.94 71.0 11.41 56.0 11.50 130.0 11.82 63.0 11.99 93.0 12.01 88.0 12.08 43.0 12.23 83.0 12.54 41.0 12.66 63.0 12.88 75.0 13.67 75.0 13.94 97.0 14.53 129.0 16.61 173.0 17.36 53.0 15.37 117.0 13.09 43.0 13.26 98.0 13.37 91.0
13.79 69.0 14.18 164.0
14.28 43.0 14.69 107.0 15.42 112.0 15.52 131.0 15.56 106.0 15.73 106.0 15.81 70.0 16.32 106.0 16.33 104.0 16.85 105.0 16.98 55.0 17.09 95.0 17.28 83.0 17.35 110.0 17.61 126.0 18.24 167.0 18.71 146.0 18 *84 146.0 19.04 91.0
Area
cone
Units
96641
99.45 ug/L
27621 1607.26 ug/L
182138 101.83 ug/L
153214
91.70 ug/L
159973
91.14 ug/L
13393M 1281.28 ug/L
212118 114.62 ug/L
307588
92.25 ug/L
77616 221.87 ug/L
86194
96.34 ug/L
247458 106.66 ug/L
223868 113.11 ug/L
143552
94.76 ug/L
310000
95.22 ug/L
284510
93.39 ug/L
124560 .. 152E-36 ug/L
183503
50.00 ug/L
122944 111.95 ug/L
407233 103.64 ug/L
382877 107.68 ug/L
180533 104.06 ug/L
193616 108.18 ug/L
81470 112.26 ug/L
230941
87.92 ug/L
324152
96.62 ug/L
194712
78.11 ug/L
128089 102.09 ug/L
327748 218.71 ug/L
134870 102.18 ug/L
160135 106.86 ug/L
292954
99.17 ug/L
451656
95.87 ug/L
46470 1508.65 ug/L
320456 101.52 ug/L
227858 111.71 ug/L
53128
83.92 ug/L
130884 100.73 ug/L
177941
77.62 ug/L
331810
81.10 ug/L
363384
81.40 ug/L
267298
94.36 ug/L
g
80 98 92
81 88 96 92 97 95 88 89 94 93 94 97 89 91 91 98 99 78 88
97 93 90 92 98 95 89 93 93 96 94 90 92 58
99 84 95 96
93
118
DU P 050308095
QUANT REPORT
Page 3
Operator ID: SAM-983 Output File: AGSMI4::FM
Data File: >GSMI4::D5 Name: VSTD100 100 ppb IC
Misc: -SAM %C @WL =1 +DCE05Y
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960924 03:44 960924 03:17
1.00000 HP03460
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Compound
82) 1,2-Dichlorobenzene 83) l,2-Dibrorno-3-Chloropropane
* Compound is ISTD
R.T. Q ion
19.40 146.0 20.62 157.0
Area
319295 4983B
Cone
Units
82.90 ug/L 90.62 ug/L
g
96 84
DUP050308096
Data File: >GSM14 Name: VSTD100 100 ppb IC
Misc: -SAM %C @WL =1 +DCE05Y-W Quant Time: 960924 03:44 Injected at: 960924 03:17
Compound No: 46
Compound Name: 1,4-Dioxane
Scan Number: 858
Retention Times 12.01 min
Quant Ion: 88.0
Area:
13393M
Concentration:
1281.28 ug/L
g-value: 96
Quant Output File: ''GSMI4 Instrument ID: HP03460
Qusnt ID File: IA4390 ' Last Calibration: 951207 01:59
This report was produced by QAREA at: 4:47 AM TUE., 24 SEPT, 1996
120
DUP0 50308097
TOTAL ION CHROMATOGRAM
Data File: >GSMI5::D5
Quant Output File: AGSMI5::FM
Name: VSTD200 200 ppb IC
Instrument ID: HP03460
MlSC: -SAM %CI @WL =1 +DCE05Y-W
Id File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Operator ID: SAM-983 Quant Time : 960924 04:16 Injected at: 960924 03:49
121
DUP050308098
QUANT REPORT
Page l
Operator ID: SAM-983 Output File: "'GSMIS: :FM
Data File: >GSMX5::D5 Name: VSTD200 200 ppblCMisc: -SAM %C @WL =1 +DCEOSY-W
Quant Rev
7 Quant Time: Injected at:
Dilution Factor: Instrument ID:
960924 04:16 960924 03:49
1.00000 HP03460
ID File: IA4390::DB
Title: 3/90 Water/Med Soil ID File for Inst HF03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Compound
1 *Bromochloromethane 2 Dichlorodifluoromethane 3 Chloromethane 4 Vinyl Chloride 5 Bromomethane 6 Chloroethane 7 Trichlorofluoromethane 8 Furfuran 9 Ethyl Ether io; Acrolein 11 1.l-Dichloroethene 12 Freon 113 13 Acetone 14 Methyl Iodide 15, carbon Disulfide 16 Allyl Chloride 17, Methylene Chloride is; t-Butyl Alcohol 19] Acrylonitrile 20] Methyl t-Butyl Ether 21 trans-l,2-Dichloroethene 22] n-Hexane 23 1,l-Dichloroethane 24] 1-Propanol 25] cis-1,2-Dichloroethene 26] 2-Butanone 27] Propionitrile 28] Ethyl Acetate 29] MethacryIonitrile 30] Tetrahydrofuran 31) Chloroform 32) Cyclohexane 33] 1,2-Dichloroethane-d4 34) 1,2-Dichloroethane 35) *1,4-Difluorofoenzene
36) Vinyl Acetate 37) lf1,l-Trichloroethane 38) carbon Tetrachloride 39) Isobutyl Alcohol 40) Benzene
R.T. Q ion
9.50 128.0 3.08 85.0 3.34 50.0 3.58 62.0 4.10 94.0 4.28 64.0 4.84 101.0 5.53 68.0 5.46 59.0 5.70 56.0 5.89 96.0 5.96 101.0 6.03 43.0 6.18 142.0 6.32 76.0 6.62 41.0 6.86 84.0 7.20 59.0 7.32 53.0 7.41 73.0 7.38 96.0 7.89 57.0 8.14 63.0 8.43 59.0 9.13 96.0 9.15 43.0 9.22 54.0 9.27 43.0 9.48 67.0 9.60 42.0 9.64 83.0 10.03 56.0 10.41 65.0 10.53 62.0 11.09 114.0 8.25 86.0 9.92 97.0 10.19 117.0 10.41 41.0 10.51 78.0
Area
Cone
Units
57852 513973
245542
250682
153149 89513
272249
285271 169891 165366 204786
798368 58672
847690 621367 407545
266336 85918
243622 556879
247474 250446
492976
10310
282002
75329 87904 272820
156959 54100
554524 331139 347154 355078
233932 48334
415759 416626
69979 640812
50.00 ug/L 178.78 ug/L 170.17 ug/L 172.93 ug/L 162.03 ug/L
112.29 ug/L 134.21 ug/L 192.23 ug/L 213.44 ug/L 960.12 ug/L 184.86 ugVL 267.12 .ug/L 197.63 ug/L. 138.06 ug/L 169.96 Ug/L 247.77 ug/L 193.13 ug/L .436E-36 ug/L 1001.35 ug/L 210.80 ug/L
187.50 ug/L 191.76 ug/L 185.01 ug/L 3243.74 ug/L
213.66 ug/L
187.68 ug/L .447E-36 ug/L
26-6.22 ug/L .797E-36 ug/L
255.07 ug/L 182.66 ug/L 203.15 ug/L 190.04 ug/L 183.42 ug/L
50.00 ug/L 211.88 ug/L
197.31 ug/L 183.61 ug/L 3414.84 ug/L 203.98 ug/L
q
70 97 98 99 98 94 96 78 75 95 97 96 93 64 100 82 94 94 96 92 93 90 96 100 96 87
91 99 79 88 98 90 97 85 95 91
92 96 88 93
ioo
DUP050308099
QUANT REPORT
Page 2
Operator ID: SAM-983 Output File: AGSMI5::FM
Data File: >GSMI5::D5Name: VSTD200 200 ppb IC Misc: -SAM %C @WL=1 +DCE05Y-W
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960924 04:16 960924 03:49
1.00000 HP03460
ID File:.IA4390::DB
^,
Title: 3>90 Water/Med Soil ID File for Inst HP03460
Last Calibration: 951207 01:59
Last Qcal Time
960924 01:40
Compound
41 n-Heptane 42 n--Butanol 43 Trichloroethene 44 1,2-Dichloropropane 45 Dibromomethane 46 1,4-Dioxane 47 n-Propyl Acetate 48] Bromodichloromethane 49, 2-Nitropropane 50] 2-Chloroethyl Vinyl Ether 51 cis-1,3-Dichloropropene 52 trans-l,3-Dichloropropene 53 1,1,2-Trichloroethane 54] Dibromochloromethane 55] Bromoform 56] trans-l,4-Dichloro-2-Butene 57] *Chlorobenzene-d5 58] 4-Methy1-2-Pentanone 59, Toluene-d8 60] Toluene 61] Ethyl Methacrylate 62] Tetrachloroethene 63] 2-Hexanone 64 1,2-Dibromoethane 65] Chlorobenzene 66] 1,1,1,2-Tetrachloroethane 67] Ethylbenzene 68] m+p-Xylene 69] Isoamyl Acetate 70] o-Xylene 71) Styrene 72) Cumene 73 Cyclohexanone 74) 4-Bromofluorobenzene 75) 1,1,2,2-Tetrachloroethane 76) 1,2,3-Trichloropropane
77 2-Chlorotoluene 78) Pentachloroethane 79) 1,3-Dichlorobenzene 80) 1,4-Dichlorobenzene 81) Benzyl Chloride
R.T. Q ion
10.93 71.0 11.41 56.0 11.50 130.0 11.82 63.0 11.99 93.0 12.02 88.0 12.07 43.0 12.24 83.0 12.53 41.0 12.65 63.0 12.87 75.0 13.67 75.0 13.93 97.0 14.52 129.0 16.61 173.0 17.35 53.0 15.36 117.0 13.08 43.0 13.27 98.0 13.36 91.0 13.79 69.0 14.17 164.0 14.29 43.0 14.68 107.0
15.41 112.0 15.51 131.0 15.56 106.0 15.73 106.0 15.82 70.0 16.31 106.0 16.33 104.0 16.85 105.0 16.99 55.0 17.08 95.0 17.27 83.0 17.34 110.0
17.60 126.0 18.23 167.0 18.70 146.0 18.84 146.0 19.03 91.0
Area
Cone
Units
165593 59373
349386
302209 291358
25833 435294 583534 158439 178885 476251 425486 274964 587790 567345 234387 172695 249995 771123 742685 353699 347155 173610 456010
622593 350002 233777 575648
268601 281804 522081 826826
92886 564555 449931
98801
241181 334267 619886 677213 518907
174.86 ug/L 3545.10 ug/L
200.43 ug/L
185.60 ug/L
170.33 ug/i*
2535.90 ug/L 241.36 ug/L 179.59 ug/L 464.74 ug/L 205.16 ug/L 210.64 ug/L 220.60 ug/L 186.24 ug/L 185.27 ug/L 191.10 ug/L
.294E-36 ug/L 50.00 ug/L
241.89 ug/L 208.53 ug/L 221.93 ug/L 216.63 ug/L 206.10 ug/L
254.19 ug/L
184.47 ug/L
197.19 ug/L 149.20 ug/L
197.99 ug/L 408.18 ug/L 216.24 ug/L 199.82 ug/L 187.80 ug/L 186.49 ug/L 3204.28 ug/L 190.05 ug/L
234.39 ug/L 165.83 ug/L
197.23 ug/L 154.95 Jig/L
160.99 ug/L 161.20 ug/L 194.64 ug/L
q
79 98 92 81 84 78 93 96 96 87 90 94 95 98 95 87 92 90 93 96 69 89
96
91 94 95
98 87 86 95 90 99 93 79 94 63
99 S3 97 96 90
DUP050308100
QUANT REPORT
Page 3
Operator ID: SAM-983
Output File: '`GSMI5:: FM
-
Data File: >GSMI5::D5
Name: VSTD200 200 ppb IC
Misc: -SAM %C @WL =1 +DCE05Y-W
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960924 04:16 960924 03:49
1.00000 HP03460
ID File: IA4390::DR
Title: 3/90 Water/Med Soil ID File for Inst. HP03460
Last Calibration: 951207 01:59
Last Qcal Time: 960924 01:40
Compound
82) 1,2-Dichlorobenzene 83) l,2-Dibromo-3-Chloropropane
* Compound is ISTD
R.T. Q ion
19.39 146.0 20.61 157.0
Area
616392 103383
Cone
Units
170.05 ug/L 199.74 ug/L
q
97 80
1-24 DUP0503081 01
6A VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: LANCASTER LABS -
contract: ______ .
Lab Code: LANCAS
Case No.: ______ . SAS No. _______. SDG No.: _______
Instrument ID: HP03046
Calibration Da'te(s) : 03/20/96
08/20/96
Heated Purge: (Y/N) N
Calibration Times: 2025
2246
GC Column: DB624
LAB FILE.ID:
:
RRF 50= >IGKI3
ID: 0.53 (mm)
RRF 10= >IGKI1 RRF100- >IGKI4
RRF 20= >I<3KI2 RRF200= >ICJKI5
COMPOUND
RRF 10 RRF 20 RRF 50 RRF100 RRF200 ESF RSD
sss ssssssssssss
=======SSSSSSESSSSS
ssasassessas ssssasasssss
Diehlorodifluororaethane
Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane
3.008
1.230
1.236 1* 1.315
.784 .907
2.790
1.143 1.167
1.236 .727
.852
2.718
1.001
1.134 1.190
.721 .893
2.913 1.132 1.230 1.205
.746 .936
2.762
1.093 1.172 1.010
.687 .877
2.838
1.120 1.188 1.191
.733 .893
4.2 7.4 3.7* 9.4* 4.8 3.5
Ethyl Ether Acrolein 1,l-Dichloroethene
Freon 113 Acetone Methyl Iodide Carbon Disulfide
Allyl Chloride Methylene Chloride
t-Butyl Alcohol Acrylonitrile Methyl t-Butyl Ether 1,2-Dichloroethene (total) 1,l-Dichloroethane
2-Butanone Propionitrile Ethyl Acetate Methacrylonitrile
Tetrahydrofuran Chloroform
Cyclohexane 1,2-Dichloroethane
Vinyl Acetate 1,1,l-Trichloroethane Carbon Tetrachloride Isobutyl Alcohol
Benzene
-.884
.142 1* 1.230
2.767
.4T0 3.163 2.965
1.507 2.141
.115
.245
3.439 1.387 i 2.602
.376 .083 1.417
.325 .254 1 3.137 1.757
* 2.373
.519 * .566
* .421 .007
* .816
.861 .138 1.153 2.342 .360
2.929 2.875 1.435 1.711
.099
.234 3.285
1.313 2.502
.395
.084 1.376
.312 .252 2.986 1.620
2.296
.522 .547 .412 .005
.779
.868 .131 1.150
2.270 .343
2.900 2.949 1.452 1.427
.088 .251
3.260
1.338 2.484
.404 .084 1.320 .326 .278 2.900 1.609
2.257
.556 .526 .398 .006
.748
.873 .148 1.189 2.446 .3743.160 3.365 1.546 1.339
.111 .263
3.257
1.367 2.623
.452
.095 1.440
.355 .315 3.003 1.703
2.299
.583 .552 .420 .008
.791
.836 .152 1.137 2.219
. 3T55 3.032 3.278
1.615 1.340
.114
.275 3.199
1.338 2.597
.449
.101 1.465
.350 .329 2.976 1.643 2.295
.595 .520
.411 . 008
.752
.864 .142 1.172
2.409 .370
3.037 3.086 1.511
1.601 .105
.254
3.288
1.348 2.562
.415 .089 1.403 .334 .286 3.001 1.666
2.304
.555 .542 .412 .007 .777
2.1
6.0
3.2* 9.0
6.8
4.1 7.1 4.8 20.9
11.0 6.3 2.7
2 .1 2 ,5*
8 .1 9 .1 4 ,1 5 ,5 12 .2 2 ,9* 3.7 |
1.8*
6.2 | 3.5* 2.3* 15.2 | 3.6*
1, ...............
A * Compounds with required minimum RRF and maximum %RSD values.
All other compounds in OLM01.S must meet a minimum RRF of 0.010.
page 1 of 3
FORM VI VOA
OLM03.0
rr
DUP050308102
6A VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: LANCASTER LABS
Contract:
Lab code: LANCAS
Case No.:
. iSAS No.
SDG No.:
Instrument ID: HP03046
Calibration Date(s): 08/20/96
08/20/96
Heated Purge: (V/N) N
Calibration Times: 2025
2246
GC column: DB624
ID: 0.53 (mm)
LAB FILE ID: RRF 50= >IGKI3
RRF 10= ">fSKn RRF100= >IGKI4
RRF 2o= >1g KI21 RRF200= >IGKI5
COMPOUND
RRF 10 RRF 20 RRF 50 RRF100 RRF200
Trichloroethene .
1 if .391
1,2-Dichloropropane
.344
Methyl Methacrylate
.226
Dibromomethane
.395
1,4-Dioxane n-Propyl Acetate
.002 .529
B romod1chloromethane
k .682
2-Nitropropane
.096
2-Chloroethyl Vinyl Ether
.206
cis-1,3-Dichloropropene
\e .562
trans-1,3-Dichloropropene * .507
1,1,2-Trichloroethane
* .335
Dibromochloromethane .
* .497
Bromoform
* .303
trans-1,4-Dichloro-2-Butene .131
4-Methy1-2-Pentanone Toluene
.447 1If 1.230
Ethyl Methacrylate Tetrachloroethene
.615 * .417
2-Hexanone
.265
1,2-Dibromoethane Chlorobenzene
.691 if .933
1,1,1,2-Tetrachloroethane
.434
Ethylbenzene
* .392
Xylene (total)
* .478
Isoamyl Acetate Styrene
.448 * .838
Cumene
1.477
1,1,2,2-Tetrachloroethane If .751
1,2,3-Trichloropropane
.196
Pentachloroethane
.321
1,3-Dichlorobenzene
.604
1,4-Dichlorobenzene
.733
.367
.334
.229 .387
.002 .524 . 695 .106 .207
.566 .527
.328 .519 .330
.142 .445 1.197
.627
.399
.278 .689
.892 .489 .380
.467 .457 .823 1.429 .753
. 190 .329 . 618
.730
.351
.329
.224
.374 .001
.508 .696 .108 .207
. 564 .524 .323
.541 .343 .143 .436 1.175
.644 .395
.280 .697
.870 .485 .372
.469 .465 .834 1.400 .736 . 189 .326 .648
.732
.368 .346
.236 .379
.002 .560
.741 .128 .227
.598 . 560
.330 .566 .373 .159 .483 1.266
.701 .413
.328 .734
.934 .499 .391
.474 .508 .896
1.443 .730 .192 .322 .658
.743
.348 .350
.236 .377
.002 .561
.734 .131
. 231 . 592 . 555 .1*26 .557 .373 .155 .487 1.243
.719
.394
.334 .745
.928 .490 .369
.453 .516 .863 1.433 .763 .189 .316 .639
.731
KKF
.3 65 .341 .230 .382 .002 .536 .710 . 114 .216 .576 .535 .328 .536 .344 .146 .460 1.222 .661 .404 .297 .711 .911 .490 .381 .468 .479 .851 1.436 .757 .191 .323 .633 .734
% RSD
4.8 2.6 2.4 2.2 14.5 4.3 3.7 13.3 5.7 3.0 4.2 1.4 5.3 8.7 7.8 5.1 3.0
7.0 2.6 10.7 3.7 3 * 2' 1.2 2.8' 2.0" 6*5 3.41.9 2.1' 1.5
1.6
3.5 .7
* Compounds with required minimum RRF'and' maximum %RSD values. All other compounds in OLMOI.8 must meet a minimum RRF of 0.010.
page 2 of 3
FORM VI VOA
0LM03.0
.26
A
DUP050308103
6A VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: LANCASTER LABS
Lab Code: LANCAS
Case No.:
Contract: . SAS No.
* SDG No . :
Instrument ID: HP03046
Calibration Date(s) : 08/20/96
08/20/96
Heated Purge: (Y/N) N
Calibration Times: 2025
2246
GC Column: DB624
ID: 0.53 (mm)
LAB FILE..ID": RRF 50= >IGKI3
RRF 10= >IGKI1 RRF100= >IGKI4
Hi'F.20= >IGKI2 RRF200= >IGKI5
COMPOUND
RRF 10 RRF 2 0 RRF 50 RRF100 RRF200 HKf
* RSD
1,2-Dichlorobenzene
.604 .618 .614 .583 .562 .596 3.9
1,2-Dichloroethane~d4
Toluene-d8 4-Bromofluorobenzene
2.166 1.204
.843
2.115
1.184 .830
2.128 1.221
861
2.119 1.233
.868
2.140 1.256
.876
2.133 1.220
.855
1.0 2.2 2.2
* Compounds with required minimum RRF andmaximum %RSD values. All other compounds in OLM01.8 must meet a minimum RRF of 0.010.
page 3 of 3
FORM VI VOA
OLM03.0
A .27
DUP050308104
Data File: >XGKX1::D9
Name: VSTD010 010 PPB IC
Wise: -SJL @WL %C +JCEO
=1
Quant Output File: AIGKI1::D7 Instrument ID: HP03046
Id File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Operator ID: SJL-176 Quant Time : 960820 20:50
Injected at: 960820 20:25
128
DUP050308105
QUANT REPORT
Page 1
Operator ID: SJL-176 Output Filei ~IGKI1::D7
Data Files >IGKX1::D9 Name: VSTD010 010 PPB IC Misc: -SJL WL %C +JCEO ' =1
Quant Revs 7
Quant Time
Injected at
Dilution Factor
Instrument ID
960820 20:50 960820 20:25
1.00000 HP03046
ID File: IA6390::DB Title: 3/90 SOW Water/Med
Soil
ID
File
for
Inst.
HP03046
Last Calibration: 951122 10:44
Last Qcal Time 960710 14:27
Compound
1) *Bromochloromethane 2) Dichlorodifluoromethane
3) Chloromethane
4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane
8) Ethyl Ether 9) Acrolein 10) l,l-Dichloroethene
11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene jChloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene
,21) 1,1-Dichloroethane
22) cis-1 2-Dichloroethene 23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,1-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) Methyl Methacrylate
R.T. Q ion
8.29 128.0 2.42 85.0 2.52 50.0 2.72 62.0 3.14 94.0 3.31 64.0 3.67 101.0 4.19 59.0 4.42 56.0 4.59 96.0 4.64 101.0 4.71 43.0 4.87 142.0 5.02 76.0 5.30 41.0 5.56 84.0 5.91 59.0 6.05 53.0 6.11 73.0 6.08 96.0 6.85 63.0 7.89 96.0 7.95 43.0
8.03 54.0 8.09 43.0
8.28 67.0 8.39 42.0 8.45 83.0 8.82 56.0
9.24 65.0 9.37 62.0 .9.96 114.0 7.01 43.0 8.72 97.0 9.00 117.0
9.31 41.0 9.32 78.0 10.36 130.0 10.68 63.0 10.90 69.0
Area
Cone
Units q
39140
23545
9629 9674 10294 6136
7098 6921 5554M 9630 43326 3213 24760
23211 11798M 16758
4502 9587
26921 10700 20371
11015 2947
3243
11095 6361
1991 24558
13754
16954 18577 162514 16863 18389 13680
2732 26513 12721 11168
7356
50.00 UG/L 12.93 UG/L
13.32 UG/L 10.81 UG/L 14.50 UG/L 13.08 UG/L
8.51 UG/L 16.28 UG/L 55.33 UG/L
9.23 UG/L 22.20 UG/L 11.24 UG/L
9.81 UG/L
8.42 UG/L 10.79 UG/L 14.32 UG/L
49.28 UG/L 53.69 UG/L 12.37 UG/L
8.94 UG/L 9.07 UG/L 9.20 UG/L 9.02 UG/L
50.07 UG/L 11.53 UG/L 25.88 UG/L
9.83 UG/L 8.88 UG/L
20.39 UG/L 9.94 UG/L 9.36 UG/L
50.00 UG/L 7.97 UG/L 8.65 UG/L 7.92 UG/L
114.91 UG/L 9.80 UG/L 9.61 UG/L 9.99 UG/L
10.84 UG/L
87 92 95 99 95 95 98 83 99 92 92 75 72 100
97 95 96 90 93 95 96 89 96 97
89 72 97 95 89 90 87 96 89 94 93 90 87 89 38
129
DUP050308106
QUANT REPORT
Page 2
Operator ID: SJL-176
Output File: AIGKI1::D7
Data File: >IGKIl::D9
Name: VSTD010 010 PFB IC
Misc: --SJL @WL %C +>CEO
=1
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
Instrument ID
960820 20:50 960820 20:25
1.00000 HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Ked Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Compound
41) 42) 43)
44) 45) 46} 47}
48) 49) 50)
51) 52) 53) 54) 55) 56) 57)
58 59 60 61] 62]
S3, 64]
65; 66; 67 68 69 70]
7i; 72; 73' 74)
75)
Dibromomethane 1,4-Dioxane
n-Propyl Acetate Bromodlchloroaethane 2-Nitropropane 2-Chloroethyl Vinyl Ether cis-l,3-Dichloropropene trans-l,3-Dichloropropene l,1,2-Trichloroethane Dibromochloromethane
Bromoform trans-l,4-Dichloro-2-Butene
* Chlorobenz ene-d5 4-Methyl-2-Pentanone Toluene-d8 Toluene Ethyl Methacrylate
Tetrachloroethene 2-Hexanone 1,2-Dibromoethane Chlorobenz ene 1,1,1,2-Tetrachloroethane
Ethylbenzene m+p-Xylene
Isoamyl Acetate o-Xylene Styrene Cumene
4-Bromofluorobenzene 1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane Pentachloroethane 1,3-Dichlorobenz ene 1,4-Dichlorobenzene 1,2-Dichlorobenzene
* Compound is ISTD
R.T. Q ion
10.87 93.0 10.92 88.0 11.01 43.0
11.11 83.0 11.45 41.0 11.58 63.0 11.78 75.0 12.59 75.0 12.85 97.0 13.42 129.0 15.51 173.0 16.29 53.0 14.26 117.0 12.01 43.0 12.16 98.0 12.25 91.0 12.73 69.0
13.04 164.0 13.23 43.0 13.58 107.0 14.30 112.0 14.43 131.0 14.47 106.0 14.64 106.0 14.78 70.0 15.22 106.0 15.24 104.0 15.75 105.0 15.99 95.0 16.20 83.0 16.25 110.0 17.14 167.0 17.59 146.0 17.73 146.0 18.28 145.0
Area
12834M 727
17194 22177
6223 6687 18265 17145 10888 16150 9847 10608 119727 10704 28830 29444 14729 9993 6334 16536 22339 11593 9379 24549 10722 11445 20058 35367 20174 17991 4685 7683 14468 17551M 14464
Cone
Units
10.85 UG/L 75.32 UG/L 10.88 UG/L
8.79 UG/L 15.86 UG/L
10.40 UG/L 9.15 UG/L 9.23 UG/L
10.26 UG/L 8.46 UG/L 7.79 UG/L
24.29 UG/L 50.00 UG/L 12.14 UG/L 10.30 UG/L
9.73 UG/L 10.57 UG/L
9.16 UG/L 12.12 UG/L 11.64 UG/L
9.92 UG/L 10.07 UG/L
9.65 UG/L 20.82 UG/L 10.23 UG/L
9.71 UG/L 9.51 UG/L 13.05 UG/L 10.64 UG/L 11.79 UG/L 11.51 UG/L 9.89 UG/L 10.43 UG/L 12.66 UG/L
10.30 UG/L
q
84 99 93 95 83 88 90 96 98 96 91 85 91 95 94 92 98 88 95 82 86 96 96 94 92 86 96 72 96 72 88 86 86 83
130
DUP050308107
Data Pile: >IGKI1
Name: VSTD010 010 PPB IC
Misc: ~SJL ML %C +>CEO
=1
Quant Time: 960320 20:50
Injected at: 960820 20:25
Quant Output File: "IGKI1 Instrument ID: HP03046
Quant ID Pile: IA6390 Last Calibration: 951122 10:44
Compound No: 9
Compound Name: Acrolein
Scan Number: 225
Retention Time: 4.42 min
Quant Ion: 56.0
Area:
5554M
Concentration:
S5.3S TJG/L
q-value: 99
This report was produced by QAREA at: 12:00 AM WED. , 21 AUG., 1996
131
DUP0503081 08
MJr\
Data File: >IGKI1
Name: VSTD010 010 PPB IC
Misc: ~SJL WL %C +JCEO
=1
Quant Time: 960820 20:50
Injected at: 960820 20:25
Compound No: 15
Compound Name: Allyl Chloride
Scan Number: 301
Retention Time: 5.30 min
Quant Ion: 41.0
Area:
il798M
Concentration:
10.79 UG/L
q-value: 0
Quant Output File: ~IGKIl Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
This report was produced by QAREA at: 12:01 AM WED., 21 AUG., 1996
132
DUP050308109
Data File: >IGKI1
Name: VSTD010 010 PPB IC
Misc: -SJL WL %C +>CEO
=1
Quant Time: 960820 20:50
Injected at: 960820 20:25
Compound No: 41
Compound Name: Dibromomethane
Scan Number: 780
Retention Time: 10.87 min
Quant Ion: 93.0
Area:
. 12834M
Concentration:
10.85 UG/L
q-value: 0
Quant Output File: MGKI1 . Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
This report was produced by QAREA at: 12:02 AM WED., 21 AUG., 1996
13
DUP050308110
Data File: >IGKI1
Name: VSTD010 010 PPB IC
Misc: ~SJL WL %C +}CEO
-1
Quant Time: 960820 20:50
Injected at: 960820 20:25
Compound No: 74
Compound Name: 1,4-Dichlprobenzene
Scan Number: 1370
Retention Time: 17.73 min
Quant Ion: 146.0
Area:
17551M
Concentration:
12.6 6 UG/L
q-value: 86
Quant Output File: ~IGKI1 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
This report was produced by QAREA at: 12:02 AM WED., 21 AUG., 1996
134
DUP050308111
TOTAL ION CHROHflTOSRflM
File >ISKIS 35.0-300;0 amu. Vggfflfeg
020 PPB IC~SJL 8L JSC +>CEQ
. - .8?. .-i-
1SQ0
200000-
Data File: >IGKI2::D9
Name: VSTD020 020 PPB IC
Misc: -SJL WL %C +}CEO
*1
Quant Output File: -'IGKI2::D7 Instrument ID: HP03046
Id File: IA6390::DB Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Operator ID: SJL-176 Quant Time : 960820 21:24 Injected at: 960820 20:59
13 r
DUP050308112
QUANT REPORT
Page 1
Operator ID: SJL-176
Output File: AIGKI2::D7
Data File: >IGKI2::D9
Name: VSTD020 020 PPB IC
Misc: -SJL @RL %C +>CEO
=1
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960820 21:24
960820 20:59 1.00000
HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time 960710 14:27
Compound
1) *Bromochloromethane 2) Dichlorodifluoromethane
3) Chloromathane 4) Vinyl Chloride 5} Bromomethane 6) Chlotoethane 7) Trichlorofluoromethane
8) Ethyl Ether 9) Acrolein 10) 1,1-Dichloroethene
11) Freon 113 12) Acetone 13) Methyl Iodide 14) carbon Disulfide 15) Allyl Chloride 16) Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile
19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene 21) l,l-Dichloroethane 22) cis-l,2-Dichloroethene
23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *l,4-Diluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane
40) Methy1 Methacrylate
R.T. Q ion Area
8.28 128.0
2.42 85.0 2.54 50.0
2.74 62.0
3.16 94.0 3.31 64.0 3.68 101.0 4.19 59.0 4.40 56.0
4.61 96.0 4.63 101.0 4.71 43.0 4.86 142.0 5.03 76.0 5.29 41.0 5.56 84.0 5.88 59.0 6.04 53.0 6.11 73.0 6.07 96.0 6.85 63.0 . 7.89 96.0 7.95 43.0
8.04 54.0 8.07 43.0
8.27 67.0 8.39 42.0
8.45 83.0
8.82 56.0
9.24 65.0 9.37 62.0 9.96 114.0 7.00 43.0 8.71 97.0 9.01 117.0 9.32 41.0
9.33 78.0
10.36 130.0 10.68 63.0 10.90 69.0
40292
44973 18428
18807 19916 11715
13739 13379 11153 18575 75483
5804 47207
46336 23129M 27575
7938
18849 52947 20966 40322
21349 6371
6773 22170
12554 4063
48129
26115 34084
37012 165797
34626 36283 27325
4517
51694
24361 22156 15177
Cone
Units
50.00 UG/L
23.99 UG/L 24.77 UG/L 20.41 UG/L 27.25 UG/L 24.25 UG/L
16.00 UG/L 31.72 UG/L 108.02 UG/L 17.29 UG/L 37.57 UG/L 19.72 UG/L 18.17 UG/L
16.32 UG/L 20.54 UG/L 22.90 UG/L
84.40 UG/L 102.53 UG/L
23.63 UG/L 17.02 UG/L
17.43 UG/L 17.33 UG/L 18.94 UG/L
101.58 UG/L 22.38 UG/L
49.62 UG/L 19.48 UG/L
16.91 UG/L 37.60 UG/L 19.41 UG/L 18.11 UG/L 50.00 UG/L 16.03 UG/L 16.73 UG/L 15.50 UG/L 186.22 UG/L 18.73 UG/L
18.04 UG/L 19.43 UG/L 21.92 UG/L
q
85 97 94 97 93 92 98 89 97 88 91 66 74 100
96 94 99 91 96 96 96 93 95 97 89 75 98 97 89 91 87 97 90 96 90 88 86 89 81
136
DUP050308113
QUANT REPORT
Page 2
Operator ID: SJL-176
Output File: AIGKI2::D7
Data File: >IGKI2s:D9
Name: VSTD020 020 PPB IC
Misc: -SJL WL %C +JCEO
=1
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960820 21:24 960820 20:59
1.00000 HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Compound
41) Dibromomethane 42} 1,4-Dioxane 43} n-Propyl Acetate 44) Bromodichloromethane 45) 2-Nitropropane 46) 2-Chloroethyl Vinyl Ether 47) cis-1,3-Dichloropropene 48) trans-1,3-Dichloropropene 49) 1,1,2-Trichloroethane 50) Dibromochloromethane 51) Bromoform 52) trans-l,4-Dichloro-2-Butene 53) *Chlorobenzene-d5 54) 4-Methyl-2-Pentanone 55) Toluene-d8 56) Toluene 57) Ethyl Methacrylate 58) Tefcrachloroethene 59) 2-Hexanone 60) 1,2-Dibromoethane 61) Chlorobenzene 62) 1,1,1,2-Tetrachloroethane 63) Ethylbenzene 64) m+p-Xylene 65) Isoamyl Acetate
66) o-Xylene
67) Styrene 68) Cumene 69) 4-Bromofluorobenzene 70) 1,1,2,2-Tetrachloroethane 71) 1,2,3-Trichloropropane 72} Pentach'loroethane 73) 1,3-Dichlorobenzene 74 1,4-Dichlorobenzene 75) l,2-Dichloroben2ene
* Compound is ISTD
R.T. Q ion
10.87 93.0 10.90 88.0 11.01 43.0 11.11 83.0 11.44 41.0
11.58 63.0 11.77 75.0 12.59 75.0 12.84 97.0 13.41 129.0 15.51 173.0 16.29 53.0 14.26 117.0 12.01 43.0 12.16 98.0 12.25 91.0 12.73 69.0 13.05 164.0 13.23 43.0 13.58 107.0 14.30 112.0 14.43 131.0 14.46 106.0 14.64 106.0
14.76 70.0 15.22 106.0 15.24 104.0 15.75 105.0 15.99 95.0 16.20 83.0 16.25 110.0 17.13 167.0 17.59 146.0 17.72 146.0 13.28 146.0
Area .
25646M 1570
34742 46108 14039 13748 37512 36359 21780 34404 21859 23474 123077 21920 53312 53926 30859 19663 13668 33941 43934
24070 18721 48673
22496 22970 40512 70373 40859 37095
9361 16217 30423 35960M 30448
Cone
Units
21.24 UG/L 159.44 UG/L
21.55 UG/L 17.92 UG/L 35.08 UG/L
20.97 UG/L 18.43 UG/L 19.19 UG/L 20.12 UG/L 17.68 UG/L
16.95 UG/L 52.69 UG/L 50.00 UG/L 24.18 UG/L 20.26 UG/L 18.94 UG/L 21.53 UG/L 17.53 UG/L 25.44 UG/L 23.24 UG/L
18.98 UG/L
20.35 UG/L
18.73 UG/L
40.15 UG/L
20.88 UG/L 18.95 UG/L
18.69 UG/L 25.26 UG/L
20.96 UG/L 23.66 UG/L 22.36 UG/L 20.30 UG/L
21.34 UG/L 25.23 UG/L
21.10 UG/L
q
83 95 97 96
87 86 89 92 99 97 87 85 91 98 96 90 98 98 95 84 89 96 96 94 93 85 96 73 95 67 87
86 86
86
137
DUP050308114
Data Pile: >IGKI2
Name: VSTD020 020 PPB IC
Misc: -SJL @WL %C +JCEO
=1
Quant Time: 960820 21:24
Injected at: 960820 20:59
Compound No: 15
Compound Name: Allyl Chloride
Scan Number: 304
Retention Time: 5.29 min
Quant Ion: 41.0
Area:
23129M
Concentration:
20.54 UG/L
q-value: o
Quant Output File: AIGKI2 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
This report was produced by QAREA at: 12:06 AM WED., 21 AUG., 1996
a O O iOO
DUP050308115
. --^ t/uhl
Data File: >IGKI2
Name: VSTD020 020 PPB 1C
Misc: -SJL @WL %C +}CEO
*1
Quant Time: 960820 21:24
Injected at: 960820 20:59
Compound No: 41
Compound Name: Dibromomethane-
Scan Number: 783
Retention Time: 10.87 min
Quant Ion: 93.0
Area: . 25646K
Concentration:
21.24 UG/L
q-value: o
Quant Output File: ~IGKI2 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
This report was produced by QAREA at: 12:07 AM WED., 21 AUG., 1996
136
DUP050308116
Name: VSTD020 020 PPB IC
Wise: -SJL @WL %C +>CEO
=1
Quant Time: 960820 21:24
Injected at: 960820 20:59
Instrument ID: HPQ3046
Quant ID Pile: IA6390 Last Calibration: 951122 10:44
Compound No: 74
Compound Name: 1,4-Dichlorobenzene
Scan Number: 1372
Retention Time: 17.72 min
Quant Ion: 146.0
Area:
35960M
Concentration:
25.23 UG/L
q-value: 86
This report was produced by QAREA at: 12:08 AM WED., 21 AUG., 1996
DUP050308117
Id File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HF0304S
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Operator ID: SJL-176 Quant Time : 960820 22:06
Injected at: 960820 21:41
141
DUP050308118
QUANT REPORT
Page l
Operator ID: SJL-176 Output File: *IGKI3::D7 Data File: >IGKI3::D9
Name: VSTD050 050 PPB IC Misc: ~SJL WL %C +J-CEO ' "1
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960820 22:06 960820 21:41
1.00000 HP03046
ID File: 1A6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Compound
1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6} Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,1-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene 21) 1,1-Dichloroethane 22) cis-i,2-Dichloroethene 23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32} *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) Carbon Tetrachloride
36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) Methyl Methacrylate
R.T. Q ion
8.30 128.0 2.43 85.0 2.54 50.0 2.74 62.0 3.15 94.0 3.30 64.0 3.67 101.0 4.19 59.0 4.40 56.0
4.61 96.0 4.63 101.0 4.69 43.0 4.87 142.0 5.03 76.0 5.28 41.0 5.57 84.0 5.89 59.0 6.03 53.0
6.12 73.0 6.07 96.0 6.86 63.0 7.89 96.0
7.94 43.0
8.03 54.0 8.09 43.0 8.27 67.0 8.38 42.0 8.46 83.0 8.82 56.0 9.24 65.0 9.37 62.0 9.96 114.0 7.01 43.0 8.73 97.0 9.01 117.0 9.32 41.0 9.33 78.0 10.36 130.0 10.68 63.0 10.91 69.0
Area
41532 112891
41562 47096 49439 29955 37077 36034 27161 47778 1SS528 14228 120428 122468 60310M 59254 18312 52092 135406 55563 103174 55539 16797 17485 54830 33891 11529 120463
66811 88376 93746 173525 96530 91344 69021 13175 129773
60832 57035 38891
Cone
Units
50.00 UG/L
58.41 UG/L 54.20 UG/L 49.60 UG/L 65.63 UG/L 60.17 UG/L
41.89 UG/L
79.89 UG/L 255.21 UG/L
43.14 UG/L 91.02 UG/L
46.91 UG/L 44.97 UG/L 41.86 UG/L 51.97 UG/L 47.73 UG/L 188.89 UG/L 274.91 UG/L 58.63 UG/L 43.75 UG/L
43.28 UG/L
43.73 UG/L
48.45 UG/L 254.40 UG/L
53.69 UG/L
129.97 UG/L 53.62 UG/L 41.06 UG/L 93.33 UG/L 48.82 UG/L 44.49 UG/L 50.00 UG/L 42.71 UG/L 40.25 UG/L 37.41 UG/L
518.97 UG/L 44.93 UG/L 43.05 UG/L 47.80 UG/L 53.66 Uci/JL
<3
83 94 94 96 96 94 95 90 95 92 91 71 72 100
97 93 96 91 95 96 96 91 93 98 88 78 97 96 91 92 88 96 88 96 96 88 S3 88 82
14
DUP050308119
QUANT REPORT
Page 2
Operator ID: SJL-176
output File: *IGKI3::D7
Data File: >IGKI3::D9 .
Name: VSTD050 050 PPB IC
Misc: -SJL WL %C +JCEO
=1
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
Instrument ID
960820 22:06
960820 21:41
1.00000 HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time 960710 14:27
Compound
41) Dibromomathan 42) 1,4-Dioxane 43} n-Propyl Acetate 44) Bromoalchloromethane 45) 2-Nitropropane 46) 2-Chloroethyl Vinyl Ether 47) cis-1,3-Dichloropropene 48} trans-1,3-Dichloropropene 49) 1,1,2-Trichloroethane 50) Dibromochloromethane 51) Bromoform 52) trans-1,4-Dichloro-2-Butene 53) *Chlorobenzene-d5 54) 4-Methyl-2-Pentanone 55) Toluene-d8 56) Toluene 57) Ethyl Methacrylate 58) Tetrachloroethene 59) 2-Hexanone 60) 1,2-Dibromoethane 61) Chlorobenzene 62) 1,l,1,2-Tetrachloroethane 63) Ethylbenzene 64) m+p-Xylene 65) Isoamyl Acetate 66) o-Xylene 67) Styrene 68) Cumene 69) 4-Bromofluorobenzene 70) 1,1,2,2-Tetrachloroethane 71) 1,2,3-Trichloropropane 72) Pentachloroethane 73) l,3-Dichlorobenzene 74 1.4-Dichlorobenzene 75) 1,2-Dichlorobenzene
* Compound is ISTD
R.T. Q ion
10.87 93.0 10.92 88.0 11.01 43.0 11.13 83.0 11,45 41.0 11.59 63.0 11.79 75.0 12.59 75.0 12.86 97.0 13.43 129.0 15.52 173.0 16.30 53.0 14.27 117.0 12.01 43.0 12.17---98-. 0 12.27 91.0 12.74 69.0 13.06 164.0 13.23 43.0 13.58 107.0 14.32 112.0 14.43 131.0
14.48 106.0 14.66 106.0 14.78 70.0 15.24 106.0 15.25 104.0 15.77 105.0 16.00 95.0 16.22 83.0 16.28 110.0 17.15 167.0 17.61 146.0 17.74 146.0 18.29 146.0
Area
Cone
Units
64864M 3193
88195 120817
37353 35926 97877 94524
56066 93875 59543 61967 126822 55285 154866
148958 81697 50150 35542 88444
110317 61551
47174 123452
58957 59522 105823
177575 109132
93391
24007 41391 82195 92865M 77874
51.33 UG/L
309.83 UG/L
52.27 UG/L
44.86 UG/L
89.17 Uta/ Jj
52.35 UG/L
45.94 UG/ L
47.67 UG/L
49.48 UG/L
46.08 UG/L
44.12 UG/L
132.89 UG/L
50.00 UG/L
59.19 UG/L
52.21 UG/L
46.46 UG/L
55.33 UG/L
43.33
l
64.20 UG/L
58.77 UG/L
46.26 UG/L
50.50 UG/L
45.80 UG/L
98.84 U^i/ L
53.10 UG/L
47.65 UG/L
47.38 UG/L
61.86 UG/L
54.34 UG/L
57.80 UG/L
55.66 UG/L
50.29 UG/L
55.96 UG/L
63.22 UG/L
52.37 UG/L
q
74 97 96 96 88 87 90 95 97 98 89 86 89 98 97 96 97 97 94 85 90 95 95 95 93 84 96 74 93 65 84 86 86 85
14
DUP050308120
Data File: >IGKI3
Name: VSTD050 050 PPB IC
Misc: ~SJL @WL %C +>CEO
=1
Quant Time: 960820 22:06
Injected at: 960820 21:41
Compound No: 15
Compound Name: Allyl Chloride
Scan Number: 296
Retention Time: 5.28 min
Quant Ion: 41.0
Area:
60310M
Concentration:
51.97 UG/L
q-value: 0
Quant Output File: -IGKI3 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
This report was produced by QAREA at: 12:13 AM WED., 21 AUG., 1996
144
DUP050308121
Data File: >IGKI3
Name: VSTD050 050 FFB IC
Misc: -SJL @WL %C +>CEO
=1
Quant Time: 960S20 22:06
Injected at: 960820 21:41
Quant output File: ~IGKI3 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
Compound No: 41
Compound Name: Dibromomethane
Scan Number: 773
Retention Time: 10.87 min
Quant Ion: 93.0
Area:
64864M
Concentration:
51.33 UG/L
q-value: 0
This report was produced by QAREA at: 12:14 AM WED., 21 AUG., 1996
145
DUP050308122
Data File: >IGKI3
Name: VSTD050 050 PPB IC
Misc: -SJL WL %C +}CEO
=1
Quant Time: 960820 22:06
Injected at: 960820 21:41
Compound No: 74
Compound Name: 1,4-Dichlorobenzene
Scan Number: 1363
Retention Time: 17.74 min
Quant Ion:.146.0
Area:
92865M
Concentration:
63.22 UG/L
q-value: 86
Quant Output File: ~IGKI3 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
This report was produced by QAREA at: 12:15 AM WED., 21 AUG., 1996
i46
DUP050308123
Data Pile: >IGKI4::D9
Name: VSTD100 100 PPB IC
Misc: ~SJL @WL %C +JCEO
1
Quant Output File: *'IGKI4::D7 Instrument ID: KP03Q46
Id File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Operator ID: SJL-176 Quant Time : 960820 22:40
Injected at: 960820 22:15
147
DUP050308124
QUANT REPORT
Page l
Operator ID: SJL-176
Output Pile: *IGKI4::D7
Data Pile: >IGKI4::D9
Name: VSTD100 100 PPB IC
Misc: -SJL eWL %C +JCEO
=1
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
Instrument ID
960820 22:40
960820 22:15 1 00000
HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Compound
1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,1-Dichloroethene ID Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl chloride 16) Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile
19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene
21) 1,l-Dichloroethane
22) cis-1,2-Dichloroethene 23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) Methyl Methacrylate
R.T. Q ion
8.29 128.0 2.42 85.0 2.57 50.0 2.75 62.0 3.15 94.0 3.31 64.0 3.69 101.0 4.19 59.0 4.41 56.0 4.61 96.0 4.64 101.0 4.70 43.0 4.88 142.0 5.03 76.0 5.30 41.0 5.56--84.0 5.90 59.0 6.03 53.0 6.12 73.0 6.08 96.0 6.86 63.0
7.89 96.0 7.94 43.0
8.02 54.0 8.08 43.0 8.28 67.0 8.38 42.0 8.45 83.0 8.82 56.0 9.24 65 ;0 9.36 62.0 9.96 114.0 7.01 43.0 8.73 97.0 9.00 117.0 9.31 41.0 9.32 78.0 10.35 130.0 10.69 63.0 10.91 69.0
Area
Cone
Units q
41622
50.-00 UG/L
242456 125.18 UG/L
94245 122.63 UG/L
102406 107.61 UG/L
100293 132.86 UG/L
62102 124.47 UG/L
77955
87.89 UG/L
72675 160.78 UG/L
61799 579.42 UG/L
93948
89.14 UG/L
407263 196.20 UG/L
31137 102.43 UG/L
263039
98.01 UG/L
280107
95.53 OG/L
128700M 110.66 UG/L
11563-4
92.95 UG/L
46120 474.70 UG/L
109431 576.26 UG/L
271132 117.14 UG/L
111234
87.39 UG/L
218346
91.39 UG/L
116354
91.41 UG/L
37628 108.30 UG/L
39595 574.85 UG/L
119853 117.11 UG/L
73821 282.48 UG/L
26204 121.61 UG/L
249991
85.03 UG/L
141736 197.57 UG/L
176412
97.25 UG/L
191367
90.63 UG/L
173227
50.00 .UG/L
201812
89.45 UG/L
191196
84.39 UG/L
145439
78.96 UG/L
33623 1326.71 UG/L
274003
95.03 UG/L
127424
90.33 UG/L
120011 100.75 UG/L
81933 113.24 UG/L
84 98 98 97 95 93 93 86 99 90 92 69 72 100
97 98 96 89 92 96 97 89 97 99 86 76 98 95 89 91 87 95 88 97 93 90 85 88 81
148
;:r -ti-'-v."-.
DUP050308125
QUANT REPORT
Page 2
Operator ID; SJL-176
Output File: AIGKI4::D7
Data File: >IGKI4::D9 -
Name; VSTD100 100 PPB IC
Misc: -SJL 6WL %C +JCEO
=1
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960820 22:40 960820 22:15
1.00000 HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Compound
41) Dibroraoraethane 42) 1,4-Dioxane 43) n-Propyl Acetate 44) Bromodichloromethane 45) 2-Nitropropane 46) 2-Chloroethyl Vinyl Ether 47) cis-1,3-Dichloropropene 48) trans-1,3-Dichloropropene 49) 1,1,2-Trichloroethane 50) Dibromochloromethane 51) Bromoform 52) trans-l,4-Dichloro-2-Butene 53) *Chlorobenzene-d5 54) 4-Methy1-2-Pentanone 55) Toluene-d8 56) Toluene 57) Ethyl Methacrylate 58) Tetrachloroethene 59) 2-Hexanone 60) 1,2-Dibromoethane 61) Chlorobenzene 62) 1,1,1*2-Tetrachloroethene
63) Ethylbenzene 64) m+p-Xylene 65) Isoamyl Acetate 66) o-Xylene 67) Styrene 68) Cumene 69) 4-Bromofluorobenzene 70) l, 1,2,2-Tetrachloroethane 71) 1,2,3-Trichloropropane 72) Pentachloroethane 73) 1,3-Dichlorobenzene 74) 1,4-Dichlorobenzene 75) 1,2-Dichlorobenzene
* Compound is ISTD
R.T. Q ion
10.86 93.0 10.92 88.0 11.00 43.0 11.12 83.0 11.44 41.0 11.58 63.0 11.78 75.0 12.59 75.0 12.85 97.0 13.43 129.0 15.51 173.0 16.29 53.0 14.26 117.0 12.01 43.0 12.17 98.0 12.26 91.0 12.74 69.0 13.06 164.0 13.23 43.0 13.58 107.0
14.31 112.0 14.43 131.0 14.47 106.0 14.65 106.0 14.76 70.0 15.22 106.0 15.24 104.0 15.77 105.0 15.99 95.0 16.20 83.0 16.26 110.0 17.13 167.0 17.60 146.0 17.73 146.0 18.29 146.0
Area
Cone
Units
131345M 9289
193973 256625
88531 73565 207262
201620 114338 196123 129391 137372 124656 120424 307471 315640 174698 102887
81801 182978
232932 124372
97554 249994 126590 118124 223314 359813
216351
194470 47988 80235
163998 185253M 145458
104.13 UG/L 902.89 UG/L 115.16 UG/L
95.45 UG/L 211.72 UG/L 114.67 UG/L
97.45 UG/L
101.86 UG/L 101.08 UG/L
96.44 UG/L 96.05 UG/L 295.11 UG/L 50.00 UG/L 131.16 UG/L 105.4-6 UG/L 100.17 UG/L 120.37 UG/L 90.55 UG/L
150.31 UG/L 123.69 UG/L
99.37 UG/L
103.81 UG/L 96.37 UG/L
203.63 UG/L 115.99 UG/L
96.22 UG/L 101.73 UG/L 127.52 UG/L
109.55 UG/L
122.44 UG/L 113.19 UG/L
99.18 UG/L 113.58 UG/L 128.30 UG/L
99.53 UG/L
<3
66 97 96 94 86 86 91 92 98 98 86 84 89 96 99 94 96 94 93
86 91 94 95 94 93 84 95 72 93 65 87 86 86 85
149
DUP050308126
Data File: >IGKI4
Name: VSTD100 100 PPB IC Misc: ~SJL @WL %C +>CEO . =1 Quant Time: 960820 22:40 Injected at: 960820 22:15
Comoound No: 15
Compound Name: Allyl Chloride
Scan Number: 305
Retention Time: 5.30 min
Quant Ion: 41.0
Area:
128700M
Concentration:
110.66 UG/L
q-value: 0
This report was produced by QAREA
Quant Output File: ~IGKI4 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44
: 12:20 AM WED., 21 AUG., 1996
I5(
DUP050308127
Data File: >IGKI4
Name: VSTD100 100 PPB IC
Kisc: ~SJL @WL %C +}CEO
=1
Quant Time: 960820 22:40
Injected at: 960820 22:15
Compound No: 41
Compound Name: Dibromomethane
Scan Number: 783
Retention Time: 10.86 min
Quant Ion: 93.0
Area:
131345M
concentration:
104.13 UG/L
q-value: 0
Quant Output File: AIGKI4 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
This report was produced by QAREA at: 12:21AM WED., 21 AUG., 1996
151
4
DUP050308128
Data File: >IGKI4
Name: VSTD100 100 PPB IC
Kiso: -SJL @WL %C +}CEO
=1
Quant Time: 960820 22:40
Injected at: 960820 22:15
Quant output File: AIGKI4 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
Compound No: 74
Compound Name: 1,4-Dichlorobenzene
Scan Number: 1372
Retention Time: 17.73 min
Quant Ion: 146.0
Area:
185253M
Concentration:
128.30 UG/L
q-value: 86
This report was produced by QAREA at: 12:22 AM WED., 21 AUG., 1996
15S
DUP050308129
Data File: >IGKI5::D9
Name: VSTD200 200 PPB IC
Misc: -SJL @WL %C +>CEO
=1
Quant Output File: AIGKI5::D7 Instrument ID: HP03046
Id File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Operator ID: SJL-176 Quant Time : 960820 23:10 Injected at: 960820 22:46
15
DUP050308130
QUANT REPORT
Operator ID: SJL-176
Output File: *IGKI5::D7
Data File: >IGKI5::D9
Name: VSTD200 200 PPB IC
Misc: -SJL @WL %C +>CEO
=1
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
Instrument ID
Tn XA39Q:?DB
Title* 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time
Page i 960820 23:10 960820 22:46
1.00000 HP03046
960710 14:27
Compound
1) *Broraochloromethane 2) Dichlorodifluoromethane
3} Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane
8) Ethyl Ether 9) Acrolein 10) i,i-Dichloroethene
11} Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Ally! Chloride 16) Methylene Chloride 17} t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-l,2-Dichloroethene 21) 1,l-Dichloroethane 22} cis-l,2-Dichloroethane
23) 2-Butanone 24} Propionitrile 25) Ethyl Acetate 26} Methacrylonitrile 27) Tetrahydrofuran 28} Chloroform 2 9) Cyclohexane 30) l,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *i,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1/l-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) Methyl Methacrylate
R.T. Q ion
8.30 128.0 2.42 85.0 2.58 50.0 2.76 62.0 3.16 94.0 3.29 64.0 3.70 101.0 4.19 59.0 4.41 56.0 4.61 96.0 4.65 101.0 4.72 43.0 4.88 142.0 5.04 76.0 5.30 41.0 5.5S --84.0 5.92 59.0 6.05 53.0 6.14 73.0 6.09 96.0 6.86 63.0 7.90 96.0 7.95 43.0 8.04 54.0 8.09 43.0 8.30 67.0 8.39 42.0 8.46 83.0 8.82 56.0 9.26 65.0 9.37 62.0 9.97 114.0 7.02 43.0 8.74 97.0 9.01 117.0 9.33 41.0 9.34 78.0
10.36 130.0 10.69 63.0 10.91 69.0
Area
Cone
Units
42601
50.00 UG/L
470730 237.46 UG/L
186279 236.82 UG/L
199740 205.06 UG/L
172150 222.81 UG/L
117100 229.30 UG/L
149368 164.54 UG/L
142425 307.85 UG/L
129868 1189.64 UG/L
193800 170.58 UG/L
756199 355.94 UG/L
62169 199.81 UG/L
516675 188.08 UG/L
558579 186.12 UG/L
275131M 231.13 UG/L
228287 179.28 -UG/L
97179 977.26 UG/L
234538 1206.68 UG/L
545201 230.14 UG/L
221303 169.87 UG/L
442580 180.99 UG/L
234471 179.97 UG/L
76460 215.01 UG/L
85986 1219.69 UG/L
249570 238.25 UG/L
149163 557.66 UG/L
56031 254.06 UG/L
507178 168.55 UG/L
280048 381.40 UG/L
364600 196.36 UG/L
391115 180.97 UG/L
178956
50.00 UG/L
426096 182.81 UG/L
372078 158.96 UG/L
293856 154.43 UG/L
69559 2656.82 UG/L
538592 180.81 UG/L
248933 170.82 UG/L
250372 203.45 UG/L
168682 225.67 UG/L
q
81 96 95 98 99 93 97 87 97 91 91 71 72 100
97 99 96 85 91 97 96 39
94 99 84 76 97 95 89 91 87 95 88 97 95 89 84 88 80
154
DUP050308131
QUANT REPORT
Page 2
Operator ID: SJL-176
Output Pile: AIGKI5::D7
Data File: >IGKI5::D9
Name: VSTD20Q 200 PPB IC
Misc: -SJL WL %C +>CEO
=1
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960820 23:10 960820 22:46
1.00000 HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960710 14:27
Compound
41) Dibromomethane 42) 1,4-Dioxane 43) n-Propyl Acetate 44) Bromodichloromethane 45) 2-Nitroprofcane 46) 2-Chloroethyl Vinyl Ether 47) cis-1,3-Dichloropropene 48) trans-1,3-Dichloropropene 49) 1,1,2-Trichloroethane 50) Dibromochloromethane 51) Bromoform 52) trans-l, 4-Dich.loro-2-Butene 53) *Chlorobenzene-d5 54) 4-Methyl-2-Pentanone 55) Toluene-ds 56) Toluene 57) Ethyl Methacrylate 58) Tetrachloroethehe 59) 2-Hexanone 60) 1,2-Dibromoethane 61) Chlorobenz ene 62) 1,1,1,2-Tetrachloroethane 63) Ethylbenzene 64) m+p-Xylene 65) Isoamyl Acetate 66) o-Xylene 67) Styrene 68) Cumene 69) 4-Bromofluorobenzene 70) 1,1,2,2-Tetrachloroethane 71) 1,2,3-Trichloropropane 72) Pantachloroethane 73) 1,3-Dichlorobenzene 74) 1,4-Dichlorobenzene 75) 1,2-Dichlorobenzene
* Compound is ISTD
R. II!1 * Q ion
10.86 93.0 10.92 88.0 11.02 43.0 11.13 83.0 11.46 41.0 11.59 63.0 11.78 75.0 12.59 75.0 12.86 97.0 13.43 129.0 15.52 173.0 16.29 53.0 14.27 117.0 12.02 43.0 12.17---98*0
12.26 91.0 12.74 69.0 13.07 164.0 13.23 43.0 13.58 107.0 14.31 112.0 14.43 131.0
14.48 106.0 14.64 106.0 14.78 70.0 15.23 106.0 15.25 104.0
15.76 105.0 16.00 95.0 16.21 83.0 16.27 110.0 17.14 167.0 17.60 146.0 17.73 146.0
18.29 146.0
Area
Cone
Units
270106M 207.28 UG/L
18835 1772.15 UG/L
401227 230.57 UG/L
525565 189.21 UG/L
187575 434.22 UG/L
165647 234.03 UG/L
423549 192.77 UG/L
413415 202.17 UG/L
233252 199.59 UG/L
398863 189.85 UG/L
267090 191.92 UG/L
278169 578.45 UG/L
126057
50.00 UG/L
245535 264.46 UG/L
633073 214-.7-2 UG/L
626588 196.64 UG/L
362606 247.06 UG/L
198722 172.94 UG/L
168438 306.08 UG/L
375779 251.20 UG/L
467820 197.36 UG/L
247253 204.07 UG/L
185863 181.56 UG/L
475823 383.26 UG/L
259938 235.53 UG/L
228534 184.03 UG/L
435280 196.09 UG/L
722381 253.18 UG/L
441866 221.26 UG/L
384770 239.57 UG/L
95237 222.13 UG/L
159152 194.53 UG/L
322133 220.63 UG/L
368459M 252.36 UG/L
283526 191.84 UG/L
q
71 97 96 94 87 87 90 94 99 99 88 81 89 96 99 91 98 94 93 86 91 93 97 91 91 84 95 70 94 61 85 86 86 84
15 5
DUP0 50308132
Data File: >IGKI5
Name: VSTD20Q 200 PFB IC
Misc: -SJL @WL %C +>CEO
=1
Quant Time: 960820 23:10
Injected at: 960820 22:46
Quant Output File: AIGKI5 Instrument ID: HPQ3046
Quant ID File: IA639G Last Calibration: 951122 10:44
Compound No: 15
Compound Name: Allyl Chloride
Scan Number: 304
Retention Time: 5-30 min
Quant Ion: 41.0
Area:
275131M
Concentration:
231.13 UG/L
q-value: 0
This report was produced by QAREA at: 12:26 AM WED., 21 AUG., 1996
15b
DUP050308133
Data File: >IGKI5
Name: VSTD200 200 PPB XC
Misc: -SJL @WL %C +}CEO
=1
Quant Time: 960820 23:10
Injected at: 960S20 22:46
Quant Output File: ~IGKI5 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
Compound No: 41
Compound Name: Dibromomethane
Scan Number: 781
Retention Time: 10.86 min
Quant Ion: 93.0
Area:
270106M
Concentration:
207.28 UG/L
q-value: 0
This report was produced by QAKEA at: 12:27 AM WED., 21 AUG., 1996
157
DUP050308134
Data File: >IGKI5
Name: VSTD200 200 PPB IC
Misc: -SJL @WL %C +JCEO
=1
Quant Time: 960820 23:10
Injected at: 960820 22:46
Compound No: 74
Compound Name: 1,4-Dichlorobenzene
Scan Number: 1369
Retention Time: 17.73 min
Quant Ion: 146.0
Area:
368459M
Concentration:
252.36 UG/L
q-value: 86
Quant Output File: -'IGKI5 Instrument ID: HP03046 Quant ID File: IA6390 Last Calibration: 951122 10:44
TUi 5
This report was produced by QAREA at: 1:43 PM WED., 21 AUG., 1996
DUP050308135
6A VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: LANCASTER: LABS
Contract: _____
Lab Code: LANCAS
Case No.: _______ . SAS No. _______. SDG No.: _______
Instrument ID: HP03046
Calibration Date(s): 09/24/96
09/24/96
Heated Purge: (Y/N) N
Calibration Times: 1135
1356
GC Column: DB624
LAB FILE ID: RRF 50= >ISOI3
ID: 0.53 (mm)
RRF 10= >IS0I1 RRF100= >IS0I4
RRF 20= >ISOI2
RRF200= >I3015
COMPOUND
RRF 10 RRF 20 RRF 50 RRF100 RRF200 RRF
Dichlorodifluoromethane
2.728
Chloromethane
.920
Vinyl Chloride
** 1.071
Bromomethane
** 1.150
Chloroethane
.739
Trichlorofluoromethane
1.203
Ethyl Ether
.972
Acrolein
.204
1,1-Dichloroethene
* 1.153
Freon 113
2.462
Acetone
.443
Methyl Iodide
4.338
Carbon Disulfide
3.105
Allyl Chloride
1.777
Methylene Chloride
1.421
t-Butyl Alcohol
.120
Aerylonitrile
.282
Methyl t-Butyl Ether
3.635
1,2-Dichloroethene (total) 1.408
1,1-Dichloroethane
* 2.457
2-Butanone
.376
Propionitrile
.079
Ethyl Acetate
1.393
Methacrylonitrile
.405
Tetrahydrofuran
.312
Chloroform
* 3.150
cyclohexane
1.623
1,2-Dichloroethane
* 2.313
Vinyl Acetate
.793
1,1,1-Trichloroethane
* .631
Carbon Tetrachloride
* .522
Isobutyl Alcohol
i .007
Benzene
* .900
2.147
.788 .799 .864 .548 1.309
.780 .172 .88 6 1.787 .394
3.434 2.428
1.375 1.094
.118 .241 3.244
1.109
1.902 .319 .076
1.435 .350 .325
2.531 1.288 1.982
.754
.547 .462 .007
.724
2.717 .961
1.083 .996 .619
1.463 .868 .176
1.098 2.277
.411 4.169 3.035 1.791 1.253
.112
.258 3.216
1.339
2.345
.402 .099 1.509 .371 .245
2.929 1.596 2.174
.736
.601 .544 .007 .787
2.669 .926
1.091 .980 .551
1.477 .865 .184
1.113 2.236
.423
4.232 3.138 1.806 1.291
.130
.293
3.172
1.355
2 401 .463 .105
1.477 .374 .306
2.951 1.581 2.196
.805
.634 .553 .009 .827
2.418 .859
1.017 .858 .423
1.328 .843 .187
1.076
2.156 . 426
4.028 3.049 1.802 1.202
.143 .292 2.971
1.300
2.371 .492 .107
1.480 .365 .325
2.925 1.616 2.191
.823 .586 .550 .009 .768
2.536 .891
1.012 .970 .576
1.356 .866 .185
1.065 2.183
.419
4.040 2.951 1.710 1.252
.125 .273 3.248
1.302 2.295
.410 .093 1.459 .373 .302 2.897 1.541 2.171
.782
.600 .526 .008 .801
* Compounds with required minimum RRF and maximum %RSD values. All other compounds in OLM01.8 must meet a minimum RRF of 0.010.
% RSD
9.9 7.7 12.1* 12.3* 20.0 8.4 8.0 6.7 9.8* 11.4 4.4 8.8 10.0 11.0 9.6 9.6 8.3 7.4 8.8 9.8* 16.8 15.7 3.1 5.3 11.0 7.8* 9.2 1 5.5* 4.6 I
6.0* 7.2* 13.4 1 8.3*
1
page 1 Of 2
FORM VI VOA
QLM03.0
i5S
DUP050308136
6A VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: LANCASTER LABS
Contract: _______.
Lab Code: LANCAS Case No.: _______ . SAS No. _______. SDG No.: _______ .
Instrument ID: HP03046
Calibration Date(s): 09/24/96
09/24/96
Heated Purge: (Y/N) N
Calibration Times: 1135
1356
GC Column: DB624
ID: 0.53 (mm)
woo too
II II
VV i>aW PnH
LAB FILE Id : RRF 50= >ISOI3
'
RRF 10= ">18011----------- -------ERF
RRF100== >ISOI4
er f ;
3012--------------------3015
COMPOUND
RRF 10 RRF 20 RRF 50 RRF100 RRF200
Trichloroethene
: r .430
1,2-Dichloropropane
.375
1,4-Dioxane
.002
n-Propyl Acetate Bromodichloromethane
.552 ik .817
2-Chloroethy1 Vinyl Ether
cis-1,3-Dichloropropens
*
trans-1,3-Dichloropropene * *
1,1,2-Trichloroethane
*
Dibromochloromethane
*
Bromoform
k
.255
.642
.614 .410
.756 .587
trans-1.4-Dichloro-2-Butene .168
4-Methyl-2-Pentanone
Toluene Tetrachloroethene
.490 J 1.337 5t .484
2-Hexanone
.276
1,2-Dibromoethane
Chlorobenz ene Ethylbenzene
.827 3k 1.027 * .440
Xylene (total)
* .547
Isoamyl Acetate Styrene
.560 * 1.011
Cumene 1,1,2,2-Tetrachloroethane
1
1.530 .937
1,2,3-Trichloropropane
.238
1,3-Dichlorobenzene
.804
1,4-Dichlorobenzene
.974
1,2-Dichlorobenzene
.842
.352 .318 .003 .502 .718
.245 .554
.546 .359 .669 .533 .159 .479 1.061 .386 .267 .728 .837
.359 .441
.500 .798 1.246 .828 .207 .637
.751 .684
.404 .336 .003 .543
.746 .237
.591 .550 .352 .683 .547 .159 .461
1.210 .452 .286 .724
.929 .407
.498 .487 .899 1.456 .788 .203
.777
.870 .776
.423 .352 .004 .587 .770
.248 .617 .577 .359 .689 .552 .169
.473 1.322
.481 .314 .757
.963 .426
.513
.510 .920 1.436 .830
.203 .764
.898
.768
.394 .351
. 003 .588
.754 .247 .577
. 556 .357
.690 .557 .160 .480 1.180 .438 .325 .721
.933 .394
.460 .491 .881 1.407 .763 .190 .739
.863 .726
RRF
.401 .346 .003 .554 .761 .246 .596 .569 .367 .697 .555 .163 .477 1.222 .448 .294 .751 .938 .405 .492 .510 .902 1.415 .829 .208 .744 .871 .759
% RSD
7.7*
6.2 I 16.5
6.4 | 4.8* 2.5 j 5.7* 4.9* 6.6* 4.8* 3.6* 3.0 | 2.3 j 9.3* 8.9* 8.5 6.0 7.3* 7.7* 8.6* 5.8 j 8.5* 7.4 [ 8.0*
8.6
8.6 9.2 7.8
1,2-Dichloroethane-d4
1.982 1.909 1.933 1.989 1.939 1.951
Toluene-d8 4-Bromofluorobenzene
1.204 1.184 1.140 1.206 1.153 1.177 * .958 .942 .927 .969 .939 .947
L
== Compounds with required minimum RRF andmaximum %RSD values
All other compounds in OLM01.8 must meet a minimum RRF of 0.010.
1.7 2.5
1.7*
1
page 2 of 2
FORM VI VOA
OLM03.0
DUP050308137
TOTAL ION CHROMATOGRAM File > I SOI! 35.0-300.0
Jt_I__L. JL--I_X4. 00
emu. VSTDQ1Q TIC
> -80iQ '
6lO PPB * >
IC~TLN 0ML 1..2I0,,,0r__ * 1
5C *1 +>CEC -I__t1_6_I0_0L.
260000-
240000
220000
200000
180000-
160000
140000
120000100000-
80000
60000
40000
2000O
Data File: >IS0I1::D9
Name: VSTD010 010 PPB IC Misc: -TLN WL %C =1 +>CEO-V
Quant Output File: AISOIl::D7 Instrument ID: HPG3046
Id File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLN-262 Quant Time : 960924 13:08 Injected at: 960924 11:35
160
DUP050308138
QUANT REPORT
Page 1
Operator ID: TLN-262 Output File: ''ISOIl: :D7 Data File: >ISOIl::D9
Name: VSTD010 010 PPB Ic Misc: -TEN @WL %C =1 +JCEO-V
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
Instrument ID
960924 13:08 960924 11:35
1.00000
HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,l-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene Chloride 17} t-Butyl Alcohol 18) Aerylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene 21) 1,1-Dichloroethane 22) cis-l,2-Dichloroethene
23) 2-Butanone 24) Propionitrile
A 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) l,2-Dichloroethane-d4 A 31) 1,2-Diehloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,1-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene A 38) Trichloroethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane
R.T. Q ion
8.18 128.0 2.28 85.0 2.43 50.0 2.61 62.0 3.04 94.0 3.19 64.0 3.58 101.0 4.07 59.0 4.28 56.0 4.46 96.0 4.53 101.0 4.60 43.0 4.73 142.0 4.85 76.0 5.18 41.0 5.44 84.0 5.80 59.0 5.94 53.0 6.01 73.0 5.96 96.0 6.75 63.0 7.79 96.0
7.87 43.0 7.94 54.0 7.98 43.0 8.18 67.0 8.26 42.0 8.35 83.0 8.70 56.0 9.13 65.0 9.24 62.0 9.84 114.0 6.91 43.0 8.61 97.0 8.88 117.0 9.21 41.0 9.20 78.0 10.23 130.0 10.56 63.0 10.83 88.0
Area
35514 19378
6537 7605 8168 5246 8547 6906 7247 8190 34974 3150M 30815 22054 12621M 10091 4275 10002 25820 9646 17455 10355
2672M 2819 9893
7186 2216 22374 11525 14078 16428 136903 21705 17272 14287 2422 24641 11779 10279
814
Cone
Units
50.00 UG/L
10.04 UG/L 11.93 UG/L 11.26 UG/L
11.01 UG/L 11.79 UG/L 13.48 UG/L 11.21 UG/L 78.01 UG/L 11.39 UG/L 21.69 UG/L
13.66 UG/L 14.96 UG/L 17.56 UG/L 12.24 UG/L 11.63 UG/L 68.25 UG/L 56.14 UG/L 11.15 UG/L 10.87 UG/L
10.10 UG/L 11.67 UG/L
9.55 UG/L 47.14 UG/L 10.55 UG/L
31.00 UG/L 11.24 UG/L
9.93 UG/L
10.09 UG/L 8.60 UG/L 9.52 UG/L
50.00 UG/L 14.25 UG/L
10.54 UG/L
10.25 UG/L
145.63 UG/L 12.36 UG/L 12.06 UG/L 11.71 UG/L
201.96 UG/L
q
96 99 98 99 90 94 93 86 93 96 97 83 71 100
94 87 97 90 96 97 90 92 93 88 94 91 96 91 90 93 88 98 90 98 88 91 90 90 90
161
A
DUP050308139
QUANT REPORT
Page 2
Operator ID: TLN-262
Output File: AXSOXl::D7 . Data File: >ISOIl::D9 Name: VSTD010 010 PPB IC Wise: ~TLN @WL %C -1 +}CEO-V
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
instrument ID
960924 13:08 960924 11:35
1.00000 HP03046
ID File: IA6390: :DEi
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-1,3-Dichloropropene 45) trans-l,3-Dichloropropene 46) 1,1,2-Trichloroethane 47) Dibromochloromethane 48) Bromoform 49) trans-l,4-Dichloro-2-Butene 50) *Chlorobenzene-d5 51) 4-Methyl-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hexanone 56) 1,2-Dibromoethane 57) Chlorobenzene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) Styrene 63) Cumene 64) 4-Bromofluorobenzene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) 1,3-Dichlorobenz ene 68) 1,4-Dichlorobenzene 69) 1,2-Dichlorobenzene
* Compound is ISTD
R.T. Q ion
10.90 43.0 11.00 83.0 11.48 63.0 11.68 75.0 12.49 75.0 12.75 97.0 13.32 129.0 15.42 173.0 16.20 53.0 14.16 117.0 11.92 43.0 12.06 98.0 12.16 91.0 12.96 164.0 13.15 43.0 13.48 107.0 14.20 112.0 14.37 106.0 14.54 106.0 14.68 70.0 15.13 106.0 15.15 104.0 15.66 105.0 15.89 95.0 16.12 83.0 16.17 110.0 17.50 146.0 17.63 146.0 18.19 146.0
Area
15106 22376
6971 17566 17483 11238 20693 16060 11479 104864 10287 25248 28038 10155
5780 17345 21535
9231 23622 11745 11475
21194 32087 20082 19656
4982 16852 20424 17660
cone
Units
10.85 UG/L 10.83 UG/L 12.3 0 UG/L
11.38 UG/L 11.78 UG/L 12.49 UG/L 12.90 UG/L 14.93 UG/L 29.35 UG/L 50.00 UG/L 11.91 UG/L 10.16 UG/L 11.38 UG/L 11.85 UG/L
11.59r-UG/L 11.86 UG/L 11.41 UG/L 11.45 UG/L 23.58 UG/L
12.05 UG/L
11.46 UG/L
11.90 UG/L 10.93 UG/L 11.57 UG/L 12.80 UG/L 12.55 UG/L 12.40 UG/L 13.30 UG/L 13.71 UG/L
q
95 95 92 87 91 95 98 95 91 86 91 97 95 97 89 94 87 96 96
94 91 84 96 81 98 67 90 91 86
16 2
DUP050308140
5^
Data File: >IS0I1 Name: VSTD010 010 PPB IC Misc: **TLN @WL %C =1 +JCEO-V
Quant Time: 960924 13:08 Injected at: 960924 11:35
Quant Output File: ''ISOU Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
compound No: 12
Compound Name: Acetone
Scan Number: 239
Retention Time: 4.60 min
A
Quant Ion: 43.0
Area:
3150M
Concentration:
13.66 UG/L
q-value: 83
This report was produced by QAREA at: 3:23 PM TUE., 24 SEPT, 1996
16
DUP050308141
S3rL
Data File: >ISOXl Name: VSTD010 010 PPB IC Misc: -TLN WL %C =1 +J-CEO-V Quant Time: 960924 13:08 Injected at: 960924 11:35
Compound No: 15
Compound Name: Allyl Chloride
Scan Number: 289
Retention Time: 5.18 min
Quant Ion: 41.0
Area:
1262161
Concentration:
12.24 UG/L
q-value: 0
Quant Output File: AISOIl Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
This report was produced by QAREA at: 3:24 PM TUE., 24 SEPT, 1996
164
DUP050308142
A
Data File: >IS0I1 Name: VSTD010 010 PPB IC
Misc: ~TLN @WL %C -1 +>CEO-V Quant Time: 960924 13:08 Injected at: 960924 11:35
Quant Output File: AIS0Ii Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
Compound No: 23
Compound Name: 2-Butanone
Scan Number: 520
Retention Time: 7.87 min
Quant Ion: 43.0
Area:
2672M
concentration:
9.55 UG/L
q-value: 92
This report was produced by QAREA at: 3:25 PM TUE., 24 SEPT, 1996
105
DUP050308143
TOTAL ION CHROMATOGRAM
Data File: >ISOI2::D9 Name: VSTD020 020 PPB IC Misc: ~TLN @WL %C =1 +JCEO-V
Quant Output File: -ISOI2: :D7 Instrument ID: HP03046
Id File: IA639Q::DB
Title; 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TIN-262 Quant Time : 960924 13:17
Injected at: 960924 12:08
166
DUP050308144
QUANT REPORT
Page 1
Operator ID: TLN-262 Output File: ''ISOI2::D7 Data File: >ISOI2::D9
Name: VSTD02Q 020 FPB IC Misc: ~TLN @WL %C ==1 +>CEO-V
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
Instrument ID
960924 13:17
960924 12:08 1.00000
HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Sromomethane
6) Chloroethane
7} Trichlorofluoromethane
8} Ethyl Ether
9} Acrolein 10) 1,l-Dichloroethene 11) Freon 113
12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-l,2-Dichloroethene 21) 1,1-Dichloroethane 22) cis-1,2-Dichloroethene
23) 2-Butanone
24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,1-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane
Q ion
8.19 128.0 2.29 85.0 2.44 50.0 2.62 62.0 3.06 94.0 3.21 64.0 3.58 101.0 4.10 59.0 4.32 56.0 4.47 96.0 4.54 101.0 4.62 43.0 4.74 142.0
4.85 76.0 5.19 41.0 5.46 -84.0 5.80 59.0 5.95 53.0 6.02 73.0 5.98 96.0 6.76 63.0 7.81 96.0
7.88 43.0
7.95 54.0 8.00 43.0 8.18 67.0 8.29 42.0 8.36 83.0 8.70 56.0 9.13 65.0 9.26 62.0 9.84 114.0 6.92 43.0 8.63 97.0 8.89 117.0 9.22 41.0 9.21 78.0 10.23 130.0 10.56 63.0 10.79 88.0
Area
25596 21981
8066 8184 8849 5613 13404 7982 8804 9068 36585 4033M 35155M 24860 14081M 11202 6018 12339 33212 10851 19471 11844
3262
3872 14692
8968 3327 25912 13183 19544 20293 95328 28753 20875 17629 3274 27594 13416 12114 1391
Cone
Units
50.00 UG/L
15.80 UG/L
20.42 UG/L
16.81 UG/L 16.56 UG/L 17.50 UG/L 29.33 UG/L 17.97 UG/L 131.49 UG/L
17.49 UG/L 31.49 UG/L 24.26 UG/L
23.68 UG/L
27.46 UG/L 18.94 UG/L 17.91 UG/L 133.31 UG/L 96.09 UG/L 19.90 UG/L 16.97 UG/L 15.63 UG/L
18.52 UG/L
16.18 UG/L
89.83 UG/L 21.74 UG/L 53.67 UG/L 23.41 UG/L 15.95 UG/L 16.01 UG/L 16.57 UG/L
16.31 UG/L 50.00 UG/L 27.11 UG/L 18.30 UG/L 18.16 UG/L 282.72 UG/L
19.87 UG/L 19.72 UG/L 19.82 UG/L 495.62 UG/L
q
98 91 98 97 98 91 99 85 97 96 96
99 100
92 93 98 91 96 96 96 97 87 93 90 71 98 93 89 92 88 97 89 97 98 87 89 90 92
167
DUP050308145
QUANT REPORT
Page 2
Operator ID: TLN-262 Output File: ~ISOI2::D7
Data File: >ISOI2::D9 Name: VSTD020 020 PPB IC Misc: ~TLN GW!. %C -1 +}CEO-V
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
Instrument ID
960924 13:17 960924 12:08
1.00000 HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03Q46
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-1,3-Dichloropropene 45) trans-1,3-Dichloropropene 46) 1,1,2-Trichloroethane 47) Dibromochloromethane 48) Bromoform 49) trans-l,4-Dichloro-2-Butene 50) *Chlorobenzene-d5 51) 4-Methyl-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hexanone 56) 1,2-Dibromoethane 57) Chlorobenz ene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) styrene 63) Cumene 64) 4-Bromofluorobenzene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) 1,3-Diehlorobenzene 68) 1,4-Dichlorobenzene 69) 1,2-Dichlorobenzene
* Compound is ISTD
R.T. Q ion
10.90 43.0 11.00 83.0 11.47 63.0 11.67 75.0 12.48 75.0 12.74 97.0 13.31 129.0 15.40 173.0 16.18 53.0 14.15 117.0 11.90 43.0 12.05 98.0 12.15 91.0 12.94 164.0 13.12 43.0 13.46 107.0 14.18 112.0 14.35 106.0 14.52 106.0 14.66 70.0 15.11 106.0 15.13 104.0 15.65 105.0 15.88 95.0
16.09 83.0 16.16 110.0 17.49 146.0 17.61 146.0 18.17 146.0
Area
19135 27380
9342 21137 21670 13678 25496 20309 15191 75567 14492 35786 32063 11665
8061 21990 25299 10854 27213 15105 13337 24130 37652 28488
25024 6250
19248 22707 20678
Cone
units
19.75 UG/L 19.02 UG/L 23.67 UG/L 19.67 UG/L 20.97 UG/L
21.83 UG/L 22.82 UG/L 27.11 UG/L 55.78 UG/L 50.00 UG/L 23.28 UG/L 19.99 UG/L
18.06 UG/L 18.88 UG/L 22*43 UG/L 20.86 UG/L 18.61 UG/L 18.69 UG/L 37.70 UG/L 21.50 UG/L 18.48 UG/L 18.80 UG/L
17.79 UG/L 22.78 UG/L
22.62 UG/L 21.85 UG/L
19.65 UG/L 20.52 UG/L
22.28 UG/L
<3
96 95 89 86 92 93 96 98 90 83 89 97 99 98 94 94 91 99 97 93 95 85
99 81 93 63 88 86 86
168
DUP050308146
5^
Data Pile: >IS0I2
Name: VSTD020 020 PPB IC Misc: ~TLN eWL %C =1 +}CEO-V
Quant Time: 960924 13:17 Injected at: 960924 12:08
Quant Output File: 'IS0I2 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
Compound No: 12
Compound Name: Acetone
Scan Number: 242
Retention Time: 4.62 min
Quant Ion: 43.0
Area:
4033M
Concentration:
24.26 UG/L
q-value: 0
This report was produced by QAREA at: 3:29 PM TTJE. , 24 SEPT, 1996
169
DUP050308147
9-34-%
Data Pile: >1S0I2 Name: VSTD020 020 PPB IC Misc: -TLN @WL %C =1 +JCEO-V Quant Time: 960924 13:17 Injected at: 060924 12:08
Quant Output File: ~ISOI2 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
Compound No: 13
Compound Name: Methyl Iodide
Scan Number: 252
Retention Time: 4.74 min
A Quant Ion: 142.0
Area:
' 35155M
Concentration:
23.68 UG/L
q-value: 99
This report was produced by QAREA at: 3:29 PM TUE., 24 SEPT, 1996
170
DUP050308148
Data Files >IS0I2
Quant Output File: AISOI2 .
A
Name: VSTD020 020 PPB IC Misc: ~TLN @WL %C -1 +J-CEO-V
Instrument ID: HP03046
Quant Time: 960924 13:17
Quant ID File: IA6390
A Injected at: 960924 12:08
Last Calibration: 951122 10:44
Compound No: 15
compound Name: Allyl Chloride
Scan Number: 291
Retention Time: 5.19 min
Quant Ion: 41.0
Area:
14081M
Concentration:
18.94 UG/L
q-value: 0
This report was produced by QAREA at: 3:30 PM TUE., 24 SEPT, 1996
171
DUP050308149
TOTAL ION CKR0MAT06RAM
Data File: >ISOl3::D9
Quant Output File: "ISOIS^D?
Name: VSTD050 050 PPB IC
Instrument ID: HP03046
Misc: ~TLN @WL %C =1 +JCEO-V =1
Id File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLN-262 Quant Time : 960924 13:25 Injected at: 960924 12:50
1j L **7*(30 DUP050308150
QUANT REPORT
Page 1
Operator ID: TLN-262
Quant Rev: 7
Quant Time
Output File: AISOI3::D7
Injected at
Data File: >IS0I3::D9
Dilution Factor
Name: VSTD050 050 PFB IC
Instrument ID
Misc: ~TLN WL %C =1 +}CEO-V =1
960924 13:25
960924 12:50 1.00000
HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,l-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-l,2-Dichloroethene 21) 1,l-Dichloroethane 22) cis-l,2-Dichloroethene
23} 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane
R.T. Q ion
8.17 128.0 2.28 85.0 2.43 50.0 2.59 62.0 3.02 94.0 3.16 64.0 3.55 101.0 4.06 59.0 4.28 56.0 4.43 96.0 4.49 101.0 4.59 43.0 4.70 142.0 4.82 76.0 5.16 41.0 5.41 84.0 5.77 59.0 5.90 53.0 6.01 73.0 5.96 96.0 6.74 63.0 7.77 96.0 7.84 43.0 7.91 54.0 7.97 43.0 8.16 67.0 8.28 42.0 8.34 83.0 8.68 56.0 9.12 65.0 9.23 62.0 9.84 114.0 6.89 43.0 8.60 97.0 8.88 117.0 9.20 41.0 9.20 78.0 10.22 130.0 10.55 63.0 10.79 88.0
Area
Cone
Units
30984
50.00 UG/L
84170
49.97 UG/L
29789
62.30 UG/L
33557
56.94 UG/L
30847
47.68 UG/L
19178
49.39 UG/L
45341
81.96 UG/L
26909
50.05 UG/L
27269 336.44 UG/L
34032
54.23 UG/L
141074 100.30 UG/L
12732
63.27 UG/L
129170
71.89 UG/L
94045
85.81 UG/L
55507M 61.68 UG/L
38836
51.28 UG/L
17408 318.57 UG/L
39903 256.70 UG/L
99636
49.32 UG/L
40057
51.76 UG/L
72665
48.18 UG/L
42952
55.50 UG/L
12457
51.04 UG/L
15300 293.23 UG/L
46741
57.13 UG/L
28767 142.22 UG/L
7581
44.07 UG/L
90745
46.16 UG/L
49437
49.59 UG/L
59899
41.95 UG/L
67354
44.73 UG/L
125072
50.00 UG/L
92070
66.16 UG/L
75122
50.18 UG/L
68021
53.41 UG/L
11466 754.65 UG/L
98416
54.02 UG/L
50590
56.68 UG/L
41988
52.37 UG/L
4280 1162.32 UG/L
q
94 99 98 98 95 93 94 89 99 95 98 70 69 100
99 94 96 90 94 98 97 85 95 97 87 73 98 95 89 92 88 98 91 98 85 87 87 89 79
iJL O
DUP050308151
QUANT REPORT
Page 2
Operator ID: TLN-262
Quant Rev: 7
Quant Time
Output File: 'ISOI3: :D7
Injected at
Data File: >ISOI3::D9
Dilution Factor
Name: VSTD050 050 PPB IC
Instrument ID
Misc: -TLN @WL %C =1 +JCEO-V =1
960924 13:25 960924 12:50
1.00000 HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-1,3-Dichloropropene 45) trans-l,3-Dichloropropene 46) 1,1,2-Trichloroethane 47) Dibromochloromethane 48) Bromoform 49) trans-l,4-Dichloro-2-Butene 50) Chlorobenzene-d5 51) 4-Methyl-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hexanone 56) 1,2-Dibroraoethane 57) Chlorobenzene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) Styrene 63) Cumene 64) 4-Bromofluorobenzene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) l,3-Dichlorobenzene 68) 1,4-Dichlorobenzene 69) 1,2-Dichlorobenzene
* Compound is ISTD
R.T. Q ion
10.89 43.0 10.99 83.0 11.47 63.0 11.67 75.0 12.48 75.0 12.74 97.0 13.31 129.0 15.40 173.0 16.18 53.0 14.15 117.0 11.90 43.0 12.05 98.0 12.15 91.0 12.95 164.0 13.13 43.0 13.46 107.0 14.20 112.0 14.36 106.0 14.52 106.0 14.67 70.0 15.11 106.0 15.13 104.0 15.66 105.0 15.88 95.0 16.09 83.0 16.15 110.0 17.49 146.0 17.62 146.0 18.17 146.0
Area
67905 93249 29687 73922 71562 44027 85449 68352 49759 97357 44860 110984 117846 43996 27876 70448 90431 39605 98618 47408 48472 87530 141745 90222 76705 19776 75650 84660 75556
Cone
Units
53.41 UG/L 49.38 UG/L 57.32 UG/L 52.42 UG/L 52.77 UG/L 53.56 UG/L 58.29 UG/L
69.54 UG/L
139.26 UG/L 50.00 UG/L 55.92 UG/L 48.13 UG/L
51.53 UG/L 55.29 UG/L 60.22 UG/L 51.88 UG/L 51.62 UG/L 52.93 UG/L 106.05 UG/L 52.37 UG/L 52.13 UG/L 52.93 UG/L
51.99 UG/L 55.99 UG/L 53.81 UG/L 53.65 UG/L 59.95 UG/L 59.38 UG/L 63.19 UG/L
q
97 95 88 88 91 95 97 97 89 86 90 95 98 98 97 94 85 96 96 94 92 85
98 82 91 67 89 89 88
174
DUP050308152
Data File: >IS0I3 Name: VSTD050 050 PPB IC Misc: ~TLN WL %C =1 +}CEO-V *1 Quant Time: 960924 13:25 Injected at: 960924 12:50
Quant Output File: "ISOI3 instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
Compound No: 15
Compound Name: Allyl Chloride
Scan Number: 287
Retention Time: 5.16 min
Quant Ion: 41.0
Area:
55507M
Concentration:
61.68 UG/L
q-value: 0
This report was produced by QAREA at: 3:36 PM TUE., 24 SEPT, 1996
.j u <J
ii'it&U; DUP0503081 53
TOTAL ION CHROKflTOeRPm
Data File: >XSGI4::D9 Name: VSTD100 100 PPB IC Misc: -TLN WL %C +JCE0-V -1
Quant Output File: AISOI4::D7 Instrument ID: HP03046
Id File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLN-262 Quant Time : 960924 13:50 Injected at: 960924 13:23
i: 1hf.ili.TM-'.;'#fc.: I
176
t d* 4lUV
*< V
DUP050308154
QUANT REPORT
Page 1
Operator ID: TLN-262 Output File; ~ISOI4::D7 Data File: >ISOI4::D9 Name: VSTD100 100 PPB IC Wise: ~TLN @WL %C +J-CBO-V =1
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960924 13:50
960924 13:23 1.00000
HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time : 960919 06:34
Compound
1) *Bromochloromethane 2) Dichiorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,l-Dichloroethene 11) Freon 113 12) Acetone 13} Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16} Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-l,2-Dichloroethene 21) 1,l-Dichloroethane 22) cis-1,2-Dichloroethene 23) 2-Butanone 24) Prop ionitrile 25} Ethyl Acetate 26) Methacrylonitrile 27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) l,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene 33) Vinyl Acetate 34) 1,1,l-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37} Benzene 38) Trichlotoethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane
R.T. Q ion
8.18 128.0 2.28 85.0 2.43 50.0 2.61 62.0 3.03 94.0 3.17 64.0 3.55 101.0 4.08 59.0 4.28 56.0 4.45 96.0 4.52 101.0 4.60 43.0 4.72 142.0 4.83 76.0 5.16 41.0 5.43 84.0 5.79 59.0 5.92 53.0 6.00 73.0 5.96 96.0 6.74 63.0 7.78 96.0
7.84 43.0 7.91 54.0 7.98 43.0 8.16 67.0 8.27 42.0 8.34 83.0 8.70 56.0 9.12 65.0 9.25 62.0 9.84 114.0 6.89 43.0 8.61 97.0 8.88 117.0 9.19 41.0 9.20 78.0 10.24 130.0 10.57 63.0
10.80 38*0
Area
Cone
Units
32401
50.00 UG/L
172957
98.19 UG/L
60025 120.04 UG/L
70707 114.73 UG/L
63525
93.89 UG/L
35691
87.89 UG/L
95718 165.46 UG/L
56022
99.64 UG/L
59632 703.55 UG/L
72145 109.94 UG/L
289732 196.99 UG/L
27380 130.12 UG/L
274221 145.94 UG/L
203319 177.41 UG/L
117035M 124.37 UG/L
83654 105.64 UG/L
42045 735.77 UG/L
94868 583.60 UG/L
205574
97.30 UG/L
84835 104.82 UG/L
155594
98.66 UG/L
90864 112.27 UG/L
30015 117.60 UG/L
34060 624.23 UG/L
95738 111.91 UG/L
60550 286.26 UG/L
19801 110.08 UG/L
191240
93.02 UG/L
102483
98.31 UG/L
128913
86.34 UG/L
142327
90.38 UG/L
129247
50.00 UG/L
207987 144.64 UG/L
163983 106.01 UG/L
142896 108.58 UG/L
28113 1790.52 UG/L
213877 113.61 UG/L
109388 118.59 UG/L
90864 109.67 UG/L
11498 3021.66 UG/L
q
97 99 99 98 92 97 97 86 98 94 98 71 71 100
98 98 96 89 93 97 98 86 97 97 86 72 98 95 90 92 85 96 92 96 91 87 88 88 85
177
DUP050308155
QUANT REPORT
Page 2
Operator ID: TLN-262 Output File: ',ISOl4::D7 Data File: >ISOI4::D9 Name: VSTD100 100 PPB IC Misc: -TLN @WL %C +)CEO-V =1
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960924 13:50 960924 13:23
1.00000 HP03046
ID File: 12*6390: :DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-1,3-Dichloropropene 45) trans-l,3-Dichloropropene 46) 1,1,2-Trichloroethane 47} Dibromochloromethane 48} Bromoform 49} trans-l,4-Dichloro-2-Butene 50) *Chlorobenzene--d5 51) 4-Methy1-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hejianone 56) 1,2-Dibromoethane 57} Chiorobenz ene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) Styrene 63) Cumene 64) 4-Bromofluorobenz ene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) 1,3-Dichlorobenzene 68) l,4-Dichlorobenzene 69) l,2-Dichlorobenzene
* Compound is ISTD
R.T. Q ion
10.89 43.0 11.01 83.0 11.48 63.0 11.67 75.0 12.49 75.0 12.75 97.0 13.32 129.0 15.41 173.0 16.19 53.0 14.16 117.0 11.91 43.0 12.06 98.0 12.16 91.0 12.96 164.0 13.13 43.0 13.48 107.0 14.20 112.0 14.37 106.0 14.54 106.0 14.67 70.0 15.12 106.0 15.14 104.0 15.66 105.0 15.89 95.0 16.11 83.0 16.17 110.0 17.50 146.0 17.63 146.0 18.19 146.0
Area
151671 199052
64170 159532 155208
92848 178145 142643 109109
99855 94445 240894 264087 96039 62798 151196 192360 84978 210645 101788 102538 183720 286845 193449 165681 40460 152661 179375 153412
Cone
Units
115.44 UG/L 102.01 UG/L 119.90 UG/L
109.48 UG/L 110.76 UG/L
109.30 UG/L
117.61 UG/L
140.43 UG/L
295.50 UG/L 50.00 UG/L
114.79 UG/L 101.85 UG/L 112.59 UG/L 117.66 UG/L 132.26 TJG/L
108.56 UG/L 107.06 UG/L 110.73 UG/L 220.86 UG/L
109.64 UG/L
107.51 UG/L 108.32 UG/L
102.58 UG/L 117.06 UG/L
113.32 UG/L
107.02 UG/L
117.94 UG/L
122.66 UG/L 125.10 UG/L
q
97 96 90 88 92 96 98 98 89 84 90 97 99 98 97 94 85 95 95 91 93 81 98 82 92 62 91 90 87
178
DUP050308156
Data File: >IS0I4 Name: VSTD100 100 PPB IC Misc: ~TLN @WL %C +}CEO-V =1 Quant Time: 960924 13:50 Injected at: 960924 13:23
Quant Output File: AIS0I4 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
Compound No: 15
compound Name: Allyl Chloride
Scan Number: 287
Retention Time: 5.16 min
Quant Ion: 41.0
Area:
117035M
Concentration:
124.37 UG/L
q-value: 0
This report was produced by QAREA at: 3:39 PM TUE., 24 SEPT, 1996
JL #
DUP050308157
TOTAL ION CHROMATOGRAM
Data File: >ISOI5::D9 Name: VSTD200 200 PPB IC
Mise: -TLN @WL %C +>CEO-V =1
Quant Output File: AISOI5::D7 Instrument ID: HP03046
Id File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLN-262 Quant Time : 960924 14:23 Injected at: 960924 13:56
180 DUP050308158
QUANT REPORT
Page 1
Operator ID: TLN-262
Output File: AISOI5::D7 Data File: >ISOI5::D9
Name: VSTD200 200 PPB IC Misc: ~TLN @WL %C +}CEO-V =1
Quant Rev: 7
Quant Time
Injected at
Dilution Factor
Instrument ID
960924 14:23
960924 13:56 1.00000
HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcai Time: 960919 06:34
Compound
1) *Bromochloromethane 2) Dichlorodifluoromethane 3) Chloromethane 4) Vinyl Chloride 5) Bromomethane 6) Chloroethane 7) Trichlorofluoromethane 8) Ethyl Ether 9) Acrolein 10) 1,l-Dichloroethene 11) Freon 113 12) Acetone 13) Methyl Iodide 14) Carbon Disulfide 15) Allyl Chloride 16) Methylene Chloride 17) t-Butyl Alcohol 18) Acrylonitrile 19) Methyl t-Butyl Ether 20) trans-1,2-Dichloroethene 21) l,l-Dichloroethane 22) cis-l,2~Dichloroethene
23) 2-Butanone 24) Propionitrile 25) Ethyl Acetate 26) Methacrylonitrile
27) Tetrahydrofuran 28) Chloroform 29) Cyclohexane 30) 1,2-Dichloroethane-d4 31) 1,2-Dichloroethane 32) *1,4-Difluorobenzene
33) Vinyl Acetate
34) 1,1,1-Trichloroethane 35) Carbon Tetrachloride 36) Isobutyl Alcohol 37) Benzene 38) Trichloroethene 39) 1,2-Dichloropropane 40) 1,4-Dioxane
R.T. Q ion
8.19 128.0 2.28 85.0 2.45 50.0 2.61 62.0 3.04 94.0 3.17 64.0 3.57 101.0 4.09 59.0 4.30 56.0 4.45 96.0 4.52 101.0 4.62 43.0 4.72 142.0 4.84 76.0 5.18 41.0 5.43 84.0 5.84 59.0 5.93 53.0 6.03 73.0 5.97 96.0 6.76 63.0 7.80 96.0 7.85 43.0 7.94 54.0 7.98 43.0 8.18 67.0 8.27 42.0 8.36 83.0 8.71 56.0 9.13 65.0 9.25 62.0 9.85 114.0 6.91 43.0 8.62 97.0 8.89 117.0 9.21 41.0 9.22 78.0 10.23 130.0 10.57 63.0 10.80 88.0
Area
Cone
Units
34578
50.00 UG/L
334455 177.92 UG/L
118801 222.63 UG/L
140669 213.88 UG/L
118622 164.29 UG/L
58558 135.12 UG/L
183719 297.58 UG/L
116651 194.41 UG/L
129044 1426.64 UG/L
148758 212.41 UG/L
596527 380.05 UG/L
58852 262.07 UG/L
557135 277.83 UG/L
421692 344.79 UG/L
249270M 248.22 UG/L
166208 196.67 UG/L
98815 1620.35 UG/L
201750 1162.96 UG/L
410933 182.26 UG/L
177567 205.58 UG/L
328000 194.89 UG/L
182049 210.77 UG/L
68000 249.65 UG/L
73866 1268.53 UG/L
204719 224.23 UG/L
126273 559.40 UG/L
44949 234.14 UG/L
404627 184.42 UG/L
223499 200.90 UG/L
268236 168.35 UG/L
303088 180.34 UG/L
137478
50.00 UG/L
452398 295.77 UG/L
322036 195.71 UG/L
302671 216.21 UG/L
63292 3789.72 UG/L
422244 210.87 UG/L
216744 220.92 UG/L
193131 219.14 UG/L
23785 5876.42 UG/L
q
92 99 99 99 94 97 98 85 98 95 98 68 71 100
97 97 96 91 94 98 97 85 94 97 84 81 99 93 91 91 87 94 91 98 93 88 84 88 85
131
t "*"-"iTWwtr jrlBifiniirfn^jOT^
DUP050308159
QUANT REPORT
Page 2
Operator ID: TLN-262 Output File: AISOI5::D7 .
Data File: >ISOI5::D9
Name: VSTD200 200 PPB IC Misc: -TLN @WL %C +)CEO-V =1
Quant Rev: 7
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
960924 14:23 960924 13:56
1.00000 HP03046
ID File: IA6390::DB
Title: 3/90 SOW Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
41) n-Propyl Acetate 42) Bromodichloromethane 43) 2-Chloroethyl Vinyl Ether 44) cis-l,3-Dichloropropene 45) trans-l,3-Dichloropropene 46) 1,1,2-Tfichloroethane 47) Dibromochloromethane 48) Bromoform 49) * trans-l,4-Dichloro-2-Butene 50) *Chlorobenzene-d5 51) 4-Methyl-2-Pentanone 52) Toluene-d8 53) Toluene 54) Tetrachloroethene 55) 2-Hexanone 56) 1,2-Dibromoethane 57) Chlorobenzene 58) Ethylbenzene 59) m+p-Xylene 60) Isoamyl Acetate 61) o-Xylene 62) Styrene 63) Cumene 64) 4-Bromofluorobenzene 65) 1,1,2,2-Tetrachloroethane 66) 1,2,3-Trichloropropane 67) 1,3-Dichlorobenzene 68) 1,4-Dichlorobenzene 69) 1,2-Dichlorobenzene
* Compound is ISTD
R.T. Q ion
10.90 43.0 11.01 83.0 11.48 63.0 11.68 75.0 12.50 75.0 12.75 97.0 13.32 129.0 15.40 173.0 16.19 53.0 14.16 117.0 11.92 43.0 12.06 98.0 12.17 91.0 12.96 164.0 13.13 43.0 13.48 107.0 14.20 112.0 14.37 106.0 14.54 106.0 14.68 70.0 15.12 106.0
15.14 104.0 15.66 105.0 15.89 95.0 16.10 83.0 16.16 110.0 17.49 146.0 17.62 146.0 18.18 146.0
Area
323088 414379 135993 317275 318054 196142 379544 306469 220053 108763 208644 501828 513395 190592 141304 313481 405697 171511 423289 213728
199948
383419 611983 408620 331906
82477 321589 375273 315996
Cone
Units
231.19 UG/L 199.64 UG/L
238.89 UG/L 204.70 UG/L 213.39 UG/L
217.07 UG/L
235.56 UG/L 283.64 UG/L 560.28 UG/L
50.00 UG/L 232.82 UG/L 194.79 UG/L 200.96 UG/L 214.38 UG/L 273.23 UG/L 206.65 UG/L 207.30 UG/L 205.18 UG/L 407.46 UG/L 211.35 UG/L
192.47 UG/L
207.54 UG/L 200.93 UG/L 227.00 UG/L
208.42 UG/L 200.30 UG/L 228.11 UG/L 235.60 UG/L 236.58 UG/L
q
96 94 88 88 92 95 97 98 90 85 91 96 99 99 98 93 85 94 95 91
91
84 96 79 95 63 88 88 85
18 o
DUP050308160
Data File: >IS0I5 Name: VSTD200 200 PPB IC
Misc: ~TLN @WL %C +}CEO-V =1
Quant Time: 960924 14:23 Injected at: 960924 13:56
Quant Output File: 'IS0I5 Instrument ID: HP03046
Quant ID File: IA6390 Last Calibration: 951122 10:44
Compound No: 15
Compound Name: Allyl Chloride
Scan Number: 288
Retention Time: 5.18 min
Quant Ion: 41.0
Area:
249270M
Concentration:
248.22 DG/L
q-value: 0
This report was produced by QAREA at: 3:43 PM TOE., 24 SEPT, 1996
i8S
DUP050308161
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DUP050308162
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DUP050308163
7A VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: LANCASTER LABS
Contract: _______.
Lab Code: LANCAS Case No.: ________. SAS No.: _______ . SDG No.: _______ .
Instrument ID: HP03460
Calibration Date: 09/25/96 Time: 0026
Lab File ID: >GSPS1
Init. Calib. Date(s): 09/24/96
09/24/96
Heated Purge: (Y/N) N
Init. Calib. Times:
0140
0349
GC Column: DB624
ID: 0.53(mm)
COMPOUND
Chloromethane Vinyl Chloride Bromomethane Chloroethane 1,1-Dichloroethene Acetone Carbon Disulfide Methylene Chloride 1,2-Dichloroethene (total) 1,1 -D ich loroethane 2-Butanone Chloroform l,2-Dichloroethane 1,1,1-Trichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane cis-i,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane Bromoform 4-Methyl-2-Pentanone Toluene
Tetrachloroethene 2-Hexanone Chlorobenzene Ethylbenzene Xylene (total) Styrene
Mi n
Ma x
SEF RRF 50 RRF %D %D
====== sasasasassiSB cnsrassss ===== a=g--
1.194 1.173
.811 .617 .940 .292 2.767 1.409 1.179
1.355 1.297 0.100
.765 0.100 .697
.962 0.100 .284 2.805 1.189
1.214
-13.5 -10.6 25.0
5.6 25.0 -12.9
-2.3 25.0 2.6
-1.4 ,15.6
-3.0
2.265 .330
2.552 1.679
.456 .465 .731 .386 .350 .661
. 530 .454 .317 .660
.604 .347 1.049
.512 .228 .918 .357
.442
.803
2.356 0.200 .399
2.612 0.200
1.678 0.100 .472 0.100 .458 0.100 .735 0.500 .385 0.300 .337
.646 0.200 .530 0.200 .453 0.100 .297 0.100 .628 0.100
.582 0.100 .313
1.021 0.400 .493 0.200 .205
.871 0.500 .366 0.100
.441 0.300 .777 0.300
-4.0 25.0 -20.9
-2.3 25.0 .0 25.0
-3.4 25.0 1.4 25.0 -.6 25.0
.2 25.0 3.7 2.2 25.0
-.0 25.0 .3 25.0
6.3 25.0 4.9 25.0 3.6 25.0 9.8 2.7 25.0 3.7 25.0 10.2 5.1 25.0
-2.6 25.0
.2 25.0 3.2 25.0
"--AiE ilsl 'oirtjhgegr^scro...m......p...o'"uj njds1 m'-l -uxs-t me. et a minimum RRF of o.oio.
page 1 Of 2
FORM VII VOA
OLM03.Q
136
A.
DUP050308164
7A VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: LANCASTER LABS
Contract: _______.
Lab Code: LANCAS Case No.: _______ . SAS No.: _______ . SDG No.: _______ .
Instrument ID: KP03460
Calibration Date: 09/25/96 Time: 0026
Lab Pile ID: >GSFS1
Init. Calib. Date(s): 09/24/96
09/24/96
Heated Purge: (Y/N) N
Init. Calib. Times:
0140
0349
GC Column: DB624 ID:
0.53(mm)
COMPOUND
1,1,2,2-Tetrachloroethane
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
.. SET" RRF RRF 50 RRF
.648 .587 0.300
1.504 1.625 1.072 1.062
.842 .845 0.200
"MAX %D %D
9.3 25.0
-8.0 1.0 -.3 25.0
page 2 of 2
FORM VII VOA
OLM03.0
i8
DUP050308165
X h Tw L T fttv C H M ^ 11 iri S? *3*
,,v* ^ -F I
vc: mono Tic-
80*:-
one, ,,pr
13.-, t a V- l e : SGBF31 : : l^i
Name : USTDUSO
050 ppb
M- -.c : ~SOM %C IdWi, =1 +>
CC &t
*5
Quant Output File! ''GSHS1 : : Ff. I ns t r ume nt IB ! HPtll-^KO
Id Fi Le: IM-'l390 : ! UB T* -3. ie : 3,'"90 Water/Mad Sot 1 ID 1' i i c da st. Ca libration: 951 2 0 ? 01 : 59
f o r I n.r. t. . H > '!! 3 4b i Last. Qcal Time :
yyijyiM
02
Operator ID : Quant Tx me i .1 njectcd 3 T. I
96 l!H25 9KI1H25
01) i52 0U ! 26
188
DUP050308166
Ope r at or ID'
983
Or-* pu* File: i'Cstpsi i : Ftf
beta File;
>09931 : : D4
Name ; OSTDOS'U
Ohil ppfi
H-sc ; ~i5HM SsC yWL ~1 *>
CC 8.5
*5
OFMNT ijuant Re'.'
y yu.-int Tune
j. f _ t <-- < (? .i ci u Dilution Factor
I r.t r urn e n t ] 1!
CjfC- : u' I C
1jI J
1 s; :: i i;
H- '
ID File; IH4330 : : DB Title: 3,'90 LJater/Med Boil ID File La;:.* Co .! i far at ion : 95120? 01:59
for
Inst, HP034SG Last Qcal
Time
9n0H29 02 : 44
Compound
1) 2J 3 'i 41 5j 6 -5 /X
8 9) 'Mi.
ii 3
3)
l --I ? 15) 16 17 ) `I LJ
i y .i *j 11 ^
2i ' 2V ' '} 1 * : /\ .
*Bromochlorcimethane
Ch;nromnthane
Cimil Chloride
Brnrnomi" thane
Chloroet ha-ne
1 * .! - D x c h 1 c r o e t he ne
Pice tone
Car bon Du sulfide
Methylene Chloride
tr nns- 1 > 2 - iJichloroethcne
1 ,i-l'ichicroethnne
t . - 1,2--Uichloroet' \ene
But. arinne
Ch ! q i*p form
1 ,2-Etichloroethane -d4
1 .,V-D:.ohicroethane
*1. ; 4-Di f luornbensene
1 ;. 1 / l-Trschlorort.hane
Carbon Tetrathloride
Benzene Trichloroethene
1 ;V-LO chloropropane
Bromodic h lor-met ha ne
- - - d -2 Tl ^ ~ U 1 -
^
~
R , T. Q ion
9.49 3.29
3.53
4.0?
4.28
c*.
_>
,.
99
b ,i x. s'
Fi .. 84
. .."ji tJU i x1 xL
12
13
9 , 63
10 40
1!! . 52
11 . 09 9 . 32
10 . 18
1 0 . 49
11 . 48
11 .80 12 o -> r *"i "v
128 .
SB
62 . 9"-'!
64
96
43 . 0 76 . n 84 . 0 96 . 0 63 . c 36
43
83 . 0 65 0
67 . 0 11 4 . 0
97 . 0 117 0
78 . 0 13 U . 0
.0 83 . 0
Area
Co nc
8- u
e, o -i `~i
78265
445 0 0 40512
5 5 919 5
16539 168083
691 23 65.2 97 136887 74881 -> I; -j cl C;
15 183 0 34447 97567
243 -176 1 'J 48 19 111674 l-'9U3ii
93803 8 2 099 157386 1 . U > 1 W ___
50 00 6 '! 89 59
5!! 70
58
58
c . 23 t-. .71
49 12 C.. 1 : .7?
.j J . 0 2
5 29
6 6 42
5 J. .55 b 4 . 37
5V . 00 L., 0 . 0 0 5 v . 67 *4 0 . 12
. 45 t2. 0 . 73 5 il .97 4 y . 59
..j.y ...
ug-'L ug/L
ug -'L
uo/i. ug. 'L uq/.,
ug'L ug-'L ug 'L ug ' ug -
uq..--L ug--'L ug--'L uq- 'L ug-- I i ug.-- ti ug 1. ug.. 7it-J Ug- 'L uq. 'L
56 c
98
c;7
94 Cl I
Mci
|i!!: y9 yu y& 96
ci O
9b 96 83 y1 88 98 91 95 82 9^
75 ' 'J -* `
' > 1../ 1
23 811; y :l yV ;
0-
* r a ns -1,3-Dichloroprope ne
i . x>2-Triehioroethane iibromoc h10r omet hane B;nmoform *Ch10 r 0 be nsene-d5 4 Me t hy J - 2 - 8 e n t an 0 ne? Toluene- d8 T;i i uenc Tetrachloroethe ne
13.67 13.94 14- 52 16.61 15.36 13.07 13.26 13.36 1 4.16
75 97 5 v9
173 117
43 yfc: 91 164
0 il 0 0 0 0 0 0 0
114 8 5 6
723 46; 152677
14 i 8 2 0 197202
61734 2099-0 2 01272
9 77 ns
5 4 . *7 -Zi ug-'L
4K . 74 u q 7 L 47 . 33 aq/L
4:-: . 10 ijq/L 5 0 . 0 0 uq.-'L 57 . 3f/ ug-'L 5 0 . 14 UC; ''L C. * ! *7 V uq/L '-i 8 . 26 u g' L
DUP050308167
94 94 93' 3G 92 9S
l_J L.
9C
QUMNT REFUK?
Or<r:rat.-.r III: SHM~983
Oat pat F3. 1 : ~UHPS1 : : FM
D.-vf.e. F'.Je:
> CHFF/i : : D4
Home; USTUOSO
05 0 ppb
Mt-ic : "Sf-'M %C- U1. =1 + >
CC
Quant
kew:
7 Qr-.-mt Time :
in'acted ,nt 1) i lutio n F a c t n r ;
Instruinerit if 1
3n':
yt-!f
HFi:
U !.1 : fc SI! !!*;!
ID File: If-l '!:^9 0 : : DB
Title:
Uator/Med. Sc 1 ID File
Oast Calibration: 95120? Q1 :t>9
for
Inst . HK0346M Last ^cal Time :
9k 0324
02 : <=*4
Compound 4:? 1,1 ^2,2-Tetrachloroethane * Compound is 1.5TD
R.T. Q ion 17.28 88.0
Area 115852
Cone
Units
4K . 06 i.iq "i.
9i;
19(
DUP050308168
Quant ID File: IA4330::DB
Title: 3/90 Uater/Med Soil ID File for Inst. HP03460
Last EDIT Date: 960725 11:46
Last .Calib Date: 951207 01:59
Last Qcal Date: 960925 00:26
Calib File: CB3904::DB
Qcal File: y'G5PSl: 14906 :FM
/.
RT Window C+min -%) Max Hits/Compound Minimum Area Peak/Base Peak Ratio Up Slope Sensitivity Down Slope Sensitivity
.2000 5
50 40.00 .2000000 .0000000
%
Subtraction Method Ignore max check Auto Qdel Method Quantitate Using Units of Cone Bunching
2 NO
5 AREA
ug/L -1
Number of Compounds! 41
Comp No .
Compound Name
Retention Time (Type > Min. (Rel)
R.F .
Cone .
1) *Bromoc hloromet hane 2) Chloromethane 3) Uinyl Chloride 4) Bromomethane
Cl) ; CT)
XT) CT)
9.49 C 3.29C 3 .53C 4.07C
1.000) .347) .372) .429)
l.ooooo 1.35493 1.29701
.76550
50.00 50.00 50.00 50.00
5) Chloroethane 6) 1,1-Dichloroethene
XT) CM)
4.2SC 5.86 C
.451) .618)
. 69690 .96152
50.00 50.00
7) Acetone
CT)
5 .93 C .631)
.28434
50.00
8) Carbon Disulfide
CT) 6 .27C .661)
2.80539
50.00
9) Methylene Chloride
CT)
6.84C .721)
1.18907
50.00
10) trans-1,2-Dichloroeihene
CT) 7.37C .777)
1.21425
50.00
11) 1,1-Dichloroethane
CT)
8.12C .855)
2.35648
50.00
12) cis-1,2-Dichloroeihene
-CT)
9.12C .961)
1.21425
50.00
13) 2-Butanone
. CT)
3.13C .962)
.39889
50.00
A 14) Chloro form
A 15) 1,2-Dichlaroethane~d4 16) 1,2-Dichloroethane
. CT) CS> XT)
9.63C 1.015) 10.40C 1.096) 10.52C 1.108)
2.61181 1.62470 1.67837
50.00 50.00 50.00
17) *1,4-Difluorobenzene
A 18 ) 1,1,1-Trichloroethane
CD 11.09C 1.000)
CT)
9.92 C .895)
1.00000 .47158
50.00 50.00
19 ) Carbon Tetrachloride
CT) 10.18C .918 )
.45846
50.00
20) Benzene
(M) 10.49C .946)
.73531
50.00
21) Trichloroethene
CM) 11.48C 1.036)
.38527
50.00
22) 1, 2-Dichloropropane
CT) 11.80C 1.064)
.33717
50.00
23) Bromodichloromethane
CT) 12.22 C 1.102)
.64821
50.00
24) cis-1,3-Dichloropropene
CT) 12.87C 1.161)
. .53004
50.00
25) trans-1,3-Dichloropropene
CT) 13.67C 1.233)
.45272
52.10
26) 1,1,2-Trichloroethane
CT) 13.94C 1.257)
.29714
50.00
27) Dibromochloromethane 28 ) Bronio form 29 ) *Chlorobenzene-d5
<T)
CT) CD
14.52 C 1.309)
16.61C 1.438 ) 15.36C 1.000 )
.62789
.5e248 1.ooooo
50.00
50.00 50.00
30) 4-Methyl-2-Pentanone
. CT) 13.07( .851)
.31305
50.00
31) Toluene-dS
CS) 13.26 C .863)
1,06170
50.00
32) Toluene
CM) 13.36 C .870)
1.02064
50.00
33 ) Tetrachloroethene
CT) 14.16C .322)
.43319
50.00
34) 2-Hexanone
(T) 14.29 C .930 )
.20467
50.00
35) Chlorobenzene
CM) 15.41C
36) Ethylbenzene
XT) 15.5SC
' 37) m+p-Xylene
CT) 15.73C
-38) - o-Xylene -- --......................- ------------------- --tTi - -16.32 C
39) Styrene
. CT) IS.33 C
40) 4-Broroofluorobenzene
CS) 17.09C
41) 1,1,2,2-Tetrachloroethane
CT) 17.28C
1.003) 1.013) 1.024) 1.062) 1.063) 1.113) 1.125)
.87102 .36642 .44111 - -*-4414-1.77717 .84478 .58748
50.00 50.00 100 .d|)91 -------- -O-j-0Q--_
50.00
5U .00 50,. 00
* Compound is 1STD
J V)C L t'.y *| {, .-r '
* `A
lJ
DUP050308169
7A VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: LANCASTER LABS
Contract:
T,ab Code: LANCAS
Case No.: _______. SAS No.: _______ . SDG No.:
Instrument ID: HP03046
Calibration Date: 09/19/96 Time: 0634
Lab File ID: >ISJS1 Heated Purge: (Y/N) N
Init. Calib. Date(s): 08/20/96 Init. Calib. Times: 2025
08/20/96 2246
GC Column: DB624
ID: 0.53(mm)
COMPOUND
Chloromethane Vinyl Chloride Bromomethane Chloroethane 1,l-Dichloroethene
Acetone Carbon Disulfide Methylene Chloride 1,2-Dichloroethene (total) 1,l-Dichloroethane
2-Butanone Chloroform l,2-Dichloroethane 1,1,l-Trichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane
cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane Bromoform 4-Methyl-2-Pentanone Toluene Tetrachloroethene 2-Hexanone Chlorobenzene Ethylbenzene Xylene (total) Styrene
WF
MlN RRF 50 RRF
1.120 1.188 1.191
.733 1.172
.370 3.086 1.601
1.348 2.562
.415 3.001 2.304
.542 .412 .777 .365
.341 .710
.576 .535
.328 .536 .344 .460 1.222 .404 .297 .911 .381 .468 .851
.772 .951 0.100 1.044 0.100
.627 1.013 0.100
.325 1.769 1.222 1.249
2.434 0.200
.394 3.173 0.200 2.430 0.100
.598 0.100 .509 0.100 .728 0.500 .357 0.300
.321 .755 0.200
.564 0.200
.542 0.100
.329 0.100 .586 0.100 .393 0.100
.412 1.174 0.400
.409 0.200 .238 .900 0.500 .384 0.100 .478 0.300
.849 0.300
MAX %D %D
31.1 19.9 25.0 12.3 25.0 14.5 13.6 25.0 12.2 42.7 23.7
7.3
5.0 25.0 5.1 -5.7 25.0 -5.5 25.0 -10.4 25.0 -23.6 25.0 6.3 25.0 2.2 25.0 6.0 -6.3 25.0 2.1 25.0 -1.3 25.0
-.2 25.0 -9.3 25.0 -14.2 25.0 10.4
3.9 25.0 -1.2 25.0 20.0
1.2 25.0 -.9 25.0 -2.0 25.0
.2 25.0
All other compounds must meet a minimum RRF of0.010.
page 1 of 2
FORM VII VOA
OLM03.0
19 S
DUP050308170
7A VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: LANCASTER LABS
Contract: _______.
Lab Code: LANCAS
Case No.: _______. SAS No.: _______.
SDG No.:
Instrument ID: HP03Q46
Calibration Date: 09/19/96 Time: 0634
Lab Pile ID: >ISJS1 Heated Purge: (Y/N) N
Init. Calib. Date(s): 08/20/96 Init. Calib. Times: 2025
08/20/96 2246
GC Column: DB624
ID: 0.53(mm)
COMPOUND
Mf
ur
RRF 50 RRF
%D
~T3S3? %D
1,1,2,2-Tetrachloroethane
.757 .732 0.300
3.3 25.0
1,2 -Dichloroethane-d4
Toluene-d8 4-Bromofluorobenzene
2.133 2.304
1.220 1.184 .855 .828 0.200
-8.0 2.9 3.2 25.0
page 2 of 2
FORM VII VOA
OLM03.0
19 S
DUP050308171
T0TOL JON CHROHftTGSRAH
Data File: >ISJS1::D3
Name: OSTDU50
U50 PPB CC
Hi sc: ~SAH |3WL 9SL =1 + >
Quant Output File: 'S1S3S1::D7 instrument ID: HP03046
Id File: 1A6390::OB
Title: 3/90 SOW Water/hed Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960917 12:33
Operator ID: SAM=983 Quant Time : 960919 06:58 Injected at: 960919 06:34
194
DUP050308172
QUANT REPORT
Page 1
Liperator ID: SAM=y83
Uutpu t File: '' 1SJS1: : D7
(Js t a File:
)iSJSI::D3
Na me: MSID050 05 0 PPB CC
nisc: -BAM |SWL %L =1 + >
Quant
Key:
7 Quant Time: In jected at:
Dilution Factor: Instrument ID:
960919' 0b: 58 9609191 06:34
1. . 0 LI U U 0 HP03046
ID File: IA6390::DB
1 11 ie : 3790' 8L!W Ulater/Msd Soil ID File for Inst . HP03U46
Last Calibration: 951122 10:44
Last Qcal Time: 960917 12:33
Compound
1.) JLi S 3) 4? t?> 6) 7) 8) V> ID) ii / 12 > 17 ) 14) 1*7 ) 16 ) 17 ) 18) 19) 20) A 1J 22) 23 J 24) 2"? ) 26 ) 27 5 28 5 29 3 30 ) 31) 32 ) 33 3 34 ) 33 2
) 37) 38 ) 39 ) ^0 )
*t)rornoch lor owe thane Chlorome thane Vinyl Chloride Br omomethane Chloroethane 1,1-Cichloroethene Acetone Carbon Disulfide Methylene Chloride trans-l,2-Dichloroethene 1 ,l-Dichloroethane cls-1,2-Dichloroethene 2-Uutanone Chloroform 1,2-Oichloroethane-d4 1,2-Dichloroethane
*1,4-Difluorobenzene X,1,1-Trichloroe thane Carbon Tetrachloride Benzene 1richloroethene 1,2-Dichloropropane Hromodichloromethane cis-l,3-Dichloropropene t rans-1,3-Dich1oropropene
1,1,2-Tr ichloroethane Uibromochloromethane Bromoform *Lh 1o robenzene-d5 4-Methy 1-2-Pentanone !o1uene-dB To 1uene letfachloroethene 2-Hsxanone Chlorobenzene E_t hy lbenzene
m+p-Xylene o-Xylene St yrer.e 4-Bromofluorobenzene
R.T. Q i on
8.34 2.57 2.74 3.17 3.31 4.65 4.77 5.05 5.61 6.13 6.91 7.94 7.99 8.50 9.29 9.41 ID. 01 8.77 9.05 9.37 10.40 10,72 11.17 11.83 12.63 12.90 13.48 15.57 14.33 12.05 12.21 12.31 13.10 13.27 14.36 14.53 14.70 15.28 15.31 16.05
128.0 50. 0 62.0 94. 0 64. 0
96. 0 43.0 76.0 84.0
96. 0 63.0 96.0 43.0 83.0 65.0 62.0 114.0
97. 0 117. 0
78.0 130. U
63.0 83. 0 75.0 75.0 97. 0 129.0 173.0 117. 0 43.0 98.0 91.0 164. 0 43.0 112.0 106.0 106.0 106.0 104,0 95.0
Area
3 0/09 23696 29205 32062 19244 31098
9972 54310 37527 35489 74735 41219 12095 97426 70/54 74628 129120 77270 65/39 94034 46U/3 41386 974/0 72787 72/94 42432 75663 50739 94592 38970 112029 111095 3866 0 22489 85105 36349 92874 45175 80336 78276
Lone
Units
q
50.00 UG/L
yli
41.67 UG/L
99
42.56 UG/L
95
56.05 UG/L
96
49.97 Uls/L.
V5
42.96 UG/L
90
38.34 UG/L
68
27.06 UG/L
100
44. 41 UG/L
97
41.34 UG/L
96
46.48 UG/L
9S
48.01 UG/L
96
37. 49 UG/C
96
50.95 UG/L
98
55.0 0 UG/L
87
52.72 UG/L
93
.50.00 UG/L
86
53.72 UG/L
90
51.72 UG/L
98
43.43 UG/L
90
46.79 UG/L
84
43.92 UG/L
94
5 0.22 UG/L
95
46.45 UG/L
87
49.68 UG/L
90
46.69 UG/L
96
51.38 UG/L
97
50.13 UG/L
99
50.00 UG/L
85
39.37 UG/L
90
47.32 IJG/L
98
44.43 UG/L
99
46.93 UG/L
97
37.71 UG/L
96
46.46 UG/L , . 86 45.68 UG/L 19 b>94
93.52 u g /l
95
45.49 UG/L
91
46.20 UG/L
84
49.29 UG/L
75
DUP050308173
QUANT REPORT
('age
Operator ID: SAM=983
Uutput File: '"'1SDS1 ::D7
Data Filet
>ISJS1::D3
Name: OSTDObti
05 0 PPB CC
Misc : -SAM WL S6C "1 +>
Quant
Reu>:
7 Quant Time: Injected at:
Dilution Factor: Instrument ID:
960919 06:58 96 UV19 06 :34
1. 00000 HP03 U46
ID File: 1A639U::D6
Title: 3/9 0 SOU Water/Med Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960917 1 2:33
Compound 41) 1,i,2,2-Tetrachloroethane * Compound is IS I'D
R.T. Q ion 16.26 83.0
Area
69249
Cone
On i ts
43.39 UC/L
q 95
196
DUP050308174
yuant ID File: IA6390::DB
title: 3/90 SOW Water/Med Soil ID File for Inst HPQ3U46
Last EDIT Date: 960129 11:59
Last Caiib Date
Last Ueal Date: 960919 06:34
Caiib File
Ocal File: 'MSJS1:14906:D7
951122 10:44 CA39U6::D8
R) Window C+min -%)
:
flax Hi ts/Compound
:
Minimum Area
:
Peak7Base Peak Ratio :
Up Slope Sensitivity :
Down Slope Sensitivity:
.2000 5
90 40.00 .2000000 .01)00000
%
Subtraction Method
Ignore max check
:
Auto Wdel Method
:
Quantitate Using
:
Units of Cone
:
Bunching
:
NO 5
AREA UG/L -1
Number of Compounds: 41
Comp No .
Compound Name
Retention Time C Type) Mxn. CRe 1 )
R.F.
Cone .
1)
2) 3) 4> 5) 6) /> a> 9)
10) 11) 12) 13) 14) 15 ) 16 ) 17) 18) ly)
20) 21) 22) 23) 2 4) 25) 26) 27) 28) 2y) 30) 31)
32) 33) 34) 35) 36 ) 37) 38 ) 3V ) 40 )
*Bromoeh loromethane
Chloromethane Uiryl Chloride Bromomethane Chloroethane 1,1-Dichloroethene Acetone Carbon Disulfide Methylene Chloride trans-1,2-Dichloroethene 1,1-Dichloroethane cis-1,2-Dichloroethene 2-Butanone Ch loroform 1,2-Dichloroethane-d4 1,2-Dichloroethene *1,4-Di 1- luorobenzene 1,1,1--T richloroethene Carbon Tetrachloride Benzene Tr ich loroethene
1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene t rans-1,J-Dichloropropene 1,1,2-Trich1o roethane Dibromochloromethane Bromoform *Chlorobenzene~d5 4-Me t hy1-2-Pentanons loluene~d8 To luene 1 et rachloroethene 2-Hexanone Ch lorobenzene
EthyIbBnzene rn + p-Xy lane o-Xylene Styrene
4-Bromofluarobenzene
C I) 8.34C 1.000)
<T) 2.57C .308)
(T ) 2.74C .329)
CT) 3.17C .381)
IT) 3.31 ( .398)
(M) 4.65C .558)
n) 4.77C .572)
(T) 5.05C .605)
tT) 5.61C .672)
(T) 6.13C .735)
m 6.91C . 829)
CT) 7.94C .953)
<T) 7.99 ( .958)
CT) 8.50C 1.020)
CS) 9.29C 1.114)
CT) 9.41C 1.128)
C I ) 10.01C 1.000)
CT) 8.77C .876)
CT) 9.05 C . y U4)
CM) 9.37C .936)
CM) 10.40C 1.038)
CT) 10.72 (. 1.071)
IT) 11.17C 1.115)
CT) 11.83 C 1.181) CT) . 12.63 C 1.262)
CT) 12.90C 1.288)
( T) 13.48 C 1.346)
CT) 15.57C 1.555)
C I ) 14.33 C 1.0UCI)
CT) 12.05 C .841)
CS) 12.21C .852)
CM) 12.31( CT) 13.1UC
.859) .yi4)
CT) 13.27C .926)
CM) 14.36 C 1.U02)
CT) 14.53 C 1.014)
C7 ) 14.70C 1.026 )
- CT)-/- 15.2SC 1.067) CT) 15.31C 1.U68 )
CS> 16.05C 1.120)
i.aouuo .77163 .95102
1.04406 .62666
1.01267 .32473
1.76854 1.222U2 1.24895 2.43365 1.24895
.39386 3.17256 2.304U2 2.43017 1.00000
.59844 .50913 .72827 .35682 .32052 .75488 .'36372 .542U9 .32862 .58599 .39296 1.ooouo .41198 1.10434 1.17446 .40870 .23775 .89971
.38427 .47758 .47758 .84929 .82751
50.00
50.00 50.00
50.00 50.00
50.00 50.0U 50.00 50.00 50.00 50.00 50. 00 50.0U 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00 52.0 0 50.00 50. UO 50.00 50.00 50.00 50.00 50.00 50.00 50.00 50.00
50.00 100 . Ut)
5 Ol TM (Ml 5 0-Lttf
50.00
41) 1,1,2,2-letrachloroathans * Compound is ISTD
CT) 16.26 C 1.135)
.73208
50 . OU
DUP0503081 75
Raw QC Data
i9S
DUP050308176
TOTAL ION CHROMATOGRAM
Data File: >GSMT3::D4
Quant Output File: '"GSMT3::FM
Name: BFBJUN2S 50nG BFB
Instrument ID: HP03460
Misc: -SAM %C =1 2uL 25ppm BFBJUN28
Id File: IDBFB::DB
Title: TUNER
Last Calibration:
: Last Qcal Time: 920618 19:58
Operator ID: SAM-983 Quant Time : 960924 01:15 Injected at: 960924 01:08
i99
DUP050308177
m/z
50 75 95 96 173 174 175 176 177
GC/MS PERFORMANCE STANDARD
Bromofluorobenzene (BFB)
Ion Abundance criteria
% Relative Abundance
Base
Appropriate
Peak
Peak
8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance
5-9% of mass 95 Less than 2% of mass 174 50-120% of mass 95
4-9% of mass 174 93-101% of mass 174
5-9% of mass 176
26.69 49.05 100.00
6.62
0.00 70.67
5.02 69.37
3.93
26.69 49.05 100.00
6.62
0.00 70.67
7.10 98.16
5.67
Injection Date Injection Time
Data File Scan
09/24/96 01:08
>GSMT3 138
status
Ok Ok Ok Ok Ok Ok Ok Ok Ok
INSTRUMENT HP03460
2oe
DUP050308178
3/90 CRITERIA ANALYSIS DATE/TIME
9/24/96 1:08 INSTRUMENT HP03460
>GSMT3 138
BFBJUN28 50nG BFB -SAM %C -1 2uL 2Sppm BFBJUN28 SUB NRM ENH
File; >GSMT3 Scan #:
m/z
Int.
m/z
36.05
37.05 38.05 39.05 44.05 45.05 46.95 48.15
49.05 50.05 51.05
1.98 9.84 7.70
3.03
1.17 1.63 2.55
.77 6.19
26.69 7.76
52.05 54.95 55.95 57.05 60.15 61.10 62.10 63.00 68.10 69.00 70.10
138 Retn. time: 4.56
Int.
m/z
Int.
m/z
.47
.43 2.12 2.89 1.30 5.26 4.76 3.18 11.56 11.00
.48
72.20 73.00 74.00
75.00 76.10 78.00 79.00 80.00
80.90 87.00
88.00
.32 91.00 4.70 92.00 15.03 93.00 49.05 94.00 4.12 95.00
.45 96.00 2.39 96.90
.77 103.85
2.49 115.85 5.84 116.75 5.27 129.75
Int.
m/z
.52 172.60
2.50 174.00 3.53 175.00 10.24 175.90 100.00 176.90 6.62 207.05
.24 207.95 .31 209.05
.16 280.85 .27 281.15
.09
Int.
.23 70.67
5.02 69.37
3.93 .17 .27 .34 .48 .13
32366.,IS THE AREA OF MASS 95 THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK
APEX (SCAN 138.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING SCAN 127.00 WHICH IS PRIOR TO THE BFB PEAK.
201
DUP050308179
TfiTOL
Tfir-J r.HROtlQTfipBJtt
r.-- "OC* . 0 SLKJ-- BCf** ''JrJ3 C>0r: J B'
''"
TIC
40 SO ISO Ifc'.O
, . t I , l.'l-l....... . B ,l..,l -L .1--1--J..I....... I,..,U.I .
! c'-`i -
0f
r ft 0 0O'*
?40C0 i !
c 00 00-`
ioOUu-i %
1200 CH
40C1*:-. 4
V
i ! i- . ...................ri-rr-rf-TT-v y*
4-
4 -
4 T i-s
5.f
Data F lie: >GHTl : : B4 '
Quant Output Files
Nam: BFBJSIN28 SOnG HFB
Instrument ID:
Mt s c : ~SHM %C "'I 2uL 25ppm BFHJUNVH
' 0 'r, y T1::FM HPO :*i <s h 0
Id tile: iDBFB::DB
Title: TUNER
Laot Co i xbr otiori:
: Last Qua ! Tim"; : 9 2 :lti 18 19: 5t:
Operator ID Quant Time Injected at
SftH-982 SHIfSat Cltl : o? 98L924 28:59
202
DUP050308180
m/z
50 75 95 96 173 174 175 176 177
GC/MS PERFORMANCE STANDARD
Broraofluorobenzene (BFB)
Ion Abundance Criteria
% Relative Abundance
Base
Appropriate
Peak
Peak
8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance
5-9% of mass 95 Less than 2% of mass 174
50-120% of mass 95 4-9% of mass 174 93-101% of mass 174 5-9% of mass 176
27.10 50.07 100.00
6.87
.42 70.19
5.01 68.55
4.52
27.10 50.07 100.00
6.87
.60 70.19
7.13 97.66
6.59
Injection Date: 09/24/96 Injection Time: 23:59
Data File: >GSPT1 Scan: 141
Status
Ok Ok Ok Ok Ok Ok Ok Ok Ok
INSTRUMENT HP03460
DUP050308181
3/90 CRITERIA ANALYSIS DATE/TIME
9/24/96 23:59
INSTRUMENT HP03460
>GSPT1 141
BFBJUN28 50nG BFB -SAM %C =1 2uL 25ppm BFBJUN28 SUB MEM ENH
File: >GSPT1 Scan #:
m/z
int.
m/z
36.05
37.05 38.05 39.05 40.05 44.05 45.05 47.05 47.85 49.05 50.05
1.61
9.65 7.51 2.77
.05 1.14 1.55 2.46 1.15 5.96 27.10
51.05 51.95 56.05 57.05 59.95 61.00 62.10 63.00 68.00 69.00
141 Retn. time: 4.59
Int.
m/z
Int.
m/z
7.86
.21 1.23 3.11 1.09 5.21
3.84 3.04 10.57 9.93
70.00
71.90 73.00 74.10 75.10 76.00 77.10 77.90 79.00 80.00
.90
.45 4.60 15.55 50.07 4.05
.44 .65 2.12 .87
80.90
81.90 86.90 88.00 92.00 93.00 94.00 95.00
96.00 116.95
Int.
m/z
2.30 118.95
.60 147.90 4.96 172.80
5.73 174.00 2.63 175.00
3.26 175.90
9.65 176.90 100.00 206.95
6.87 208.05 .54 281.15
Int.
.32 .20 .42 70.19 5.01 68.55 4.52 .95 .61 .74
31066.,IS THE AREA OF MASS 95
THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK APEX (SCAN 141.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING SCAN 130.00 WHICH IS PRIOR TO THE BFB PEAK.
2G4
DUP050308182
TOTAL ION CHROMATOGRAM
Data File: >IGKT2::D2
Quant output File: *IGKT2::D7
Name: BFB 2uL 50ng BFB
Instrument ID: HP03046
Misc: -SJL %C -1 2uL (25ppm) BFBJUN28
Id File: IDBFB::DB Title:
Last Calibration:
: Last Qcal Time: <none>
Operator ID: SJL-176 Quant Time : 960820 20:01 Injected at: 960820 19:52
20
DUP050308183
m/z
so 75 95 96 173 174 175 17 6 177
GC/MS PERFORMANCE STANDARD
Bromofluorobenzene (BFB)
Ion Abundance Criteria
8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance 5-9% of mass 95 Less than 2% of mass 174 50-120% of mass 95 4-9% of mass 174 93-101% of mass 174 5-9% of mass 176
% Relative Abundance
Base
Appropriate
Peak
Peak
26.46
55.31 100.00
7.23 0.00 56.57
4.49 55.49
3.83
26.46 55.31 100.00
7.23 0.00 56.57
7.93 98.10
6.90
Status
Ok Ok Ok Ok Ok Ok Ok Ok Ok
Infection Date: 08/20/96 Injection Time: 19:52
Data File: >IGKT2 Scan: 133
INSTRUMENT HP03046
206
DUP050308184
3/90 CRITERIA
ANALYSIS DATE/TIME 8/20/96 19:52
INSTRUMENT HP03046
>IGKT2 133
BFB 2uL 50ng BFB -SJL %C =1 2uL (25ppm) BFBJUN28 SUB NRM ENH
File: >IGKT2 Scan #:
m/z
Int.
m/z
35.95 37.05 38.05 39.05 44.05 44.95 48.05
1.40
7.SO 7.01
.72 .30 1.09 .33
49.10
50.10 51.10 56.00 57.10 59.90
61.00
133 Retn. time:
Int.
m/z
Int.
6.32
26.46 7.94 .94 4.10
1.13 5.66
62.10
63.10 68.00 69.05 73.05 74.05 75.05
5.63
3.70 12.49 11.70
5.14
17.26 55.31
4.50
m/z
76.05 79.05 86.95 88.00 92.00 93.10 94.10
Int.
m/z
4.71
2.79 4.68 3.74 2.33 4.04
11.09
95.10 96.10 174.00 175.00 176.00 177.00
Int.
100.00 7.23
56.57 4.49
55.49 3.83
18754. IS THE AREA OF MASS 95 THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK
APEX (SCAN 13 3.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING SCAN 123.00 WHICH IS PRIOR TO THE BFB PEAK.
A
DUP050308185
TOTCtl TON CHROHOTOSRfiM
Bata Files > 1S2JT1: :D2
Quant Output File! ''ISJT1::D7
Name: BF-tJ
2uL 50ng Bf B
instrument IDs HP03U46
nisc: ~Sn %C = 1 2uL (25ppm) BFB0UN28
id File;, lDBF 8: :OB
f 11 1 e :
Last Calibration!
: Last Qcal Time: <none>
Uperator lu: SftF1=9B3 Buant Time : 960919 06:19 Injected at: 96CJ919 06:10
DUP050308186
m/z
50 75 95 96 173 174 175 176 177
GC/MS PERFORMANCE STANDARD
Bromofluorobenzene (BFB)
Ion Abundance Criteria
% Relative Abundance
Base
Appropriate
Peak
Peak
8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance
5-9% of mass 95 Less than 2% of mass 174 50-120% of mass 95 4- 9% of mass 174 93-101% of mass 174
5- 9% of mass 176
26.90 57.89 100.00
6.63
0.00
57.99 4.84
56.13 3.93
26.90 57.89
100.00
6.63
0.00 57.99
8.35 96.79
7.01
Injection Date: 09/19/96 Injection Time: 06:10
Data File: >ISJT1 Scan: 137
Status
Ok Ok Ok Ok Ok ok ok Ok Ok
INSTRUMENT HP03046
to
DUP050308187
3/90 CRITERIA ANALYSIS DATE/TIME
9/19/96 6:10 INSTRUMENT HP03046
>ISJT1 137
BFB 2UL 50ng BFB -SAM %C *=1 2uL (25ppxa) BFBJUN28 SUB NRM ENH
File: >ISJT1 Scan #:
xa/z
Int.
m/z
36.05 37.05 38.05 39.85 43.95 44.95 49.10
1.72 8.41 4.20
.33
.92 1.16 6.69
50.10 51.10 57.10 60.00 61.00 62.00
63.10
137 RetH. time:
Int.
m/Z
Int.
26.90 8.16 3.70 .94
6.44 5.69
4.01
68.00 69.05 73.05
74.05 75.05 76.05 76.85
13.41 12.12
5.37
18.19 57.89
5.58 .37
4.54
m/z
78.95 80.95 86.95 88.00 92.00 93.00 94.00
Int.
m/z
3.04 95.10 3.70 96.10 3.70 174.00 3.95 175.00
2.81 176.00 4.50 177.00
12.23
Int.
100.00 6.63
57.99 4.84
56.13 3.93
20955.,IS THE AREA OF MASS 95 THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK APEX (SCAN 137.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING SCAN 126.00 WHICH IS PRIOR TO THE BFB PEAK.
MJL DUP050308188
TOTAL ION CHROHRTOGRAH__________________________________________________ .
File >ISOTi 35.0-300.0 amu. BFB 2uL 50ng 8FB ~TLN 7.C 1 uL <5f
Data File: >IS0T1::D4
Quant Output File: AISOTl::D7
Name: BFB 2uL 50ng BFB
Instrument ID: HP03046
Misc: -TLN %C ==1 2uL (25ppm) BFBJUN28
Id File: IDBFB::DB
Title:
Last Calibration:
: Last Gcal Time: <none>
Operator ID: TLN-262 Quant Time : 960924 11:18 Injected at: 960924 11:10
2:
DUP050308189
m/z
50 75 95 96 173 174 175 176 177
GC/MS PERFORMANCE STANDARD
Bromofluorobenzene (BFB)
Ion Abundance Criteria
% Relative Abundance
Base
Appropriate
Peak
Peak
Status
8-40% of mass 95 30-66% of mass 95 Base peak, 100% relative abundance
5-9% of mass 95 Less than 2% of mass 174 50-120% of mass 95
4-9% of mass 174 93-101% of mass 174 5-9% of mass 176
21.53 49.65 100.00
7.04 1.14 64.17 4.90 62.76 4.21
21.53 49.65 100.00
7.04
1.78 64.17
7.63 97.80
6.71
Ok Ok Ok
ok
Ok Ok
ok Ok ok
Injection Date: 09/24/96 Injection Time: 11:10
Data File: >IS0T1 Scan: 76
INSTRUMENT HP03046
DU P050308190
3/90 CRITERIA ANALYSIS DATE/TIME
9/24/96 11:10 INSTRUMENT HP03046
>IS0T1 76
BFB 2uL 50ng BFB -TLN %C =1 2uL (25ppm) BFBJUN28 SUB NRM ENH
File: >IS0T1 Scan #
m/z
Int.
m/s
36.05
37.05
38.05
39.15 44.05 45.05 46.95 49.05 50.05 51.05
1.78
6.79 5.56
2.60 .52
1.05 .71
4.93 21.53
6.36
55.05
56.05 57.10
60.00
61.10
62.10 63.00 67.10 68.00
76 Retn. time:
Int.
m/z
Int.
1.58
1.90 2.69
1.29 4.52 4.27 2.77
.56 10.97
69.00
70.10 73.00
74.00
75.00 76.00 77.00 78.00 79.00
10.33
.77
4.07
14.61 49.65
3.97 .65 .21
2.00
4.38
m/z
81.05 81.95 83.15 87.05 87.95 91.05 92.05 93.05 94.05
Int.
m/z
2.45 95.05
.62 96.05 .40 116.80
3.65 142.95 3.66 172.95
. 44 173.95 2.27 174.95 3.52 175.95 10.61 176.95
Int.
100.00 7.04 .16 .47 1.14
64.17 4.90
62.76 4.21
29721..rS THE AREA OF MASS 95 THIS SPECTRUM WAS OBTAINED BY AVERAGING THE SCAN AT THE BFB PEAK
APEX (SCAN
76.00 ) WITH THE TWO ADJACENT SCANS AND SUBTRACTING
SCAN
67.00 WHICH IS PRIOR TO THE BFB PEAK.
fj JLO
DUP0 50308191
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract:
VBLKG24
Lab Code: LANCAS
Case No.: ____
SAS No.:
SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: VBLKG24
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >GSPB1
Level: (low/med) LOW
Date Received: _______.
% Moisture: not dec.
Date Analyzed: 09/25/96
GC Column: DB624
ID: 0.53
Dilution Factor:
l.o
Soil Extract Volume:
(uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3----------------- Chioromethane 75-01-4-------- --------Vinyl Chloride 74-83-9------------------ Bromomethane
75-00-3------------------ Chloroethane 75-35-4------------------ 1,1-Dichloroethene
67-64-1------------------ Acetone 75-15-0------------------ Carbon Disulfide 75-09-2------------------ Methylene Chloride 75-34-3-------------------1,1-Dichloroethane 540-59-0--------------- 1,2-Dichloroethene {total) 78-93-3----------------- 2 -Butanone 67-66-3------------------ Chloroform 107-06-2---------------- 1,2 -Dichloroethane 71-55-6--------- --------- 1,1, l-Trichloroethane
56-23-5------------------ Carbon Tetrachloride 71-43-2------------------ Benzene 79-01-6----------------- Trichloroethene 78-87-5----------------- 1,2 -Dichloropropane
75-27-4----------- ------- Bromodichloromethane 10061-01-5------------ cis-i,3-Dichloropropene 10061-02-6------------ trans-1,3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane 124 -48-1------------- Dibromochloromethane 75-25-2------------------ Bromoform 108-10-1--------------- 4 -Methyl-2 -Pentanone 108 -88-3--------------- Toluene 127-18-4---------------- Tetrachloroethene 591-78-6---------------- 2-Hexanone
108-90-7---------------- Chlorobenzene 100-41-4-- --------- Ethylbenzene 1330-20-7-------------- Xylene (total)
100-42-5---------------- Styrene 79-34-5------------------ 1,1,2,2-Tetrachloroethane
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VOA
OLM03.Q
DUP050308192
=:o ooo-;
J
-i
400
ve il*:
200000-'
ii i . Ki'nnr.4
i >000*V;
-Hit eoooc-j
i i
40000-j
j
1 s
l', ll I<SIti [I
j......:---. 4
-a 3 3i? ii-- `S JL 17
55 J
i* n i !iw ;-....-------r--T--1--
6 8 10 x>
c Ca\J
1
fc m
X. w
- . i i 16 16 0
L)-, u Fi ie: > GSPUl : ; DP
Norris i JBLK 02 4 OBLK.02 4
MiOC !
-ir,
@WL =1 + >
Qaant Output F; le ; instrument ID :
831. HR
"tlSHBI : ;FK p p n 'i c.; jj
I d F i le ! I
9 D * DB
T i 1 e : .3 4 U tiJa t <sr /Mncl Sot l' ID F ilc
ii a s *t Cal ibrat.ion : 95 i 2 O'? 01:53
f or Inst. HF 0348 Last- Qcal Ti me :
360925
0
Op;..: r a lf.r ID: Quant i' i me ; i, I ; Jj 5 ted at :
SRM~983 9 6 U 9 2 5 01 : 29 9fe'i!25 01 : 04
oi Si-1
DUP050308193
Kh *">]?!
Ope rotor ID: SflH-W83
Output File : 'NSSHHl : s FM
Data Fi 1 :
>(..3PB1: : 1)8
Marne : UHLK.G24
UFUCG24
Hiac i ~Sf4M %C jctlilL "1 + >
Oaarit Kev 1 *K396 2 68 IFlPi &5 *5
T*' * : .riant Tme : In.jester a r -
Dilut i on Factor Inst ruiner.t I !:
W ... : V 1 1 ;f*y -j :
ID Fxif?: IR4390 : iDF Title: 3,'SO Uater/Med Soil ID File Last Ca!lbrationt S5I207 01:59
for
Inst . HP 03 46 0 Last ^JjC-Ctl. *1 i Tii r2 !
9- ;?y2b
Compound
1) 15 : 17) 29 ) 31) 40 5
rrBroTnochloroTnethane 1 ;.V-Diohloroethane-d4
*1p4~Difluorobenzene *Cb 1 o r o be. ns e ne - d.5
Toluene-dB 4- Hromot lanraberisene
* Compound xs ISTD
R .T. Q j on
9.50 1U . 42 11.10 15.37 13,27 17.09
128 . 0 65 U
114.0 117.0
8B . 0 95 0
Fir ea
472 73 7120b 18762 0 153010 162,-48 137840
vpnc
3 lj . Ij 0 *4 o b 3 1j . 0 0 5 ' ' 0 0 50 . 09 5 : 36
lO i.(!| i.O
O-i ~s
4 DUP050308194
Lancaster Laboratories Quantitation keport-GC/MS Ooiatiies
LUI: KJ JH JL.K
-3
- -! r-
File: -SSPB1 Injected: 01:04 09/25/96
Sample: UBUCG24
UBLKG24
Dilation Factor:
1.0
Initial De luTie/llt..:
.5.0
Standard: AGSPSl Inst. H8U34t;u
Batch:
G9S2681HA
Final Dolaue/Ut.: 5.0
Method-: 7156 Matrix/Ieuei: liL. Blank;
f Internal Standards
R.T. (+/-RT) Scan Qion
Area(*/-tArea) Cone.
QC Fiao Con: Units * ug-'L
1. Bromochloromethane T'. 1.4-Dirluorobenzene
29 Chiarobenzene-d5 t = r e t e n t io n t ime OUT OF RANGE
3.5014.011.2) 644 128
47273(-13!
50.00
11.101.OB/?) 781 114
187820(-23!
5ll. 0U
15.371.0077) 1148
117
153Q10C-22)
50.00
* - INTERNAL STANDARD AREA OUT OF RANGE
NC * NOT ABLE TO CALCULATE--NO STANDARD.
S Surrogate Standards
R.T. (+/-BET) Scan
Qion
SSSSS5S
15. l,2-Dichloroethane-d4
10.421.00031
723
S5
31. Totuene-dfl
13.275.00U5)
968
98
40. 4-Broaofluorobenzene
17.03(-.000) 1296
35
} = RELttTiOE RETENTION TIME OUT OF RANGE * = *RC OUT OF RANGE
Area
Cone.
.%Rec. Q
71206
46.36
33
162748
50.09
100
132840
51.38
1A t? v
D = SURROGATES DILUTED OFT NC = COULD HOT CALCULATE
S Target Compounds
R.T.(+/-8RT.1
Scan Qion
Area
Cone.A
Conc.B
Cone. Blank Q
Quantitation Limit
2. Chloromethane 3- U-.nyJ Chloride
4. SroiBMiethane 5. Chlornethans S. 1,1-Bichioroethene 7. Acetone 8. Carbon Disulfide 3. Methylene Chloride 11. 1,1-Dichlaroethane 12. 1,2-Dschloroethene (total) 13. 2-Butanone IT. Chloroform 16. 1,5-Dichloroethane 18. 1.1,1-Trichloroethane 19. Carbon Tetrachloride 20 Benzene 21. Trichloroethene 22. 1,2-Biehioropropane 23. Bromodichioromethane 29. cis-lj3-Cichloropropene
25. trars-l,3-Diehloropropene 28. 1 >1 ,2-Tnchloroethane
------------------------------------- --------------------- :---------------------------------------------------------------------------------------------------*---------------- ---------------------------------------------------------------------------
----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- ---------------------------------
--------------------------------------------------------------------------------------------------------------------------------
18 18 ID id 10 1U 10 18 10 10 10 1C 30 111 10 111 10 111 10 10 10 111
ft RAW CONC. 8 = CONC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CAL. RANGE * SVi.ftTJ.OE RETENTION TIME OUT OF RANGE
Lab Chronicle:
Ent. by
PAGE 1 OF 2
Uer.
bu '
asir-*4: ri--
DUP050308195
Lancaster Laboratories Quantitation Heport-GCvMS Uoiaiiies
LLU: U'fciLK
File: AGSPB1 Injected: 01014 119/25/96
Sample: (JBL1CG24
UBUCG24
Dilution Factor:
1.0
Initial Uoiurae/(i)t.:
5.0
Standard: AGSPS1
Inst. HP!i346C
Batch:
G362S8lftft
Final Uolame/ldt.: 5.0
Method: 71Sfc Matm/Ievei. li!!, Blank:
I Target Compounds
27. Dibromochloromethane 29. Bros form 30. 4-Methyi-2-Pentanone 32. Toluene 33. Tetrachloroethene 34. 2-Hexanone 35. Chlorobenzene 30. Ethylhensane 38. Xylene (total) 33. Styrene 41. 1,1,2,2-Tetrachloroethane
Cone.
R.T.f+/-RRT)
Scan Qion
Area
Cone, ft
Conc'.B
Blank 0
issssssssssssssssssssaKzassnsaiasirssasssavesseesBteeesssssseassssissssssssasess'
Quantitation Limn
10 11! IS
10 10
10
IB
113
in
ft = Bull C0NC. B = CUNC. MULTIPLIED BY DILUTION FACTOR E = CONC. OUT OF CftL. RANGE I * RELATIVE RETENTION TIME OUT OF RANGE
Lab Chronicle:
Erst, by
Uer. by
Analyst:
A Auditor:
.Date: Date: PAGE 2 OF 2
DUP050308196
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER LABS
Contract:
VBLKI93
Lab Code: LANCAS
Case No.: _______ SAS No.:
SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: VBLKI93
Sample wt/vol: 5.0
(g/mL) ML
Lab Pile ID: >ISJB2
Level: (low/med) LOW
Date Received:
.
% Moisture: not dec. _______
Date Analyzed: 09/19/96
GC column: DB624
ID: 0.53 (mm)
Dilution Factor:
l.o
Soil Extract Volume: _______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
O
74-87-3------------------ Cb.lorometh.ane 75-01-4------------------ Vinyl Chloride 74-83 -9----------------- Bromomethane 75-00-3------------------ Chloroethane 75-35-4-------------------1,1-Dichloroethene
67-64-1------------------ Acetone 75-15-0------------------ Carbon Disulfide
75-09-2------------------ Methylene Chloride 75-34-3---------- -------- 1,1-Dichloroethane 540-59-0-------------- 1,2-Dichloroethene (total) 78-93-3------------------ 2-Butanone 67-66-3------------------ Chloroform 107-06-2---------------1,2 -Dichloroethane
71-55-6----------------- 1,1,1-Trichloroethane 56-23-5------------------ Carbon Tetrachloride
71-43-2------------------ Benzene 79-01-6------------------ Trichloroethene 78-87-5------------------ 1,2-Dichloropropane 75-27-4----------------- Bromodichloromethane 10061-01-5----------- cis-l, 3-Dichloropropene 10061-02-6------------ trans-1,3-Dichloropropene
7 9 -00-5------------------ 1,1,2 -Trichloroethane 124-48-1---------------- Dibromochloromethane
75-25-2----------------- Bromoform 108-10-1--------------- 4-Methyl-2-Pentanone
108-88-3---------------- Toluene 127-18-4--------------- Tetrachloroethene 591-78-6--------------- 2 -Hexanone 108-90-7--------------- Chlorobenzene 100-41-4---------------- Ethylbenzene 1330-20-7-------------- Xylene (total)
100-42-5---------------- Styrene 79-34-5------------------ 1,1,2,2-Tetrachloroethane
10 u 10 u 10 u 10 u 10 u 10 u 10 u
10 u 10 u 10 u 10 u 10 u
10 u 10 u 10 u 10 u 10 u 10 u 10 u
10 u 10 u
10 u 10 u 10 u 10 u 10 u
10 u 10 u 10 u
10 u 10 u 10 u 10 u
FORM I VOA
OLM03.QwI9
DUP050308197
TfiTcu. rnM cHBOMaroecflH
Data File: >ISJB2: : D4
Quant Output File: /s ISJB2: : D7
Name: U8L.K193
UEJLKI93
instrument ID: HP03046
ruse: ~TLH WC %C = 1 +> #1962631AA &5 *5
id File: 1A6390: :L>B
'lit let 3/90 SOU Water/Med Soil ID File for Inst. HPQ3046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLN-262 Quant Time : 960919 09:09 Injected at: 960919 08:44
09f
DUP050308198
QUANT REPORT
Uperator 1U: Tl .Nt -262
Output File: 1S3B2 5 : D? Uat a File: >ib JB2 : :U4
Name: UBL.KI93
UBLKI93
msc: ~1LN 1QL %L =1 +>
Quant
#196263lRft &5
Kev:
*5
7 Quant Time: Injected at:
Di lut ion Factor: Instrument ID:
Page 1
960919 09:UV 960919 OB:44
1 . uuuuu HP03046
1L> File: IA639Q::DB
litie: 3^90 BUUI Weter/Med Boil ID File For Inst. HH03U46
Last Calibration*. 951122 10:44
Last Qcal Time: 960919 06:34
Compound
1? 15 ; 191 29) 31) 40)
*tiromocti lo remethane 1 ,2-DicFi 1 oroetFiane-d4
*1,4-Uifluorobenzene *Ch1orobenzene~d5
loiuena-d8 4-Bromofluorobenzene
* Compound is IBID
R.T. Q ion
B. 35 128 . U 9. 30 65.0 10. 02 114.0 14. 33 117. 0 12. 22 98.0 16. 05' 95.0
Area
59611 86141 163966 121256 143591 98437
Cone
Units
80.00 47.19 50. 00 50.00 50.69 49.05
UC2 C UtC'L US/L UL/L LIG/L
ue/L
q
V3 89 88 85 95 78
OOf*iHij
DUP050308199
Lancaster Laboratories Uuantitation Report-GC/MS Volatiles
LLl*: UBL.K 193
T L_M
I-lie: AiSJU2 Injected: 08:44 09/19/96
Sample: VBLK193
VBLK193
L)i lution factor:
1.0
initial Volume/Dt.:
5.0
Standard: A1SJS1
inst. HP03046
Batch:
1962631AA
Final Volume/Ut.: 5.0
Method: 7156 Matrix/level: tIL Blank:
t internal Standards
R.l. HART) Scan Ition AreaHV-Jifirea) Cone.
UL Flag Lone Units = ug/L
asse**KB*aa^maaa!**aTOm*Kaa* e***aa* **a W** **** *^******** ****w** * *******m***********st,,**s**t!ss*:a*"*,s,
1. Bromoehloromethane
8.3541.0159) 563 128
396111 29)
50.06
17. 1,4-Difluorobenzene 2V. Cblorobenzene-d5
10.021.0026) 14,53(-.001)
706 107?
114 117
1639661 27) 1212561 28)
50.00 30.00
* = RETENTION TIME DUT OF RANGE * * INTERNAL STANDARD AREA OUT OF RftRGE NC NOT ABLE TO CALCULATE--N0 STANDARD.
$ Surrogate Standards
K.T. H/-RRI) Scan Dion
Area
Cone.
Wise. a
>s9gssKiiniu>a9:uunntniannunuin>iian>3ninninimnn>un>iun>ciKi::uniE9>:an>nnuni:
13. l,2-l)ichloroethana-d4
9.2951-.U02)
644
65
31. Totuene-d8
12.22l.006S)
896
98
40. 4-Broaafiuorobenzene
16.05t-.000) 1225
95
4 - RELATIVE RETENTION TIME BUT OF RANGE * * 5SREC OUT OF RANEE
86141
47.19
94
145591
50.69
101
98437
49.05
98
D - SURROGATES DILUTED OUT NC COULD NOT CALCULATE
* target Compounds
2. Ctiloromethane 3. Vinyl Chloride 4. Broisoaeihane 9. Chlornethane 6. 1,1-Dichtoroethene
Acetone li. Carbon Disulfide V. Methylene Chloride 11. 1,3-Dicfttoroethane 12. 1,2-Dichloroethene (total) 15. 2-tlutanone 14. Chloroform 16. 1,2-Dichloroethane IB. 1,1,1-Trichloroethane IV. Carbon letrachloride 211. tlanzene 21. Irichloroethene 22. 1,2-Dtchloropropane 25. Bromodichlorousthane 24. cis-l,3-Otchioropropane 22. trans-l,3-Oichloropropene 26. 1,1,2-Trichloroethane
R.T.H/-RKI)
Scan Qion
Area Cone.A Cone.8
Lone. Blank U
Uuar.t l tat lor.
Limit
10 10
1(1
10 iu 10 ID 10
10
18
10 10 10 10 10 10 10 10
10 10
111 10
A > RfM CONC. 8 CONC. MULTIPLIED BY DILUTION FACTOR E - CONC. OUT OF CAL. RANGE 4 RELATIVE RETENTION TIME OUT OF RANGE
Lab Chronicle:
.Ent, by
PAGE 1 Of 2
Oer. by___QMSiS1-Ji
DUP050308200
Lancaster Laboratories Quantitation Report-GC/MS Uolatiles
LLI#: UB1__K 193
.M
Fiie: A1SJB2 injected! U8i44 09/19/56
Sample: UBCKI95
UBLK193
Uilution l-actor:
1.8
Initial Uolume/Ut.:
5.0
Standard: A1S3S1
Inst. HP03046
Batch!
I962631ftft
Final Itolime/Ut.: 5.0
Method: 7156 ttatrix/level! UL Blank:
t target Compounds
R. I.IV-RRI) Scan
ctee **s^sesstsHss*a:tta**ie*** *atamawsMarassamsaiat*ataeatwa*M*ai
27. UibroiFiOChSoroifiethane
------------------------------------
Qion
Brea
Cone.ft
Conc.B
Coni:. Blank Q
Quantitation Limit
MtBWUSMtlMftffmMSIUtltlHUmnUIRRXaMSCSSHBBlS
--------------------------------------------------------
Ill
28. uroaoform 38. 4-rtetnyl-2-P,entanone
32. toluene Ji. letrachloroethene
34. 2-Haxanone 35. Chlorobenzene i6. Lthytbenzene ill. Xylene (total) i9. Styrene 41. l,l,2,2-t8trachloroethsne
------------------------------------
------------------------------------
1U
------------------------------------
10
-------------------------------- ---
10
---------------- --------------------------------- -------------------
10 10
------------------------------------
10
------------------------------------
10
-------------------- --------------
id
------------------------------------
10
aaSBBB*inSBS1IBaBliBSKXBBBtaaCBBBBBEaRC8B*BRBleBB*BBBSXaaaSaSXasaXBBSBBBaBBC3
RAR CONC. B = CUMC. MULT1PLIED BY DILUTION FACTOR E = CUiC. OUT OF CAL. RANGE T = RELAT1UE RETENTION TINE UUT OF RANGE
Lab Chronic la:
JEnt. by
Bar. by
Analyst! Auditor:
..... ---------------------------- Date; _____4//q/n,
________________________.__________2kSO*t>: ?/lf/&
PAGE 2 OF 2
23
DUPO 50308201
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract:
VBLKI95
Lab Code: LANCAS
Case No.: _______ SAS No.:
SDG No.
Matrix: (soil/water) WATER
Lab Sample ID: VBLKI95
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >ISOB3
Level: (low/med) LOW
Date Received: _______.
% Moisture: not dec. _______
Date Analyzed: 09/24/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
1.0
Soil Extract Volume: _______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3----------------- Chloromethane
75-01-4------------------ Vinyl Chloride
74-83-9------------------ Bromomethane
75-00-3------------------ Chloroethane
7 5-3 5-4---------- -------- 1,1-Dichloroethene
67-64 -1----------------- Acetone
75-15-0------------------- Carbon Disulfide
75-09-2------------------ Methylene Chloride
75-34-3----------------- 1,1-Dichloroethane
540-59-0---------------- 1,2-Dichloroethene (total)
A 78-93 -3------------------ 2-Butanone
67-66-3------------------ Chloroform
107-06-2--------------- 1,2 -Dichloroethane
71-55-6------------------ 1, If 1-Trichloroethane
56-23-5------------------ Carbon Tetrachloride
71-4 3 -2----------------- Benzene
A 79-01-6------------------ Trichloroethene
78-87-5-----------------112-Dichloropropane
75-27-4----------------- Bromodichloromethane
10061-01-5------------ cis-1,3-Dichloropropene
10061-02-6-----------trans-1,3-Dichloropropene
79-00-5----------------- 1,1,2-Trichloroethane
124-48-1---------------- Dibromochloromethane
75-25-2----------------- Bromoform
108-10-1------------ --4 -Methyl-2-Pentanone
108-8 8-3---------------- Toluene
127-18-4---------------- Tetrachloroethene
591-78-6--------------- 2 -Hexanone
A
108-90-7----------------- Chlorobenzene 100-41-4---------------- Ethylbenzene
1330-20-7-------------- Xylene (total) A 100-42-5---------------- Styrene
79-34-5---------- --------1,1,2,2-Tetrachloroethane
10 u
10 u 10 u 10 u 10 u 10 u 10 U
10 u 10 u 10 u 10 u
10 u
10 u 10 u
10 u 10 U
10 u 10 u
10 u
10 u 10 u
10 u 10 u 10 u 10 u 10 u
10 u
10 u
10 u 10 u
10 u
10 u
10 u
FORM I VOA
OLMQ3.0'*'*
DUP050308202
T0TO!. TON CHROKPTOeRPM___________ ______ _____ File' >1 SOBS 35.0-300.0 *mu. VBLK195 WU<TW
400 800
"SUL SUL SC =1 > #] 1200
LSCfQOO*}
i60ooo4 ft
Data File: >IS0B3::D4
Quant Output File: ^1S0B3::D7
Name: UQLKi95 U8LK195
Instrument ID: HP03046
disc: "SJL $Wl *SC 1 +> #I96263lftB &5 *5
id File: 106390::DB
Title: 3/90 SOUS Ufater/Med Soil ID File for Inst. HP03046
Last Lalibration: 991122 10:44
Last Goal Time: 96U924 12:50
Operator ID: SJL-176 Quant Time : 960924 16:07 Injected at: 960924 15:43
235
DUP050308203
QUANT REPORT
Page 1
Operator- ID: SOL-176
Uutput FT let IS0B3: : D7
Data File:
>ibUB3::U4
Name: UBLKI95 UBLKI95
ruse: "SOL jaJWL ssc *1 +>
Quant #1962&31AB &5
Reu: *5
7 Quant Time: Injected at:
Dilution Factor: Instrument ID:
960724 16: U > 960924 15:43
1 . UUUUU
HPG3046
iU File: IAfc390::DB
Title: 5790 SCj Q Water/'fled Soil ID File For Inst. HPD3046
Last Calibration: 951122 10:44
Last Qcal Time: 960924 12:50
Compound
1) l`>) 17) 27) 31) 4U)
^Bromochloromethane 1,2-Diehloroethane-d4
*1,4~0ifluorobenzene *Chlorobenzene-d5
loiuene-dQ 4-Bromof luorobenzene
* Compound is 1CTD
R.T. Q ion
a. 19 9.13 9.85 14.18 12.06 15.90
128.0 65.0
114.0 117.0
98.0 95.0
Area
18B42 34766 y 3 21) 4 55305 65343 51399
Cone
Un i t.s
50.00 47.72 50. UO 50.00 51.82 50.14
Ub/L UG/L LiG/L UG/L UG.'-'L UG7L
q
97 95
82 9y 82
O
DUP050308204
Lancaster Laboratories Quantitation Report-C/WS Uolatiles
ILl*: t~*fc3L_K 195
GJI--
tile: AlSiJ)3 Injected: 15:4? (I9724/96
Sample: UBLK195
UBLK199
Dilution Factor:
1.0
Initial Volurae/Ut.:
9.0
Standard: 'HSIS13
Inst. HP03046
Batch:
19&2631AB
Final Uolume/Ut.: 9.0
Method: 7156 Matrix/level: UL Blank:
* internal Standards
R. 1. 1+/-RO Scan Clion Areal*/-Sftrea> Cone.
sss3ts*ssmtst*SB*stt*ss*3teas*ss*tsM*essB******s****s*************n*!
QC Flag Lone Urats = uq/L
1. Bromochloromethane
8.187(.ai9i) 991 128
I8842(-39)
98.80
17. 1,4-Difluorobenzene
29. Chiorobenzene-db * = RETENTION TIME OUT OF RANGE
9.890C.0118) 694 114
73204C-413
90.90
14.181.0292) 1066
117
59389C-43)
90, BIS
* * INTERNAL STANDARD AREA OUT OF RANGE 1NC - NOT ABLE TO CALQJLATE-NO STANDARD.
* Surrogate Standards
R.T. (*/-RRT) Scan Uinn
Area
Cone.
XRac. U
S3S8B8S8B88SS8SSBSS8*3E8888BaBBS3B98V8SB88SSXBBS3S8BWIC8BB8BB aBIBIBIXBBBBBBSBBBBIiaBBIBBflBBBBBS:XSBB8S8BaS8BSB8B88B8Sa8a3S8XaBBS8S
19. l,2-Uichloroetbane-d4
9.129(-.081)
632
69
31. Taluene-d8
12.U6C-.0I11)
8B4
98
4U. 4-Broiofluorobenzene
19.98(-.081) 1214
99
4 RELAT1UE RETENTION TIME OUT OF RANGE * SREC OUT OF RANGE
34766
47./2
95
69343
51.82
104
91399
50.14
luu
D = SURROGATES DILUTED CUT NC - COULD NOT CALCULATE
Cone.
Quantitation
* target Compounds
R.T.(+/-RRT)
Scan Uion
Area Cone.A Conc.U Blank U
Limit
ssrsesssssses3&sse33S3BS3ss=B8BC88sae3>B3sr38aBisaxsskaaxa8Bsassss3SSBBBsxQS8V8assasasB3cc8Bi8s*seat:BSSSsssaa:asi:saDsssasss83Kaa3
2. Chloromethane
-------------------------------------------------- :---------------------------------------------------------------------
18
3. Vinyl Chloride
------------------------------------------ ----------------- ----------------------------------------------------------
10
4. Bromom&thane 9. Chi or oe thane
----------------------------------------------------- ------------------------------------------------------:------------------------------- ----------------------------------------------------------------------------------------------------
18 10
6. 1,1-Uichlorcethene 7. Acetone
-------------------------------------------------------------------------------------------------------------------------------------------------- -------------------- -----------------------
10 10
8. Carbon Disulfide
---------------------------------------------------------------------------------------------------------------- ----------------
10
9. Methylene Chloride
--------------------------------- *-------------------------------------------------------------------------------------
10
11. 1.1-Qichloroethane
--------------------------------------------------- ;-------------------------------------------------------------------
10
12. 1,2-Dichloroethene (total) ----------------------------------------------------------------------
ii. 2-Butanone
14. Chloroform
16. 1,2-Uiehloroethane
18. 1,1,1-Iriehloroethane
19. Carbon tetrachloride
2U. Benzene
21. Irichloroethene
22. 1,2-Diehlorepropane
23. Broiriodi chloromethane
24. cis-l,3-D>chloropropene
-----------------------------------------------------------------------------------------------------------------------------
10
2b. trans-1 fj-U3Chloropropene
---------- ------ ---------------------- ------ -- ------------------------------ ----------------------------------------
18
26. 1,1,2-1richloroethane
----------------------------------------- ---------------------------------------------------------------------------------------
10
88SSaaB3BX3SeBBBB88eSSSSBSSCSB3S::afiSSSBBS83SSBtt8SSS88SSaBasSSBSBS!:XBSS8SSSSSSSS&SBSSSSS:3SSSSSSSSaSSZZSSBSSSaS&SSSSSSEBtESSSSBSSSS
A = RAbJ Ct)C. B = COtC. MULTIPLIED BY DILUTION FACTOR E EffiiC. CUT OF CAL. RANGE * - RELATIVE RETENTION TIME OUT OF RANGE
tab Chronicle:
Ent, by
*r. by
PAGE 1 UF 2
DUP050308205
Lancaster Laboratories Uuantstation Report-GC/MS Uolatites
LL1#: UBI-- K 1 95
&L3 L_
File: "ISUtSi injected: 15:43 09/24/96
Sample: UBLKl95>
UBUCI95
Uilution tactor:
1.0
Initial Voluma/Ut.:
5.0
Standard: 'V1SUI3
Inst. HP03046
Batch:
1962631AB
Final Uolurae/ttt.: 5.0
Method: 715a Matrix/level: UL Blank:
target Compounds
R. T.(V-HRT)
Scan Oion
Brea
Lone.ft
lonc.B
Cone. Blank U
Quantitation Limit
2/. Uibromochloromethane 2B. brotaofora 3U. 4-Methyl-'2-l:'entanane 37. Toluene 33. ietrachloroethene 34. 2-Hexanone 35. Chlorobenzene 36. Ethylbenzene 3B. Xylene (total) 39. Styrene 41, 1,1,2.2-Tetraehloraethane
ss***tsseaassBss*ass*sa*iB3*i
A fifty tatc. b = LUNC. MULTIPLIED BY D1LUT1UN 1-ftClUR
1U 10 J.U 10 1U 10 1U 10 lu 10 1U
* CUNC. OUT UF CftL. RANGE * = RtLftUUE REiENUUN TIME UUT 111 KftNUt
Leb Chronicle:
Ent. by
228
DUP050308206
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER LABS
Contract:
BRS3DMS
Lab Code: LANCAS
Case No.: _______ SAS No.:
SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: 2583209
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >ISJ12
Level: (low/med) LOW
Date Received: 09/18/96
% Moisture: not dec., _______
Date Analyzed: 09/19/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
1.0
Soil Extract Volumes _______ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87-3---------------- -Chloromethane 75-01-4------------- --Vinyl Chloride 74-83-9---------- -------- Bromomethane 75-00-3------------------ Chloroethane 75-35-4------------------ 1,1-Dichloroethene 67-64-1------------------ Acetone 75-15-0------------------ Carbon Disulfide 75-09-2------------------ Methylene Chloride 75-34-3----------------- 1,1-Dichloroethane
540-59-0--------------- 1,2-Dichloroethene (total) 78-93-3------------------ 2-Butanone 67-66-3------------------ Chloroform 107-06-2--------------- 1,2-Dichloroethane 71-55-6----------------- 1,1,1-Trichloroethane 56-23-5------------------ Carbon Tetrachloride 71-43-2---------------- -Benzene A 79-01-6------------------ Trichloroethene 78-87-5------------------ 1,2-Dichloropropane 75-27-4----------------- Bromodich1oromethane 10061-01-5------------ cis-1,3-Dichloropropene 10061-02-6----------- trans-1,3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane 124-4 8-1---------------- Dibromochloromethane 75-25-2------------------ Bromoform 108-10-1--------------- 4 -Methyl-2 -Pentanone 108-88-3---------------- Toluene 127-18-4---------------- Tetrachloroethene 591-78-6---------------- 2-Hexanone 108-90-7---------------- chlorobenzene 100-41-4---------------- Ethylbenzene
1330-20-7----------- Xylene (total) 100-42-5------------Styrene 79-34-5---------------1,1,2,2-Tetrachloroethane
FORM I VOA
10 u 10 u 10 u 10 u
59
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
58 57
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
55
10 u 10 u
52
10 u 10 u
10 u
10 u
Q9Q OLM03.0
DUP050308207
TClTOt TOW CHROMOTOSRRh
Data File: >1SJ12::D3
Quant Output File: AISJ12::D7
Name: BRS3DNS 25832U9
instrument ID: HP03046
flisc: ~TLN @WL %C -1 + > #I962631AA $'"ISJB2 &5 *5
id File: ift6390:sDB
Title: 3-'90 SOW Water/Med Soil ID File for Inst. HPQ3Q46
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLN-262 Quant Time : 960919 11:59 Injected at: 960919 11:35
OU
DUP050308208
QUANT REPORT
Paae 1
Uperator ID: TLN-262
Output File: /SIS012::D7
Data File:
>iSJ12::D3
Name: BRS3DMS 2583209
M1 sc: ~TLN (ajUIL %C = 1 + >
Quant Reu: #!962631Aft S'"1SJB2
7 Qusnt Tlme: Injected at:
Dilution Factor: Instrument ID:
&5 *5
960919 11:59 960919 11:35
1. U 0 0 U 0 HP03 046
ID File: IA639G::DB
Title : 3290 SOU Water/fted Soil ID File for Inst. HP03046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
1) 6) 15) 17) 20) 21) 29) 31) 32) 35) 40)
*8roraochloromethane 1,1-Dichloroethene 1,2-Dichtcroethane-d4
*1,4-Difluorobenzene Benzene Trich loroethene
*Chlorobenzane-d5 To luene-d8 To luene Chlorobenzene 4-Bromofluorobenzene
* Compound is ISTD
R. T. Q ion
8.36 128.0 4.67 96. 0 9.30 65.0 10.02 114.0 9.40 78.0 10.42 130.0 14.32 117. 0 12.22 98.0 12.31 91. 0 14.36 112.0 16.04 95.0
Area
39 U18 46615 84080 162767 137U58 65756 121783 144561 156760 115255 98289
Cone
Units
50.00 UbC'L 58.99 UG7L 46.76 U&/L 50.00 UG7L 57.81 UQ7L 56.61 U67L 50.00 US7L 50.11 UG/L 54.80 U/L 52.59 UG7L 48.77 UG7L
q
91 92 89 87 88 84 83 96 98 84 76
231
A
DUP050308209
Lancaster Laboratories Quantitation Report-GC/MS Uolatiles
LLI*: 2 5 8 3 2 0 9
File: AiSvJ12 Lmeeted: 11:35 89/19/96
Sample: BRS3DMS
2583289
Dilution Factor:
1.0
Initial Dolume/Ut.:
5.0
Standard: "tSJSl
Inst. HP03046
Hatch:
1962631fift
final Volume/Ut.: 5.0
rtethod: ?156 ttatrix/level: UL Dlank: AlSJtri
Internal Standards
R.T. 1+/-RTJ Scan Dion ftrea(+/-Sflrea) Cone.
UL flag Lone Units * ug-'L
==*333diaa3BSKacasms3essaassa**XBUStsaBB33Ks3Bars*n3sssssasssmsxssisssainBSCEBXsm*sssaftassBxmBSKsaKBKaiEBxett2333=3saKaBBxasaisBB3
DUP050308210
Lancaster Laboratories fluentitation Report-GC/ttS Volatiles
LLl*i 2 9 e 3 2 Q 9
TLN
File: A(SJ12 Injected: 11:35 05/19/%
banpla: BRS3BHS
2583209
Dilution Factor:
1.0
Initial Volume/tlt.:
9.B
Standard: A1S<1S1
Inst. HPBJ046
Batch:
1962631AA
Final Valuae/Ut.: 5.0
Method: 7156 Matrix/level: UL Blank: ALSJH2
$ larget Laapeunds
R.T.l*/-RRI)
Scan Qion
Area
Conc.fi
tone.B
Cone. Blank U
Quantitation Limit
2/. Dibromochioroffiethane
28. Bromoform
3D. 4-ftet by l-2-Fentanone
32.. Toluene
12.311 .0811 908 91 156760 54.808
55
yj - letraEhloroethene
34. 2-Hexanone 35. Chlorobenzene
14.361 .800)
1084
X12 115255 52.695
52
36. Ethylbenzene
58. Xylene ltotal!
59. Styrene
41. 1,1,2,2-Tetrachloroethane 8BXSS8SS8eKSSSS8*BaSSBas882Xa8SttSI88>MMSM8B8MmmimCet8laMUSMatmnSSSQUBnn8SS8aSlKSBBW
in
10 10 10 10 10 10 10 10 10 111
fl RflW CUNC. B * CUNC, RULl 1PL1ED BY DILUTION FACIUR t - CUNC. OUT IF CAL. RANGE * RELATIVE RETENTION TIME OUT OF RANGE
lab Chronic leJ
_nt. by
DUP050308211
1A VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER LABS
Contract:
BRS3DMSD
Lab Code: LANCAS
Case No.: _______ SAS No.:
SDG No.:
Matrix: (soil/water) WATER
Lab Sample ID: 2583209
Sample wt/vol: 5.0
(g/mL) ML
Lab File ID: >ISJ13
Level: {low/med) LOW
Date Received: 09/18/96
% Moisture: not dec. _______
Date Analyzed: 09/19/96
GC Column: DB624
ID: 0.53 (mm)
Dilution Factor:
1.0
Soil Extract Volume: ____ (uL)
Soil Aliquot Volume: _______ (uL)
CAS NO.
COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
Q
74-87 -3----------------- Chloromethane 75-01-4---------- -------- Vinyl Chloride
74-8 3 -9----------------- Bromomethane 75-00-3------------------ chloroethane 75-35-4----------------- 1,1-Dichloroethene
67-64-1--------------- Acetone 75-15-0------------------ Carbon Disulfide
75-09-2------------------ Methylene Chloride 75-34-3------------------ 1,1-Dichloroethane
540-59-0--------------- 1,2-Dichloroethene (total) 78-93-3---------------- -2-Butanone 67--66--3------------------ Chloroform 107-06-2--------------- 1,2-Dichloroethane 71-55-6----------------- 1,1,1-Trichloroethane 56-23-5------------------ Carbon Tetrachloride
71-43-2------------------ Benzene 79-01-6------------------ Trichloroethene 78-87-5------- ----------- 1,2-Dichloropropane 75-27-4--------------- Bromodichloromethane 10061-01-5------------ cis-l,3-Dichloropropene 10061-02-6----------- trans-1,3-Dichloropropene 79-00-5----------------- 1,1,2-Trichloroethane
124-48-1----------- --Dibromochloromethane
75-25-2------------------ Bromoform 108-10-1---------------- 4-Methyl-2-Pentanone 108-88-3---------------- Toluene 127-18-4---------------- Tetrachloroethene 591-78 -6--------------- 2 -Hexanone 108-90-7--------------- chlorobenz ene 100-41-4---------------- Ethylbenzene 1330-20-7-------------- Xylene (total)
100-42-5---------------- Styrene 79-34-5----- `------------ 1,1,2,2-Tetrachloroethane
10 u 10 u 10 u 10 u
59
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
58
57
10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u
54
10 u 10 u
53
10 u 10 u 10 u 10 u
FORM I VOA
OLM032<8 4
DUP050308212
t o t a l ION CHROflOTOeRfiM
Data File: >ISJ13::D3
Quant Output File: '''ISO 13 : : D?
[ lame: BRS3DriSO 2583209
Instrument ID: HP03046
nisc: ~TLN WL 5SC =1 +> #I962631AA $^IS0B2 &5 *5
Id File: IA6390::DB
Title: 3/90 SOU) Water/'tled Soil ID File for Inst. HP03Q46
Oast Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Operator ID: TLN-262 Quant Time : 960919 12:36 Injected at: 960919 12:11
235
DUP050308213
QUANT REPORT
Operator ID: TLN-262
Output File: "'IS.313: : D?
Data File:
>IB013::D3
Name: 8RS3DMSD 2583209
ruse: ~TLN WL C *1 +>
Qu ant Re v: #1962631AA $''ISJB2
7 iQuant Tlme: Injected at:
Dilution Factor: Instrument ID:
&3 *5
Page 1
96U919 12:36 960919 12: 11
1 . UUU0U HP03046
ID Fi le: 1A6390::DB
'< 11 1 e : 3^90 BOW U)ater2F1ed Soil ID File for Inst . HPQ3 046
Last Calibration: 951122 10:44
Last Qcal Time: 960919 06:34
Compound
1? 6) 15) 17) 20) 21) 29) 31) 32) 35) 40)
*Bromoch1aromethane 1,1-Dichloroethene 1,2-Dichioroethane~d4
*1,4~Difluorobenzene Benzene Tr ich loroethene
*Chlorobenzene-d5 ToIuene-d8 Toluene Chlorobenzene 4-Bromofluorobenzene
* Compound is ISTD
R.T. Q ion
8.35 4.65 9.30 10.01 9.38 10.41 14.32 12.22 12.31 14.36 16.04
128.0 96.0 65.0
114.0 78.0
130. 0 117. 0
98.0 91.0 112.0 95.0
Area
40297 47939 85333 167429 142425 68413 125468 144106 160454 120237 101642
Cone
Units
50 . UO 58.74 45.95 50.00 58.40 57.26 50.00 40.49 54.44
53.26 49.04
UG/L
UG/L
UG/L
UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L
q
90
91 89 8? 88 84 85 98 96 87 74
236
DUPO 50308214
Lancaster Laboratories Quantitation Report-GC/MS Uolatiles
LL1*: S ^ S 32 0 9*
TLN
Hie: A1SJ13 Injected: 12:11 119/19/96
Sample*. BRS3WSD 2585209
Uilution factors
1.0
Initial Volume/Wt.:
5.0
Standard*. ''LSJSl
Inst. HP03846
Batch:
1962631RA
Final Volume/Wt.: 5.0
Method: 7156 Matrix/leyel*. ML Blank: A'lSJt52
* Internal Standards
ft.T. IV-RT) Scan Qian Areal+/-XArea) Cone.
UL Flag Lone Units = ug/L
1. Bromochloromethane 17. 1,4-Bifluorobenzene
29. Chlorobenzene-d5 i m RETENTION TINE OUT OF RANGE
8.3501.0114) 563 128
482971 31)
50. Ill)
10.8K-.S82) 786 114
1674291 38)
50.80
14.32t-.884) 1877
117
125468( 33)
58.81)
* - INTERNAL STANDARD AREA OUT OF RANGE NC * NOT ABLE TO CALCULATE--! STANDARD.
Surrogate Standards
R.T. (*/-RRT) Scan Cion
Area
Cone.
SRec. U
sssasvsBcseBBVEXvMeiBesaaBaassBsaBBB&BsmattaBKSsBinxmaxaxvsHxastsnssatsaaMaaBtiesitHMasBRavnwniiuWMBSssBsaxaBsustBs&asssBBa
15. l,2-Oichlornethane-d4
9.3021-.8B8)
645
65
31. Toluene-dB
12.221.0007)
896
98
40. 4-Bromo fluorobenzene
16.041-.08Q) 1225
95
4 RELATIVE RETENTION TIME CUT OF RANGE * XREC OUT OF RANK
85333
45.95
144186
48.49
101842
49.04
D SURROGATES DILUTED OUT
92 97 9tJ
NC
COULD NOT CALCULATE
Cone.
Quantitation
f Target Compounds
R.T.D/-RRT)
Scan Oion
Area
Cone.A
tone.8
Blank Q
Limit
5:~3:l!-B.I:-asBBBaBa3e83s*BMSBa8*BBamaBBBBBseaBa8*BBXBnreBe*ata*B*B****B***B**a(s*E8**BBSB8B*88B8*BBnmmBBBB*8n**BBBSBm*BBeB
2. Chloromethane 3. Vinyl Chloride 4. Bromomethane 5. Chloroethane 6. 1,1-Dichloroethene 7. Acetone B. Carbon Disulfide
4.651-.008) 245 96 47959 58.738
59
10 10 1ft 10 lu 10.
Ill
9. Methylene Chloride 11. 1,1-Uichloroethane 12. 1,2-Dschloroethene (total) 13. 2-Butanone 14. Chloroform 16. 1,2-Dichloroethane 18. 1,1,1-Trichloroethene 19. Carbon Tetrachloride 20. Benzene 21. Trichloroethene 22. 1,2-Dichloropropane 23. Bromodichioromethane 24. cis-l,3-Dichloropropene 25. trsns-l^-DiehSoropropene 26. 1,1,2-Tnchloroetbane
9.301 .001) 10.411 .001)
652 70 142425 740 130 68413
58.403 57.257
58 57
ssbbsscssstsssscBSsasassesessaeesssBSBasrBisststssBtSB&SBseassssssssssaBStsssssssssdssBsaaeajssaBi
10
la 10 in 10 lft
10 ID
10 11!
10 111 10 10
10
A = RAU CISC. El * COMC. MULTIPLIED BY DILUTION FACTOR - CONC. OUT OF CAL. RANGE * - RELATIUE RETENTION TIME OUT OF RANGE
Lab Chronicle*.
Ent. by
Ver. by_g_^.
PAGE 1 OF 2
DUP050308215
-^^ '*uwHn.w--'W'fltfiioiBaiiu,-.as-iiiiiniii-.,,.. ^i,.-^.^,;*,, . .
Lancaster Laboratories Quantitation Report-GC/MB Volatiles
Lilt: 25832 5*
Tl--1^4
tiie: A1SJ13 injected: 12:11 89/19/96
Sanple: BRS3DMSD 2583209
Dilution Factor:
1.(1
Initial Volume/tili.:
5.0
Standard: AiSJSl
Inst. HP03046
Batch:
I962631AA
Final Uolume/Ut.: 5.0
Method: 7156 Matrix/level: UL Blank: A1SJB2
Cone.
Quantitation .
t target Compounds
R.T.l*/-RRf)
Scan tlion
Area Cone.A Cone.B Blank Q
Limit
ssEas6asaa83a8ss3BBBSB8eafSiuaais*Mtn8BS88iM*si8seaBaBKaBK>BtasssasB8BS3BsaeBsat8aiia3assKSBsBssss:s*saBss3s
27. Dibromoehioromethane 28. Brosmform ill. 4-ttethyl-2-Pentanone 32. Toluene 33. letrachloroethene 34. 2-Hexanone 35. Chlorobenzene
36. Ethylbenzene 38. Xylene (total)
*------------------------------------- -------- --------- -------------------- --------------------
12.311 .001) 904 91 160454 54.444
54
--------------------------------- *------------------ *----------------------------------------------------------------
--------------------- -----~-------------------- ----------------------------------------------------------
14.361 .0001
1(180 112 120237 53.257
53
------------------------------- -----------------------------------------------------
10
10 10 10 10
41. 1,1,2,2-Tetraefiloroethane ------------------------------- :---------------------------------------------------------------------------------------------
1U
aaaaaaasaa#!sa*aa*aasBsai!*a*jani*:aBeu6*BaB*a*****aa*Ji**sii***aB6iitiKKit**Kamm*05acs**aaaEB3**sa**asa***Bia*a*ffi3Be3a**aoai
ft = RAW CUNC. S = CUNC. MULTIPLIED BY DIUJTSUN FACTOR E = CUNC. OLU QF Cftt. RANGE t - KLLftl IDE RETEOT1UN TIME OUT UF RANGE
Lab Chronicle:
JEnt. by
analyst:
.Date:
Q(lcl
Dor. by
Auditor:
.Date:
PfiGE 2 QF 2
238
DUP050308216
**
LANCASTER LABORATORIES INC.
LANCASTER LABORATORIES INC.
RUNLOG FOR HEWLETT PACKARD GC/MS SYSTEM #HP03460
* * _______
_________________________ First Shift
,,
fksu-
* _-
________ Second Shift
*Third Shift * *
<?A-rs
(HP4)
* * * ' *
* * * *
*
* * * * * * * * *
FILE SAMPLE
LLI#
DATE TIME BATCH
>GSMT1 BFBJUN28 >GSMT2 BFBJUN28 >GSMT3 BFBJON28 >GSMI1 VSTD010 >GSMI2 VSTD020 >GSMI2 VSTD020
>GSMI3 VSTD050 >GSMI4 VSTDIOO
>GSMI5 VSTD200 >GSMB1 VBLKG22 >GSMB1 VBLKG22
>GSMB1 VBLKG22 >GSM01 FTWAS
>GSM02 F8WAS >GSM03 F6WAS
>GSM04 DU-P>GSM05 FSWASDL >GSM06 DU-P-DL
>GSM07 F6WASMS >GSM05 FSWASDL
>GSM07 F6WASMS >GSM06 DU-P-DL >GSM08 F6WASMSD
>GSM09 3------->GSM10 5--------
>GSM11 T------B >GSM12 3-------DL >GSM12 3r-----DL >GSM13 FGWASMSD >GSM14 FSWASMS
50nG BFB 09/24/96 00:30
5 OnG BFB 09/24/96 00:48
50nG BFB 09/24/96 01:08
010 ppb IC 09/24/96 01:40
020 ppb IC 09/24/96 02:12
020 ppb IC 09/24/96 02:12
050 ppb IC 09/24/96 02:44
100 ppb IC 09/24/96 03:17
200 ppb IC 09/24/96 03:49
VBLKG22
09/24/96 04:50 52S1T
VBLKG22
09/24/96 04:50 G2661
VBLKG22
09/24/96 04:50 G2661
2585266
09/24/96 05:33 G2661
2585227
09/24/96 06:03 G2661
2585228
09/24/96 06:32 G2661
2585229
09/24/96 07:02 G2661
2585227
09/24/96 07:37 G2661
2585229
09/24/96 08:07 G2661
2585228
09/24/96 08:36 G2661
2585227
09/24/96 07:37 G2661
2585228
09/24/96 08:36 G2661
2585229
09/24/96 08:07 G2661
2585228
09/24/96 09:06 G2661
2585230
09/24/96 09:41 G2661
2585231
09/24/96 10:13 G2661
2585232
09/24/96 10:42 G2661
2585233
09/24/96 11:21 G2661
2585230
09/24/96 11:21 G2661
2585228
09/24/96 11:53 G2661
2585228
09/24/96 12:41 G2661
D.F. NOTES
u.uu
jSi/\
%
0.00
0.00
1.00
1.00
1.OOREPROCESSED1.
1.00
1.00
1.00
1.00
1.OOREPROCESSED!.
1.OOREPROCESSED!.
1.00
1.00
1.00
1.00
2.00
1.00
.40
/'w'vA
.
5.00 r<vsf cc.ff&'i .
1.00
2.50
1.00 1.00
^ <A_
1.00
1.00
2.50
2.50 t <5
'SliA
1.00
1.00
23S
DUP050308217
I ANGASTFR LARDRATriRIFS INF..
RUNI OG FOR HEWLETT PACKARD GC.XMS SYSTEM $KP0346n
(HP4)
*r
First Shift
* Second Shift
*
Third Shif t
Sa <
*
*
H
II II
li
II
II
F f 1. F SAMPLE
LI I*
DATE TIME BA FCH D. E.
saesssasaa sssKssasaHWBsssasssarta sat as as as as asr aa as ssssas s
= as as at as ssr as -a as ~ ss as as
>r::-.pn > GSPS1 > JhP.PR I
>GSPCl! >g s p o ? > GSP03 >GAP04 > GSP05 >g s p o 6 >GSPfl7 >GSP0S >GSP09
>nspin
> GSP 11 > RSP12 >GSP13 >g s p i.4
>GSP15 >GSP16 > ESP]7 >GSP18 > GSP19 >GSPX!
>GS.X2 > GSPX3 >GSPX4
BFfl.1t.SN78 USTO030
URl KG74
BBA2D 8RA2S BRAID 8RAIS MRA2S MRA2SMS MRA2SMSD BRAF1 BRAT? MRA IS MRA1D MRA20 TB3FM MRftAS
MRA IS MPA3D MR3DD MRAFB MRT84 TB96261
T896264 TR9626S TB96269
5 0r.G BFS 09724X96 23 59
030 ppb CC 09X25X96 0 0 26
UR! .KG? 4
09X25X96 01 04 G2681
2583823
09X25X96 01 57 G2681
2583824
09X25X96 0? 30 G2681
2583825
09X25X96 03 02 G2681
2583826
09X25X96 03 34 G2681
2585279
09X25X96 04 05 G2681
2585279
09X25X96 04 36 G2681
2585279
09X25X96 05 06 G2681
2583827
09X25X96 05 39 G2681
2583828
09X25X96 06 11 92681
2 5 P.5 2 76
09X25X96 116 47 G2681
2585277
09X25X96 07 1.3 G2681
2585278
09X25X96 0 7
G26S1
2585280 2585281
09X25X96 08 17 G2681 09X25X96 08 5 0 G76S1
2585282
09X25X96 09 22 G2681
2585285
09X25X96 09 55 132.681
2585284
09X25X96 1 0 27 G2681
2585285
09X25X96 11 00 G2681
2585286
09X25X96 11 33 G2681
TR96261
09X25X96 12 22 G? 681
TB96264
09x25X96 12 55 G2681
TP.96268
09X25X96 13 28 G2681
TR96269
09X25X96 14 0 0 G2681
o. ft n l. no
1. o n
1.00 1.00
1 - 00 1.00 1.00 1.00
1.00 i. o n
1.00 1.00 1.00
1.00
l. no
1 .00
l. no
1.00 1.00 1.00 1.00 1.00
1.00
l. no
1.00
NOTES
-*i
a
*
*
*
240
DUP050308218
LANCASTER LABORATORIES tf-iC. RUNLOG FOR HEWLETT PflCKARO GC/MS SYS TEH SHP03046
_F rs Sh j f t lUi
.8.5 co ~ - h i ? 3
ThsrcJ S* :Fi:
(HP6 )
f i l e s a mp l e
LL I v
DA!
1 ! ME
* st * s rp mavmv 5T K=r snwmsttneennssvsceBnsnss = ="
> IGKT2 BPS
2uL 5 On g K.c8
OS/2 0.*96 19 52
> EGKf1 vsionle
010 PPS IC 08/20/96 20
>IGKI2 USTD020 > I Gs< I3 vsrooso
020 PPS 1C 08/20/96 20 v 050 PPS IC 02/20/96 O. T4k 41
> <14 USTO20G
100 PPS IC 08/20/96 22 15
> e g k !5 us r0*2 oo
200 PPS !C 03/20/96 22 46
>IGKS3 U8LKI50 > 1GKS4 L'SLK [ 5 0
U8LKI50 VBLK f 5 0
03/20/96 23 46 08/21/96 00 fl
>IGK85 UBLKI5Q
UBLKI50
03/21/96 01 38
>IGK86 U8LKI50 J U8LKI50
03/21/96 02 26
>IGK20 00199
25*2933
03/21/96 03 08
> IGK21 U18LK 5 C1 UIBLKIC1
03/21/96 04 00
>IGK22 0 0199 DL
256292?
03/21/96 04 34
>IGK23 002 00 > IG!<24 00201
> tG*2*5 U0201DL
2562925 2562929 2562989
03/21/96 05 2 3
08/22/96
06
>
V*
1J.
08/21/96 06 6P
> ICK26 00200
2562925
08/21/96 0? 24
> I GK2 ? Ul8LKl02 V1BLKI02
08/21/96 03 06
>IGK2S 'JISLKI03 VIBLK103
08/22/96 08 36
BATCH
12331 12331 J 2331 12331 12331 12531 12331 12 331 12531 12 351 12531 12331 12 331
0. F.
NO! ES
serr^asr a as*TS w m
o.uo
2.0 U
1.00
1.00 i_
1. UO 1.00 _ 1 . UO 1.00 1.U0 1.00'
16.00' 1.00
400.00
m
| \y
*
10IJ . 0 u 16.0 0
wo-
i . u
40.00 1.00 1.00
W.U Jy
241
DUP050308219
************* *
LANCASTER LABORATORIES INC. RUNLOG FOR HEWLETT PACKARD GC/MS SYSTEM #HP03046
First Shift TLu
Second Shift :TL
Third Shift SArvv 1
fHP6>
FILE SAMPLE
LLI#
SATE TIME BATCH
>ISJT1 BFB 2uL 50ng BFB 09/19/96 06:10
>ISJS1 VSTD050 050 PPB CC 09/19/96 06:34
>ISJB1 VBLKI92 VBLKI92
09/19/96 07:14 12571
>ISJ01 TB909
2578563
09/19/96 07:51 12571
>ISJB2 VBLKI93 VBLKI93
09/19/96 08:44 12631
>ISJ10 BRATB
2583211
09/19/96 10:34 12631
>ISJ11 BRS3D
2583209
09/19/96 11:04 12631
>ISJ12 BRS3DMS 2583209
09/19/96 11:35 12631
>ISJ13 BRS3DMSD 2583209
09/19/96 12:11 12631
>ISJ14 DRA3S
2583210
09/19/96 12:41 12631
>ISJ15 BRS4S
2583208
09/19/96 13:12 12631
>ISJ16 BR4DD
2583207
09/19/96 14:11 12631
>ISJ17 BRA4D
2583206
09/19/96 14:41 12631
>ISJ18 BRA5S
2583205
09/19/96 15:27 12631
>ISJ19 BRA5S
2583205
09/19/96 16:04 12631
>ISJ20 BRA5S
2583205
09/19/96 16:40 12631
>ISJ21 BRA5S
2583205
09/19/96 17:25 12631
>ISJ22 BRA5S
2583205
09/19/96 17:56 12631
D.F. NOTES
0.00
1.00 " 1.00 1.00 " 1.00
1.00 " 1.00 " 1.00 ' 1.00 " 1.00 1.00 " 1.00 '
1.00 "
1.00 " 1.00 "
1.00 ' 1.00 " 1.00
SJu. 1
AJ
* * * * * * * * *
* *
*
* *
* * .
*
DUP050308220
LANCASTER LABORATORIES INC.
RUNLOG FOR HEWLETT PACKARD GC/MS SYSTEM #HF03046 (HP6) **
*
______________ First Shift TLi
*
**
* _____________._______________________ Second Shift
*
**
*
_______ Third shift
*
**
**
**
**
**
**
**
*
___ _____
*
FILE SAMPLE
LLI#
DATE TIME BATCH D.F. NOTES
>ISOTl BFB 2UL 50ng BFB 09/24/96 11:10
>ISOIl VSTD010 010 PPB IC 09/24/96 11:35
>ISOI2 VSTD020 020 PPB IC 09/24/96 12:08
>ISOIl VSTD010 010 PPB IC 09/24/96 11:35
>ISOI2 VSTD020 020 PPB IC 09/24/96 12:08
>ISOI3 VSTD050 050 PPB IC 09/24/96 12:50
>ISOI4 VSTDIOO 100 PPB IC 09/24/96 13:23
>ISOI5 VSTD200 200 PPB IC 09/24/96 13:56
>ISOBl VBLKI95 VBLKI95
09/24/96 14:29 12681
>ISOB2 VBLKI95 VBLKI95
09/24/96 15:04 12631
>ISOB3 VBLKI95 VBLKI95
09/24/96 15:43 12631
>ISO01 BRA5S
2583205
09/24/96 16:23 12631
>IS002 BRA2D
2583823
09/24/96 16:55 12631
>IS003 BRA2S
2583824
09/24/96 17:25 12631
>ISOXl CLEANING BLANK
09/24/96 18:18 12631
>ISOX2 CLEANING BLANK
09/24/96 19:33 12631
0.00
1.00 '
1.00
1.OOREPk OCESSEDT
l.OOREPROCESSEDi
1.00
1.00 '
1.00 '
1.00 " uu
1.00 '
1.00 '
1.00 "
1.00 " MU
1.00 "
t
1.00 '
|
*
1.00 "
24
DUP050308221