Document 2M3QzxaK80xyBpQ4RGOZo0DN

STARTUP MANUAL D-?flO PVC REACTORS ABERDEEN; MISSISSIPPI January 24, 1978 Chemicals Division Process Engineering Department Approved by: J. Robert Rolfes Senior Process Engineer Chemicals Division Process Engineering Department DTH 00008911 Cconoco) Interoffice Communication To f -n Distribution P. F. Fetizanan Date January 24, 1978 Subject D-700 Unit Startup Manual--Aberdeen PVC Plant Attached is the startup manual for the D-700 PVC reactors incorporating plant comments. This manual outlines the steps to prepare the unit for operation from the time the unit is turned over to the plant by the con tractor until each reactor is ready for normal charge. The primary steps involved are flushing of lines and leak testing, checking of individual systems, and introduction of VCM and final reactor checks. Based on these work items and available manpower, MED will prepare a CPM Chemicals Division Process Engineering Department lkm Enc CC: ELK(16):DLH:ARP:JHM:WCW Approved by 'JL File P-63 DTH 000089111 TABLE OF CONTENTS STARTUP MANUAL D-700 PVC REACTORS ABERDEEN, MISSISSIPPI Page No. I. INTRODUCTION ...................................................................................................................... 1 II. BASES................................................................................................................................... 2 III. FLUSHING AND LEAK TESTING OF LINES.................................................................. 5 A. Work Items before Water Flush ................................................................. 7 B. Process Water................................................... ,...................................... . 11 C. HPSW, MSPW, and Initiator................................................................................ 12 D. Chem Wash..................................................................................................................... 14 E. Colloid.......................................................................................................................... 15 F. Water Charge, Rinse, and Dump....................................................................... 16 G. VCM Charge Lines and Tanks................................................................................ 17 H. Recovery System................................ 18 I. Work Items before Leak Testing....................................................................... 20 J. Leak Testing Loops........................... 21 IV. CHECKING OF INDIVIDUAL SYSTEMS................................................................................. 30 A. Steam and Condensate System............................................................................30 B. Cooling Tower and Water System ................................................................. 32 C. Colloid System............................................................................................................ 34 D. Chem Wash System....................................................................................................... 35 E. Initiator Injection System..................................... 36 F. Hydroquinone System................................................... .... ........................... . 36 G. AMS System..................................................................................................................... 36 H. Nitric Oxide (NO) System.....................................................................................37 I. Sewer System................................................... 37 J. Dump System ................................................................................................................. 37 K. HPSW System..................................................................................................................38 L. MSPW System..................................................................................................................40 M. Seal Oil System............................ 41 V. INTRODUCTION OF VCM AND FINAL REACTOR CHECKS ........................................... 43 A. Work Items before Water Charge ....................................................................... 43 B. Water Charge to All Four Reactors......................................... 44 C. Introduction of VCM.............................................................................................. 46 D. False Charge for Reactor 45-741 48 E. Work Items before First Real Charge.........................................................50 DTH 000089112 Table of Contents Page 2 Page No. VI. APPENDICES Appendix A - Process Operating Checks ................................................... Appendix B - Strapping Tables ...................................................................... Appendix C - Equipment List.......................................... ................................ Appendix D - Steam Tracing Isometrics ................................................... Appendix E - P&I Diagrams ............................................................................... 51 58 97 101 139 dTH 000089113 STARTUP MANUAL D-700 PVC REACTORS ABERDEEN, MISSISSIPPI Page 1 I. INTRODUCTION The purpose of this manual is to outline the steps to prepare the D-700 unit for operation. The scope starts from the time Tellepsen, the project contractor, turns over the unit to the plant until each reactor is ready for normal charge. The status of the unit and other associated systems are shown in the bases. The work items required for this manual are divided into three main groups. The first group (Section III) covers the flushing of lines with water and leak testing those that are in chemical service. The second group (Section IV) deals with the checking or testing of the various systems of the unit. The third group (Section V) covers the introduction of VCM and final reactor checkups prior to the first actual charge. Based on these work items and available manpower, MED will prepare a CPM (critical path method) schedule.^ Cl) CPM schedule is a method of scheduling work to be performed on a project by separating the project into independent activities and determining the sequence of these activities. The schedule is presented on a CPM chart depicting the order of activities that must be completed as work on the project progresses. DTH 000089114 Page 2 II. BASES The following are the bases of this startup manual: A. The unit is mechanically complete. B. All motors have been oiled and checked for correct rotation. C. All instrumentation has been checked by Contractor and Conoco and is properly functioning. D. Safety devices such as alarms, safety valves, and shutdown switches have been checked by Contractor and Conoco. E. All lines have been flushed with water, hydrotested, and drained by Contractor. All blinds have been removed by Contractor, except blinds at the tie-in to the VCM supply and tie-in to the existing inert recovery system. F. The unit and all associated systems have been field checked per P&I diagrams by Conoco and any deficiencies corrected. G. The Modicon has been completely checked as to interlocks, sequencing and opening of all on-off valves. H. Spools for the following meters have been installed by the con tractor: 1. VCM charge meters FQIC-701A and 701B. 2. Water charge meter FQIC-704. 3. Initiator charge meter FQIC-703. 4. Colloid charge meter FQIC-705, 5. Water meter for colloid makeup FQIC-706. 6. RVCM meter FQIC-702. I. Elements of filters are not to he installed by the contractor. These are to be installed hy Conoco after water flush, J. Individual systems are as shown on "Status of Individual Systems." DTH 000089115 STATUS OF INDIVIDUAL SYSTEMS Page 3 Systems Operating or Previously Operated New Cooling Tower X Cooling Water in Battery Limits VCM Supply System X(l) Slurry Transfer System X(2) Air Stripping to Silos and Blend Tanks X Breathing Air X Instrument Air <X Seal Oil X Steam and Condensate in Battery Limits Process Water Colloid Chem Wash Initiator Hydroquinone Injection AMS Emergency Short Stop Addition HPSW 7 ^ U MSPW ) ^ ** Sewer Blowdown Line Flushing Required X X X X X X X X X X Leak Testing Required X (5) X(5) X(6) X(6) X Checking and/or Lining Up of Pipes Required X X X X X X X X X X X X X X 1 X DTH 000089116 STATUS OF INDIVIDUAL SYSTEMS (CONTINUED) Systems Evacuation Charge Recovery Dump Rinse Firewater Reactors Operating or Previously Operated , 3> Line Flushing Required X X X X X Leak Testing Required XC6) X(5) (7) X(4) Checking and/ur Lining Up of Pipes Required X X X X Notes: (1) VCM supply system is assumed to be operating and line from VCM transfer pumps to fresh VCM storage tank has been flushed and leak tested, (2) Revised slurry transfer system will be operating. Lines from battery limits to this system will be flushed. (3) Firewater system is assumed to have been previously checked by Contractor and Conoco. Check should have included actual activation of deluge system at set point specified by design. (4) Two leak tests of each reactor system are required--one with the reactor system blocked up to the first valves of its main lines and another with the reactor system blocked up to the second valves of its main lines. (5) Leak testing to be done immediately after flush. (6) Included in leak test of reactor systems. (7) Contractor to hydrotest recovery system as one integral unit. DTH 000089117 Page 5 III. FLUSHING AND LEAK TESTING OF LINES This section contains guides for flushing lines in the various systems and leak testing those that are in chemical service. The systems are grouped into different flushing areas. Since piping in the unit is interconnected, part of the piping in one system may be included in more than one flushing area. The flushing guide is shown as diagrams consisting of vertical and horizontal lines. Each horizontal line defines a flushing route. The vertical lines indicate the point where a flushing route connects to another route. Flush routes or systems connected to a common vertical line may be flushed simultaneously. fZ'C-oS'ck 1/u^vIia^ Process water will be used for flushing. Main headers of the process water system are initially flushed. Using water from these headers, the following areas may be flushed simultaneously: Chem Wash Area; HPSW, MSPW, and Initiator Area; Colloid Area; and Water Charge, Rinse, and Dump Area. As soon as charge, rinse, and dump lines in reactor 45-741 are flushed, this reactor is filled with water using the water charge pumps. The reactor is opened to the recovery system through the main recovery header. Process water flowing in the main recovery header is used to flush the recovery area. The three VCM tanks will be set up to be filled with water from a fire hydrant to facilitate flushing of the VCM charge lines and tanks area. To ensure that all lines in the system are flushed, the flushing crew should mark out in the P&I diagrams the routes that are done. DTH 000089118 Page 6 111 FLUSHING AND LEAK TESTING OF LINES (CONTINUED) The HPSW system is put into service before flushing areas requiring HPSW seals to pumps or compressors. The seal oil system is checked and put into service before leak testing of the reactor systems. Checking of the HPSW and seal oil systems are discussed in Section IV. With the HPSW and seal oil systems in service, the leak testing of lines in NO service^ and the reactor systems can be started. First, each reactor is blocked up to the first valves of its main lines and pressured. Then each reactor is blocked up to the second valves of its main lines and pressured. The NO systems for each reactor are leak tested separately. Leak test pressure will be limited to 85 percent of the lowest set pressure of safety valve or rupture disc in each loop. Test pressure of loops without safety valve or rupture disc will be limited to 150 psig. DTH 000089119 Cl) Leak testing of other lines in chemical service such as VCM charge, colloid, and chem wash is done immediately after flush. This is ac complished by running the pumps in the chemical lines and visually checking for leaks. Page 7 III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) A. Work Items before Water Flush The following work items are required before flushing of lines: 1. Disconnect HPSW supply to seals of the following pumps and compressors. / a. VCM charge pumps 72-875 and 876. b. RVCM charge pumps 72-877 and 878. c. Water recirculation pumps 72-889 and 890. d. Seal water pumps 72-891 and 892. "T i ie' RVCM transfer pumps 72-893 and 894. Slurry transfer pumps 72-896 and 897. . Recovery vacuum pumps 72-901 and 902. |h. Recovery compressors 72-903, 904, and 905. 2. Disconnect MSPW supply to the following agitators: 51-101 b. 51-102 I 51-103 \}J< 3. Set up the fresh VCM and RVCM storage tanks to be filled with vj\\\ w-* water from the fire hydrant located south of battery limits. Tellepsen are to install two-inch valves at PG nozzles at the bottom of each vessel. Pull PG connection and hookup hose adapter. Start filling vessels. \\<Q ^ y 4. Flush and leak test inert line tie-in to the existing recovery \vO-fe system. Refer to Section III.H, Item No. 47. DTH 000089120 f5. Bring m sLeam lo Lh'e'last block valve in-each equipment. Also; oggir-aJr--steam tracing lines. This -Xs -the--fi~rsF part of sffeym -mrf-wvndansflfa rhepknnf <H grugsgd Ifrgm-*-;--gprHnn IV. Page 8 /"N III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) A. Work Items before Water Flush (Continued) 6. Close the following miscellaneous valves prior to water flush: a. At chem wash area: (1) Process water valve on line WP-7001 at cleaning solu tion tank 45-767. (2) Process water valve on line WP-7002 at intersection of line XO-7001. b. At dump system: (1) Process water valve on line WP-7005 at suction line of slurry transfer pump 72-897. (2) Process water valve on line WP-7004 at the suction line of slurry transfer pump 72-896. (3) On-off valve CV-863 on line WP-7010 at the intersec tion of line WP-7003. (4) Process water valve on line WP-7009 at the intersec tion of line WP-7003. (5) Slurry control valve LIC-725 at the slurry inlet line to the Sweco.* (6) On-off valve CV-864 on HPSW line to the seal of slurry transfer pump 72-896. (7) On-off valve CV-866 on the HPSW line to the seal of slurry transfer pump 72-897. c. At HPSW, MSPW, and initiator systems: (1) Inlet valve of service water filter 64-724. (2) Bypass valve of service water filter 64-724. (3) Block valve immediately before initiator charge meter FQIC-703. DTH 000089121 *Registered Trademark Page 9 III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) A. Work Items before Water Flush (Continued) (4) Inlet valve of MSFW surge drum 45-759. (5) Block valve and bypass valve of pressure controller PCi-818 at the common discharge piping of MSPW pumps 72-887 and 888. d. At recovery systems: (1) Process water valve on line WP-7128 at recovery knock out drum 45-760. (2) Process water valve on line WP-7129 at recovery knock out drum 45-761. (3) Process water valve on line WP-7125 at hydroquinone tank 45-765. (4) HPSW valve on line WP-7026 at seal water separator 45-762. (.5) HPSW valve on line WP-7027 at seal water separator 45-763. (6) HPSW valves to rotameters FI-726 and 727. (7) HPSW valves to seals of water recirculation pumps 72-889 and 890. (8) HPSW valves to seals of seal water pumps 72-891 and 892. (9) On-off valve CV-813 on line WP-7028 to vacuum pump 72-901. (10) On-off valve CV-823 on line WP-7029 to vacuum pump 72-902. DTH 000089122 Page 10 III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) A. Work Items before Water Flush (Continued) e. At colloid system: (1) Process water valve at the inlet of colloid makeup filter 64-721. (2) Bypass valve of colloid makeup filter 64-721. (3) Process water valve on line WP-7177 before control valve manifold of TCV-704B. f f. At water charge and rinse systems: (1) Process water valve on line WP-7083 at hot water tank 45-748. (2) Block valve of control valve TRC-703 on bypass line of hot water tank 45-748. (3) On-off bypass valve CV-808 of control valve TRC-303. (4) On-off valve CV-709 on line WP-7064. g. Reactor area: (1) HPSW valves at initiator injection lines of reactors 45-741, 742, 743, and 744. (2) HPSW valves at AMS short stop charge pots 45-755, 756, 757, and 758. (3) MSPW valves at water injection lines of reactors 45-741, 742, 743, and 744. h. Blowdown tank area: (1) HPSW valve on line WP-7179 to the blowdown tank 45-319. (2) HPSW valve before rotameter FI-808 (flush to level con trol float), DTH 000089123 (3) HPSW valves before rotameters FI-814 and 815 (to pump seal of blowdown tank pump 72-900). I I I . FLUSHING AND LEAK TESTING OF LINES (CONTINUED) Page 11 C-J H CD CD O O O O X Page 12 I I I . FLUSHING AND LEAK TESTING OF LINES (CONTINUED) Page 13 CD <N H CT) 03 Page 14 360 to Q) 4H=I taQ> T3 GtO ca 0) 0oo0 o o K E-t o t0o1 Vl GtoO 0) 43 qj 4= 0) 0) a4c3=o (0 0) U CO 3 60 QJ O 33 H H rl 4J CO rH cj O QJ iH QJ g U 45 3 P o o p3 O u a 0) QJ o 4= IJ to o rH O > CO & H e 43 p 4-> Cm JJ >n CO rH 0) Ps rH rH cO 3 CO rl > a 4J -0 a tpo 4* <0 3 3 QJ 60 c rH 3 H iH 4-> >> CO r--1 P QJ cO QJ 4J CJ o CO Vi H 43 CO 3 t-H Mu 3 -a QJ 0 O QJ rH u CO a a rl JS 0) Vi > u to QJ 4J # Q. & tO 4= 3 CO 3 0) 3 a CJ QJ rH QJ AJ -3o Sto Mu 00 QJ C jC MOW M *rl U muVim u w dQJ VI W H Uqj c 4: uu <3 qj p u pd Q 205 FLUSHINGI I I . AND LEAK TESTING OF LIS E S ( CONTINUED) Page 15 CD <rN'H <35 CD O O O O ^ j- U M *3 co G r 1>1 C_ 3 Cu)tHr1 5g C/5 K I I . FLUSHING AND LEAK TESTING OF LINES (CONTINUED) N o te s : (1 ) See Ite m 2 in "P ro c e s s W a te r" f lu s h . C.2) P lu sh t o s lu r r y t r a n s f e r lin e s in v o lv e s flu s h in g a l l lin e s to b le n d ta n k s T -6 4 6 , 647, 648, 6 4 9 , 4 0 7 , and 661. Page 16 05 CO T"t 05 CO O O o o Page 17 O C1--OI 03 00 o o o o (sHc Q N otes: (1) A ll tanks should be in it ia lly f u ll o f w a te r. (2 ) Run th e pump w h ile flu s h in g and v is u a lly c h e c k th e lin e s f o r le a k s . Page 18 S3 I I I . FLUSHING AND LEAK TESTING OF LINES (CONTINUED) N o te : (1 ) See Ite m 19 o f "W a te r C harge, R in s e , and Dump" flu s h . Page 19 a <N CO rO mI O) n 00 O r** mI O O O 1 K EH Q o s rH X n3 orH Q> X 0) \C n r- SS a 0 rH O T3 H a> o> gXO C -u* > o P4 h ou o> U (HI *8 C C S *H *H ,* rH O- O 3 0 0) Stf iH X O X +J M >> oi (ft in > H 01 CO 0) X O0) 4J u>. 0) X 0) X4J M3 Xu FLUSHINGI I I . AND LEAK TESTING OF LINES (CONTINUED) > TJ 00 a0j inI <u zo Page 20 III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) Work Items before Leak Testing 1. Remove the spools and install meters listed in Item H of "Bases." 2. Reconnect MSPW supply to agitators in Item 2 of "Work Items before Water Flush." 3. Check and put the seal oil system into service. The procedure for check is in Section IV. DTH 000089133 Page 21 /---V III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) J. Leak Testing Loops 1. Loop No 1--Reactor 45-741 system up to first valve of the main lines. The test pressure is 130 psig. Pressurize the loop with HPSW. The following valves are to be closed: a. Vent valve CV-714. b. Condenser rinse valve CV-713. c. Inert vent valve CV-715. d. RVCM valve CV-716. e. Reactor rinse valve CV-717. f. Steam stripping valve CV-712. g. Resin sampler ram valve. h. Initiator injection valve CV-753. i. Colloid charge valve CV-711. j. Block valve on AMS line closest to the reactor. NO charge valve CV-885 and its bypass valve. 1. Main reactor charge valve CV-710 vw*'a*/*l4s. Water injection valve to the reactor. Seal water valve to the agitator and its bypass valve. au aXtL- > DTH 000089134 Page 22 III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) J. Leak Testing Loops (Continued) 2. Loop No. 2^^--Reactor 45-741 system up to second valve of the main lines. The test pressure is 130 psig. Pressurize loop with HPSW through the initiator charge system. The following *valves are to be closed: a. Vent valve CV-714. ^f^ c. Inert vent valve CV-715. Evacuation valve CV-762. \\aXv j> RVCM valve CV-752. ^ e. Chem wash valve CV-751. f. Rinse valve CV-750. g. Resin sampler ram valve. h. NO charge valve CV-885 and its bypass valve. Block valve on AMS line closest to the reactor. Initiator charge valve CV-763. Initiator sewer valve CV-757. VCM charge valve CV-754. m. Slurry dump valve CV-758. n. Chem wash return valve CV-760. co. Hot water charge valve CV-755. p. Sewer valve CV-759. q. Colloid charge ram valve CV-711. r. Water injection valve to the reactor. s. Seal water valve to the agitator and its bypass valve. oX- vvi^ H DTH 000089135 Cl) After leak test of this loop, blow steam into the reactor through the steam stripping line. Page 23 ^ III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) J. Leak Testing Loops (Continued) 3. Loop No. 3--Reactor 45-742 system up to first valve of the main lines. Test pressure is 130 psig. Pressurize the loop with HPSW through the initiator charge system. The following valves are to be closed; a. Vent valve CV-724. b. Condenser rinse valve CV-723. c. Inert vent valve CV-725. d. RVCM valve CV-726. e. Reactor rinse valve CV-727. f. Steam stripping valve CV-722. g. Resin sampler ram valve. h. Initiator injection valve CV-768. i. Colloid charge valve CV-721. j. Block valve on AMS line closest to the reactor. k. ' NO charge valve CV-886 and its bypass valve. l. Main reactor charge valve CV-720. m. Water injection valve to the reactor. n. Seal water valve to the agitator and its bypass valve. DTH 000089136 III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) J. Leak Testing Loops (Continued) 4. Loop No. 4^^--Reactor 45-742 system up to second valve of the main lines. Test pressure is 130 psig. Pressurize the loop with HPSW through the initiator charge system. The following valves are to be closed: a. Vent valve CV-724. b. Inert vent valve CV-725. c. Evacuation valve CV-765. d. RVCM valve CV-7d7. e. Chem wash valve CV-766. f. Rinse valve CV-764. g. Resin sampler ram valve. h. Steam stripping valve CV-722. i. NO charge valve CV-886 and its bypass valve. j. Block valve on AMS line closest to the reactor. k. Initiator charge valve CV-776. l. Initiator sewer valve CV-777. m. VCM charge valve CV-769. n. Slurry dump valve CV-772. o. Chem wash return valve CV-773. p. Hot water charge valve CV-770. q. Sewer valve CV-774. r. Colloid charge ram valve CV-721. s. Water injection valve to the reactor. DTH 000089137 t. Seal water valve to the agitator and its bypass valve. CL) After leak test of this loop, blow steam into the reactor through the steam stripping line. Page 25 III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) J. Leak Testing Loops (Continued) 5. Loop No. 5--Reactor 45-743 system up to first valve of the main lines. Test pressure is 130 psig. Pressurize the loop with HPSW through the initiator charge system. The following valves are to be closed: a. Vent valve CV-734. b. Condenser rinse valve CV-733. c. Inert vent valve CV-735. d. RVCM valve CV-736. e. Reactor rinse valve CV-737. f. Steam stripping valve CV-732. g. Resin sampler ram valve. h. Initiator injection valve CV-782. i. Colloid charge valve CV-731. j. Block valve on AMS line closest to the reactor. k. NO charge valve CV-887 and its bypass valve. l. Main reactor charge valve CV-730. m. Water injection valve to the reactor. n. Seal water valve to the agitator and its bypass valve. DTH 000089138 Page 26 III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) J. Leak Testing Loops (Continued) 6. Loop No. 6^--Reactor 45-743 system up to second valve of the main lines. Test pressure is 130 psig. Pressurize the loop with HPSW through the initiator charge system. The fol lowing valves are to be closed: a. Vent valve CV-734. b. Inert vent valve CV-735. c. Evacuation valve CV-779. d. RVCM valve CV-781. e. Chem wash valve CV-780. f. Rinse valve CV-778. g- Resin sampler ram valve. h. Steam stripping valve CV-732. i. NO charge valve CV-887 and its bypass valve. 3- Block valve on AMS line closest to the reactor. k. Initiator charge valve CV-790. 1. Initiator sewer valve CV-791. m. VCM charge valve CV-783. n. Slurry dump valve CV-786. 0. Chem wash return valve CV-787. P* Hot water charge valve CV-784. q- Sewer valve CV-788. r. Colloid charge ram valve CV-731. 000089139 s. Water inject valve to the reactor. t. Seal water valve to the agitator and its bypass valve. (1) After leak test of this loop, blow Steam into the reactor through the steam stripping line. Page 27 ^ III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) J. Leak Testing Loops (Continued) 7. Loop No. 7--Reactor 45-744 system up to first valve of the main lines. Test pressure is 130 psig. Pressurize the loop with HPSW through the initiator charge system. The following valves are to be closed: a. Vent valve CV-744. b. Condenser rinse valve CV-743. c. Inert vent valve CV-745. d. RVCM valve CV-746. e. Reactor rinse valve CV-747. f. Steam stripping valve CV-742. g. Resin sampler ram valve. h. Initiator injection valve CV-795. i. Colloid charge valve CV-741. j. Block valve on AMS line closest to the reactor. k. NO charge valve CV-888 and its bypass valve. l. Main reactor charge valve CV-740. m. Water injection valves to the reactor. n. Seal water valve to the agitators and its bypass valve. DTH 000089140 III. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) J. Leak Testing Loops (Continued) 8. Loop No. 8^^--Reactor 45-744 system up to second valve of the main lines. Test pressure is 130 psig. Pressurize the loop with HPSW through the initiator charge system. The fol lowing valves are to be closed: a. Vent valve CV-744. b. Inert vent valve CV-745. c. Evacuation valve CV-793. d. RVCM valve CV-8G5. e. Chem wash valve CV-794. f. Rinse valve CV-792. g. Resin sampler ram valve. h. Steam stripping valve CV-742. i. NO charge valve CV-888 and its bypass valve. j. Block valve on AMS line closest to the reactor. k. Initiator charge valve CV-803. l. Initiator sewer valve CV-804. m. VCM charge valve CV-796. n. Slurry dump valve CV-799. o. Chem wash return valve CV-800, p. Hot water charge valve CV-797. q. Sewer valve CV-801. r. Colloid charge ram valve CV-741. s. Water injection valve to the reactor. 000089141 t. Seal water valve to the agitator and its bypass valve. (1) After leak test of this loop, blow steam into the reactor through the steam stripping line. Page 29 m. FLUSHING AND LEAK TESTING OF LINES (CONTINUED) J. Leak Testing Loops (Continued) Loop No. 9--NO system for reactor 45-741. Test with N2 from N2 bottle equipped with pressure regulator. Hold the test pres sure at 150 pslg for at least thirty minutes. Introduce N2 at the bleed valve of PG-798. Close the following valves: a. Block valve at NO bottles manifold. b. CV-885 and its bypass valve. 10. Loop No. 10--NO system for reactor 45-742. Test with N2 from the N2 bottles equipped with pressure regulator. Hold test pressure at 150 psig for at least thirty minutes. Introduce N2 at the bleed valve of PG-799. Close the following valves: a. Block valve at NO bottles manifold. t-- b. CV-886 and its bypass valve. 11. Loop No. 11--NO system for reactor 45-743. Test with N2 from the N2 bottle equippped with pressure regulator. Hold test pressure at 150 psig for at least thirty minutes. Introduce N2 at the bleed valve of PG-800. Close the following valves: a. Block valve at NO bottles manifold. b. CV-887 and its bypass valve. 12. Loop No. 12--NO system for reactor 45-744. Test with N2 from the N2 bottle equipped with pressure regulator. Hold test pres sure at 150 psig for at least thirty minutes. Introduce N2 at the bleed valve of PG-801. Close the following valves: a. Block valve at NO bottles manifold. b. CV-888 and its bypass valve. DTH 000089142 CHECKING OF INDIVIDUAL SYSTEMS Before putting the systems into actual service, each system is to be checked to make sure it operates properly. The specific items to be checked and the detailed procedure for each system are covered in this section. Checking of evacuation, charge, recovery, and blowdown systems are included in Section V. A. Steam and Condensate Systems a A <A aXL W'' jl> a -t The checkout of the steam and condensate systems primarily involves lining up pipes from steam headers to equipment and the condensate return lines to condensate headers. This is to be done in two parts. The first part, to be done before the start of water flush to systems will consist of bringing steam up to the last block valve at each equipment and opening steam tracing lines. The second part, to be done after the water flush to the systems, involves admitting steam to the equipment by opening the remaining block valve and lining out the condensate return lines to headers. The steam and conden sate lines are as follows: 1. Steam to hot water preheater 55-332 and its condensate return linnee.. 2. Steam to hot water tank heater 55-333 and its condensate return line. 3. Steam to colloid makeup tank 45-731 and its condensate return line. 4. Steam to reactor ejector cyclone separator 45-768. 5. Steam to blowdown tank sparger. DTH 000089143 6. Steam to blowdown tank 45-319 pressure control. 7. Steam to reactor jacket eductor EE-701. Page 31 y/-~N IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) . A. Steam and Condensate Systems (Continued) 8. Steam to reactor jacket eductor EE-702. 9. Steam to reactor jacket eductor EE-703. 10. Steam to reactor jacket eductor EE-704. 11. Steam to cleaning solution heater 55-339 and its condensate return line. 12. Steam stripping line to reactor 45-741. 13. Steam stripping line to reactor 45-742. 14. Steam stripping line to reactor 45-743. 15. Steam stripping line to reactor 45-744. 16. Steam to utility station No. 1, operating level. 17. Steam to utility station No. 2, grade level. f 18. Steam to utility station No. 3, grade level. 19. Steam to utility station No. 4, second level. '20. Steam Tracings--The steam-traced pipes are divided into twenty separate groups in the isometric drawings. Steam to each group of lines is controlled by one valve. Open this valve. In the condensate return line from each group, there is a valve before and after the trap. These valves should be opened. The iso metric drawings are in Appendix D. A summary of these drawings 'TW is as follows: DTH 000089144 IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) A. Steam and Condensate Systems (Continued) Group No. LOCATION OF STEAM VALVE Drawing Sheet No. No. LOCATION OF TRAP Drawing Sheet No. No. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 7-1 Z.-Z- ST-8 ST-37 ST-37 ST-13 ST-129 ST-12 ST-128 ST-129 ST-128 ST-3 ST-51 ST-45 ST-45 ST-7 ST-8 ST-6 ST-9 ST-10 ST-11 ST-11 5 of 5 6 of 24 14 of 24 5 of 7 2 of 2 2 of 7 2 of 2 1 of 2 1 of 2 l 1 of 1 ! 2 of 3 4 of 4 2 of 4 1 of 1 1 of 1 1 of 1 1 of 1 1 of 1 1 of 2 2 of 2 Cooling Tower and Water System ST-122 ST-37 ST-3 7 ST-37 ST-19 ST-1 ST-21 ST-3 7 ST-37 ST-2 ST-51 ST-5 ST-46 ST-4 ST-5 ST-6 ST-9 ST-12A ST-11 ST-11 7 of 7 12 of 24 20 of 24 23 of 24 1 of 1 1 of 1 1 of 1 3 of 24 4 of 24 1 of 1 3 of 3 4 of 4 2 of 3 1 of 1 1 of 1 1 of 1 1 of 1 1 of 1 1 of 2 2 of 2 The new cooling tower, 50-006, supplies the cooling water to battery limits. The cooling tower will have to be checked and put into service. The checkout of the cooling water system in the unit will involve lining up supply and return lines and making sure there is actual flow. . Cooling Tower Check and Startup Line up piping from pumps 72-906, 907, and 908 through bypass control valve PIC-245 back to the cooling tower. Make sure butterfly valves on top of the tower are open. Leave the bypass valve of the control valve closed. b. Put controller PIC-245 on automatic. DTH 000089145 Page 33 IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) B. Cooling Tower and Water System (Continued) 1. Cooling Tower Check and Startup (Continued) c. Start pump 72-908 and check for flow. d. Shut down pump 72-908, start pump 72-907, and check for flow. e. Shut down pump 72-907, start pump 72-906, and check for flow. f* Leave pump 72-906 running. / 2. Line Up Lines in the Unit With one cooling tower pump on and water recirculating through the bypass line, line up the following lines in the unit. After f j4. lining up these pipes, start one additional cooling tower pump 72-907. Leave both pumps 72-9,06 and 907 running. -j ys'l 1 a. Cooling water supply and return line for reactor condenser 55-328. v b. Cooling water supply and return line for reactor jacket 45-741. c. Cooling water supply and return line for reactor condenser 55-329. d. Cooling water supply and return line for reactor jacket 45-742. e. Cooling water supply and return line for reactor condenser 55-330. f. Cooling water supply and return line for reactor jacket /""V 45-743. g. Cooling water supply and return line for reactor condenser 55~331- DTH 000089146 Page 34 IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) B. Cooling Tower and Water System (Continued) 2. Line Up Lines in the Unit (Continued) h. Cooling water supply and return line for reactor jacket 45-744. i. Cooling water supply and return line for seal oil reser voir of seal oil pressure unit PA-701. j. Cooling water supply and return line for seal oil reser voir of seal oil pressure unit PA-702. k. Cooling water supply and return line for water circula tion cooler 55^334. l. Cooling water supply and return line for seal water cooler 55-335. m. Cooling water supply and return line for seal water cooler 55-336. n. Cooling water supply and return line for RVCM condensers 55-337 and 338. o. Cooling water supply and return line for colloid makeup tank 46-751. C. Colloid System(l) The checkout of the colloid system will consist of lining up the pipes and installing filter elements. Checkout of water meter ^ W and heating and cooling systems will be done during initial col* J loid makeup. \ 1. Install elements of filters 64-722, 723, and 724. 2. Line up process water to colloid makeup tank 45-751 through filter 64-721. DTH 000089147 (1) Checkout to be done right after leak test of colloid system. Page 35 IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) C. Colloid System (Continued) 3. Line up outlet from colloid makeup tank 45-751 to colloid storage tank 45-752 through pump 72-881 and filter 64-722. 4. Line up outlet from colloid storage tank 45-752 to colloid charge tank 45-753 through pump 72-882 and filter 64-723. Leave outlet valve at the colloid storage tank closed. 5. Line up outlet from colloid charge tank 45-753 to colloid charge header through pump 72-883/884. D. Chen Wash System The checkout of the chem wash system will consist of lining up of pipes and checking the cleaning solution heater. 1. Install element of cleaning solution strainer 64-734. 2. Line up caustic line to cleaning solution tank 45-767. Leave valve at the tank closed. 3. Line up the tank recirculation loop from the tank through pump 72-898/899, cleaning solution heater 55-339, and back to the tank. 4. Add water to the tank until it is about 75 percent full. 5. Open valve CV-873 and start pump 72-898/899. 6. Set the heater temperature controller to 190F and activate the controller. Check to see that the water in the tank heats up. 7. Shut down pump 72-898/899 and close valve CV-873. 8. Line up the heater outlet piping to the reactor system. 9. Line up the chem wash return line from reactors to the suction of pumps 72-898 and 72-899 through filter 64-734. ^ 000089148 10. Drain water in the tank to the sewer. Page 36 IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) E. Initiator Injection System Purposes of the initiator injection check are to make sure pressure switch PS-703 and meter of FQIC-703 are functioning properly. Procedure 1. Block in initiator pot 45-750 but leave the valve at the funnel open. 2. Manually add from the board enough water (about 15 gallons) until the pot overflows to grade through the funnel. 3. Manually add from the board ten gallons of water and catch the overflow in a ten-gallon bucket. Check to see if the meter is correct. Do this step two times. 4. Close the valve at the initiator funnel. 5. Pressurize the pot with HPSW and check to see if the light indicator comes on at the panel when the pressure is 180 psig. 6. Drain the pot to the sewer. F. Hydroquinone System 1. Line up the hydroquinone tank outlet to the suction of pumps 72-891 and 72-892 through hydroquinone injection pump 72-895. 2. Block in the hydroquinone tank and open the nitrogen line. Check to see if the pressure is about 1 psig. G. AMS System Check to see if lines are clear by flushing the line to the agi tators with HPSW. Note the flow on the rotameter. DTH 000089149 Page 37 IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) H. Nitric Oxide (NO) System Check to make sure the valves between the emergency NO short stop bottles and the pressure alarm probe are open. Leave all other valves closed. Check to see that six emergency short stop bottles are secured in place for each reactor. I. Sewer System The sewer system is to be visually inspected. The sewer must be free of blocking materials or other objects which might cause the sewer to overflow or backup. J. Dump System The purposes of the check are to make sure the level controller of the slurry dump tank works properly and sequencing of the valves and pumps are correct. Procedure 1. Install the element of slurry strainer 64-733. 2. Line up the piping from the reactor systems to either slurry blend tanks 89-646, 647, 648, or 649 through slurry strainer 64-733, slurry dump tank 45-766, and pumps 72-896 and 897. 3. Charge 1,000 counts of water to reactor 45-741j vent the reactor. 4. Start the Sweco* strainer. 5. Start the Sweco* exhauster and leave it continuously running. 6. Turn the interlock selector switch to "dump." 7. Put pumps 72-896 and 897 on "run" position. 8. Check to see if the pump seal water valves are open before the pumps start. DTH 000089150 *Registered Trademark Page 38 n- IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) J. Dump System (Continued) 9. Observe if the level in the dump tank is automatically con trolled. 10. When dumping of water is complete, put the pumps on "stop" position. The pumps must shut down and the seal water valves close. K. HPSW System(1) The purposes of the HPSW check are as follows: 1. Line up of piping and checking of the mechanical seal flow rates to the pumps. 2. Check to see if the spare pump comes on on low pressure. Procedure 1. Install the filter element of service water filter 64-724. 2. Line up the process water line to the different HPSW headers through filter 64-724 and pump 72-885/886. 3. Start one HPSW pump, 72-885/886. 4. Line up the HPSW piping to the following pumps and adjust the mechanical seal flow to the normal rates. a. VCM charge pumps 72-875 and 72-876, 1.3 gpm. b. RVCM charge pumps 72-877 and 72-878, 1.3 gpm. c. Water recirculation pumps 72-889 and 72-890, 1 gpm. d. Seal water pumps 72-891 and 72-892, 2 gpm. e. RVCM transfer pumps 72-893 and 72-894, 1.3 gpm. f. Slurry transfer pumps 72-896 and 72-897, 3 gpm. g. Blowdown tank pump 72-900, 3 gpm. DTH 000089151 (1) The HPSW system is to be checked and put into service before flush to areas requiring HPSW seals. Page 39 IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) K. HPSW System (Continued) 5. Line up HPSW piping to the following vacuum pumps and com pressors. Adjust the inboard seal flush to 0.5 gpm and the mechanical seal flush to 1 gpm. a. Recovery vacuum pumps 72-901 and 72-902. b. Recovery compressors 72-903, 72-904, and 72-905. 6. Line up HPSW piping to the following pipes and vessels. Leave the last valve in the HPSW line to each user closed. a. Seal water separators 45-762 and 45-763. b. Initiator injection pot 45-750. c. Blowdown tank 45-319. d. AMS short stop charge pots 45-755, 45-756, 45-757, and 45-758. e. Steam stripping line SL-7008. f. Steam stripping line SL-7009. g- Steam stripping line SL-7010. h. Steam stripping line SL-7011. i. Line HM-7050. j- Line HM-7051. k. Line HM-7052. 1. Line HM-7053. m. Line HM-7225. n. Line HM-7228. o. Line HM-7231. Line HM-7234. P q- Line HM-7108 through FI-744 bullseye. MH 0089162 Page 40 ^ IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) K. HPSW System (Continued) 7. Test both HPSW pumps to see whether one will start automati cally while the other is running and discharge pressure drops below 180 psig. a. Start one pump. b. Slowly pinch the block valve of the running pump until PG-774 shows about 180 psig. Check to see if the other pump automatically starts (do not completely close the pump discharge valve). 8. Start and leave one pump, 72-885/886, running. L. MSPW System The purposes of the MSPW check are as follows: 1. Normal pipe lineup. 2. Adjustment of mechanical seal flow rate. 3. Check to see if spare pump starts automatically on the low discharge pressure. Procedure 1. Line up the process water from filter 64-724 to the MSPW header through pump 72-887/888. 2. Start one pump. 3. Line up water injection lines and adjust the flow to 2 gpm rate to reactors 45-741, 742, 743, and 744. 4. Line up seal water lines and adjust the flow to 5 gpm rate to agitators 51-101, 102, 103, and 104. DTH 000089153 5. Test both MSPW pumps to see whether one will start automati cally while the other is running and discharge pressure drops below 180 psig. Page 41 IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) L. MSPW System (Continued) a. Start one pump. b. Slowly pinch the block valve of the running pump until PG-775 shows about 180 psig. Check to see if the other pump automatically starts (do not completely close the pump discharge valve). 6. Fill up MSPW surge drum 45-759 to the normal level. Block it in and leave the nitrogen line open. 7. Start up the MSPW system. Adjust the flow rate to the agi tators to 5 gpm. M. Seal Oil System(l) The purposes of the check are to: 1. Make sure one seal oil unit starts automatically on the low oil level or discharge pressure. 2. The emergency oil drums are full. 3. Adjust the flow of the seal oil. Procedure 1. Adjust presssure regulator PCi-764 to 240 psig. 2. Test both seal oil units to see whether one unit starts auto matically on low discharge pressure (below 205 psig). Make sure all reactor agitators are off. DTH 000089154 (1) The seal oil system is to be checked and put into service before leak testing of the reactor systems. Page 42 IV. CHECKING OF INDIVIDUAL SYSTEMS (CONTINUED) M. Seal Oil System (Continued) a. Start one unit. b. While watching the pressure gauge at the pump discharge, slowly pinch the valve at the pump discharge until PG-786 shows about 205 psig. Check to see if the other unit starts automatically and the unit running shuts down (do not com pletely close the valve at the pump discharge). 3. Test both seal oil units to see whether one unit starts auto` matically on low oil reservoir level. Make sure all the reactor agitators are off. a. Start one unit. b. Slowly drain the oil to the sewer from the seal oil reser voir of the running unit. Check to see if the other unit starts automatically and the running unit shuts down when the low oil level is sensed. 4. Check and make sure that the emergency seal oil drums for each unit are filled to normal level, the drums are blocked in, and the nitrogen lines are open. 5. Start one unit. Adjust the flow rates to the agitators to 1 gpm. DTH 000089155 Page 43 V. INTRODUCTION OF VCM AND FINAL REACTOR CHECKS The final preparations for the first real charge are covered in this section. Using water instead of VCM, initiator, and colloid, each reactor is actually charged using normal procedure. During this charge, the sequencing of valves is carefully checked. The colloid and water charge meters are also calibrated. After the water charge to each reactor, VCM from outside battery limits is initially transferred to the VCM receiver. Reactor 45-741 is charged with VCM and its jacket temperature maintained at 100F. The recovery system is then opened to the reactor and VCM storage tanks to displace the water with VCM vapor. Vessels in the recovery system are drained to normal levels. A false charge of 300 counts of VCM is done on reactor 45-741 to cali brate the VCM charge meter. The charged VCM is then actually recovered using normal recovery procedure. Operation of the recovery train is carefully checked while recovery is going on. A. Work Items before Water Charge 1. Make sure all lines are full of water. 2. Drain water from all four reactors to the sewer. 3. Rinse all four reactors and condensers; drain water. 4. Open the manhead and inspect the reactors to make sure they are clean. 5. Make up hydroquinone solution. DTH 000089156 V. INTRODUCTION OF VCM AND FINAL REACTOR CHECKS (CONTINUED) A. Work Items before Water Charge (Continued) 6. Make up colloid solution and leave it at the makeup tank until needed.^ Make up colloid solution at least twelve hours beofre the false charge. 7. Install elements of the following filters: a. Process water charge filter 64-716. b. Process water filter 64-720. c. RVCM filter 64-719. d. VCM charge filters 64-718 and 742. e. Seal water filters 64-731 and 732. f. Blowdown tank drain strainer 64-741. B. Water Charge to All Four Reactors 1. Purposes a. Check the reactor evacuation system. b. Simulate and check the charge sequence using water. c. Calibrate water charge meter. d. Calibrate the colloid charge meter. e. Line up of piping for reactor charge. 2. Procedure a. Line up the following streams: (1) Process water to hot water tank 45-748 through filter 64-720 and heater 55-332. (2) Hot water from hot water tank 45-748 to hot water charge header through pumps 72-879 and 880. DTH 000089157 (1) During initial colloid makeup, check water meter FQIC-706 and observe carefully the operation of the heating and cooling systems. V. INTRODUCTION OF VCM AND FINAL REACTOR CHECKS (CONTINUED) B. Water Charge to All Four Reactors (Continued) 2. Procedure (Continued) (3) VCM charge line from VCM receiver 45-745 to VCM charger header through pump 72-885/886 and filter 64-718/742. (4) RVCM charge line from RVCM receivers 89-520 to the suction of pump 72-875/876 through pump 72-877/878. (5) Water bypass through TRC-706. b. Prepare a "dummy" recipe consisting of the following: (1) One-hundred counts on VCM meter. (2) Forty counts on RVCM meter. (3) Five-hundred counts on water charge meter (4) Fifty counts on colloid charge meter(5) c. Make precharge checks. d. Evacuate the reactor to 28.5 inches Hg. Follow the normal procedure. e. Prepare the initiator charge pot for charge. Follow the normal procedure (omit addition of initiator). f. Proceed with the normal reactor charge using the "dummy" recipe in Item No. 2.b. g. Dump water to the sewer. DTH 000089158 (1) Charge reactor in this order: 45-741, 742, 743, and 744. (2) For reactor 45-741, follow procedures a through g. (3) For reactor 45-742, calibrate water charge meter. Follow procedures c through g. (4) For reactor 45-743, calibrate water and colloid charge meters. Use actual colloid solution for colloid charge. Follow procedures c through g. (5) For reactor 45-744, calibrate colloid charge meter using actual col- solution. Follow procedures c through g. (6) Refer to "Process Operating Checks, Water Charge to All Four Reactors" in Appendix A. Page 46 V. INTRODUCTION OF VCM AND FINAL REACTOR CHECKS (CONTINUED) C. Introduction of VCM 1. Purposes a. Clear the VCM storage tanks of water. b. Bring in VCM from outside the battery limits to the fresh VCM storage tank. c. Displace water in the recovery system and drain vessels to normal levels. 2. Procedure a. Make sure the recovery system, blowdown system, and VCM storage tanks are full of water.^ If not, fill up one reactor with water and fill up the whole system through the filled-up reactor's recovery header. b. Pull blinds at the tie-in to the VCM supply and tie-in to the existing inerts recovery system. c. Evacuate reactor 45-741 to 28.5 inches Hg. d. Manually open reactor main charge valve CV-710, VCM valve CV-754, and CV-701 at the VCM storage tank and open the valve at the VCM supply line located at the intersection of the VCM line to the existing reactors. Pump water from VCM storage to the reactor. Opening the VCM supply valve causes the VCM vapor to dis place water in the lines and the fresh VCM storage tank. The displaced water is pumped to reactor 45-741. ^0Um\ DTH 000089159 (1) Open the high point vent on the recovery condenser and receivers to see if the system is full. Page 47 V. INTRODUCTION OF VCM AND FINAL REACTOR CHECKS (CONTINUED) C. Introduction of VCM (Continued) 2. Procedure (Continued) e. When the pump loses suction, shut down the pump. Allow the VCM vapor to displace the remaining water into the reactor until the water level is at the bottom of the sight glass on the storage tank. f. Shut in the VCM header to the reactors by closing valve CV-701 at the VCM storage tank. g. Pump VCM into the fresh VCM storage tank. h. Charge sixty counts of VCM to the reactor. Keep the reactor temperature at 100F. i. Open the lines from the VCM storage tanks and reactor 45-741 to the recovery system. Manually open all on-off valves in the recovery system. j. Drain the recovery system to the blowdown tank 64-741. Drain the following vessels to their normal level (below inlet): (1) Knockout pots 45-760 and 761. (2) Seal water separators 45-762 and 763. k. Activate the level control in the blowdown tank to drain the liquid. l. Open the line from the existing inerts recovery system to the new receivers to remove water in the line. m. Drain RVCM receivers to the ground until the water level is in the bottom of the sight glass (pressure supplied from Item "1"). DTH 000089160 Page 48 V. INTRODUCTION OF VCM AND FINAL REACTOR CHECKS (CONTINUED) D. False Charge for Reactor 45-741 1. Purposes a. Calibrate VCM charge meter.^ b. Line up piping in the recovery system. c. Check the recovery system. 2. Procedure a. Line up the following: (1) Recovery line header from the reactors to the first knockout pot 45-760. (2) Vapor line from first knockout pot 45-760 to the second knockout pot 45-761. (3) Knockout pot 45-760 recirculation line through pump f" 72-889 and cooler 55-334 to the top spray. (4) Knockout pot 45-761 recirculation line through pump 72-890 to the top spray. (5) Vapor line from kncokout pot 45-761 to the suction of vacuum pumps 72-901 and 902. (6) Discharge from the vacuum pumps to the suction of compressors 72-902, 903, and 904. (7) Discharge from the compressors to seal water separators 45-762 and 763. (8) Vapor line from seal water separators 45-762 and 763 to RVCM collect tank 45-764 through condenser 55-335/ 336. DTH 000089161 (1) RVCM charge meter needs to be calibrated after the false charge. Page 49 V. INTRODUCTION OF VCM AND FINAL REACTOR CHECKS (CONTINUED) D. False Charge for Reactor 45-741 (Continued) 2. Procedure (Continued) (9) Vapor lines from seal water separators 45-762 and 763 and collect tank 45-764 to the suction of vacuum pumps 72-901 and 902. (10) Seal water from seal water separator 45-762 to vacuum pumps 72-901 and 902 and compressors 72-903, 904, and 905 through pump 72-891, filter 64-731, and cooler 55-335. (11) Seal water from seal water separator 45-763 to the outlet of cooler 55-335 through pump 72-892, filter 64-732, and cooler 55-336. (12) Vent line from collect tank 45-764 to the vent line header. (13) Liquid outlet from the RVCM collect tank to RVCM storage tanks 89-520 and 45-317 through pump 72-893/894. b. Manually close all on-off valves in the recovery section. c. Charge 300 counts of VCM. Make sure the initial and final VCM levels in the tank can be observed in the sight glass. d. Recover the VCM from the charged reactor. Follow the normal recovery procedure, including steam stripping. e. After the recovery system is in operation, steam strip water in the reactor and drain water to the sewer. dTH 000089162 (1) Refer to "Process Operating Checks, Reactor Recovery System" in Appendix A. Page 50 V. INTRODUCTION OF VCH AM) FINAL REACTOR CHECKS (CONTINUED) E. Work Items before First Real Charge In addition to the normal precharge check list, the following work items are to be done before the first real charge: 1. Drain the water in the VCM storage tanks to the blowdown tank. 2. Check the operation of the blowdown system by recovering VCM from it. DTH 000089163 Page 51 APPENDIX A PROCESS OPERATING CHECKS dth 000089164 PROCESS OPERATING CHECKS WATER CHARGE TO ALL FOUR REACTORS Reactor No._________ _ I. SYSTEM CONDITIONS PRIOR TO START A. The following vessels should be full (Yes/No): 1. Hot water tank 2. Fresh VCM tank 3. Colloid charge tank 4. RVCM storage tank Page 52 B. MSPW rate to agitator (.5 gpm normal) gpm C. Seal oil pressure (.230-250 psig normal) psig D. Seal oil flow (1 gpm normal) gpm E. Initiator pot pressure (at least 180 psig) psig F. All reactor valves closed (Yes/No) G. Charge meters should be reset (Yes/No) 1. Water charge 2. VCM charge 3. Colloid charge 4. RVCM charge H. Temperature of water charge (.140F normal) F II. EVACUATION A. Emergency CWS to condenser should be opened (Yes/No) B. Pressure after evacuation (at least 28.5 Inches Hg) "Hg DTH 000089165 Page 53 Process Operating Checks Page 2 III. CHARGE A. Check the following (Yes/No) 1. VCM transfer in manual ___________ 2. VCM charge in auto 3. RVCM charge in auto 4. Water charge in auto _ 5. Initiator charge in auto 6. Colloid charge in auto 7. Initiator charge light on B. When the charge button is pushed, observe the following occur in sequence (Yes/No 1. Reactor water valve opens 2. "A" hot water pump start Valves open 3. Valves from the fresh VCM tank to the VCM charge pump and dis- charge valve open 4. Set point No. 1 on water meter: a. "B" hot water pump starts opens . Discharge valve b. Colloid charge pump valve opens . Pump starts c. Colloid set point is reached, pump shuts off Discharge valve closes Reactor colloid valve closes . 5. At set point No. 2 on water meter: a. Reactor VCM charge valve opens _______ b. VCM pumps start . RVCM pumps start DTH 000089166 Page 54 Process Operating Checks Page 3 III. CHARGE (CONTINUED) 6. At set point No. 3 on water meter: a. "B" hot water pump stops . Discharge valves close . b. VCM meter set point is reached, VCM pump stops _________ outlet valve closes , inlet valve closes reactor VCM valve closes , "B" hot water pump starts , and discharge valve opens . 7. At set point No. 4 on water meter: "A" and "B" hot water pumps stop _, discharge valves close, reactor water charge valve closes , main dump valve closes . DTH 000089167 PROCESS OPERATING CHECKS REACTOR RECOVERY SYSTEM Page 55 I. SYSTEM CONDITIONS PRIOR TO COMPRESSOR STARTUP A. Vessel water levels (at or below inlet): North Knockout Tank South Knockout Tank North Seal Water Separator South Seal Water Separator B. Compressor inlet, outlet, seal water valves; positions as indi cated (Yes/No): "A" Vacuum Pump Inlet closed ; Outlet closed ___________; Seal water closed "B" Vacuum Pump Inlet closed _____ ; Outlet closed ; Seal water closed "A" Compressor Inlet closed _____ ; Outlet closed _____ ; Seal water closed "B" Compressor Inlet closed ; Outlet closed ; Seal water closed HC" Compressor Inlet closed _____ ; Outlet closed ; Seal water closed Compressor Bypass Valve, Open Vacuum Pump Bypass Valve, Open C. Mechanical seal rates: Inboard Seal (0.5 gpm Normal) DTH 000089168 Double Mechanical Seal (1 gpm Normal) 'A" Vacuum Pump B" Vacuum Pump A" Compressor B" Compressor 'C" Compressor gpm gpm gpm gpm gpm gpm gpm gpm gpm gpm Page 56 Process Operating Checks Page 2 II. SYSTEM CONDITIONS DURING INITIAL PART OF RECOVERY A. Compressor inlet, outlet, seal water valves; positions as indi cated (Yes/No): "A" Vacuum Pump Inlet closed ; Outlet closed ; Seal water closed "B" Vacuum Pump Inlet closed ; Outlet closed ; Seal water closed "A" Compressor Inlet open ; outlet open ; Seal water open "B" Compressor Inlet open; Outlet open; Seal water open "C" Compressor Inlet open; Outlet open; Seal water open Compressor Bypass Valve, Closed Vacuum Pump Bypass Valve, Open B. Seal water rates (50 gpm normal): A" Compressor, B" Compressor, c" Compressor, gpm gpm gpm C. System operating pressures: North Knockout Tank Pressure, 24" Hg - 35 psig, Compressor Discharge Pressure, 40-80 psig, psig North Knockout Tank Pump Discharge Pressure, 40-75 psig, psig South Knockout Tank Pump Discharge Pressure, 40-75 psig, psig North Seal Water Pump Discharge Pressure, 90-130 psig, psig South Seal Water Pump Discharge Pressure, 90-130 psig, psig D. Collect tank pumps should be open (Yes/No) DTH 000089169 Page 57 Process Operating Checks Page 3 TTT. SYSTEM CONDITIONS FOLLOWING STARTUP OF VACUUM PUMPS A. Compressor inlet, outlet, seal water valves; positions as indicated (Yes/No): "A" Vacuum Pump Inlet open ; Outlet open ; Seal water open "B" Vacuum Pump Inlet open ; Outlet open ; Seal water open "A" Compressor Inlet open ; Outlet open; Seal water closed "B" Compressor Inlet Open; Outlet open; Seal water closed "C" Compressor Inlet closed ; Outlet closed ; Seal water closed Compressor Bypass Valve, Closed Vacuum Pump Bypass Valve, Closed B. Seal water rate, 50 gpm normal: "A" Vacuum Pump, gpm "R" Vacuum Pump, gpm C. System operating pressures: Pressure at Inlet (Backpressure Controller), 24" Hg - 35 psig, Backpressure Controller Set Point, 35 psig Normal, psig Compressor Discharge Pressure, 40-80 psig, psig D. Vessel water levels (at or below inlet): North Knockout Tank; South Knocout Tank____________ North Seal Separator South Seal Separator E. Hydroquinone operation: Pump should be running (Yes/No) Level in hydroquinone tank, Inches DTH 000089170 APPENDIX B STRAPPING TABLES DTH 000089171 Page 59 / O/m.jf WSSL. 4-s- 748 !' FT. j/A/OV ; Gals. 0 / .^U j 36-0 1 70.0 ! /as-o 2 140' 6 2'/z 13 3% 4 ffc 6 sy /76'G 2/0-0 1 24S.Q 2 80*/ i 3/6, / i 350./ 3&S' / c 420./ 6k 466- / 7 400. / 7^ <626- / 8 <660'/ 8Vz 3 ek 10 696-/ 630'/ 066* / 700'/ fOl/z 736-4 // 770'/ //kz &06-2 /0 $40'2 yz $y76-2 / 9/0 .2 t* ?<^r-2 2 JZ0.2 2k /o/6- 2 3 / 060' 2 3k 7086-2 4 //20'2 Hot water taa/mt FT INCH ; GALS. 4>A Z766-2 1 s //30.2 !/z /22S 2 C / 2&0'2 ! f ck Z296-2 7 7330 *2 7^2 7306-3 8 7400 '3 : sk 74 36'3 3 /4 7o -3 3l/z 7606-3 /O 764 0- 3 , /oy2 7676'3 !/ 76/0*3 n/2 76 45-3 2 0 768 0'3 !/z 77/33 / 7730 3 ik 7 7 8\T* 3 2 7820 3 2yz /8*66'4 3 7830 '4- 3k 7 826-4 4 /360 >4- 4k /336 4 6 2030'4 1/2 2066.4 C 2/00-4 6 A 2/36' 4 7 2/ 70-4 7k 72064 8 2246-4 &A 2 2 76'4 |PT. \ INCH GALS. 1'3 - 23/0 4 -9{i 2346.4^ 70 /ok 24Z6'6 // 2460-S* //`A 2426^6 3 0 2620-6 a 25S6-6' 7 Z690'S /*$ 26 26-6 2 26 60 '6 2'4 26 96-6 3 2730 -6 3k 2766'6 4 2800 '6 4k 2% 26' 6 6 2&70 .6 S'/z 2906. C 6 2940. G 6>/z 29 76-0 7 30/0-8 7^ 3046.6 8 3080. 6 8ti 3/ As 3 3 3/60'6 sk 3/ 86'0 70 3220.6 /ok 3266'6 77 3290.<8 7/J/z 3326-6 4- 0 3360-6 DTH 000089170 <: \ - i ' - - r v- ' ' --7T~^urzrr^TT7-- Page 60 $HEG7 2 .000 VSL. 4-6-74-2 FT. |/A/OV i1 .. gals . -- 0 3360-6 __ii 3 39o 6 / .JLW3Q-7 _/j 3 465* 7 2 315V 0*7 i 2'A 3535*7 3 3 570.7 1 3'A 360*5*7 4 36 40*7 4`/z 3% 75.1 5 37/6.7 'SPk 3745.7 a 3780.7 l'/z 38/6.7 T 3350.7 7'/z 3885.7 e 3720.7 8VZ 3355.8 3 333o.& 3'A 7 02-3 8 10 4060.8 lo'/z 40 95-8 // 4/30*8 //A 4/6&-8 5 0 4-200*8 Xz 42358 / 4270*8 4305* 8 ' z 43 40. Q 2l/2 43 75. 8 3 44/0*8' SXz 4 <745*8 4 4420*3 HOT mT# taa/# I :ft* /NCH , gals. 4 A 45/5-3 5 46 6 o, 3 5A 4525 3 0 4320-3 I eA 4655-3 7 4690-3 * 7'A 4 725-3 8 9^76 o 5. 8% 47 955 3 ' 4-230-3 oXz 4865* 3 ! ! /O 49)00. s t /OA 43353 // 4370*3 a'/z 5006-0 6 0 50/// . 0 A 5076-0 / 5// / - 0 /!/z 5/46-0 2 5/8 /-O 2*4 52l6*0 3 625/ .6 3'A 5283-0 4 532/-0 4*/2 5356 O 5 53 9/-O 5'/2 54 26*0 C 54 6/.0 6 A 543 6*0 7 653/ / 7>A 556 & - / 8 56 O/ */ 8`A 5&36 - / FT. inch ' 11 L. 1 3 567/ ./ : 3'A 570 6 : / I /o 574/i/ ! /oA 5776*/ | >/ 38//'-/ 1 u'A 5846'./ 1 7 d 582/* i y\ 59/6* / 1 / 595/*/ iA 5986*! 2 602/./ 2 A 6056 *2 3 603/ *2 3A 6/26-2 4 0/6/*2 4X1 0/30*2 5 623/. 2 S'/i 6266- 2 6 630/*2 V/z 6 336-2 7 6 37/-2 7 A 6406*2 8 644/* 2 8A 6 476-2 9 G5//*2 9A 6546*2 /o G58A 3 tc>'A 66/6-3 // 665/* 3 //J/z 6 686*3 3 0 672/*3 DTP[ 00008 Q 1 77 c - fj;' " 1 ' f. * * r --- y Page 61- SN7 3 // ^ VESSEL. FT. 45-742 j .Gals n8 0 6JZ/..3 6\76.3 / A73/.3 *h 4826.3 1 2 68S/-3 2'A $836.3 3 $S'3/-3 3'/2 6366.3 4 700/. 3 *4 7036.3 5 707/. 3 S& 7/06.3 6 7/<7/ .4 0>z 7/ 76 4 T 72/ /. 4 7y2 72 <16. 4 8 72Q/.4 8Vz 73/6-4 3 13S/. 4 Q'A 7386.4- 10 742/* 4 lo'/z 7</ 4 // 743/. 4 ///z 7326.4 30 76 /. <$. ki 73?6.4 / 763/. 4 /K 766.S' 2 770/. 2l/z 7736.5 3 77 7/.5 3'/z 78 06.3 4 78 4/5 //Or wat/z 'Tank 1. FT. ,/MCH gals. 4'A 7876.3 - 737/ .& l/z 7346.3 !1 1 f C 798/5 6l/z 80/ 6.6 7 8 &/. 7,/2 8086-3 11 :1 8 8/2/-S 8Yz 8/565 8 9/3/. 6 ' $`/z 8226.6 I j 70 8 26/.J6 /o'/t 8296. 6 7/ 833/ 6 n'/z 8366-0, /O 0 8 40/. & f/z 8 436-6 7 847/. 6 /*/z 9&06. 2 8347.6 2'/z SS76.6 3 86// .6 3'/2 4 4i/t <9646-6 868/.6 87/6.7 8737-7 s!/2 8786. 7 6 QS2/.7 6 `/l & 86> 7 7 88 7/. 7 7^2 8926.7 8 996/.7 89?67 i /. i ' `' ` r FT. INCH \. GALS. 3 .903/.7' 9<A 90661 7l /o 9/0/17! 70`/z 9/36 '. 7 j 77 9/7/ I7 1 n'/z 9206.7' // 6 924/> 8 Yz 9276.8' / 93//.8 ' t'A 2 2'4 3 9346-8 938/. 8 94/6*8 3 45/. 8 3`/z 3486*8 4 3752/. 8 4^2 3<56.& 9537.8 &/i 3626*8 6 366/a v/z 3636 8 7 973/. 8 7^ 9 766* 3 8 3go/s3 Sit 9836-3 3 987/.a 9'A 6306.3 /o 894/*3 /o'A 9976.3 // /OO //.3 //A 70046.9 u 0 /oos/ .~3 r1)TH ouuuoyx^ [ Page 62 5FE7 4 OF JF. EZ.. &45- y4 i1 . ' FT. Gals. 72 0 700 gj .3 ___il 70//6.3 / /d/5/ .3 76/86 -O' 1 2 7412/ -O 2/ 7d ZS6.3 3 /6 24 Z. 0 \ 3'A 7032.7.0 ! ^ /O 362.0 l'/z 70397.0 5 7Q432.0 <5^ /Q 46 7-0 70502.0 fi/i /QS37-0 7 /OS72-0 7^2 70607-0 8 7064 2*0 706 77.d 70 7 / 2.0 3lA 70747.0 70 /07 & 2.0 td'/z /OQ/7-7 77 76 8324 /il/i /08874 72 0 /09Z24 'A 70937-/ / 700024 7/0274 2 770 82.7 2A 7/037 4 3 77 732.7 3^2 777 6 7-7 4 7/202-7 807 WA7B/j TAA/X ft. fts/CH : gals. 4'A 77237-7 - 1 7/272-7 S'4. 7736 74 ,1 I f. c 7/342 2 6l/i 77377- 2 7 7/ 47 2- 2 '. ! 7 A 7/447-2 8 77482-2 8`A 77-77- 2 1 9 7/S5Z- 2 o'/z 7/587-2. ; ' 70 77 622-2 , /0>/z 77 637-2. 77 77,602-2 nVz 7/727-2. /4 0 /776 Z 2. A 77 70 7 -2 7 7/832-2 7 A 7/867.2 2 77302-3 7/337-3 3 7/372-3 3y2 72007-3 4 720 42-3 4`A 12 0 77-3 5 72772-3 5lA 72747-3 6 72782-3 6 A 722/7-3 7 / 2 252-3 7^2 72287-3 8 7 2322-3 8'A 7 2357-3 i 'M : *> i f\ t wiL. _L*La i t" *' m ; CC. : '.; ( ft: INCH \. gals. ; '3 7 2392-4-' $!A 72427141 70 7Z462l4\ 70'/t 72437.4] 77 7 2/532.4' 77lA 72567- 4 76 " 0 726 02 -4 '/z 7263 7.4' 7 7 Z6 12- <7L !`A 72107. 4 2 7 27 42-6- 7 2.7 77.4 3 72Z/2.4 3'/z /Z947-4 4 72282*4 4'a 72977-5 5 72 952.75 s'/l 72 987-5 6 73022.75 6Yz 73057-S7 73092-75 7 Vt 73/2.7. s 8 7376>Z S 8ti 737 9 7 -75 3 7323 2-59'/z 73 267 5 70 7330Z.5 76 A 73537 S' 77 73372S 77 A 7340 7-5 /*> 0 1344-2-6 1 DTPt 000089175 i : Page 63 $>HtE7 S 6F if ' 4SEL> 45-748 j FT. | INCH gals. / b 0 1344-2 * & Vt /.&7 7.C, / /3\5~/ 2, c -JJL /3tSV7.& 2 /3\5& z. & s 2/2 7A>*7.6 3 /3t6 2. 6 3% 43687.-6 4 7372 2 *(> *& 43TS7 >6 ' 5 /3i 73 2 *6 /3$27 *> c /3?t>z . 6ft 73*97 *6 7 7393 2*6 7'ft 73,3 67-7 8 /4-0 02* 7 8ft 74-037* 7 3 740 72*7 9ft / 4/ 0 7.7 70 74/42.7 76'ft 74777 -7 7/ 74 2/2*7 77 ft 74 247*7 77 0 7429 Z. 7 'ft 74.3/7 *7 7 74-3/52* 7 143*7*7 2 74 422-7 2ft 74 457*7 3 74492*8 3ft 79527*8 4 745G 2 *8 Nor \ajAtejI taa/K FT- INCH GALS. ; 4>A /4^7-a 74632*8 sH 74667*8' ,' 1 6 74702*8 6ft 74737*8 7 74772*8 \ . 7ft 74807*8 ' 8 748 9-2*8 \ !1 * 8A 748 77*3 3 743/2*8 3ft 74897*8 70 74 3 82* 8 , /oy2 Aif0 J 7*3 77 /0*52*3 n'ft 'S'087.3 78 0 757 2 2*9 A A57< 7 -3 7 AS73Z*3 7ft 7S227 *9 2 A5~262 3 2ft 45297*3 3 75332*3 3ft 45367*3 4 AS 902* 3 4ft AS 437*9 AS472* 3 sft AS 507*3 c AS s43*0 6 ft. ASS78*0 7 AS6A3 *0 ?ft AS69 2-0 8 7s6 23*0 8'ft 7S7/&.Q : FT. ).INC. H GALS. ' * 3 f7JS30 ' e'A 757 88* 01 70 AS8 Z3* 0! 70 ft AS8SQ. O! U 7S893l*0 1 lift AS9 28* O' rs 0 75963*0 A 75912*0' 7 76033 O /A 76 068*7 2 7C 7 03* 7 2^ 76732*7 ' 3 76/73*7 3`/z 76208*7 4 76 243* 7 I'/! iTo 278* 1 s 763/3*7 76 342*7 6 16 383*7 76 978*7 7 /6 453* / 7ft 76 4&2* 7 8 76 523*7 ' 8!i 76 558/ 3 76 593*2 9ft 76 628*2 70 76 6 63*2 /oA 76698* 2 77 76733.2 71 ft 76 76Q*2 3D 0 76903*2 1 DTH 00008fli7o < :'Ti ; 1 '** > ''/ ` , M- - ' k L, \2 L.A i > V* r J l* t - j Page 64 SVE7 < VSS&EL. 45-74-8 Nor wat&z 7aajk u \MCH !i ' Gals . 1 :FT. INCH gals. 2'.) ' 0 /6]QQ3-Z' h 16 23%.2 J 16 873.2 /to 16 9o g. 2 2 /6\ 9*3.2 1 2* !(o 9 7 2.2 I 3 n 0 1372 3'A /7\042 *2 ' ^JL___ >7.0/3.2. I7\tt 2.3 5 /7-J53.3 J7/%% .3 H223.3 S'/z 1725i .3 7 172^3-3 7yz 17,37%. 3 8 it36 2.3 8Vz 17,39%.3 3 17433.3 3'A 17462-3 10 17s03.3 lo'A 1753?-3 u i75-73.3 u!/z 1760 2 9 2/ 0 17 4-3 -4 yz !7G7 2 .4 / 17713 <2 /`/i 17742.4 i 177 63 .4 * 2l/z 17%7% . 4 3' 17 $53.4 3j7z !7 2 ' 4 17? 23.4 4`/z 17958' 4 s 17333.4 S'/z J7022. /7O63.4. 1 6Y2. 17098.4 1 7 17/33-4 i 7V2 17/6 8-5 i` : i' ' 8 17203-6 a`/z 1723 8-5 >9 17 273-5 o'/z 1730a. 5 i 10 17 3435 / /0>/z 17378.5 11 17 4135 n'/z /7 4L<l%.S 22 0 18483-5 */z 125185 1 18-633-5 1% 185885 2 196 23-5 12 6525 3 28 693.6 SVz 18 228-6 4 16763-6 4>/2 18 722-6 5 19 933-6 '/z 78 962-6 73903.6 Yz 18938.6 ' 7 73975-6 7^2 1300 ?. 6 8 13073-6 Q'A /3 78 . v< -n 1 ' /. ' .. 37orr^r7nrF~T j FT, INCH 5 i!GALS. 1 3 . 131/3.6' 13!?ei6l 10 13/23 141 lo`/t 132.7 pi 7 i 11 73253.71 U*/z 132 88*7' 23 0 13323-7' to 13358.71 1 /3a93` 7\ /^2 13426.7' 2 13463. 7' 2'4 13 438-7 ` 3 19533.7 3to 13568. 7 4 13603. 7 4^2 13 63g .7 5 13673.7 sto 19709 .7 6 19 743.6 6Yz 19 778.8 7 138/3-8 13 848- 8 8 13 223. S' ay2 13 3/8.8 3 19 353.8 o!7z 19388-8 10 20023*8 iolA 20058-8 11 Z0093.8 1/ l/z 20/22- g 24 0 20/63-8 11 fDIH (J 00089177 -- VSS EL. ~ 4-74 8 FT. ; | MCH \- ! 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FT, /NCH '5 . OA/.B.y 224?4^3\ 22 tfOOl 3 1 /O 2 Z9&3\ /oVx 22S73\3 1 // 726/#{3 i/A 2 Z643\3\ 27 0 22634-3' 1 /2 227/3-3' / Z2.7&3\ * i'A 227/73* 3\ 1 2 22924-3' 24 22??*3' 3 22994.3 43^2 22323-4 223G4 4 4-A 22333-4 23034 4l ^z 230 64* 4 G 23/04.4. tyz 23/33.4 7 23/74-4 23203'- 4- 8 23244,4' 23273-4 3 233/4-4 $A 23343-4 /O 23324-4 /a A 234/6 -4 // 234/74. //l/i 23413. 26 0 23Z4'<5~ DTH nr\r\r\Joyi78 Page 66^6 SHET Q OF /! St. VESSEL. FT. \ffJCH 45-748 7/0T iMATm TANK ii Gals, . FT. 7A/C8 ' GATS. 2\ Q 23524-5 y-i 2 $53-5 / 235-34. m 2^6 235 2 23 G 64-5 2/(2. 2^630.5 3 2873 4-5 3/2 2.376 3 <5~ 1 4 23804-5 4'Ai 23833. 5 238 74- 5 sy 23303-5 6 233 44-5 6/z 233 73- 6 7 24014.6 7/z 24043-a 8 240 $4-6 8A 24 /73-6 3 24 754-G 3'A 24/%3-G 10 24224-6 /o!/z 242535 77 24294-G 7l/z 24323-C 2-1 0 U3(i4--t> A 24333 -6 / 244-34-Q /% 24463-6 2 24504-7 2A 24533- 7 3 24574-7 3A 24G03-7 4 24 644-7 4`A 24673- 7 5 24774-1 5/z 24243-7 24784-7 GA 248/3- 7 7 24854*7 ?A 24883 - 7 8 24324 7 8A 24&S3-7 3 24394- 7 oAz 24073-2 70 24064-8 /O'/z 24033-8 77 24/34- 8 n'/z 24703-8 30 0 25204-8 A 25233-8 7 25274-8 7 A 25303-8 2 2s 2448 2A 2s3 73-Q 3 -2S474 - 8 3'A 2S443- Q 4 2S484-8 4A 255/5.8 5 25554-3 5A 25589-3 25 G 24- 3 & A 25653-3 7 2s<G34-9 lA 25723-3 8 257& 4-3 QA 25733 -3 , - ' 1 : 1 FT. INCH i . I GALS. "3 . 25334-3 ' $y 25863 -3 ' 70 25304.9'' 70 A 25933.3 ! 7/ 259 74-3 uA 2 6063-3 3/ 6 26044-3 a 2p>SO-0 7 26 7 7T. 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FT- (HCH gais. 32 0 26885-/ ._ii 2923- / / 2 955/ .-JLUl 2k 93 0- / 2 2\7025/ 2'A 27060./ 1 3 27035- / 3V2 27/ 30 -Z 4 27/S-2 4A 21200.2 5 27233-2 27270.2 6 27303.2 <c'/l 27240-2 7 27 37S2 7yz 27 4/0-2 a 27 4/AS- 2 8% 2 7 480-2 3 2 7 S/5.2 9A 27 550.2 iO 27 585-2 to'/z 2 7 9 20-2 // 2 7655-3 n`/z 2 7 90.3 33 0 2772S. 3 x/z 27760-3 / 27 7as-3 /% 27830-3 2 2786S-3 2lA 2 7300.3 3 27&3S.3 3'A 2 7970.3 -4 2 80OS-3 4>A 280403 s 2 W75.3 5'/z 2f/ /0.3 G Z p/45-3 G A 2V/Z0-3 7 282/5-3 7A 2-22*50'3 8 2&2l is 4 8A Z23Z0-4 9 Z% 355-4 3 A 28390-4 /o 22425- 4 /O'/i 2 $>450-4 // 2 P 435- 4- nVi 2 &S30- 4- 34 0 285654- A 23600-4- / 29633'4 / !/z 23 670-4 2 2<5>745 2A 2 8 740-S 3 2 2 7755 3</z 298/OS 4 28845-5 aA zssdo-s s 22-9 As-S sA 22SSOS G 2S9&S-S 6 A 23020-5 7 23055-5 7^ 23030,5 8 23/ 25.5 8A. 23/60S .LFT inch GALS. 1 1 3 23)35S' 23236:6 1 /o 2q265.6\ /oA 23300. i3 ; // Z33356 //A 20370. c, 35 0 274-05.6 a 23440.6 / 294-70- 6 ' /% 295/0-6 2 2354S. 2^ 23580.6 3 29<o/S. 3a 2 9650-6 4 23 685. Q 4A 29720-6 s 237S5.7 s'/i 23790.7 6 23825 7 &Y* 29860-7 7 835- 7 7^ 930-7 8 365. 7 -ML 30 000-7 9 035-7 $A 010-7 /o / 05. 7 /6'/t /40-7 // //^ / 75.7 2/0- 7 36 0 30245- 7 DTH 00 OOR9180 - VSSEL. 4^-748 FT. j MCH !i GAlIS. 36 0 30246-7 ___& 3Qz0- 2 / 3o\ 3 /6- 2 .611 3$360. 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INCH GALS. . \ 3 - 2433.3 9 ^2 2440- 7 /O 244%. / /o`/z 24S. t/ 2462.9 u'A 24 70 4 / 6 2477 9 Vz 24 85 2 / 7492-6 1 ' i'/z 2500- 0 2 2507-4 2'4 25/4.8 3 2Z2.2 j 3'/z 2529.5 j 4 2537.0 1 4*/z 254-<7-4 255/. t S'/z 2S5Q-2 G 25&. & GVz 2574-0 7 258/. ^ - 0ii a lank. S/rcuQbi d Wa/t n inch - 7 4052 9Ah , ! / /bch =/4. %/3 ?<?A* U :i DTH 000089209 V- < . Conoco Accounting No. 45-741 45-742 45-743 45-744 55-328 55-328 55-330 55-331 55-332 55-333 55-334 55-335 55-336 55-337 55-338 55-339 - 45-301 45-745 89-520 45-317 45-748 45-750 45-751 45-752 45-753 45-754 45-755 45-756 45-757 45-758 APPENDIX C EQUIPMENT LIST Page 97 Reactors DC-701 DC-702 DC-703 DC-704 Heat Exchangers EA-701 EA-702 EA-703 EA-704 EA-705 EA-706 EA-707 EA-708 EA-709 EA-710 EA-711 EA-712 EA-713 Eductors and Ejectors EE-701 EE-702 EE-703 EE-704 EE-705 EE-706 Tanks and Vessels FA-701 FA-702 FA-703 FA-704 FA-705 FA-706 FA-707 FA-708 FA-709 FA-710 FA-711 FA-712 FA-713 FA-714 FA-715 Service Polymerization Reactor Polymerization Reactor Polymerization Reactor Polymerization Reactor Reactor Condenser Reactor Condenser Reactor Condenser Reactor Condenser Deleted Hot Water Preheater Hot Water Tank Heater Water Recirculation Cooler Seal Water Cooler Seal Water Cooler Recovered VCM Condenser Recovered VCM Condenser Cleaning Solution Heater Reactor Jacket Eductor Reactor Jacket Eductor Reactor Jacket Eductor Reactor Jacket Eductor Deleted Reactor Steam Ejector Instrument Air Capacity Tank Fresh VCM Storage Tank Recovered VCM Storage Tank Recovered VCM Storage Tank Hot Water Tank Deleted Initiator Injection Pot Colloid Makeup Tank Colloid Storage Tank Colloid Charge Tank Seal Oil Storage Drum Deleted AMS Short Stop Charge Pot AMS Short Stop Charge Pot AMS Short Stop Charge Pot AMS Short Stop Charge Pot DTH 000089210 Conoco Accounting No. - 45-759 45-760 45-761 45-762 45-763 45-764 45-765 45-766 - 45-767 45-768 45-319 - 45-770 64-716 64-718 64-719 64-720 64-721 64-722 64-723 64-724 64-725 64-726 64-727 64-728 64-729 64-730 64-731 64-732 64-733 64-734 64-735 64-736 64-737 64-738 64-739 APPENDIX C EQUIPMENT LIST (CONTINUED) Page 98 Tanks and Vessels (Continued) FA-716 FA-717 FA-718 FA-719 FA-720 FA-721 FA-722 FA-723 FA-724 FA-725 FA-726 FA-727 FA-728 FA-729 FA-730 Filters - FD-701 FD-702 FD-703 FD-704 FD-705 FD-706 FD-707 FD-708 FD-709 FD-710 FD-711 FD-712 FD-713 FD-714 FD-715 FD-716 FD-717 FD-718 FD-719 FD-720 FD-721 FD-722 FD-723 FD-724 Service Deleted Mechanical Seal Purge Water Surge Drum Recovery Knockout Drum Recovery Knockout Drum Seal Water Separator Seal Water Separator Recovered VCM Collect Tank Hydroquinone Storage Tank Slurry Dump Tank Deleted Cleaning Solution Tank Reactor Ejector Cyclone Separator Blowdown Tank Deleted Reactor Sampling Bomb Process Water Charge Filter VCM Charge Filter Recovered VCM Filter Process Water Filter Deleted Colloid Makeup Water Filter Colloid Transfer Filter Colloid Transfer Filter Service Water Filter Seal Oil Supply Filter Seal Oil Supply Filter Seal Oil Return Filter Seal Oil Return Filter Deleted Deleted Seal Water Filter Seal Water Filter Slurry Strainer Deleted Cleaning Solution Strainer Breathing Air Filter Breathing Air Filter Breathing Air Filter Breathing Air Filter Breathing Air Filter DTH 000089211 Conoco Accounting No. 64-740 64-741 64-742 72-875 72-876 72-877 72-878 72-879 72-880 72-881 72-882 72-883 72-884 72-885 72-886 72-887 72-888 72-889 - 72-890 72-891 72-892 72-893 72-894 72-895 72-896 72-897 - - 72-898 72-899 72-900 72-901 72-902 72-903 72-904 72-905 49-368 APPENDIX C EQUIPMENT LIST (CONTINUED) Page 99 Filter (Continued) FD-725 FD-726 FD-727 Pumps GA-701 GA-702 GA-703 GA-704 GA-705 GA-706 GA-707 GA-708 GA-709 GA-710 GA-711 GA-712 GA-713 GA-714 GA-715 GA-716 GA-717 GA-718 GA-719 GA-720 GA-721 GA-722 GA-723 GA-724 GA-725 GA-726 GA-727 GA-728 GA-729 GA-730 Compressors and Fans GB-701 GB-702 GB-703 GB-904 GB-705 GB-706 Service Breathing Air Filter Blowdown Tank Drain Strainer VCM Charge Filter VCM Charge Pump VCM Charge Pump Recovered VCM Charge Pump Recovered VCM Charge Pump Hot Water Charge Pump Hot Water Charge Pump Colloid Batch Transfer Pump Colloid Circulation Pump Colloid Charge Pump Colloid Charge Pump Deleted Service Water Pump Service Water Pump Mechanical Seal Purge Water Pump Mechanical Seal Purge Water Pump Water Recirculation Pump Deleted Water Recirculation Pump Seal Water Pump Seal Water Pump Recovered VCM Transfer Pump Recovered VCM Transfer Pump Hydroquinone Injection Pump Slurry Transfer Pump Slurry Transfer Pump Deleted Deleted Cleaning Solution Pump Cleaning Solution Pump Blowdown Tank Pump Recovery Vacuum Pump Recovery Vacuum Pump Recovery Compressor Recovery Compressor Recovery Compressor Slurry Strainer Exhauster DTH 000089212 Conoco Accounting No. 51-101 51-102 51-103 51-104 - 51-105 51-106 95-299 95-300 - " - - - - - - - APPENDIX C EQUIPMENT LIST (CONTINUED) Page 100 Agitators GD-701 GD-702 GD-703 GD-704 GD-705 GD-706 GD-707 Package Units PA-701 PA-702 PA-703 PA-704 PA-705 PA-706 PA-707 PA-708 PA-709 PA-710 PA-711 PA-712 PA-713 PA-714 PA-715 PA-716 PA-717 Service Reactor Agitator Reactor Agitator Reactor Agitator Reactor Agitator Deleted Colloid Makeup Tank Agitator Hydroquinone Storage Tank Agitator Seal Oil Pressure Unit Seal Oil Pressure Unit Deluge System Deluge System Combustible Hydrocarbon Analyzer Fire Monitor Fire Monitor Fire Monitor Fire Monitor Fire Monitor Fire Monitor Deleted Fixed Point VCM Monitor Emergency NO Short Stop Bottles Emergency NO Short Stop Bottles Emergency NO Short Stop Bottles Emergency NO Short Stop Bottles Programmable Controller PFF-lkm 12/9/77 DTH 000089213 Page 101 APPENDIX D STEAM TRACING ISOMETRICS DTH 000089214 mT-l cn CooD oo # i > Page 104 '> t CO CD 0o0 O" Oo ' SC H Q OP MA BH_L or ;. t DTH 0 0 0 0 8 9 2 1 9 i jo nu j /'* - 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""4 05; CD 4a* ^ O O O O, HSC' Q 6H_L O F M Page 124 Page 125 i CO CO <N 05 CO O O O O K H P i !i (C//0T' DTH 0 0 0 0 8 9 2 3 9 BK.L. O F M A TE . DTH 0 0 0 0 8 9 2 4 0 Page 127 {U Ot) '.ttF-I 'i y i h j i -?n j o t i o Q tLL O F M A T E R IA L Page 131 . ' Page 132 ' <N CD 03 O O O O 8 I'L L O F M Page 133 CD <N 05 CO O O O O X H Q S ` ' (, r l !* ! t ! r l V Page 134 C<N 05 03 O O O O W O T*fg, 135 CD 'T CO CD 00 O O O t o. CHAD Page 136 05 CM CD o00 oo o Jr R Q Page. 137 O lT5 <M 05 CO O O O O Page 138 in CO 05 CO ooo o % Si; 01) Page 139 APPENDIX E P&I DIAGRAMS DTH 000089252